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Search Results (3,602)

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Keywords = wear and friction

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29 pages, 2636 KiB  
Review
Review on Tribological and Vibration Aspects in Mechanical Bearings of Electric Vehicles: Effect of Bearing Current, Shaft Voltage, and Electric Discharge Material Spalling Current
by Rohan Lokhande, Sitesh Kumar Mishra, Deepak Ronanki, Piyush Shakya, Vimal Edachery and Lijesh Koottaparambil
Lubricants 2025, 13(8), 349; https://doi.org/10.3390/lubricants13080349 - 5 Aug 2025
Abstract
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to [...] Read more.
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to bearing degradation include shaft voltage, bearing current, and electric discharge material spalling current, especially in motors powered by inverters or variable frequency drives. This review explores the tribological and vibrational aspects of bearing currents, analyzing their mechanisms and influence on electric motor performance. It addresses the challenges faced by electric vehicles, such as high-speed operation, elevated temperatures, electrical conductivity, and energy efficiency. This study investigates the origins of bearing currents, damage linked to shaft voltage and electric discharge material spalling current, and the effects of lubricant properties on bearing functionality. Moreover, it covers various methods for measuring shaft voltage and bearing current, as well as strategies to alleviate the adverse impacts of bearing currents. This comprehensive analysis aims to shed light on the detrimental effects of bearing currents on the performance and lifespan of electric motors in electric vehicles, emphasizing the importance of tribological considerations for reliable operation and durability. The aim of this study is to address the engineering problem of bearing failure in inverter-fed EV motors by integrating electrical, tribological, and lubrication perspectives. The novelty lies in proposing a conceptual link between lubricant breakdown and damage morphology to guide mitigation strategies. The study tasks include literature review, analysis of bearing current mechanisms and diagnostics, and identification of technological trends. The findings provide insights into lubricant properties and diagnostic approaches that can support industrial solutions. Full article
(This article belongs to the Special Issue Tribology of Electric Vehicles)
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22 pages, 24500 KiB  
Article
Ambient to Elevated Temperature: Ecotribology of Water-Based Lubricants Incorporating hBN/TiO2 Nanoadditives
by Afshana Morshed, Fei Lin, Hui Wu, Zhao Xing, Sihai Jiao and Zhengyi Jiang
Lubricants 2025, 13(8), 344; https://doi.org/10.3390/lubricants13080344 - 1 Aug 2025
Viewed by 194
Abstract
Ecotribology focuses on both saving energy resources and reducing environmental pollution. Considering environmental concerns, water-based nanolubricants have gained significant attention over conventional oil-based ones. Non-ecotoxic and highly environmentally friendly nanoadditives were chosen for nanolubricant synthesis, especially considering their use at elevated temperatures. In [...] Read more.
Ecotribology focuses on both saving energy resources and reducing environmental pollution. Considering environmental concerns, water-based nanolubricants have gained significant attention over conventional oil-based ones. Non-ecotoxic and highly environmentally friendly nanoadditives were chosen for nanolubricant synthesis, especially considering their use at elevated temperatures. In this study, hexagonal boron nitride nanosheets (hBNNSs) and titanium dioxide nanoparticles (TiO2 NPs) were used to prepare water-based lubricants with glycerol and surfactant sodium dodecyl benzene sulfonate (SDBS) in water under ultrasonication. An Rtec ball-on-disk tribometer was used to investigate the tribological performance of the synthesised water-based lubricants containing different nano-hBN/TiO2 concentrations, with dry and water conditions used as benchmarks. The results indicated that the water-based nanolubricant containing 0.5 wt% hBN and 0.5 wt% TiO2 exhibited the best tribological performance at both ambient (25 °C) and elevated (500 °C) temperatures. This optimal concentration leads to a reduction in the coefficient of friction (COF) by 72.9% and 37.5%, wear of disk by 62.5% and 49%, and wear of ball by 74% and 69% at ambient and elevated temperatures, respectively, compared to that of distilled water. Lubrication mechanisms were attributed to the rolling, mending, tribofilm, solid layer formation, and synergistic effects of hBNNSs and TiO2 NPs. Full article
(This article belongs to the Special Issue Tribology in Manufacturing Engineering)
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22 pages, 29737 KiB  
Article
A Comparative Investigation of CFD Approaches for Oil–Air Two-Phase Flow in High-Speed Lubricated Rolling Bearings
by Ruifeng Zhao, Pengfei Zhou, Jianfeng Zhong, Duan Yang and Jie Ling
Machines 2025, 13(8), 678; https://doi.org/10.3390/machines13080678 - 1 Aug 2025
Viewed by 118
Abstract
Analyzing the two-phase flow behavior in bearing lubrication is crucial for understanding friction and wear mechanisms, optimizing lubrication design, and improving bearing operational efficiency and reliability. However, the complexity of oil–air two-phase flow in high-speed bearings poses significant research challenges. Currently, there is [...] Read more.
