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20 pages, 4901 KiB  
Article
Study on the Adaptability of FBG Sensors Encapsulated in CNT-Modified Gel Material for Asphalt Pavement
by Tengteng Guo, Xu Guo, Yuanzhao Chen, Chenze Fang, Jingyu Yang, Zhenxia Li, Jiajie Feng, Jiahua Kong, Haijun Chen, Chaohui Wang, Qian Chen and Jiachen Wang
Gels 2025, 11(8), 590; https://doi.org/10.3390/gels11080590 (registering DOI) - 31 Jul 2025
Abstract
To prolong the service life of asphalt pavement and reduce its maintenance cost, a fiber Bragg grating (FBG) sensor encapsulated in carboxylated carbon nanotube (CNT-COOH)-modified gel material suitable for strain monitoring of asphalt pavement was developed. Through tensile and bending tests, the effects [...] Read more.
To prolong the service life of asphalt pavement and reduce its maintenance cost, a fiber Bragg grating (FBG) sensor encapsulated in carboxylated carbon nanotube (CNT-COOH)-modified gel material suitable for strain monitoring of asphalt pavement was developed. Through tensile and bending tests, the effects of carboxylated carbon nanotubes on the mechanical properties of gel materials under different dosages were evaluated and the optimal dosage of carbon nanotubes was determined. Infrared spectrometer and scanning electron microscopy were used to compare and analyze the infrared spectra and microstructure of carbon nanotubes before and after carboxyl functionalization and modified gel materials. The results show that the incorporation of CNTs-COOH increased the tensile strength, elongation at break, and tensile modulus of the gel material by 36.2%, 47%, and 17.2%, respectively, and increased the flexural strength, flexural modulus, and flexural strain by 89.7%, 7.5%, and 63.8%, respectively. Through infrared spectrum analysis, it was determined that carboxyl (COOH) and hydroxyl (OH) were successfully introduced on the surface of carbon nanotubes. By analyzing the microstructure, it can be seen that the carboxyl functionalization of CNTs improved the agglomeration of carbon nanotubes. The tensile section of the modified gel material is rougher than that of the pure epoxy resin, showing obvious plastic deformation, and the toughness is improved. According to the data from the calibration experiment, the strain and temperature sensitivity coefficients of the packaged sensor are 1.9864 pm/μm and 0.0383 nm/°C, respectively, which are 1.63 times and 3.61 times higher than those of the bare fiber grating. The results of an applicability study show that the internal structure strain of asphalt rutting specimen changed linearly with the external static load, and the fitting sensitivity is 0.0286 με/N. Combined with ANSYS finite element analysis, it is verified that the simulation analysis results are close to the measured data, which verifies the effectiveness and monitoring accuracy of the sensor. The dynamic load test results reflect the internal strain change trend of asphalt mixture under external rutting load, confirming that the encapsulated FBG sensor is suitable for the long-term monitoring of asphalt pavement strain. Full article
(This article belongs to the Special Issue Synthesis, Properties, and Applications of Novel Polymer-Based Gels)
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21 pages, 3663 KiB  
Article
A Study on the Road Performance of the Self-Healing Microcapsule for Asphalt Pavement
by Pei Li, Rongyi Ji, Chenlong Zhang, Jinghan Xu, Mulian Zheng and Xinghan Song
Materials 2025, 18(15), 3483; https://doi.org/10.3390/ma18153483 - 25 Jul 2025
Viewed by 277
Abstract
Asphalt pavement cracking is an important factor affecting its service life. Under certain conditions, the self-healing behavior of asphalt itself can repair pavement cracks. However, the self-healing ability of asphalt itself is limited. In order to strengthen the self-healing ability of asphalt, the [...] Read more.
