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Molbank 2016, 2016(2), M900;

2II-VII, 3I-VII, 6I-VII-Icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose

Department of Materials Science and Engineering, Graduate School of Engineering, Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya 466-8555, Japan
Author to whom correspondence should be addressed.
Academic Editor: Norbert Haider
Received: 18 April 2016 / Revised: 23 May 2016 / Accepted: 23 May 2016 / Published: 31 May 2016
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Deoxygenation of a secondary hydroxy group on β-cyclodextrin was conducted to prepare the title compound 2II-VII, 3I-VII, 6I-VII-icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. The synthetic procedure comprised a two-step reaction—phenoxythiocarbonylation and Barton-McCombie deoxygenation. The synthesized compound was characterized by 1H-NMR, 13C-NMR, HRMS, and elemental analysis. View Full-Text
Keywords: cyclodextrin; deoxygenation; Barton-McCombie deoxygenation cyclodextrin; deoxygenation; Barton-McCombie deoxygenation

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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0).

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Miyagawa, A.; Kano, K.; Yoshida, A.; Yamamura, H. 2II-VII, 3I-VII, 6I-VII-Icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. Molbank 2016, 2016, M900.

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