Analyzing the two-phase flow behavior in bearing lubrication is crucial for understanding friction and wear mechanisms, optimizing lubrication design, and improving bearing operational efficiency and reliability. However, the complexity of oil–air two-phase flow in high-speed bearings poses significant research challenges. Currently, there is a lack of comparative studies employing different simulation strategies to address this issue, leaving a gap in evidence-based guidance for selecting appropriate simulation approaches in practical applications. This study begins with a comparative analysis between experimental and simulation results to validate the reliability of the adopted simulation approach. Subsequently, a comparative evaluation of different simulation methods is conducted to provide a scientific basis for relevant decision-making. Evaluated from three dimensions—adaptability to rotational speed conditions, research focuses (oil distribution and power loss), and computational economy—the findings reveal that FVM excels at medium-to-high speeds, accurately predicting continuous oil film distribution and power loss, while MPS, leveraging its meshless Lagrangian characteristics, demonstrates superior capability in describing physical phenomena under extreme conditions, albeit with higher computational costs. Economically, FVM, supported by mature software ecosystems and parallel computing optimization, is more suitable for industrial design applications, whereas MPS, being more reliant on high-performance hardware, is better suited for academic research and customized scenarios. The study further proposes that future research could adopt an FVM-MPS coupled approach to balance efficiency and precision, offering a new paradigm for multi-scale lubrication analysis in bearings. Full article
(This article belongs to the Section Machine Design and Theory)
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25 pages, 5020 KiB  
Review
Research Progress on Tribological Properties of High-Entropy Alloys
by Shuai Zhang, Zhaofeng Wang, Wenqing Lin and Haoyu Guo
Lubricants 2025, 13(8), 342; https://doi.org/10.3390/lubricants13080342 - 1 Aug 2025
Viewed by 181
Abstract
As a new type of alloy system composed of five or more principal components, high-entropy alloys demonstrate outstanding comprehensive performance in the field of friction and wear through the synergistic effects of the high-entropy effect, lattice distortion effect, hysteresis diffusion effect and cocktail [...] Read more.
As a new type of alloy system composed of five or more principal components, high-entropy alloys demonstrate outstanding comprehensive performance in the field of friction and wear through the synergistic effects of the high-entropy effect, lattice distortion effect, hysteresis diffusion effect and cocktail effect. This paper systematically reviews the research progress on the friction and wear properties of high-entropy alloys. The mechanisms of metal elements such as Al, Ti, Cu and Nb through solid solution strengthening, second-phase precipitation and oxide film formation were analyzed emphatically. And non-metallic elements such as C, Si, and B form and strengthen the regulation laws of their tribological properties. The influence of working conditions, such as high temperature, ocean, and hydrogen peroxide on the friction and wear behavior of high-entropy alloys by altering the wear mechanism, was discussed. The influence of test conditions such as load, sliding velocity and friction pair matching on its friction coefficient and wear rate was expounded. It is pointed out that high-entropy alloys have significant application potential in key friction components, providing reference and guidance for the further development and application of high-entropy alloys. Full article
(This article belongs to the Special Issue Tribological Performance of High-Entropy Alloys)
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4 pages, 134 KiB  
Editorial
Tribology of Textured Surfaces
by Min Zou, Mahyar Afshar-Mohajer and Robert A. Fleming
Lubricants 2025, 13(8), 339; https://doi.org/10.3390/lubricants13080339 - 31 Jul 2025
Viewed by 108
Abstract
Surface texturing has emerged as a transformative approach to improving friction, lubrication, and wear across a wide range of mechanical components [...] Full article
(This article belongs to the Special Issue Tribology of Textured Surfaces)
18 pages, 8192 KiB  
Article
Microstructure, Mechanical Properties, and Tribological Behavior of Friction Stir Lap-Welded Joints Between SiCp/Al–Fe–V–Si Composites and an Al–Si Alloy
by Shunfa Xiao, Pinming Feng, Xiangping Li, Yishan Sun, Haiyang Liu, Jie Teng and Fulin Jiang
Materials 2025, 18(15), 3589; https://doi.org/10.3390/ma18153589 - 30 Jul 2025
Viewed by 221
Abstract
Aluminum matrix composites provide an ideal solution for lightweight brake disks, but conventional casting processes are prone to crack initiation due to inhomogeneous reinforcement dispersion, gas porosity, and inadequate toughness. To break the conventional trade-off between high wear resistance and low toughness of [...] Read more.