Asphalt pavement cracking is an important factor affecting its service life. Under certain conditions, the self-healing behavior of asphalt itself can repair pavement cracks. However, the self-healing ability of asphalt itself is limited. In order to strengthen the self-healing ability of asphalt, the microcapsule wrapped with a repair agent is pre-mixed into the asphalt mixture. When the crack occurs and spreads to the surface of the microcapsule, the microcapsule ruptures and the healing agent flows out to realize the self-healing of the crack. Current microcapsules are mostly prepared with healing agents and bio-oil as core materials, and their high-temperature resistance to rutting is poor. While the epoxy resin contains a three-membered cyclic ether, it can undergo ring-opening polymerization to bond and repair the asphalt matrix. In addition, research on microcapsules mainly focuses on the self-healing properties of microcapsule-modified asphalt. In fact, before adding microcapsules to asphalt to improve its self-healing performance, it is necessary to ensure that the asphalt has a good road performance. On this basis, the self-healing performance of asphalt is improved, thereby extending the service life of asphalt pavement. Therefore, two-component epoxy self-healing microcapsules (E-mic and G-mic) were first prepared in this paper. Then, a temperature scanning test, rheological test of bending beams, and linear amplitude scanning test were, respectively, conducted for the microcapsule/asphalt to evaluate its road performance, including the high-temperature performance, low-temperature crack resistance, and fatigue performance. Finally, the self-healing performance of microcapsules/asphalt was tested. The results showed that the self-developed epoxy self-healing microcapsules were well encapsulated and presented as spherical micron-sized particles. The average particle size of the E-mic was approximately 23.582 μm, while the average particle size of the G-mic was approximately 22.440 μm, exhibiting a good normal distribution. In addition, they can remain intact and unbroken under high-temperature conditions. The results of road performance tests indicated that the microcapsule/asphalt mixture exhibits an excellent high-temperature resistance to permanent deformation, low-temperature crack resistance, and fatigue resistance. The self-healing test demonstrated that the microcapsule/asphalt exhibited an excellent self-healing performance. When the microcapsule content was 4%, the self-healing rate reached its optimal level of 67.8%, which was 149.2% higher than that of the base asphalt. Full article
(This article belongs to the Special Issue Innovative Approaches in Asphalt Binder Modification and Performance)
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18 pages, 4110 KiB  
Article
Characterization of Asphalt Binder and Mixture for Enhanced Railway Applications
by Ilho Na, Hyemin Park, Jihyeon Yun, Ju Dong Park and Hyunhwan Kim
Materials 2025, 18(14), 3265; https://doi.org/10.3390/ma18143265 - 10 Jul 2025
Viewed by 230
Abstract
Although asphalt mixtures can be applied to railway tracks due to their viscoelastic properties, caution is required, as their ductility and brittleness are highly sensitive to temperature variations. In recent years, interest in the application of asphalt in railway infrastructure has increased, driven [...] Read more.
Although asphalt mixtures can be applied to railway tracks due to their viscoelastic properties, caution is required, as their ductility and brittleness are highly sensitive to temperature variations. In recent years, interest in the application of asphalt in railway infrastructure has increased, driven by the development of modified mixtures and the broader availability of performance-enhancing additives. Additionally, evaluation methods for railway tracks should be adapted to account for the distinct loading mechanisms involved, which differ from those of conventional roadways. In this study, the comprehensive properties of asphalt binders, mixtures, and testing methods—including physical and engineering characteristics—were assessed to improve the performance of asphalt concrete layers for potential applications in railroad infrastructure. The results of this study indicate that (1) the higher the performance grade (PG), the higher the indirect tensile strength (ITS) value achieved by the 13 mm mixture using PG76-22, which is higher than that of the PG64-22 mixture. This indicates that higher PG grades and modification contribute to improved tensile strength, beneficial for upper layers subjected to dynamic railroad loads. (2) The tensile strength ratio (TSR) increased from the unmodified mixture to over 92% in mixtures containing crumb rubber modifier (CRM) and styrenic thermoplastic elastomer (STE), demonstrating enhanced durability under freeze–thaw conditions. (3) Wheel tracking test results showed that modified mixtures exhibited more than twice the rutting resistance compared to PG64-22. The 13 mm aggregate mixtures also generally performed better than the 19 mm mixtures, indicating reduced permanent deformation under repeated loading. (4) It was concluded that asphalt is a suitable material for railroads, as its overall characteristics comply with standard specifications. Full article
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29 pages, 6769 KiB  
Article
Assessment of Asphalt Mixtures Enhanced with Styrene–Butadiene–Styrene and Polyvinyl Chloride Through Rheological, Physical, Microscopic, and Workability Analyses
by Hawraa F. Jabbar, Miami M. Hilal and Mohammed Y. Fattah
J. Compos. Sci. 2025, 9(7), 341; https://doi.org/10.3390/jcs9070341 - 1 Jul 2025
Viewed by 480
Abstract
This study investigates the performance improvement of asphalt binders through the incorporation of two polymers, polyvinyl chloride (PVC) and styrene–butadiene–styrene (SBS), with asphalt grade (60–70), to address the growing demand for durable and climate-resilient pavement materials, particularly in areas exposed to high temperatures [...] Read more.
