The Fabrication of Microstructures from Powders and Their Applications in Microsystems

A special issue of Micromachines (ISSN 2072-666X). This special issue belongs to the section "D:Materials and Processing".

Deadline for manuscript submissions: closed (31 December 2021) | Viewed by 19807

Special Issue Editor


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Guest Editor
Fraunhofer Institute for Silicon Technology ISIT, Itzehoe 25524, Schleswig-Holstein, Germany
Interests: micro systems; MEMS technology; MEMS development and design; new materials and processes; novel MEMS devices

Special Issue Information

Dear Colleagues,

The application potential of microsystem technology is continuously increasing as new fabrication processes overcome substantial constraints. Among them is the realization of three-dimensional (3D) microstructures with sizes between tens and hundreds of microns from a broad variety of materials. Common MEMS and IC processes do not meet these requirements adequately. A promising alternative is the utilization of micron-sized powder to create 3D microstructures. Although numerous approaches have been presented already, the application of powder-based techniques for MEMS is still in its initial stages. To enable cost-effective production, it should be possible to integrate powder-based 3D microstructures into proven fabrication processes on large-scale silicon, glass, ceramic or plastic substrates, panels or boards.

Accordingly, this Special Issue seeks to showcase research papers and review articles that focus on: (1) powder-based techniques for 3D microstructure fabrication compatible to silicon, glass, ceramic or plastic substrates, panels or boards; (2) simulation and characterization of powder-based 3D microstructures fabricated from various materials; (3) fabrication, simulation and characterization of MEMS devices utilizing powder-based 3D microstructures; (4) novel functionalities and applications for MEMS due to powder-based 3D microstructures; (5) durability, reliability and long-term stability of powder-based 3D microstructures.

Dr. Thomas Lisec
Guest Editor

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Keywords

  • powder-based techniques
  • 3D microstructures
  • MEMS

Published Papers (8 papers)

