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64 pages, 1175 KB  
Review
On Recent Advances in Design of Transimpedance Amplifiers in CMOS: A Taxonomy of Topological Enhancements Beyond the Transimpedance Limit
by Agata Romanova and Vaidotas Barzdenas
Electronics 2026, 15(15), 3322; https://doi.org/10.3390/electronics15153322 - 28 Jul 2026
Viewed by 552
Abstract
Transimpedance amplifiers (TIAs) are the critical components for current-to-voltage interfaces in optical receivers, LiDAR front-ends, biomedical sensors, and unconventional applications such as magnetic-resonance receiver-coil arrays and wide-bandgap ultraviolet detectors, and their CMOS design is governed by a fundamental gain-bandwidth-noise trade-off whose structure is [...] Read more.
Transimpedance amplifiers (TIAs) are the critical components for current-to-voltage interfaces in optical receivers, LiDAR front-ends, biomedical sensors, and unconventional applications such as magnetic-resonance receiver-coil arrays and wide-bandgap ultraviolet detectors, and their CMOS design is governed by a fundamental gain-bandwidth-noise trade-off whose structure is rarely made explicit. This review introduces a unifying framework rooted in three explicit assumptions underlying the classical shunt-feedback TIA limit: a single-pole core amplifier (A1), a resistive feedback element (A2), and the full input capacitance loading the feedback summing node (A3). Relaxing one or more of these assumptions is shown to be the common structural thread behind every class of bandwidth or noise enhancement in the recent literature, and all surveyed architectures are organized into a six-tier taxonomy, from Tier 0 designs operating within the classical limit to Tier 5 topologies that bypass all three assumptions simultaneously. This taxonomy is supplemented by an orthogonal configurability axis spanning single- and dual-control reconfigurable, variable-gain, and dynamic-range-extension designs. We further show that stability is not removed by these relaxations but migrates with the tier, from the global phase margin of the classical loop to a local regulating loop, a group-delay-flatness constraint, an input-passivity condition, or a multi-loop interaction, so that each architecture carries a predictable stability locus. The taxonomy is cross-referenced with application domains and closed-form noise-floor boundary plots parametrized by input capacitance and amplifier gain-bandwidth product, and with the CMOS technology landscape, where we argue that the most advanced node is not universally optimal and that node and topology act as complementary rather than competing levers. A single consistent figure of merit, applied uniformly to a representative set of CMOS realizations from 0.6 μm to 16 nm FinFET, shows no monotonic improvement with publication year or node and is presented as a diagnostic indicator rather than an absolute ranking. The review closes with an outlook on 200 Gb/s/lane links, wide-bandgap sensor integration, and the FinFET-to-gate-all-around device transition. Full article
(This article belongs to the Section Microelectronics)
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14 pages, 2541 KB  
Article
Influence of Ultrasonic Impact Number on the Contact Fatigue Performance of Cr12Mo1V1 Die Steel Component
by Jian Wei, Qirong Xiao, Mengyu Cao, Hao Gao, Yuhong Liu and Chaoyu Li
Materials 2026, 19(14), 3011; https://doi.org/10.3390/ma19143011 - 13 Jul 2026
Cited by 1 | Viewed by 321
Abstract
In order to enhance the contact fatigue performance of the Cr12Mo1V1 die steel component, the ultrasonic impact surface-modification process was introduced into the heat treatment process of 1060 °C quenching + cryogenic treatment (−150 °C × 2 h) + two times of tempering [...] Read more.
