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26 pages, 15885 KiB  
Article
Comparative Analysis of Fully Floating and Semi-Floating Ring Bearings in High-Speed Turbocharger Rotordynamics
by Kyuman Kim and Keun Ryu
Lubricants 2025, 13(8), 338; https://doi.org/10.3390/lubricants13080338 (registering DOI) - 31 Jul 2025
Viewed by 45
Abstract
This study presents a detailed experimental comparison of the rotordynamic and thermal performance of automotive turbochargers supported by two distinct hydrodynamic bearing configurations: fully floating ring bearings (FFRBs) and semi-floating ring bearings (SFRBs). While both designs are widely used in commercial turbochargers, they [...] Read more.
This study presents a detailed experimental comparison of the rotordynamic and thermal performance of automotive turbochargers supported by two distinct hydrodynamic bearing configurations: fully floating ring bearings (FFRBs) and semi-floating ring bearings (SFRBs). While both designs are widely used in commercial turbochargers, they exhibit significantly different dynamic behaviors due to differences in ring motion and fluid film interaction. A cold air-driven test rig was employed to assess vibration and temperature characteristics across a range of controlled lubricant conditions. The test matrix included oil supply pressures from 2 bar (g) to 4 bar (g) and temperatures between 30 °C and 70 °C. Rotor speeds reached up to 200 krpm (thousands of revolutions per minute), and data were collected using a high-speed data acquisition system, triaxial accelerometers, and infrared (IR) thermal imaging. Rotor vibration was characterized through waterfall and Bode plots, while jump speeds and thermal profiles were analyzed to evaluate the onset and severity of instability. The results demonstrate that the FFRB configuration is highly sensitive to oil supply parameters, exhibiting strong subsynchronous instabilities and hysteresis during acceleration–deceleration cycles. In contrast, the SFRB configuration consistently provided superior vibrational stability and reduced sensitivity to lubricant conditions. Changes in lubricant supply conditions induced a jump speed variation in floating ring bearing (FRB) turbochargers that was approximately 3.47 times larger than that experienced by semi-floating ring bearing (SFRB) turbochargers. Furthermore, IR images and oil outlet temperature data confirm that the FFRB system experiences greater heat generation and thermal gradients, consistent with higher energy dissipation through viscous shear. This study provides a comprehensive assessment of both bearing types under realistic high-speed conditions and highlights the advantages of the SFRB configuration in improving turbocharger reliability, thermal performance, and noise suppression. The findings support the application of SFRBs in high-performance automotive systems where mechanical stability and reduced frictional losses are critical. Full article
(This article belongs to the Collection Rising Stars in Tribological Research)
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22 pages, 13186 KiB  
Article
Detection of Steel Reinforcement in Concrete Using Active Microwave Thermography and Neural Network-Based Analysis
by Barbara Szymanik, Maja Kocoń, Sam Ang Keo, Franck Brachelet and Didier Defer
Appl. Sci. 2025, 15(15), 8419; https://doi.org/10.3390/app15158419 (registering DOI) - 29 Jul 2025
Viewed by 172
Abstract
Non-destructive evaluation of reinforced concrete structures is essential for effective maintenance and safety assessments. This study explores the combined use of active microwave thermography and deep learning to detect and localize steel reinforcement within concrete elements. Numerical simulations were developed to model the [...] Read more.