This study investigates the performance improvement of asphalt binders through the incorporation of two polymers, polyvinyl chloride (PVC) and styrene–butadiene–styrene (SBS), with asphalt grade (60–70), to address the growing demand for durable and climate-resilient pavement materials, particularly in areas exposed to high temperatures like Iraq. The main objective is to improve the mechanical characteristics, thermal stability, and workability of typical asphalt mixtures to extend pavement lifespan and lessen maintenance costs. A thorough set of rheological, physical, morphological, and workability tests was performed on asphalt binders modified with varying content of PVC (3%, 5%, 7%, and 9%) and SBS (3%, 4%, and 5%). The significance of this research lies in optimizing binder formulations to enhance resistance to deformation and failure modes such as rutting and thermal cracking, which are common in extreme climates. The results indicate that PVC enhances performance grade (PG), softening point, and viscosity, although higher contents (7% and 9%) exceeded penetration grade specifications. SBS-modified binders demonstrated marked improvements in softening point, viscosity, and rutting resistance, with PG values increasing from PG64-x (unmodified) to PG82-x at 5% SBS. Fluorescence microscopy confirmed optimal polymer dispersion at 5% concentration for both SBS and PVC, ensuring compatibility with the base asphalt. Workability testing revealed that SBS-modified mixtures exhibited higher torque requirements, indicating reduced workability compared to both PVC-modified and unmodified binders. These findings offer valuable insights for the design of high-performance asphalt mixtures suitable for hot-climate applications and contribute to the development of more durable and cost-effective road infrastructure. Full article
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16 pages, 2504 KiB  
Article
Thermal Field and High-Temperature Performance of Epoxy Resin System Steel Bridge Deck Pavement
by Rui Mao, Xingyu Gu, Jiwang Jiang, Zhu Zhang and Kaiwen Lei
Materials 2025, 18(13), 3109; https://doi.org/10.3390/ma18133109 - 1 Jul 2025
Viewed by 324
Abstract
Epoxy Resin System (ERS) steel bridge pavement, which comprises a resin asphalt (RA) base layer and a modified asphalt wearing course, offers cost efficiency and rapid installation. However, the combined effects of traffic loads and environmental conditions pose significant challenges, requiring greater high-temperature [...] Read more.
Epoxy Resin System (ERS) steel bridge pavement, which comprises a resin asphalt (RA) base layer and a modified asphalt wearing course, offers cost efficiency and rapid installation. However, the combined effects of traffic loads and environmental conditions pose significant challenges, requiring greater high-temperature stability than conventional pavements. The thermal sensitivity of resin materials and the use of conventional asphalt mixtures may weaken deformation resistance under elevated temperature conditions. This study investigates the thermal field distribution and high-temperature performance of ERS pavements under extreme conditions and explores temperature reduction strategies. A three-dimensional thermal field model developed using finite element analysis software analyzes interactions between the steel box girder and pavement layers. Based on simulation results, wheel tracking and dynamic creep tests confirm the superior performance of the RA05 mixture, with dynamic stability reaching 23,318 cycles/mm at 70 °C and a 2.1-fold improvement in rutting resistance in Stone Mastic Asphalt (SMA)-13 + RA05 composites. Model-driven optimization identifies that enhancing internal airflow within the steel box girder is possible without compromising its structural integrity. The cooling effect is particularly significant when the internal airflow aligns with ambient wind speeds (open-girder configuration). Surface peak temperatures can be reduced by up to 20 °C and high-temperature durations can be shortened by 3–7 h. Full article
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15 pages, 1659 KiB  
Article
Predictive Performance Evaluation of an Eco-Friendly Pavement Using Baosteel’s Slag Short Flow (BSSF) Steel Slag
by Livia Costa, Iuri Bessa, Juceline Bastos, Aline Vale and Teresa Farias
Appl. Mech. 2025, 6(2), 45; https://doi.org/10.3390/applmech6020045 - 16 Jun 2025
Viewed by 476
Abstract
Predicting pavement performance is essential for highway planning and construction, considering traffic, climate, material quality, and maintenance. This study’s main objective is to evaluate Baosteel’s Slag Short Flow (BSSF) steel slag as a sustainable aggregate in pavement engineering by means of durability. The [...] Read more.