In order to enhance the contact fatigue performance of the Cr12Mo1V1 die steel component, the ultrasonic impact surface-modification process was introduced into the heat treatment process of 1060 °C quenching + cryogenic treatment (−150 °C × 2 h) + two times of tempering at 520 °C × 2 h in this paper. The influence of the ultrasonic impact number on the surface morphology, roughness, micro-hardness value, residual stress, microscopic morphology of spalling pits, contact fatigue life, and EBSD inverse pole figure of the Cr12Mo1V1 die steel component were investigated utilizing a laser confocal microscope, 3D laser confocal microscope, micro-hardness tester, X-ray stress meter, scanning electron microscope, rolling contact fatigue testing machine, and EDAX-TSL system equipped with a field-emission scanning electron microscope, respectively. In comparison to other ultrasonic impact numbers, the Cr12Mo1V1 die steel component owned the smallest roughness of 0.027 μm, the highest micro-hardness value of 867 Hv0.1 and the largest residual compressive stress of −1318 MPa, respectively. Meanwhile, the contact fatigue life of the Cr12Mo1V1 die steel component was significantly improved by 223% to 5.231 × 107 cycles. After ultrasonic impact treatment, the spalling pits revealed that the crack propagation angle increased from 28° to 34°, the depth increased from 153 μm to 175 μm, and the failure mode consisted of Hertz’s contact theory. This study provides an effective surface strengthening solution for enhancing the contact fatigue performance of Cr12Mo1V1 die steel components. Full article
(This article belongs to the Section Metals and Alloys)
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15 pages, 16325 KB  
Article
Combined Electron Backscattered Diffraction (EBSD) and SEM-EDX Investigation of the Calcitic Annelid Tube of Ditrupa (Annelida, Serpulidae)
by Jim Buckman, Meriem Ben Haj Slama and Heath Young
Minerals 2026, 16(7), 728; https://doi.org/10.3390/min16070728 - 11 Jul 2026
Viewed by 353
Abstract
The calcareous tubes of the annelid worm Ditrupa are known from the Eocene to present-day marine settings. It has a distinctive and unique outer layer comprising regularly ridged prismatic fabric (RRP), and a more chaotic inner layer of semi-oriented, needle-to-thread-like calcite, simple preferentially [...] Read more.
The calcareous tubes of the annelid worm Ditrupa are known from the Eocene to present-day marine settings. It has a distinctive and unique outer layer comprising regularly ridged prismatic fabric (RRP), and a more chaotic inner layer of semi-oriented, needle-to-thread-like calcite, simple preferentially orientated prismatic (SPOP) fabric. We use electron backscattered diffraction (EBSD) analysis in conjunction with scanning electron microscopy (SEM) backscattered (BSE) imaging and energy dispersive X-ray (EDX) mapping in the study of the tube structure of (?)Eocene Ditrupa sp. The fabric of both layers can often be observed even within the older fossil materials. EBSD Inverse Pole Figures and pole figure plots show that the crystallographic c-axis is orientated parallel to both of the elongate calcite crystals of the two fabric layers, although orientation between the two layers is perpendicular to each other. The crystals and c-axis of the RRP fabric is approximately perpendicular to the outer tube margin, while those in the SPOP fabric are more distributed with an orientation parallel to the tube circumference. The current work confirms the single crystal origin of RRP fabric crystals and indicates that these grew incrementally and were likely controlled by an organic framework. The inner layer fabric is also shown to be unique to Ditrupa, and although it has elements similar to lamello-fibrillar (LF) and irregular orientated prismatic (IOP) fabrics, should be assigned to simple preferentially orientated prismatic (SPOP) fabric previously noted from Ditrupa bartonensis. Given the range of unusual features associated with the latter fabric, it may also at least in part be controlled through an in situ organic framework. Therefore, both layers of the tube of Ditrupa may be unique amongst the annelids, as well as being organic framework controlled or influenced. Full article
(This article belongs to the Section Biomineralization and Biominerals)
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20 pages, 18876 KB  
Article
Surface Morphology, Relative Density, Microhardness and Microstructure of Tungsten Fabricated by Laser Powder Bed Fusion
by Fang Wu, Fuping Liao, Zhihua Ju, Fangyuan Chen and Delin Yuan
Metals 2026, 16(7), 741; https://doi.org/10.3390/met16070741 - 5 Jul 2026
Viewed by 325
Abstract
This study investigates the effects of laser power and scanning rate on the surface morphology, relative density, microhardness and microstructure of pure tungsten fabricated by laser powder bed fusion (LPBF). Increasing the laser power or decreasing the scanning rate effectively suppresses spheroidisation and [...] Read more.