Non-destructive evaluation of reinforced concrete structures is essential for effective maintenance and safety assessments. This study explores the combined use of active microwave thermography and deep learning to detect and localize steel reinforcement within concrete elements. Numerical simulations were developed to model the thermal response of reinforced concrete subjected to microwave excitation, generating synthetic thermal images representing the surface temperature patterns of reinforced concrete, influenced by subsurface steel reinforcement. These images served as training data for a deep neural network designed to identify and localize rebar positions based on thermal patterns. The model was trained exclusively on simulation data and subsequently validated using experimental measurements obtained from large-format concrete slabs incorporating a structured layout of embedded steel reinforcement bars. Surface temperature distributions obtained through infrared imaging were compared with model predictions to evaluate detection accuracy. The results demonstrate that the proposed method can successfully identify the presence and approximate location of internal reinforcement without damaging the concrete surface. This approach introduces a new pathway for contactless, automated inspection using a combination of physical modeling and data-driven analysis. While the current work focuses on rebar detection and localization, the methodology lays the foundation for broader applications in non-destructive testing of concrete infrastructure. Full article
(This article belongs to the Special Issue Innovations in Artificial Neural Network Applications)
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22 pages, 9343 KiB  
Article
Effect of Polymer Molecular Weight on the Structure and Properties of Ultra-High-Molecular-Weight Polyethylene Membranes Prepared via Controlled Swelling
by Andrey V. Basko, Konstantin V. Pochivalov, Tatyana N. Lebedeva, Mikhail Y. Yurov, Alexander S. Zabolotnov, Sergey S. Gostev, Alexey A. Yushkin, Alexey V. Volkov and Sergei V. Bronnikov
Polymers 2025, 17(15), 2044; https://doi.org/10.3390/polym17152044 - 26 Jul 2025
Viewed by 301
Abstract
A recently proposed method called “controlled swelling of monolithic films” was implemented to prepare ultra-high-molecular-weight polyethylene (UHMWPE) ultrafiltration membranes. For the first time, the effect of UHMWPE molecular weight (MW) on the structure and properties of the membranes prepared via this special case [...] Read more.
A recently proposed method called “controlled swelling of monolithic films” was implemented to prepare ultra-high-molecular-weight polyethylene (UHMWPE) ultrafiltration membranes. For the first time, the effect of UHMWPE molecular weight (MW) on the structure and properties of the membranes prepared via this special case of thermally induced phase separation was studied in detail. The morphology and properties of the membranes were studied using SEM, DSC, liquid–liquid displacement porometry, and standard methods for the evaluation of mechanical properties, permeance, rejection, and abrasion resistance. High-quality membranes with a tensile strength of 5.0–17.8 MPa, a mean pore size of 25–50 nm, permeance of 17–107 L m−2 h−1 bar−1, rejection of model contaminant (blue dextran) of 72–98%, and great abrasion resistance can be prepared only if the MW of the polymer in the initial monolithic film is sufficiently high. The properties of the membranes can effectively be controlled by changing the MW of the polymer and the mass fraction of the latter in the swollen film. Shrinkage is responsible for the variation in the membrane properties. The membranes prepared from a higher-MW polymer are more prone to shrinking after the removal of the solvent. Shrinkage decreases before rising again and minimizes with an increase in the polymer content in the swollen film. Full article
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27 pages, 3540 KiB  
Article
Multi-Objective Optimization of IME-Based Acoustic Tweezers for Mitigating Node Displacements
by Hanjui Chang, Yue Sun, Fei Long and Jiaquan Li
Polymers 2025, 17(15), 2018; https://doi.org/10.3390/polym17152018 - 24 Jul 2025
Viewed by 242
Abstract
Acoustic tweezers, as advanced micro/nano manipulation tools, play a pivotal role in biomedical engineering, microfluidics, and precision manufacturing. However, piezoelectric-based acoustic tweezers face performance limitations due to multi-physical coupling effects during microfabrication. This study proposes a novel approach using injection molding with embedded [...] Read more.
