Molecules, Volume 5, Issue 12

*Editor's Note: The brief summary and the contents of the books are reported as provided by the author or the publishers.[...]

To a mixture of 0.8 g (4.7 mmol) of metachloroperbenzoique acid (mCPBA) and 1.58g (18.8mmol) of sodium hydrogenocarbonate (NaHCO3) in 15 ml of dichloromethane was added 1 g (2.35 mmol) of 1 in 5 ml of CH2Cl2.[...]

5-[o-(2-bromo-1-ethoxy)]phenyl-10,15,20-triphenylporphyrin (1) was prepared according to published method [1].[...]

As part of a research programme targeting novel molecules as potential anti-inflammatory agents we synthesised 3-Chloro-5-methoxy-1-benzo[b]thiophene-2-sulphonylamide base on the reported anti-inflammatory activity of the structurally related molecul...

In the course of our recent studies on the synthesis, solid phase structure, solution and solid phase 13C CPMAS [1], and its application in Ion Selective Electrodes [2] of the smallest benzo crown ether, Benzo-9-Crown-3, B9C3, we accomplished the syn...

The experimental procedure follows a novel protocol developed recently by us [1].[...]

The title compound was prepared from imidazolinone 1 whose synthesis as well as 1H and 13C NMR spectra were published previously [1].[...]

To sodium hydride (0.3g, 12.7 mmole) carefully washed with anhydrous benzene under nitrogen (to eliminate mineral oil from the commercial product) [1], was added (0.8 ml, 8.43 mmole) of dimethylcarbonate (freshly distilled) in dry benzene (20 ml).[...]

Disulfides that mimic the pentapeptide Phe-D-Leu-Gly-D-Leu-Phe can be obtained in high yield from the corresponding thioacetate via the intermediate mercaptan by prolonged standing in alkali [1].[...]

Disulfides that mimic the pentapeptide Phe-Leu-Gly-Leu-Phe can be obtained in high yield from the corresponding thioacetate via the intermediate mercaptan by prolonged standing in alkali [1].[...]