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Research

13 pages, 5463 KiB  
Article
Towards Robust Thermal MEMS: Demonstration of a Novel Approach for Solid Thermal Isolation by Substrate-Level Integrated Porous Microstructures
by Ole Behrmann, Thomas Lisec and Björn Gojdka
Micromachines 2022, 13(8), 1178; https://doi.org/10.3390/mi13081178 - 26 Jul 2022
Cited by 6 | Viewed by 1869
Abstract
Most current thermal MEMS use fragile structures such as thin-film membranes or microcantilevers for thermal isolation. To increase the robustness of these devices, solid thermal insulators that are compatible with MEMS cleanroom processing are needed. This work introduces a novel approach for microscale [...] Read more.
Most current thermal MEMS use fragile structures such as thin-film membranes or microcantilevers for thermal isolation. To increase the robustness of these devices, solid thermal insulators that are compatible with MEMS cleanroom processing are needed. This work introduces a novel approach for microscale thermal isolation using porous microstructures created with the recently developed PowderMEMS wafer-level process. MEMS devices consisting of heaters on a thin-film membrane were modified with porous microstructures made from three different materials. A thermal model for the estimation of the resulting thermal conductivity was developed, and measurements for porous structures in ambient air and under vacuum were performed. The PowderMEMS process was successfully used to create microscale thermal insulators in silicon cavities at the wafer level. Measurements indicate thermal conductivities of close to 0.1 W/mK in ambient air and close to 0.04 W/mK for porous structures under vacuum for the best-performing material. The obtained thermal conductivities are lower than those reported for both glass and porous silicon, making PowderMEMS a very interesting alternative for solid microscale thermal isolation. Full article
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23 pages, 8600 KiB  
Article
Fully Integrated High-Performance MEMS Energy Harvester for Mechanical and Contactless Magnetic Excitation in Resonance and at Low Frequencies
by Mani Teja Bodduluri, Torben Dankwort, Thomas Lisec, Sven Grünzig, Anmol Khare, Minhaz Ahmed and Björn Gojdka
Micromachines 2022, 13(6), 863; https://doi.org/10.3390/mi13060863 - 30 May 2022
Cited by 9 | Viewed by 2482
Abstract
Energy harvesting and storage is highly demanded to enhance the lifetime of autonomous systems, such as IoT sensor nodes, avoiding costly and time-consuming battery replacement. However, cost efficient and small-scale energy harvesting systems with reasonable power output are still subjects of current development. [...] Read more.
Energy harvesting and storage is highly demanded to enhance the lifetime of autonomous systems, such as IoT sensor nodes, avoiding costly and time-consuming battery replacement. However, cost efficient and small-scale energy harvesting systems with reasonable power output are still subjects of current development. In this work, we present a mechanically and magnetically excitable MEMS vibrational piezoelectric energy harvester featuring wafer-level integrated rare-earth micromagnets. The latter enable harvesting of energy efficiently both in resonance and from low-g, low-frequency mechanical energy sources. Under rotational magnetic excitation at frequencies below 50 Hz, RMS power output up to 74.11 µW is demonstrated in frequency up-conversion. Magnetic excitation in resonance results in open-circuit voltages > 9 V and RMS power output up to 139.39 µW. For purely mechanical excitation, the powder-based integration process allows the realization of high-density and thus compact proof masses in the cantilever design. Accordingly, the device achieves 24.75 µW power output under mechanical excitation of 0.75 g at resonance. The ability to load a capacitance of 2.8 µF at 2.5 V within 30 s is demonstrated, facilitating a custom design low-power ASIC. Full article
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17 pages, 11302 KiB  
Article
Investigation of Wafer-Level Fabricated Permanent Micromagnets for MEMS
by Mani Teja Bodduluri, Björn Gojdka, Niklas Wolff, Lorenz Kienle, Thomas Lisec and Fabian Lofink
Micromachines 2022, 13(5), 742; https://doi.org/10.3390/mi13050742 - 7 May 2022
Cited by 8 | Viewed by 2681
Abstract
Monolithic integration of permanent micromagnets into MEMS structures offers many advantages in magnetic MEMS applications. A novel technique called PowderMEMS, based on the agglomeration of micron-sized powders by atomic layer deposition (ALD), has been used to fabricate permanent micromagnets on 8-inch wafers. In [...] Read more.
Monolithic integration of permanent micromagnets into MEMS structures offers many advantages in magnetic MEMS applications. A novel technique called PowderMEMS, based on the agglomeration of micron-sized powders by atomic layer deposition (ALD), has been used to fabricate permanent micromagnets on 8-inch wafers. In this paper, we report the fabrication and magnetic characterization of PowderMEMS micromagnets prepared from two different NdFeB powder particle sizes. A remanence of 423 mT and intrinsic coercivity of 924 mT is achieved at the low ALD process temperature of 75 °C, making this process compatible with MEMS technology. The magnetic reversible mechanism in the micromagnets is discussed with the help of the Wohlfarth equation. To ensure the operability of such integrated micromagnets in different application environments, we conducted a set of experiments to systematically investigate the thermal and corrosive stability. NdFeB micromagnets with larger powder particle size (d50 = 25 µm) exhibit high thermal stability in air. Furthermore, the corrosion stability of the micromagnets is significantly improved by an additional silicon oxide passivation layer deposited by plasma-enhanced chemical vapor deposition (PECVD). The presented results demonstrate the durability of PowderMEMS micromagnets, enabling their application in various fields, e.g., microfluidics, sensors, actuators, and microelectronics. Full article
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13 pages, 3406 KiB  
Article
Broadband Zero-Power Wakeup MEMS Device for Energy-Efficient Sensor Nodes
by Minhaz Ahmed, Torben Dankwort, Sven Grünzig, Volker Lange and Björn Gojdka
Micromachines 2022, 13(3), 407; https://doi.org/10.3390/mi13030407 - 2 Mar 2022
Cited by 4 | Viewed by 2680
Abstract
A zero-power wakeup scheme for energy-efficient sensor applications is presented in this study based on a piezoelectric MEMS energy harvester featuring wafer-level-integrated micromagnets. The proposed setup overcomes a hybrid assembly of magnets on a chip-level, a major drawback of similar existing solutions. The [...] Read more.
A zero-power wakeup scheme for energy-efficient sensor applications is presented in this study based on a piezoelectric MEMS energy harvester featuring wafer-level-integrated micromagnets. The proposed setup overcomes a hybrid assembly of magnets on a chip-level, a major drawback of similar existing solutions. The wakeup device can be excited at low frequencies by frequency up-conversion, both in mechanical contact and contactless methods due to magnetic force coupling, allowing various application scenarios. In a discrete circuit, a wakeup within 30–50 ms is realized in frequency up-conversion at excitation frequencies < 50 Hz. A power loss in the off state of 0.1 nW renders the scheme virtually lossless. The potential extension of battery lifetime compared to cyclical wakeup schemes is discussed for a typical wireless sensor node configuration. Full article