Acoustic tweezers, as advanced micro/nano manipulation tools, play a pivotal role in biomedical engineering, microfluidics, and precision manufacturing. However, piezoelectric-based acoustic tweezers face performance limitations due to multi-physical coupling effects during microfabrication. This study proposes a novel approach using injection molding with embedded electronics (IMEs) technology to fabricate piezoelectric micro-ultrasonic transducers with micron-scale precision, addressing the critical issue of acoustic node displacement caused by thermal–mechanical coupling in injection molding—a problem that impairs wave transmission efficiency and operational stability. To optimize the IME process parameters, a hybrid multi-objective optimization framework integrating NSGA-II and MOPSO is developed, aiming to simultaneously minimize acoustic node displacement, volumetric shrinkage, and residual stress distribution. Key process variables—packing pressure (80–120 MPa), melt temperature (230–280 °C), and packing time (15–30 s)—are analyzed via finite element modeling (FEM) and validated through in situ tie bar elongation measurements. The results show a 27.3% reduction in node displacement amplitude and a 19.6% improvement in wave transmission uniformity compared to conventional methods. This methodology enhances acoustic tweezers’ operational stability and provides a generalizable framework for multi-physics optimization in MEMS manufacturing, laying a foundation for next-generation applications in single-cell manipulation, lab-on-a-chip systems, and nanomaterial assembly. Full article
(This article belongs to the Collection Feature Papers in Polymer Processing and Engineering)
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18 pages, 2410 KiB  
Article
Nanostructured Cellulose Acetate Membranes Embedded with Al2O3 Nanoparticles for Sustainable Wastewater Treatment
by Ines Elaissaoui, Soumaya Sayeb, Mouna Mekki, Francesca Russo, Alberto Figoli, Karima Horchani-Naifer and Dorra Jellouli Ennigrou
Coatings 2025, 15(7), 823; https://doi.org/10.3390/coatings15070823 - 15 Jul 2025
Viewed by 340
Abstract
Electrospun nanofiber membranes based on cellulose acetate (CA) have gained increasing attention for wastewater treatment due to their high surface area, tuneable structure, and ease of functionalization. In this study, the performance of CA membranes was enhanced by incorporating aluminum oxide (Al2 [...] Read more.
Electrospun nanofiber membranes based on cellulose acetate (CA) have gained increasing attention for wastewater treatment due to their high surface area, tuneable structure, and ease of functionalization. In this study, the performance of CA membranes was enhanced by incorporating aluminum oxide (Al2O3) nanoparticles (NPs) at varying concentrations (0–2 wt.%). The structural, morphological, and thermal properties of the resulting CA/Al2O3 nanocomposite membranes were investigated through FTIR, XRD, SEM, water contact angle (WCA), pore size measurements, and DSC analyses. FTIR and XRD confirmed strong interactions and the uniform dispersion of the Al2O3 NPs within the CA matrix. The incorporation of Al2O3 improved membrane hydrophilicity, reducing the WCA from 107° to 35°, and increased the average pore size from 0.62 µm to 0.86 µm. These modifications led to enhanced filtration performance, with the membrane containing 2 wt.% Al2O3 achieving a 99% removal efficiency for Indigo Carmine (IC) dye, a maximum adsorption capacity of 45.59 mg/g, and a high permeate flux of 175.47 L·m−2 h−1 bar−1. Additionally, phytotoxicity tests using Lactuca sativa seeds showed a significant increase in germination index from 20% (untreated) to 88% (treated), confirming the safety of the permeate for potential reuse in agricultural irrigation. These results highlight the effectiveness of Al2O3-modified CA electrospun membranes for sustainable wastewater treatment and water reuse. Full article
(This article belongs to the Section Environmental Aspects in Colloid and Interface Science)
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20 pages, 3537 KiB  
Article
A New Sulfur-Containing Copolymer Created Through the Thermally Induced Radical Copolymerization of Elemental Sulfur with N2,N2-Diallylmelamine Comonomer for Potential CO2 Capture
by Dharrinesh Narendiran, Nurul Hazirah Sumadi, Ali Shaan Manzoor Ghumman, Noor Ashikin Mohamad, Mohamed Mahmoud Nasef, Amin Abbasi and Rashid Shamsuddin
J. Compos. Sci. 2025, 9(7), 362; https://doi.org/10.3390/jcs9070362 - 11 Jul 2025
Viewed by 403
Abstract
Sulfur-containing polymers are unique sustainable materials with promise for the development of various adsorbents for environmental remediation. However, they have not been explored for CO2 capture despite reports on its ability to decontaminate various aqueous pollutants. This study reports on the single-step [...] Read more.