Aluminum matrix composites provide an ideal solution for lightweight brake disks, but conventional casting processes are prone to crack initiation due to inhomogeneous reinforcement dispersion, gas porosity, and inadequate toughness. To break the conventional trade-off between high wear resistance and low toughness of brake disks, this study fabricated a bimetallic structure of SiCp/Al–Fe–V–Si aluminum matrix composite and cast ZL101 alloy using friction stir lap welding (FSLW). Then, the microstructural evolution, mechanical properties, and tribological behavior of the FSLW joints were studied by XRD, SEM, TEM, tensile testing, and tribological tests. The results showed that the FSLW process homogenized the distribution of SiC particle reinforcements in the SiCp/Al–Fe–V–Si composites. The Al12(Fe,V)3Si heat-resistant phase was not decomposed or coarsened, and the mechanical properties were maintained. The FSLW process refined the grains of the ZL101 aluminum alloy through recrystallization and fragmented eutectic silicon, improving elongation to 22%. A metallurgical bond formed at the joint interface. Tensile fracture occurred within the ZL101 matrix, demonstrating that the interfacial bond strength exceeded the alloy’s load-bearing capacity. In addition, the composites exhibited significantly enhanced wear resistance after FSLW, with their wear rate reduced by approximately 40% compared to the as-received materials, which was attributed to the homogenized SiC particle distribution and the activation of an oxidative wear mechanism. Full article
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30 pages, 3838 KiB  
Review
Advances in the Tribological Performance of Graphene Oxide and Its Composites
by Mayur B. Wakchaure and Pradeep L. Menezes
Materials 2025, 18(15), 3587; https://doi.org/10.3390/ma18153587 - 30 Jul 2025
Viewed by 280
Abstract
Graphene oxide (GO), a derivative of graphene, has attracted significant attention in tribological applications due to its unique structural, mechanical, and chemical properties. This review highlights the influence of GO and its composites on friction and wear performance across various engineering systems. The [...] Read more.
Graphene oxide (GO), a derivative of graphene, has attracted significant attention in tribological applications due to its unique structural, mechanical, and chemical properties. This review highlights the influence of GO and its composites on friction and wear performance across various engineering systems. The paper explores GO’s key properties, such as its high surface area, layered morphology, and abundant functional groups. These features contribute to reduced shear resistance, tribofilm formation, and improved load-bearing capacity. A detailed analysis of GO-based composites, including polymer, metal, and ceramic matrices, reveals those small additions of GO (typically 0.1–2 wt%) result in substantial reductions in coefficient of friction and wear rate, with improvements ranging between 30–70%, depending on the application. The tribological mechanisms, including self-lubrication, dispersion, thermal stability, and interface interactions, are discussed to provide insights into performance enhancement. Furthermore, the effects of electrochemical environment, functional group modifications, and external loading conditions on GO’s tribological behavior are examined. Despite these advantages, challenges such as scalability, agglomeration, and material compatibility persist. Overall, the paper demonstrates that GO is a promising additive for advanced tribological systems, while also identifying key limitations and future research directions. Full article
(This article belongs to the Special Issue Tribology in Advanced Materials)
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15 pages, 4423 KiB  
Article
Effect of B Element Doping on High-Temperature Tribological Properties of WS2-Based Composite Coatings
by Songmin Zhang, Xiaopeng Zhang, Haichao Cai, Zixuan Huang, Yujun Xue, Lulu Pei and Bowei Kang
Lubricants 2025, 13(8), 332; https://doi.org/10.3390/lubricants13080332 - 30 Jul 2025
Viewed by 172
Abstract
WS2 coating, as a solid lubricating material, plays a significant role in the lubrication of rotating components in spacecraft. During the launch process, however, spacecraft are exposed to high-temperature and humid atmospheric environments, which can lead to oxidative failure in the coating, [...] Read more.