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22 pages, 9879 KiB  
Article
PowderMEMS—A Generic Microfabrication Technology for Integrated Three-Dimensional Functional Microstructures
by Thomas Lisec, Ole Behrmann and Björn Gojdka
Micromachines 2022, 13(3), 398; https://doi.org/10.3390/mi13030398 - 28 Feb 2022
Cited by 12 | Viewed by 3121
Abstract
A comprehensive overview of PowderMEMS—a novel back-end-of-line-compatible microfabrication technology—is presented in this paper. The PowderMEMS process solidifies micron-sized particles via atomic layer deposition (ALD) to create three-dimensional microstructures on planar substrates from a wide variety of materials. The process offers numerous degrees of [...] Read more.
A comprehensive overview of PowderMEMS—a novel back-end-of-line-compatible microfabrication technology—is presented in this paper. The PowderMEMS process solidifies micron-sized particles via atomic layer deposition (ALD) to create three-dimensional microstructures on planar substrates from a wide variety of materials. The process offers numerous degrees of freedom for the design of functional MEMSs, such as a wide choice of different material properties and the precise definition of 3D volumes at the substrate level, with a defined degree of porosity. This work details the characteristics of PowderMEMS materials as well as the maturity of the fabrication technology, while highlighting prospects for future microdevices. Applications of PowderMEMS in the fields of magnetic, thermal, optical, fluidic, and electrochemical MEMSs are described, and future developments and challenges of the technology are discussed. Full article
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14 pages, 23890 KiB  
Article
High Temperature Magnetic Cores Based on PowderMEMS Technique for Integrated Inductors with Active Cooling
by Malte Paesler, Thomas Lisec and Holger Kapels
Micromachines 2022, 13(3), 347; https://doi.org/10.3390/mi13030347 - 22 Feb 2022
Cited by 2 | Viewed by 1730
Abstract
The paper presents the realization and characterization of micro-inductors with core with active cooling capability for future integrated DC/DC converter solutions operating with wide bandgap semiconductors at high temperatures with high power densities. The cores are fabricated backend-of-line compatible by filling cavities in [...] Read more.
The paper presents the realization and characterization of micro-inductors with core with active cooling capability for future integrated DC/DC converter solutions operating with wide bandgap semiconductors at high temperatures with high power densities. The cores are fabricated backend-of-line compatible by filling cavities in silicon wafers with soft magnetic iron particles and their subsequent agglomeration to rigid, porous 3D microstructures by atomic layer deposition. Wafer processing is presented as well as measurement results at up to 400 C operating temperature in comparison to of-the-shelf inductors. Using a DC/DC converter operating at 25 MHz switching frequency efficiencies of 81 to 83% are demonstrated for input voltages between 5 V and 12 V. It is shown that the temperature of the novel micro-inductors decreases if an air flow through its porous core is applied. This feature could be especially helpful for the realization of resonant power converters with larger temperature stress to passive components. Full article
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10 pages, 4700 KiB  
Article
Demonstration of Fully Integrable Long-Range Microposition Detection with Wafer-Level Embedded Micromagnets
by Björn Gojdka, Daniel Cichon, Yannik Lembrecht, Mani Teja Bodduluri, Thomas Lisec, Markus Stahl-Offergeld, Hans-Peter Hohe and Florian Niekiel
Micromachines 2022, 13(2), 235; https://doi.org/10.3390/mi13020235 - 30 Jan 2022
Cited by 3 | Viewed by 2014
Abstract
A fully integrable magnetic microposition detection for miniaturized systems like MEMS devices is demonstrated. Whereas current magnetic solutions are based on the use of hybrid mounted magnets, here a combination of Hall sensors with a novel kind of wafer-level integrable micromagnet is presented. [...] Read more.
A fully integrable magnetic microposition detection for miniaturized systems like MEMS devices is demonstrated. Whereas current magnetic solutions are based on the use of hybrid mounted magnets, here a combination of Hall sensors with a novel kind of wafer-level integrable micromagnet is presented. 1D measurements achieve a precision <10 µm within a distance of 1000 µm. Three-dimensional (3D) measurements demonstrate the resolution of complex trajectories in a millimeter-sized space with precision better than 50 µm in real time. The demonstrated combination of a CMOS Hall sensor and wafer-level embedded micromagnets enables a fully integrable magnetic position detection for microdevices such as scanners, switches, valves and flow regulators, endoscopes or tactile sensors. Full article
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14 pages, 5555 KiB  
Article
Automated Filling of Dry Micron-Sized Particles into Micro Mold Pattern within Planar Substrates for the Fabrication of Powder-Based 3D Microstructures
by Cris Kostmann, Thomas Lisec, Mani Teja Bodduluri and Olaf Andersen
Micromachines 2021, 12(10), 1176; https://doi.org/10.3390/mi12101176 - 29 Sep 2021
Cited by 11 | Viewed by 1927
Abstract
Powder-based techniques are gaining increasing interest for the fabrication of microstructures on planar substrates. A typical approach comprises the filling of a mold pattern with micron-sized particles of the desired material, and their fixation there. Commonly powder-loaded pastes or inks are filled into [...] Read more.
Powder-based techniques are gaining increasing interest for the fabrication of microstructures on planar substrates. A typical approach comprises the filling of a mold pattern with micron-sized particles of the desired material, and their fixation there. Commonly powder-loaded pastes or inks are filled into the molds. To meet the smallest dimensions and highest filling factors, the utilization of dry powder as the raw material is more beneficial. However, an appropriate automated technique for filling a micro mold pattern with dry micron-sized particles is missing up to now. This paper presents a corresponding approach based on the superimposition of high- and low-frequency oscillations for particle mobilization. Rubber balls are utilized to achieve dense packing. For verification, micromagnets are created from 5 µm NdFeB powder on 8” Si substrates, using the novel automated mold filling technique, as well as an existing manual one. Subsequent atomic layer deposition is utilized to agglomerate the loose NdFeB particles into rigid microstructures. The magnetic properties and inner structure of the NdFeB micromagnets are investigated. It is shown that the novel automated technique outperforms the manual one in major terms. Full article
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