Sulfur-containing polymers are unique sustainable materials with promise for the development of various adsorbents for environmental remediation. However, they have not been explored for CO2 capture despite reports on its ability to decontaminate various aqueous pollutants. This study reports on the single-step synthesis of a diamine-functionalized sulfur-containing copolymer by the thermally induced radical copolymerization of N2,N2-Diallylmelamine (NDAM), a difunctional monomer, with sulfur and explores its use for CO2 capture. The influence of reaction parameters such as the weight ratios of sulfur to NDAM, reaction temperature, time, and the addition of a porogen on the properties of aminated copolymer was investigated. The resulting copolymers were characterized using FTIR, TGA, DSC, SEM, XRD, and BET surface area analyses. The incorporation of NDAM directly imparted amine functionality while stabilizing the polysulfide chains by crosslinking, leading to a thermoset copolymer with an amorphous structure. The addition of a NaCl particle porogen to the S/NDAM mixture generated a mesoporous structure, enabling the resulting copolymer to be tested for CO2 adsorption under varying pressures, leading to an adsorption capacity as high as 517 mg/g at 25 bar. This work not only promotes sustainable hybrid materials that advance green chemistry while aiding CO2 mitigation efforts but also adds value to the abundant amount of sulfur by-products from petroleum refineries. Full article
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18 pages, 5009 KiB  
Article
Preparation of Glass Fiber Reinforced Polypropylene Bending Plate and Its Long-Term Performance Exposed in Alkaline Solution Environment
by Zhan Peng, Anji Wang, Chen Wang and Chenggao Li
Polymers 2025, 17(13), 1844; https://doi.org/10.3390/polym17131844 - 30 Jun 2025
Viewed by 300
Abstract
Glass fiber reinforced polypropylene composite plates have gradually attracted more attention because of their repeated molding, higher toughness, higher durability, and fatigue resistance compared to glass fiber reinforced thermosetting composites. In practical engineering applications, composite plates have to undergo bending effect at different [...] Read more.
Glass fiber reinforced polypropylene composite plates have gradually attracted more attention because of their repeated molding, higher toughness, higher durability, and fatigue resistance compared to glass fiber reinforced thermosetting composites. In practical engineering applications, composite plates have to undergo bending effect at different angles in corrosive environment of concrete, including bending bars from 0~90°, and stirrups of 90°, which may lead to long-term performance degradation. Therefore, it is important to evaluate the long-term performance of glass fiber reinforced polypropylene composite bending plates in an alkali environment. In the current paper, a new bending device is developed to prepare glass fiber reinforced polypropylene bending plates with the bending angles of 60° and 90°. It should be pointed out that the above two bending angles are simulated typical bending bars and stirrups, respectively. The plate is immersed in the alkali solution environment for up to 90 days for long-term exposure. Mechanical properties (tensile properties and shear properties), thermal properties (dynamic mechanical properties and thermogravimetric analysis) and micro-morphology analysis (surface morphology analysis) were systematically designed to evaluate the influence mechanism of bending angle and alkali solution immersion on the long-term mechanical properties. The results show the bending effect leads to the continuous failure of fibers, and the outer fibers break under tension, and the inner fibers buckle under compression, resulting in debonding of the fiber–matrix interface. Alkali solution (OH ions) corrode the surface of glass fiber to form soluble silicate, which is proved by the mass fraction of glass fiber decreased obviously from 79.9% to 73.65% from thermogravimetric analysis. This contributes to the highest degradation ratio of tensile strength was 71.6% (60° bending) and 65.6% (90° bending), respectively, compared to the plate with bending angles of 0°. A high curvature bending angle (such as 90°) leads to local buckling of fibers and plastic deformation of the matrix, forming microcracks and fiber–resin interface bonding at the bending area, which accelerates the chemical erosion and debonding process in the interface area, bringing about an additional maximum 10.56% degradation rate of the shear strength. In addition, the alkali immersion leads to the obvious degradation of storage modulus and thermal decomposition temperature of composite plate. Compared with the other works on the long-term mechanical properties of glass fiber reinforced polypropylene, it can be found that the long-term performance of glass fiber reinforced polypropylene composites is controlled by the corrosive media type, bending angle and immersion time. The research results will provide durability data for glass fiber reinforced polypropylene composites used in concrete as stirrups. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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30 pages, 13022 KiB  
Article
Dynamic Mechanical Characteristics and Fracture Size Effect of Coal Sandstone Under High-Temperature and High-Strain Rate Coupling Action
by Ming Li, Fuqiang Zhu, Yiwen Mao, Fangwei Fan, Boyuan Wu and Jishuo Deng
Fractal Fract. 2025, 9(6), 381; https://doi.org/10.3390/fractalfract9060381 - 15 Jun 2025
Cited by 2 | Viewed by 472
Abstract
The deformation control of surrounding rock in the combustion air zone is crucial for the safety and efficiency of underground coal gasification (UCG) projects. Coal-bearing sandstone, a common surrounding rock in UCG chambers, features a brittle structure composed mainly of quartz, feldspar, and [...] Read more.