Predicting pavement performance is essential for highway planning and construction, considering traffic, climate, material quality, and maintenance. This study’s main objective is to evaluate Baosteel’s Slag Short Flow (BSSF) steel slag as a sustainable aggregate in pavement engineering by means of durability. The research integrates pavement performance prediction using BSSF and assesses its impact on fatigue resistance and percentage of cracked area (%CA). Using the Brazilian mechanistic-empirical design method (MeDiNa), eight scenarios were analyzed with soil–slag mixtures (0%, 25%, 50%, and 75% slag) in base and subbase layers under two traffic levels over 10 years. An asphalt mixture with 15% steel slag aggregate (SSA) was used in the surface layer and compared to a reference mixture. Higher SSA percentages were applied to the base layer, while lower percentages were used in subbase layers, facilitating field implementation. The resilient modulus (MR) and permanent deformation (PD) were design inputs. The results show that 15% SSA does not affect rutting damage, with %CA values below Brazilian limits for traffic of 1 × 106. The simulations confirm BSSF as an effective and sustainable alternative for highway pavement construction, demonstrating its potential to improve durability and environmental impact while maintaining performance standards. Full article
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21 pages, 5570 KiB  
Article
Influence of Mineral Powder Content and Gradation on the Aging and High-Temperature Rheological Properties of Styrene-Butadiene-Styrene (SBS) Modified Asphalt
by Chengwei Xing, Zhibin Chang, Bohan Zhu, Tian Jin, Qing Ma and Jie Wang
Materials 2025, 18(12), 2785; https://doi.org/10.3390/ma18122785 - 13 Jun 2025
Viewed by 370
Abstract
This paper aims to explore the influences of the content and gradation of mineral powder on the rheological properties of styrene-butadiene-styrene (SBS) modified asphalt mastic at different aging stages and temperatures. In the experiment, SBS modified asphalt mastic samples with different powder-to-binder ratios [...] Read more.
This paper aims to explore the influences of the content and gradation of mineral powder on the rheological properties of styrene-butadiene-styrene (SBS) modified asphalt mastic at different aging stages and temperatures. In the experiment, SBS modified asphalt mastic samples with different powder-to-binder ratios (0.6, 0.8, and 1.0) and different mineral powder gradations (500 mesh passing rates of 76.89% and 100%) were prepared. Following aging periods of 5, 25, and 45 h in the pressure aging vessel (PAV), the asphalt underwent comprehensive rheological characterization using a dynamic shear rheometer (DSR). The research shows that mineral powder can boost mastic’s deformation resistance and elastic effect. When aged by PAV for 45 h, the powder-to-binder ratio increased from 0.6 to 1.0, and its complex modulus increased by nearly 2.5 times at 58 °C. For SBS modified asphalt mastic of PAV 0 h, the powder-to-binder ratio increased from 0.6 to 1.0 and its phase angle was reduced from 59.6 to 53.2, which indicated that the elasticity of mastic was improved. However, this accelerated the degradation rate of SBS, making the aging process more complex. Fine-grained mineral powder is more effective in enhancing mastic’s deformation resistance than coarse-grained mineral powder. The fine-graded mastic had better rutting resistance after 45 h of aging than after 25 h of aging because the mineral powder compensated for the SBS loss-induced elasticity reduction. Smaller mineral powder particles lead to better a mastic anti-aging effect. After 45 h of aging, fine-grained mineral powder offered a better elastic effect. But the ways in which mineral powder and SBS boost mastic elasticity differ greatly. The results of this study provide a reference for optimizing the design of asphalt mixtures. Full article
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16 pages, 2820 KiB  
Article
Rutting Behavior of Dual-Layer Asphalt Pavements Subjected to Variable Temperature
by Ya Tan, Yingjun Jiang, Chenfan Bai, Hongjiang Zhang, Yingchao Liang, Wenhui Lou and Zhejiang Chen
Materials 2025, 18(11), 2603; https://doi.org/10.3390/ma18112603 - 3 Jun 2025
Viewed by 438
Abstract
Traditional laboratory rutting tests are performed at a constant temperature by neglecting pavement temperature variation. The mechanical properties of asphalt are susceptible to temperature variation. This sensitivity to temperature variations significantly influences the performance and durability of asphalt pavements. Following this purpose, a [...] Read more.