WS2 coating, as a solid lubricating material, plays a significant role in the lubrication of rotating components in spacecraft. During the launch process, however, spacecraft are exposed to high-temperature and humid atmospheric environments, which can lead to oxidative failure in the coating, thereby limiting its engineering applications. By doping with B elements, B/WS2 was successfully prepared as a composite coating. The results demonstrate that the fabricated coating exhibits excellent high-temperature tribological performance in atmospheric environments. The mechanism through which B doping improves the high-temperature friction and wear properties of the WS2 composite coating was revealed through high-temperature friction and wear tests. With the incorporation of B elements, the average friction coefficient of the coating was 0.071, and the wear rate was 7.63 × 10−7 mm3·N−1·m−1, with the wear mechanisms identified as abrasive wear and spalling. Due to high-temperature oxidation, thermal decomposition effects, and the formation of WB4 during sputtering, the wear resistance and anti-plastic deformation capability of the coating were further improved. Compared to room-temperature test conditions, the B/WS2 composite coating at different high temperatures exhibited superior friction coefficients and wear rates. Notably, at 150 °C, the average friction coefficient was as low as 0.015, and the wear forms were abrasive wear and adhesive wear. Full article
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25 pages, 2151 KiB  
Article
A Possibility of Tribological Investigation of Physicochemical Processes in a Friction Pair Operating Under Selective Transfer Conditions
by Filip Ilie, Daniel Constantin Cotici and Andrei-Florin Hristache
Lubricants 2025, 13(8), 331; https://doi.org/10.3390/lubricants13080331 - 30 Jul 2025
Viewed by 211
Abstract
The physicochemical processes that occur during selective transfer in the contact area of a bronze/steel friction pair lubricated with glycerin are experimentally studied by the polarization method to observe how they influence the tribological properties (friction and wear) of the pair. The proposed [...] Read more.
The physicochemical processes that occur during selective transfer in the contact area of a bronze/steel friction pair lubricated with glycerin are experimentally studied by the polarization method to observe how they influence the tribological properties (friction and wear) of the pair. The proposed method allows for the study of tribochemical transformations of glycerin and the friction pair materials during the work process with selective transfer. The analysis of the experimental results allows for the establishment of the conditions for a stable and stationary selective transfer during the operation of the bronze/steel pair, by friction, at which the friction coefficient (COF) values and wear are low. This was achieved by implementing continuous lubrication with fresh glycerin in the contact area, choosing the optimal flow rate, and maintaining an optimal ratio between glycerin and the chemical transformation products, within well-established limits, to avoid undesirable consequences. Acrolein, as a product of chemical transformation (resulting from the catalytic dehydration of glycerin), is the most important for the initiation and stability of the selective transfer, and as the main reaction product, also represents a pathway of regeneration. Thus, it was found that the friction relative moments and the acrolein concentration presented conclusive/specific results at loads of 4–15 MPa and a sliding speed of 0.3 m/s. The optimum lubricant entry speed is 15–30 mg/min, for a minimum COF and reduced wear (about 0.028–0.03 at relatively high operating temperatures (45 and 60 °C)), and at low temperatures (30 °C) the minimum COF is about 0.038, but the lubricant inlet entry speed increases considerably, by around 1000 mg/min. Therefore, this paper aims to demonstrate the possibility of moving to another stage of practical use of a friction pair (with greatly improved tribological properties) that operates with selective transfer, much different from the ones still present, using a lubricant with special properties (glycerin). The research method used (polarization) highlights the physicochemical properties, tribochemical transformations of the lubricant, and the friction pair materials present in the contact area, for the understanding, maintenance, and stability of selective transfer, based on experiments, as a novelty compared to other studies. Full article
(This article belongs to the Special Issue Experimental Modelling of Tribosystems)
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15 pages, 2519 KiB  
Article
Twin-Disc Wear Assessment of Solid Stick Flange Lubricants
by Martin David Evans, Zing Siang Lee and Roger Lewis
Lubricants 2025, 13(8), 330; https://doi.org/10.3390/lubricants13080330 - 29 Jul 2025
Viewed by 208
Abstract
Lubrication between the rail gauge face and wheel flange is necessary to improve vehicle performance and reduce component wear. One way to achieve this is to use a solid stick loaded against the wheel flange. This paper details twin-disc testing of eight stick [...] Read more.