The deformation control of surrounding rock in the combustion air zone is crucial for the safety and efficiency of underground coal gasification (UCG) projects. Coal-bearing sandstone, a common surrounding rock in UCG chambers, features a brittle structure composed mainly of quartz, feldspar, and clay minerals. Its mechanical behavior under high-temperature and dynamic loading is complex and significantly affects rock stability. To investigate the deformation and failure mechanisms under thermal–dynamic coupling, this study conducted uniaxial impact compression tests using a high-temperature split Hopkinson pressure bar (HT-SHPB) system. The focus was on analyzing mechanical response, energy dissipation, and fragmentation characteristics under varying temperature and strain rate conditions. The results show that the dynamic elastic modulus, compressive strength, fractal dimension of fragments, energy dissipation density, and energy consumption rate all increase initially with temperature and then decrease, with inflection points observed at 400 °C. Conversely, dynamic peak strain first decreases and then increases with rising temperature, also showing a turning point at 400 °C. This indicates a shift in the deformation and failure mode of the material. The findings provide critical insights into the thermo-mechanical behavior of coal-bearing sandstone under extreme conditions and offer a theoretical basis for designing effective deformation control strategies in underground coal gasification projects. Full article
(This article belongs to the Section Engineering)
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13 pages, 4682 KiB  
Communication
Seven-Channel Polyethersulfone Hollow-Fiber Membrane Preparation with Vapor-Induced Phase Separation
by Xiaoyao Wang, Zhiyuan Hao, Rui Huang, Yajing Huang, Huiqun Zhang and Xiujuan Hao
Membranes 2025, 15(6), 175; https://doi.org/10.3390/membranes15060175 - 10 Jun 2025
Viewed by 924
Abstract
Polyethersulfone (PES) has been widely used to fabricate hollow-fiber ultrafiltration membranes due to its good oxidative, thermal, and hydrolytic stability. Typical PES hollow-fiber membranes with a single bore have limited strength and may break under uneven pressure and vibration during membrane backwashing. Multi-channel [...] Read more.
Polyethersulfone (PES) has been widely used to fabricate hollow-fiber ultrafiltration membranes due to its good oxidative, thermal, and hydrolytic stability. Typical PES hollow-fiber membranes with a single bore have limited strength and may break under uneven pressure and vibration during membrane backwashing. Multi-channel hollow-fiber membranes have stronger breaking force due to their larger cross-sectional area, but fabricating them remains challenging due to the difficulty in controlling the phase inversion process. This study uses the vapor-induced phase separation (VIPS) method to fabricate a seven-channel PES hollow-fiber membrane, and the air gap and air relative humidity can help in membrane morphology control. Moreover, carboxylic graphene quantum dots (CGQDs) are first used in ultrafiltration membranes to increase membrane porosity and hydrophilicity. We found that the membrane prepared with a 7.5% CGQD mass fraction, a 10 cm air gap, and 99% relative humidity had the highest flux and porosity; the membrane pore size distribution was concentrated at 72 nm, and the pure water flux could reach 464 L·m−2 h−1·bar−1. In the long-term filtration performance test, the membrane can reject more than about 15% TOC and 84% turbidity at 50 L·m−2 h−1 flux, confirming its stability for water purification applications. Full article
(This article belongs to the Special Issue Membrane Technologies for Water Purification)
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20 pages, 10830 KiB  
Article
An Experimental Study of Glycerol Carbonate Synthesis over g-C3N4 Catalysts
by Mirna Lea Charif, Dragoș Mihael Ciuparu, Ioana Lavinia Lixandru Matei, Gabriel Vasilievici, Ionuț Banu, Marian Băjan, Dorin Bomboș, Cristina Dușescu-Vasile, Iuliana Veronica Ghețiu, Cașen Panaitescu and Rami Doukeh
Appl. Sci. 2025, 15(11), 6236; https://doi.org/10.3390/app15116236 - 1 Jun 2025
Viewed by 2275
Abstract
This study examines a catalyst based on graphitic carbon nitride (g-C3N4) for synthesizing glycerol carbonate through the coupling reaction of glycerol and CO2. In this research, we focus on simultaneously improving CO2 emission reduction and glycerol [...] Read more.