This study investigates the effects of laser power and scanning rate on the surface morphology, relative density, microhardness and microstructure of pure tungsten fabricated by laser powder bed fusion (LPBF). Increasing the laser power or decreasing the scanning rate effectively suppresses spheroidisation and enhances densification, achieving a maximum relative density of ~98%. However, excessive laser power intensifies Marangoni convection, leading to surface protrusions that reduce density. Microstructural analysis reveals that the laser-scanned surface is dominated by fine columnar grains (390–480 HV), whereas the side surface comprises coarser columnar grains with lower hardness (~390 HV). Electron backscatter diffraction analysis confirms that the side surface contains a high proportion of grains exceeding 100 μm and reveals a significant peak (~41.8%) at ~3.5° for low-angle grain boundaries, indicating substantial internal stress and microstrain. Pole figures show a weak preferred orientation (maximum texture intensity of 3.161). Phase analysis shows no significant phase transformation after LPBF, while internal stress and microstrain increase notably. Full article
(This article belongs to the Special Issue Rare-Earth Alloying Effects in Advanced Metallic Materials)
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13 pages, 2982 KB  
Article
Effect of Double Cold Rolling and Annealing on Texture Evolution and Mechanical Response of Ultrathin Ferritic Steel
by Laura G. Castruita-Ávila, Francisco Alfredo García-Pastor, Manuel de Jesús Castro-Román, Jesús Emilio Camporredondo-Saucedo, Fabián Equihua-Guillén, Adrián Moisés García-Lara and Jimy Unfried-Silgado
Appl. Sci. 2026, 16(12), 6071; https://doi.org/10.3390/app16126071 - 16 Jun 2026
Viewed by 320
Abstract
The influence of double continuous cold rolling followed by annealing on the texture evolution and mechanical properties of a commercial low-carbon ferritic steel was investigated. Ultrathin sheets (final thickness 0.22 mm) were produced through a two-stage cold rolling process with intermediate and final [...] Read more.
The influence of double continuous cold rolling followed by annealing on the texture evolution and mechanical properties of a commercial low-carbon ferritic steel was investigated. Ultrathin sheets (final thickness 0.22 mm) were produced through a two-stage cold rolling process with intermediate and final annealing at 690 °C for 35 s, followed by light temper rolling at 100 °C for 20 s. Texture evolution was characterized using Electron Backscatter Diffraction (EBSD) with Orientation Imaging Microscopy (OIM), producing pole figures and orientation distribution functions (ODFs). Mechanical properties were evaluated through Vickers microhardness and ultimate tensile strength measurements obtained from three independent locations per sample. Quantitative ODF analysis (φ2 = 45°) revealed that γ-fiber ({111}//ND) intensity increased after each cold reduction stage and decreased after annealing due to recrystallization. The α-fiber (110/RD) and cube components (001//RD) showed a slight increase after annealing. The final ultrathin sheet exhibited moderate γ-fiber intensity (≈3 M.R.D), low Vickers microhardness (100–150 HV), and tensile strength (400–450 MPa). These results demonstrate controlled evolution of texture and microstructure during double cold rolling and annealing, providing a basis for future studies on forming-related behavior without directly assessing formability. Full article
(This article belongs to the Special Issue Processing and Microstructural Evolution of Alloys)
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15 pages, 26537 KB  
Article
Effect of Hot Rolling Temperature on the Microstructure and Macro-Texture Evolution Laws of TC2 Titanium Alloy and Their Influence on Mechanical Properties
by Jiazhi Yuan, Qingfu Qian, Zaijiu Li, Qinglin Jin, Zhongxue Feng, Yanying Li and Zhaosong Chen
Metals 2026, 16(6), 651; https://doi.org/10.3390/met16060651 - 13 Jun 2026
Viewed by 346
Abstract
TC2 titanium alloy (Ti-4Al-1.5Mn, wt.%) is a near-α titanium alloy with promising aerospace and biomedical applications, but its limited room temperature ductility and strong texture sensitivity hinder the fabrication of high-performance sheets. In this study, the effects of hot rolling at 830 °C [...] Read more.