Traditional laboratory rutting tests are performed at a constant temperature by neglecting pavement temperature variation. The mechanical properties of asphalt are susceptible to temperature variation. This sensitivity to temperature variations significantly influences the performance and durability of asphalt pavements. Following this purpose, a stepwise temperature-controlled rutting test method was proposed to investigate the rutting development of double-layer asphalt pavement (DLAP) under variable temperature. A time-hardening model was developed and employed to evaluate the rutting performance of DLAP under variable temperature. Results indicate that the rutting development of DLAP exhibits a stepwise variation when subjected to variable temperatures. Within a specific constant temperature range, rutting development can be fitted using a power function of load cycles. The rutting deformation of DLAP predominantly occurs at 20 °C; once the temperature exceeds 50 °C, the rutting development accelerates and becomes difficult to stabilize. The time-hardening model effectively captures the rutting development under variable temperature. The predicted values align closely with field values, which demonstrates the model’s feasibility in calculating rutting deformation under variable temperature. Under actual service conditions, the rutting development of DLAP follows a periodic S-shaped growth, yet this trend can still be represented by a power-law function. DLAP exhibits satisfactory durability and structural stability, effectively addressing the challenges posed by traffic loads and high temperatures in test sections. Full article
(This article belongs to the Section Construction and Building Materials)
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25 pages, 150744 KiB  
Article
Permanent Deformation Mechanism of Steel Bridge Deck Pavement Using Three-Dimensional Discrete–Continuous Coupling Method on the Mesoscopic Scale
by Xingchen Min and Yun Liu
Appl. Sci. 2025, 15(11), 6187; https://doi.org/10.3390/app15116187 - 30 May 2025
Viewed by 345
Abstract
Unlike conventional asphalt pavements, steel bridge deck pavement (SBDP) is directly constructed on orthotropic steel deck plates characterized by relatively low flexural stiffness, rendering it more susceptible to rutting deformation under elevated temperatures and repeated loading. To investigate the mesoscopic mechanism underlying rutting [...] Read more.
Unlike conventional asphalt pavements, steel bridge deck pavement (SBDP) is directly constructed on orthotropic steel deck plates characterized by relatively low flexural stiffness, rendering it more susceptible to rutting deformation under elevated temperatures and repeated loading. To investigate the mesoscopic mechanism underlying rutting formation in SBDP, a three-dimensional (3D) discrete–continuous coupled model of a steel–asphalt composite structural specimen (SACSS) was developed and employed to conduct virtual rutting simulations, which were subsequently validated against laboratory test results. The impact of surface cracking on rutting progression was then explored. In addition, the spatial motion and contact interactions of particles during the rutting process were monitored and analyzed. The influence of steel plate stiffness on the rutting resistance of SBDP was also evaluated. The numerical analyses yielded the following key findings: (1) Under three steel–asphalt interface bonding (SAIB) failure conditions (0%, 17%, and 100%), the virtual simulation results exhibited strong agreement with experimental trends in rutting depth over time, thereby confirming the validity and reliability of the coupled modeling approach. (2) At 30 °C, the presence of surface cracks is found to increase the rutting depth by 35.77%, whereas this effect is mitigated at 45 °C. (3) The meso-mechanical mechanisms governing rutting deformation in SBDP are further elucidated under different temperature conditions. (4) Moreover, at elevated temperatures, the use of a steel plate with an elastic modulus of 206 MPa effectively inhibit rutting development. This study offers mesoscopic-level insights into the effects of temperature, SAIB conditions, steel plate stiffness, and surface cracking on the macroscopic rutting behavior of SBDP, thereby providing a theoretical foundation for the design and optimization of long-lasting SBDPs. Full article
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26 pages, 3986 KiB  
Article
Research on the Rheological Properties and Modification Mechanisms of MWCNTs-OH/SBS-Modified Asphalt Binder
by Manman Su, Qi Ding, Zuohong He, Xuling Huang, Leilei He and Enlong Zhao
Coatings 2025, 15(6), 625; https://doi.org/10.3390/coatings15060625 - 23 May 2025
Viewed by 407
Abstract
The objective of this study is to explore the high-temperature rheological properties and microscopic interaction mechanisms of styrene–butadiene–styrene (SBS) composite-modified asphalt with hydroxylated multi-walled carbon nanotubes (MWCNT-OH). SBS-modified asphalt, MWCNT-modified asphalt and MWCNT/SBS composite-modified asphalt were prepared with high-speed shearing apparatus and machine [...] Read more.