Lubrication between the rail gauge face and wheel flange is necessary to improve vehicle performance and reduce component wear. One way to achieve this is to use a solid stick loaded against the wheel flange. This paper details twin-disc testing of eight stick products according to Annex H of EN 15427-2-1:2022 (previously Annex L of EN 16028:2012) and then describes a new assessment methodology using conditions more relevant to field application. EN 15427-2-1:2022 specifies a test involving the application of the product during wheel–rail specimen contact. Once a specified time has elapsed, product application ceases, and performance is assessed as the time taken for the friction coefficient to return to a nominal dry value. This is described as “retentivity”. In the new test, the product is applied whilst wheel and rail are out of contact, to allow the product to build up on the wheel, then the specimens are put into contact, under conditions representing 150 m of continuous, heavy flange contact; this process is repeated a set number of times. The new test showed that products that failed the current friction criteria successfully protect the wheel and rail from wear, which is ultimately the aim of the product application. Full article
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16 pages, 14261 KiB  
Article
Effect of Er Microalloying and Zn/Mg Ratio on Dry Sliding Wear Properties of Al-Zn-Mg Alloy
by Hanyu Chen, Xiaolan Wu, Xuxu Ding, Shengping Wen, Liang Hong, Kunyuan Gao, Wu Wei, Li Rong, Hui Huang and Zuoren Nie
Materials 2025, 18(15), 3541; https://doi.org/10.3390/ma18153541 - 29 Jul 2025
Viewed by 256
Abstract
In this study, dry sliding wear tests were carried out on Er, Zr-microalloyed Al-Zn-Mg alloys with different Zn/Mg ratios under 30–70 N loads. The effects of the Zn/Mg content ratio and Er microalloying on the friction coefficient, wear volume loss, worn surface, and [...] Read more.
In this study, dry sliding wear tests were carried out on Er, Zr-microalloyed Al-Zn-Mg alloys with different Zn/Mg ratios under 30–70 N loads. The effects of the Zn/Mg content ratio and Er microalloying on the friction coefficient, wear volume loss, worn surface, and wear debris during the friction process of Al-Zn-Mg alloys were analyzed. At the load of 30 N, abrasive wear, fatigue wear, and adhesive wear were synergistically involved. At a load of 50 N, the abrasive wear dominated, accompanied by fatigue wear and adhesive wear. At a load of 70 N, the primary wear mechanisms transitioned to abrasive wear and fatigue wear, with additional adhesive wear and oxidative wear observed. Reducing the Zn/Mg ratio mitigated wear volume across all tested loads. For the Al4.5Zn1.5Mg alloy, Er microalloying significantly reduced wear volume under moderate-to-low loads (30 N, 50 N). Full article
(This article belongs to the Section Metals and Alloys)
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32 pages, 1403 KiB  
Review
Advancements in Environmentally Friendly Lubricant Technologies: Towards Sustainable Performance and Efficiency
by Iwona Wilińska and Sabina Wilkanowicz
Energies 2025, 18(15), 4006; https://doi.org/10.3390/en18154006 - 28 Jul 2025
Viewed by 325
Abstract
The advancement of next-generation lubricants is pivotal for enhancing energy efficiency and mitigating environmental impacts across diverse industrial applications. This review systematically examines recent developments in lubricant technologies, with a particular focus on sustainable strategies incorporating bio-based feedstocks, nanostructured additives, and hybrid formulations. [...] Read more.
