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Molbank 2016, 2016(2), M900; doi:10.3390/M900

2II-VII, 3I-VII, 6I-VII-Icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose

Department of Materials Science and Engineering, Graduate School of Engineering, Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya 466-8555, Japan
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Academic Editor: Norbert Haider
Received: 18 April 2016 / Revised: 23 May 2016 / Accepted: 23 May 2016 / Published: 31 May 2016
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Abstract

Deoxygenation of a secondary hydroxy group on β-cyclodextrin was conducted to prepare the title compound 2II-VII, 3I-VII, 6I-VII-icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. The synthetic procedure comprised a two-step reaction—phenoxythiocarbonylation and Barton-McCombie deoxygenation. The synthesized compound was characterized by 1H-NMR, 13C-NMR, HRMS, and elemental analysis. View Full-Text
Keywords: cyclodextrin; deoxygenation; Barton-McCombie deoxygenation cyclodextrin; deoxygenation; Barton-McCombie deoxygenation
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MDPI and ACS Style

Miyagawa, A.; Kano, K.; Yoshida, A.; Yamamura, H. 2II-VII, 3I-VII, 6I-VII-Icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. Molbank 2016, 2016, M900.

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