The objective of this study is to explore the high-temperature rheological properties and microscopic interaction mechanisms of styrene–butadiene–styrene (SBS) composite-modified asphalt with hydroxylated multi-walled carbon nanotubes (MWCNT-OH). SBS-modified asphalt, MWCNT-modified asphalt and MWCNT/SBS composite-modified asphalt were prepared with high-speed shearing apparatus and machine mixer. Physical property tests, dynamic shear rheological (DSR) tests, multiple stress creep recovery (MSCR) tests, X-ray diffraction (XRD) and Raman spectroscopy analyses were carried out to systematically compare the differences in macroscopic performance and changes in microscopic structure of different types of asphalts. According to the results of physical property tests, DSR tests and MSCR tests, the composite-modified asphalt was superior to the single-component-modified asphalt in terms of complex modulus (G*) and rutting factor (G*/sin δ). Its creep recovery rate (R) and unrecoverable compliance (Jnr) exhibited better anti-deformation ability under high temperatures, verifying the synergistic effect of SBS and MWCNTs-OH. XRD analysis showed that composite modification reduced the disorder degree of the crystalline phase of asphalt. Raman spectroscopy confirmed that there were changes in the vibration of chemical bonds between the modifier and asphalt, indicating that the modifier and asphalt acted on the asphalt system through physical dispersion and chemical cross-linking. Full article
(This article belongs to the Section Environmental Aspects in Colloid and Interface Science)
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20 pages, 3018 KiB  
Article
Performance Evaluation of Desulfurized Rubber Powder and Styrene-Butadiene-Styrene Composite-Modified Asphalt
by Bin Liu, Kai Zhang, Xiangyang Fan and Chongzhi Tu
Coatings 2025, 15(5), 607; https://doi.org/10.3390/coatings15050607 - 19 May 2025
Viewed by 493
Abstract
Rubber powder asphalt has been widely studied due to its favorable temperature sensitivity and fatigue resistance. However, because rubber powder does not easily swell in asphalt, it leads to poor storage stability and high viscosity, limiting its large-scale application. In this study, modified [...] Read more.
Rubber powder asphalt has been widely studied due to its favorable temperature sensitivity and fatigue resistance. However, because rubber powder does not easily swell in asphalt, it leads to poor storage stability and high viscosity, limiting its large-scale application. In this study, modified asphalt was prepared using desulfurized rubber powder (DRP) and styrene-butadiene-styrene (SBS) modifiers, aiming to identify the optimal formulation for enhanced performance. It was hypothesized that the combined use of DRP and SBS would produce synergistic effects, improving the overall mechanical and rheological properties of the asphalt. To test this, the effects of this composite modification were evaluated using Marshall tests (penetration, softening point, ductility, elastic recovery, and Brookfield viscosity) and Superpave tests (shear modulus, high-performance grade, rutting factor, fatigue factor, and creep and recovery). Additionally, moisture susceptibility, high-temperature stability, low-temperature cracking resistance, and fatigue resistance at the mixture level were assessed. Performance was evaluated according to the Chinese standard JT/T 798-2019 for rubberized asphalt using reclaimed tire rubber. Results show that DRP-modified asphalt demonstrates excellent temperature sensitivity, rutting resistance, deformation resistance, and fatigue performance. However, an