This study examines a catalyst based on graphitic carbon nitride (g-C3N4) for synthesizing glycerol carbonate through the coupling reaction of glycerol and CO2. In this research, we focus on simultaneously improving CO2 emission reduction and glycerol valorization by co-doping g-C3N4 with phosphorus (P), sulfur (S), magnesium (Mg), and lithium (Li) for a better catalytic performance. The catalysts were prepared through a one-step thermal condensation process and characterized using XRD, SEM, TGA, FTIR, and nitrogen adsorption–desorption techniques. The co-doping further enhanced the surface chemical properties, Lewis acidity, basicity, and thermal stability, evidenced by the lower crystallinity, wider pore, and better catalytic performance as assessed through glycerol carbonylation reaction, optimized using a Box–Behnken design. The MgPSCN catalyst exhibited the highest glycerol conversion (68.72%) and glycerol carbonate yield (44.90%) at 250 °C, using 50 mg catalyst and 10 bar pressure. The model accuracy was validated by ANOVA (R2 > 0.99; p values < 0.0001). The results indicated that doping significantly enhanced the catalytic performance, most likely due to improved electron charge transfer and structural distortions within the g-C3N4 framework. Such a process highlights the potential of co-doped g-C3N4 catalysts for the sustainable glycerol utilization and valorization of CO2 through a scalable pathway toward green chemical synthesis—an approach that comes in line with worldwide decarbonization goals. Full article
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15 pages, 2358 KiB  
Article
Effect of Print Orientation and Thermal Aging on the Flexural Strength of Zirconia-Reinforced Three-Dimensional-Printed Restorative Resin Materials
by Yunus Emre Özden, Bengü Doğu Kaya, Pınar Yılmaz Atalı, Fusun Ozer and Zeynep Ozkurt Kayahan
Molecules 2025, 30(11), 2337; https://doi.org/10.3390/molecules30112337 - 27 May 2025
Cited by 1 | Viewed by 627
Abstract
This study evaluated the effects of print orientation and thermal aging on the flexural strength (FS) and flexural modulus (FM) of novel permanent three-dimensional (3D)-printed polymethyl methacrylate (PMMA) resins reinforced with nano-zirconia and nano-silica. Bar-shaped specimens (25 × 2 × 2 mm) were [...] Read more.