The advancement of next-generation lubricants is pivotal for enhancing energy efficiency and mitigating environmental impacts across diverse industrial applications. This review systematically examines recent developments in lubricant technologies, with a particular focus on sustainable strategies incorporating bio-based feedstocks, nanostructured additives, and hybrid formulations. These innovations are designed to reduce friction and wear, decrease energy consumption, and prolong the operational lifespan of mechanical systems. A critical assessment of tribological behavior, environmental compatibility, and functional performance is presented. Furthermore, the integration of artificial intelligence (AI) into lubricant formulation and performance prediction is explored, highlighting its potential to accelerate development cycles and enable application-specific optimization through data-driven approaches. The findings emphasize the strategic role of eco-innovative lubricants in supporting low-carbon technologies and facilitating the transition toward sustainable energy systems. Full article
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18 pages, 3569 KiB  
Article
The Influence of Carbon Nanotube Additives on the Efficiency and Vibrations of Worm Gears
by Milan Bukvić, Aleksandar Vencl, Saša Milojević, Aleksandar Skulić, Sandra Gajević and Blaža Stojanović
Lubricants 2025, 13(8), 327; https://doi.org/10.3390/lubricants13080327 - 26 Jul 2025
Viewed by 251
Abstract
Worm gears are used in various mechanical constructions, especially in heavy industrial plants, where they are exposed to high operating loads, large torques, and high temperatures, particularly in conditions where it is necessary for the input and output shafts to be at an [...] Read more.
Worm gears are used in various mechanical constructions, especially in heavy industrial plants, where they are exposed to high operating loads, large torques, and high temperatures, particularly in conditions where it is necessary for the input and output shafts to be at an angle of 90°. Regarding tribological optimization, the application of carbon nanotube in lubricants can lead to significant improvements in the performance characteristics of worm gears, both in terms of increasing efficiency and reducing the coefficient of friction and wear, as well as minimizing mechanical losses, noise, and vibrations. The objective of this study is for the research results, through the use of oil with varying percentages of carbon nanotube additives (CNTs), to contribute to the optimization of worm gears by improving efficiency, extending service life, and reducing vibrations—both within the gearbox itself and within the industrial facility where it is applied. The research methodology involved laboratory testing of a worm gear using lubricants with varying concentrations of carbon nanotube. During the experiment, measurements of efficiency, vibrations, and noise levels were conducted in order to determine the impact of these additives on the operational performance of the gear system. The main contribution of this research is reflected in the experimental confirmation that the use of lubricants with optimized concentrations of carbon nanotube significantly enhances the operational performance of worm gears by increasing efficiency and reducing vibrations and noise, thereby enabling tribological optimization that contributes to improved reliability, extended service life, and enhanced workplace ergonomics under demanding industrial conditions. Furthermore, experimental investigations have shown that the efficiency of the gearbox increases from an initial value of 0.42–0.65, which represents an increase of 54%, the vibrations of the worm gear decrease from an initial value of 5.83–2.56 mm/s2, which represents an decrease of 56%, while the noise was reduced from 87.5 to 77.2 dB, which represents an decrease of 12% with the increasing percentage of carbon nanotube additives in the lubricant, up to a maximum value of 1%. However, beyond this experimentally determined threshold, a decrease in the efficiency of the tested worm gearbox, as well as an increase in noise and vibration levels was recorded. Full article
(This article belongs to the Special Issue Friction–Vibration Interactions)
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26 pages, 10667 KiB  
Article
Influence of Nitrogen and Hydrogen Addition on Composition, Morphology, Adhesion, and Wear Resistance of Amorphous Carbon Coatings Produced by RFCVD Method on Surface-Hardened Ultra-Fine Grained Bainitic 30HGSNA Steel
by Karol Wunsch, Tomasz Borowski, Emilia Skołek, Agata Roguska, Rafał Chodun, Michał Urbańczyk, Krzysztof Kulikowski, Maciej Spychalski, Andrzej Wieczorek and Jerzy Robert Sobiecki
Coatings 2025, 15(8), 877; https://doi.org/10.3390/coatings15080877 - 26 Jul 2025
Viewed by 319
Abstract
Ultra-fine-grained bainitic (UFGB) steels offer excellent mechanical properties, which can be further improved by applying diamond-like carbon (DLC) coatings. However, poor adhesion between the coating and substrate remains a key limitation. Since the steel’s microstructure degrades at high temperatures, enhancing adhesion without heating [...] Read more.