excessive amount of DRP increases Brookfield viscosity, which negatively affects the workability of the asphalt binder. The addition of SBS further improves the softening point, ductility, and deformation recovery of the binder. Considering cost-effectiveness and overall performance, the optimal formulation was determined to be 25% DRP and 1% SBS. At this dosage, all performance indicators met the required standards. The rotational viscosity at 180 °C was approximately 35% lower than that of conventional rubber powder–modified asphalt, while the high-temperature rutting factor and fatigue resistance at medium-to-low temperatures outperformed those of SBS-modified asphalt. The mixture test results reveal that the gradation has an impact on the performance of the obtained mixture, but overall, the DRP-SBS composite-modified asphalt mixture has significant advantages in terms of performance and cost-effectiveness. Full article
(This article belongs to the Special Issue Advances in Asphalt and Concrete Coatings)
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31 pages, 7113 KiB  
Article
Advanced Rheological Characterization of Asphalt Binders Modified with Eco-Friendly and Polymer-Based Additives Under Dynamic Loading
by Ali Almusawi and Shvan Tahir Nasraldeen Nasraldeen
Appl. Sci. 2025, 15(10), 5552; https://doi.org/10.3390/app15105552 - 15 May 2025
Cited by 1 | Viewed by 540
Abstract
This study explores the rheological performance of bitumen modified with a synthetic polymer (styrene–butadiene–styrene, SBS) and two environmentally sustainable additives—animal bone ash (AB) and waste cooking oil (WCO)—to enhance durability and deformation resistance under dynamic loading. Frequency sweep and linear amplitude sweep (LAS) [...] Read more.
This study explores the rheological performance of bitumen modified with a synthetic polymer (styrene–butadiene–styrene, SBS) and two environmentally sustainable additives—animal bone ash (AB) and waste cooking oil (WCO)—to enhance durability and deformation resistance under dynamic loading. Frequency sweep and linear amplitude sweep (LAS) tests were conducted to evaluate viscoelastic and fatigue behavior. SBS at 5% showed the highest elasticity and fatigue life, making it optimal for heavily trafficked pavements. Among bio-waste additives, 6% AB provided the highest stiffness and rutting resistance in laboratory tests; however, 5% AB offered a better balance between structural integrity and cracking resistance, making it more suitable for general pavement applications. WCO-modified binders demonstrated improved flexibility, with 4% WCO achieving the best balance between elasticity and softening, ideal for low-load or temperate environments. These results highlight the potential of combining synthetic and bio-based waste materials to tailor bitumen properties for sustainable and climate-responsive pavement design. Full article
(This article belongs to the Special Issue Innovations in Binder and Asphalt Mixture Rheology)
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12 pages, 2269 KiB  
Article
Investigation of Rutting and Aging Performance of Gap-Graded Rubberized Asphalt Mixtures
by Marek Pszczola and Bohdan Dolzycki
Materials 2025, 18(10), 2263; https://doi.org/10.3390/ma18102263 - 13 May 2025
Viewed by 435
Abstract
Gap-graded asphalt mixtures like stone mastic asphalt (SMA), porous asphalt (PA), and asphalt mixtures for very thin layers (fr. Béton Bitumineuse Très Mince—BBTM) are usually made with the use of SBS (styrene-butadiene-styrene) polymer-modified bitumen. This is a binder that allows one to achieve [...] Read more.