This study evaluated the effects of print orientation and thermal aging on the flexural strength (FS) and flexural modulus (FM) of novel permanent three-dimensional (3D)-printed polymethyl methacrylate (PMMA) resins reinforced with nano-zirconia and nano-silica. Bar-shaped specimens (25 × 2 × 2 mm) were fabricated using a digital light processing (DLP) 3D printer (Asiga Max UV, Asiga Inc., Australia) in two orientations (0° and 90°). Specimens underwent three-point bending tests at 24 h and after artificial thermal aging (10,000 and 30,000 cycles) to simulate one and three years of intraoral conditions. Scanning electron microscopy (SEM) was used to analyze fracture patterns. Print orientation did not significantly affect FS or FM (p > 0.05). However, artificial aging significantly reduced FS and FM after 10,000 cycles (p < 0.001), with further deterioration after 30,000 cycles. The micro hybrid resin composite exhibited higher FS than the 3D-printed materials throughout aging. SEM analysis revealed distinct fracture patterns, with 3D-printed resins displaying radial fractures and the micro hybrid composite exhibiting horizontal fractures. These findings indicate that aging plays a more critical role in the long-term mechanical performance of 3D-printed restorative resins than print orientation. This study provides original data on the effects of print orientation and prolonged thermal aging on the mechanical behavior of permanent three-dimensional (3D)-printed dental resins. Furthermore, the comparative evaluation of aging protocols simulating one and three years of intraoral service represents a novel contribution to the existing literature. Further studies are required to optimize the mechanical durability of 3D-printed dental restorations. Full article
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26 pages, 947 KiB  
Systematic Review
Systematic Review on the Behaviour of Carbon and Stainless Steel Reinforcing Bars in Buildings Under High Temperatures
by Alberto Leal Matilla, Daniel Ferrández, Maria Isabel Prieto Barrio and Humberto Varum
Buildings 2025, 15(9), 1539; https://doi.org/10.3390/buildings15091539 - 2 May 2025
Viewed by 701
Abstract
Carbon and stainless steel reinforcing bar behaviour at high temperatures and subsequent cooling is central to fire safety for buildings. This systematic review examines the peer-reviewed literature between 2015 and 2024, concentrating on mechanical performance, microstructural transformation, and responses under various cooling conditions. [...] Read more.
Carbon and stainless steel reinforcing bar behaviour at high temperatures and subsequent cooling is central to fire safety for buildings. This systematic review examines the peer-reviewed literature between 2015 and 2024, concentrating on mechanical performance, microstructural transformation, and responses under various cooling conditions. Since experimental studies on some reinforcing steels in building construction are scarce, based on the selection criteria, they were selected on different standards. Austenitic stainless steels like show better thermal stability, here determined by their ability to preserve mechanical strength and ductility after exposure to fires, compared with carbon steel. Several studies indicate that rapid cooling, especially after exceeding critical transformation temperatures, can induce the formation of martensitic structures in carbon steel. These structures can increase toughness but often lead to reduced ductility and a more brittle mechanical response. These effects are particularly relevant in contexts where structural elements remain in service after a fire. The methodology adheres to PRISMA guidelines, providing transparency and an easily traced choice process. Key gaps in the post-fire performance of reinforcing bar in buildings are established by this review, with future directions in standard fire tests and an examination of effects from cooling under conditions that mimic building settings. Full article
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19 pages, 1731 KiB  
Article
Microbial Decontamination of Fresh-Cut Carrots via Cold Atmospheric Plasma Treatment: Effect on Physicochemical and Nutritional Properties During Storage
by Efe Bakla and Ufuk Bağcı
Foods 2025, 14(9), 1599; https://doi.org/10.3390/foods14091599 - 1 May 2025
Viewed by 635
Abstract
The extension of shelf-life and enhancement of the safety and quality of fresh-cut ready-to-eat vegetables is an ongoing public health concern. The present study investigated the efficacy of cold atmospheric plasma (CAP) treatment for the decontamination of fresh-cut carrots inoculated with Escherichia coli [...] Read more.