TC2 titanium alloy (Ti-4Al-1.5Mn, wt.%) is a near-α titanium alloy with promising aerospace and biomedical applications, but its limited room temperature ductility and strong texture sensitivity hinder the fabrication of high-performance sheets. In this study, the effects of hot rolling at 830 °C and 930 °C on the microstructure, macro-texture, mechanical properties, and fracture behavior of TC2 alloy were investigated. Compared with the 830 °C rolled sample, the 930 °C rolled sample exhibited finer primary α grains, a higher volume fraction of fine and dispersed secondary αs phase, and more uniform Mn distribution, while both samples retained an α + β phase constitution. Texture and ODF (orientation distribution function) analyses revealed that increasing the rolling temperature reduced the maximum intensity of the (0001) pole figure from 6.68 to 5.23 m.r.d. (multiples of a random distribution) and increased that of the (10-10) pole figure to 9.62 m.r.d., indicating weakened basal texture, enhanced prismatic texture, and more dispersed orientation distribution. Consequently, although the tensile strength slightly decreased to approximately 730 MPa, the elongation increased from approximately 24% to 28%. The finer and denser dimples observed after 930 °C rolling further confirmed improved plastic deformation coordination. Full article
(This article belongs to the Special Issue Innovations in Heat Treatment of Metallic Materials)
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12 pages, 20109 KB  
Article
A Numerical Assessment on the Textural Stability of {112}<111> After Asymmetric Accumulative Roll-Bonding (AARB)
by Rui Wang, Xuhui Bai, Lihong Su, Guangyang Jiang, Yu Sun, Yu Liu, Yu Zhu and Xi Huang
Metals 2026, 16(6), 576; https://doi.org/10.3390/met16060576 - 25 May 2026
Viewed by 271
Abstract
In this study, the stability of the {112}<111> rolling texture component during asymmetric accumulative roll-bonding (AARB) was systematically investigated using a crystal plasticity finite element method (CPFEM) model. The CPFEM predictions showed that the plastic deformation was inhomogeneous along the thickness for all [...] Read more.
In this study, the stability of the {112}<111> rolling texture component during asymmetric accumulative roll-bonding (AARB) was systematically investigated using a crystal plasticity finite element method (CPFEM) model. The CPFEM predictions showed that the plastic deformation was inhomogeneous along the thickness for all five asymmetric ratios (1.0, 1.2, 1.5, 0.83, and 0.66). To characterize the plastic deformation and texture evolution, through-thickness shear strain, slip-system shear strain, crystal rotation behaviour, pole figures, and the retained area fraction of the {1 1 2}<1 1 1> texture component were analyzed. It was found that the asymmetric ratio, surface friction, and cutting-stacking pattern in AARB played a critical role in the preservation of initial {1 1 2}<1 1 1>. Full article
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17 pages, 7855 KB  
Article
Microstructural Evaluation and Tensile Properties for GTAW Weldments of Stainless Steel 304 Seam Pipes
by Eunhye Park and Byounglok Jang
Metals 2026, 16(6), 565; https://doi.org/10.3390/met16060565 - 22 May 2026
Viewed by 521
Abstract
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment [...] Read more.
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment current profile was employed using an AMI 8-4000 orbital system, with peak currents of 70, 67, and 65 A for the penetration, remelting, and downslope (crater-fill) segments, respectively, under high-purity Ar (99.999%) shielding with back purging. Electron backscatter diffraction (EBSD) analysis, including image quality (IQ), inverse pole figure (IPF), and kernel average misorientation (KAM) mapping, showed that the weld metal consists of epitaxially grown columnar austenite grains strongly oriented along the solidification direction, whereas the heat-affected zone (HAZ) exhibits finer equiaxed grains with an increased Σ3 twin boundary fraction and elevated low-angle boundary fraction, indicative of partial recrystallization. Only sparse, discontinuous δ-ferrite stringers were detected in the fusion zone, and no non-metallic inclusions were observed on fracture surfaces, supporting the weld metal’s suitability for semiconductor-grade cleanliness. Vickers microhardness profiles revealed modest hardness differences (typically within 10–20 HV) between the weld metal, HAZ, and base metal, with no pronounced HAZ softening. Cross-weld tensile tests conducted in accordance with ASTM E8/E8M-22 yielded yield strengths above 200 MPa, ultimate tensile strengths of 650–680 MPa, and total elongations approaching 40%, comparable to the as-received pipe. Scanning electron fractography confirmed fully ductile failure via microvoid coalescence without evidence of cleavage, intergranular decohesion, or weld-defect-induced embrittlement. Collectively, these results demonstrate that the three-segment autogenous orbital GTAW procedure produces structurally sound, particle-clean joints suitable for 304 stainless steel seam pipes used in high-purity industrial piping. Full article
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23 pages, 5405 KB  
Article
A Fully Integrated Gate-Pole-Dominant Low-Dropout Regulator with Loop-Gain Booster for Maintaining High Power-Supply Rejection over a Wide Load Current Range
by Deok Won Koh, Changin Yoon, Jeong Hoan Park, Seung Hwan Lee and Younghyun Lim
Electronics 2026, 15(9), 1825; https://doi.org/10.3390/electronics15091825 - 24 Apr 2026
Viewed by 601
Abstract
This paper introduces a fully integrated gate-pole-dominant low-dropout regulator (LDO) that eliminates the need for external capacitors while sustaining high power-supply rejection (PSR) over a broad load current range. A loop-gain booster (LGB) is proposed to maintain the DC operating point of the [...] Read more.