Gap-graded asphalt mixtures like stone mastic asphalt (SMA), porous asphalt (PA), and asphalt mixtures for very thin layers (fr. Béton Bitumineuse Très Mince—BBTM) are usually made with the use of SBS (styrene-butadiene-styrene) polymer-modified bitumen. This is a binder that allows one to achieve the required parameters, but at the same time, its use increases the costs of making pavement layers. An alternative to polymer-modified bitumen (SBS) is rubber-modified bitumen. The research presented in this publication includes an assessment of the resistance to permanent deformation and susceptibility to aging of SMA and porous asphalt (PA) mixtures containing both SBS polymer-modified bitumen and rubber-modified bitumen, where the modification process was carried out directly in the refinery. The laboratory tests of resistance to deformation were assessed based on the rutting test and on the assessment of the dynamic modulus (SPT). The changes in the tested asphalt mixtures after aging in laboratory conditions were assessed based on the changes in the stiffness modulus (IT-CY) and the changes in the indirect tensile strength (ITS) after the short-term and long-term aging processes. The presented research results clearly show that the use of rubber-modified bitumen produced in industrial conditions (i.e., in a refinery) allows one to obtain gap-graded mixtures that are as resistant to permanent deformation as mixtures containing SBS polymer-modified bitumen. Similar conclusions resulted from the study of susceptibility to aging. Changes after aging for both types of asphalt mixtures were at a similar level. The presented results clearly indicate that, in the case of gap-graded mixtures such as SMA- and PA-type mixtures, they meet the rutting and aging expectations when either expensive modified bitumen or a cheaper, more environmentally friendly alternative (rubber-modified bitumen) is used. Full article
(This article belongs to the Special Issue Innovative Approaches in Asphalt Binder Modification and Performance)
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13 pages, 1356 KiB  
Article
Investigating the Impact of Surfactant-Based Warm-Mix Additives on the Performance of Recycled Asphalt Mixtures
by Hao Xiang, Desheng Yang, Shunxian Peng and Wei Gao
Materials 2025, 18(8), 1732; https://doi.org/10.3390/ma18081732 - 10 Apr 2025
Viewed by 430
Abstract
This investigation aimed to assess the influence of warm-mix additives on the performance characteristics of recycled asphalt mixtures. Pressure-aging vessels were employed to simulate the aging of asphalt binders. Warm-mix recycled asphalt (WMRA) and mixtures were prepared by incorporating self-developed plant-oil-based rejuvenators and [...] Read more.
This investigation aimed to assess the influence of warm-mix additives on the performance characteristics of recycled asphalt mixtures. Pressure-aging vessels were employed to simulate the aging of asphalt binders. Warm-mix recycled asphalt (WMRA) and mixtures were prepared by incorporating self-developed plant-oil-based rejuvenators and surfactant-based warm-mix additives. The rheological properties of asphalt were tested by a dynamic shear rheometer (DSR). Furthermore, the pavement performance of the asphalt mixture was evaluated by a rutting test, beam bending test, Marshall stability test, and freeze–thaw splitting test. The experimental results demonstrated that the addition of warm-mix additives reduces the penetration and softening point of recycled asphalt while enhancing its ductility. Performance improvement was quantitatively evaluated using a recovery index. The complex modulus and rutting factor of the WMRA were found to be lower than those of recycled asphalt, indicating a decrease in the asphalt’s resistance to deformation owing to the surfactant. Both the hot-mix and warm-mix recycled asphalt mixtures met the specified requirements for various performance indicators. The warm-mix rejuvenator outperformed the regular rejuvenator in evaluating water stability using the soaked Marshall residual stability method, whereas the evaluation based on the freeze–thaw splitting strength ratio demonstrated the opposite trend. Full article
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32 pages, 328 KiB  
Review
Rutting and Aging Properties of Recycled Polymer-Modified Pavement Materials
by Nuha S. Mashaan and Chathurika Dassanayake
Recycling 2025, 10(2), 60; https://doi.org/10.3390/recycling10020060 - 1 Apr 2025
Viewed by 1309
Abstract
Recycled polymer-modified binders have emerged as a sustainable solution for improving the performance and durability of pavement materials. This review examines the rutting and aging properties of pavements modified with recycled polymers, highlighting their potential for sustainable infrastructure development. The incorporation of recycled [...] Read more.
Recycled polymer-modified binders have emerged as a sustainable solution for improving the performance and durability of pavement materials. This review examines the rutting and aging properties of pavements modified with recycled polymers, highlighting their potential for sustainable infrastructure development. The incorporation of recycled polymers into bitumen enhances resistance to rutting and aging by improving the binder’s mechanical stability and oxidative durability. Key laboratory techniques, including the rolling thin-film oven test (RTFOT) and the pressure aging vessel (PAV), are evaluated for their effectiveness in assessing the thermal and oxidative aging behavior of modified binders. The review demonstrates that recycled polymers improve binder elasticity, delay oxidative degradation, and mitigate deformation under repeated loading, thus extending pavement lifespan and reducing maintenance costs. However, challenges such as optimizing polymer dosage, ensuring homogeneity, and predicting long-term performance require further investigation. This paper underscores the environmental and economic benefits of utilizing recycled polymers in pavement construction and advocates for improved testing protocols and advanced characterization techniques to enhance the reliability and sustainability of polymer-modified pavements. Full article
(This article belongs to the Special Issue Recycled Materials in Sustainable Pavement Innovation)
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