The extension of shelf-life and enhancement of the safety and quality of fresh-cut ready-to-eat vegetables is an ongoing public health concern. The present study investigated the efficacy of cold atmospheric plasma (CAP) treatment for the decontamination of fresh-cut carrots inoculated with Escherichia coli. An atmospheric plasma jet system operating at 1 kVA was utilized for treatment with varying plasma jet nozzle to sample distances (10–40 mm), exposure times (10–60 s) and either argon or dry air at 3 bar as working gases. It was demonstrated that both working gases achieved more than 4 log reductions in E. coli within 60 s of treatment while maintaining carrot surface temperatures below 50 °C. During 3-week storage at 4 °C, the immediate effects of plasma treatment on quality parameters were found to be minimal, with no significant changes observed in color (ΔE < 3.0) parameters, β-carotene content, ascorbic acid levels, total phenolic content (TPC), or total antioxidant activity (TAA) following either treatment. Additionally, plasma-treated carrots retained their firmness, showing no significant texture loss, whereas untreated controls experienced a firmness decline of approximately 9% by the end of storage. Notably, TPC increased by up to 41%, and TAA increased significantly (p < 0.05) in plasma-treated samples during storage, especially in dry air plasma-treated carrots. These results demonstrated that CAP treatment can be successfully applied for rapid inactivation of E. coli on fresh-cut carrot surfaces while preserving original quality characteristics during refrigerated storage, offering potential as non-thermal preservation technology for fresh produce. Full article
(This article belongs to the Section Food Microbiology)
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13 pages, 2131 KiB  
Article
The Impact of Tributary Mineralization on Deep-Water Renewal in Lake Baikal During the Thermal Bar
by Bair Tsydenov, Vladislava Churuksaeva, Nikita Trunov, Andrey Bart and Dmitriy Degi
Water 2025, 17(9), 1315; https://doi.org/10.3390/w17091315 - 28 Apr 2025
Viewed by 424
Abstract
Numerical modeling methods were used to study the combined effects of the autumn thermal bar and river inflow mineralization on deep-water renewal processes in Lake Baikal. A cross-section from the Boldakov River to Maloye More strait characterized by great depths was chosen for [...] Read more.
Numerical modeling methods were used to study the combined effects of the autumn thermal bar and river inflow mineralization on deep-water renewal processes in Lake Baikal. A cross-section from the Boldakov River to Maloye More strait characterized by great depths was chosen for the study. Numerical experiments showed that under low levels of river mineralization, downwelling in the thermal bar front played a key role in water mixing. Under high levels of mineralization, the crucial factor was the large-scale near-slope circulation appearing when the stable temperature stratification of deep waters was broken. The haline characteristics of river inflow influenced the time of thermal bar appearance and the speed of propagation in the open lake. Moreover, it was shown that eddy structures can form on both sides of the thermal bar only under minor differences between river and lake mineralization levels. Full article
(This article belongs to the Section Hydrology)
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11 pages, 7699 KiB  
Article
Mechanical and Failure Properties of Deep Grouted Fractured Rock Under Real-Time Coupling of Temperature and Dynamic Load
by Yuhao Jin, Shuo Yang, Hui Guo, Lijun Han, Lanying Huang, Shanjie Su, Pengcheng Huang, Hao Shan and Qian He
Processes 2025, 13(4), 1249; https://doi.org/10.3390/pr13041249 - 21 Apr 2025
Viewed by 502
Abstract
Deep grouting rock engineering is faced with the dual influence of high temperature and dynamic load, which has become a hot issue in geotechnical engineering. This study analyzes the mechanical responses and failure properties of deep-grouted fractured rock under real-time coupling of temperature [...] Read more.
Deep grouting rock engineering is faced with the dual influence of high temperature and dynamic load, which has become a hot issue in geotechnical engineering. This study analyzes the mechanical responses and failure properties of deep-grouted fractured rock under real-time coupling of temperature and dynamic loads through the high-temperature-split Hopkinson pressure bar (HT-SHPB), high-speed imaging, and scanning electron microscopy (SEM) tests. Key findings reveal that (1) the dynamic compressive strength of grouted fractured rock exhibits significant temperature dependency, where the strength increases with the increase of temperature, which has been verified by relevant references. From indoor temperature to 100 °C, the dynamic strength increases moderately, while a pronounced increase is observed between 100 °C and 300 °C. (2) In contrast, the dynamic peak strain demonstrates a two-stage evolution, which sharply rises from indoor temperature to 100 °C, followed by a slowly rise from 100 °C to 300 °C. (3) Macroscopically, impact fractures preferentially initiate as parallel lines at the extremities of pre-existing grouted fractures, consistent with stress concentration patterns under dynamic loading. Microscopic analysis reveals that grouting materials effectively suppress micro-crack generation and propagation at 300 °C, attributed to thermally enhanced cementation and pore-filling effects, explaining the variation of the macroscopic dynamic strength with temperature from the microscopic point of view. Full article
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