Ultra-fine-grained bainitic (UFGB) steels offer excellent mechanical properties, which can be further improved by applying diamond-like carbon (DLC) coatings. However, poor adhesion between the coating and substrate remains a key limitation. Since the steel’s microstructure degrades at high temperatures, enhancing adhesion without heating the substrate is essential. This study investigates surface hardening combined with simultaneous nitrogen and hydrogen doping during the Radio Frequency Chemical Vapor Deposition (RFCVD) process to improve coating performance. Varying gas compositions were tested to assess their effects on coating properties. Nitrogen incorporation decreased hardness from 12 GPa to 9 GPa but improved adhesion, while hydrogen limited damage after coating failure. Optimizing the gas mixture led to enhanced adhesion and wear resistance. Raman and X-ray photoelectron spectroscopy (XPS) analyses confirmed that the optimized coatings had the highest sp3 bond content and elevated nitrogen levels. While both hardness and adhesion contributed to wear resistance, no direct link to coating thickness was found. Overall, co-doping with nitrogen and hydrogen is an effective approach to improve adhesion and wear resistance without requiring high processing temperatures or complex equipment. Full article
(This article belongs to the Special Issue Recent Advances in Surface Functionalisation, 2nd Edition)
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14 pages, 2733 KiB  
Article
Study on Microstructure and Wear Resistance of Multi-Layer Laser Cladding Fe901 Coating on 65 Mn Steel
by Yuzhen Yu, Weikang Ding, Xi Wang, Donglu Mo and Fan Chen
Materials 2025, 18(15), 3505; https://doi.org/10.3390/ma18153505 - 26 Jul 2025
Viewed by 254
Abstract
65 Mn is a high-quality carbon structural steel that exhibits excellent mechanical properties and machinability. It finds broad applications in machinery manufacturing, agricultural tools, and mining equipment, and is commonly used for producing mechanical parts, springs, and cutting tools. Fe901 is an iron-based [...] Read more.
65 Mn is a high-quality carbon structural steel that exhibits excellent mechanical properties and machinability. It finds broad applications in machinery manufacturing, agricultural tools, and mining equipment, and is commonly used for producing mechanical parts, springs, and cutting tools. Fe901 is an iron-based alloy that exhibits excellent hardness, structural stability, and wear resistance. It is widely used in surface engineering applications, especially laser cladding, due to its ability to form dense and crack-free metallurgical coatings. To enhance the surface hardness and wear resistance of 65 Mn steel, this study employs a laser melting process to deposit a multi-layer Fe901 alloy coating. The phase composition, microstructure, microhardness, and wear resistance of the coatings are investigated using X-ray diffraction (XRD), optical microscopy, scanning electron microscopy (SEM), Vickers hardness testing, and friction-wear testing. The results show that the coatings are dense and uniform, without visible defects. The main phases in the coating include solid solution, carbides, and α-phase. The microstructure comprises dendritic, columnar, and equiaxed crystals. The microhardness of the cladding layer increases significantly, with the multilayer coating reaching 3.59 times the hardness of the 65 Mn substrate. The coatings exhibit stable and relatively low friction coefficients ranging from 0.38 to 0.58. Under identical testing conditions, the wear resistance of the coating surpasses that of the substrate, and the multilayer coating shows better wear performance than the single-layer one. Full article
(This article belongs to the Section Advanced Composites)
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