This paper introduces a fully integrated gate-pole-dominant low-dropout regulator (LDO) that eliminates the need for external capacitors while sustaining high power-supply rejection (PSR) over a broad load current range. A loop-gain booster (LGB) is proposed to maintain the DC operating point of the error amplifier output at its optimal value, thereby preserving a high unity-gain frequency (UGF) even as the load current varies from zero to 200 mA. The parallel signal paths within the LGB inherently produce a left-half-plane (LHP) zero, which cancels one of the poles within the UGF of the feedback loop and guarantees robust stability under diverse operating conditions. Fabricated in a 40 nm CMOS technology, the prototype occupies only 0.008 mm2 with a 4 pF on-chip compensation capacitor. The proposed LDO achieves a PSR of −72 dB at 1 MHz and −40 dB at 10 MHz when IL = 200 mA and VDO = 0.1 V, and maintains a PSR better than −78 dB at 1 MHz and −42 dB at 10 MHz when IL = 1 mA and VDO = 0.1 V. The LGB-enhanced regulator achieves excellent load and line regulation figures of 29 μV/mA and 0.75 mV/V, while the LGB itself consumes merely 7 μA out of a total quiescent current of 108 μA. Full article
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11 pages, 15320 KB  
Article
Hidden Patterns in Pottery Fabrics: X-Ray µCT-Based 3D Pore Orientation Analysis to Differentiate Wheel-Throwing and Wheel-Coiling Ceramic Forming Techniques in Whole Vessels
by Ilaria Caloi, Federico Bernardini and Marco Voltolini
Heritage 2026, 9(5), 157; https://doi.org/10.3390/heritage9050157 - 22 Apr 2026
Cited by 1 | Viewed by 832
Abstract
Identifying primary ceramic forming techniques is often problematic when surface traces are altered or erased by secondary shaping on the potter’s wheel, particularly in vessels combining hand-building and wheel use. This study aims to develop a quantitative, non-destructive method to distinguish wheel-throwing and [...] Read more.
Identifying primary ceramic forming techniques is often problematic when surface traces are altered or erased by secondary shaping on the potter’s wheel, particularly in vessels combining hand-building and wheel use. This study aims to develop a quantitative, non-destructive method to distinguish wheel-throwing and wheel-coiling techniques by analyzing internal fabric features. Experimental replicas of Middle Minoan handleless conical cups (18th cent. BC), produced using wheel-throwing-off-the-hump and wheel-coiling techniques, were investigated using X-ray micro-computed tomography (µCT). Macropores were segmented from complete 3D µCT datasets and their shape preferred orientation was quantitatively assessed through ellipsoid fitting, orientation distribution functions, and pole figure analysis. The results reveal systematic and reproducible differences between the two forming techniques: wheel-coiled vessels show predominantly horizontal pore elongation, expressed as equatorial girdle textures and vertically clustered short axes, whereas wheel-thrown vessels display inclined pore orientations, forming displaced girdles and ring-like short-axis distributions. These contrasting orientation patterns reflect distinct deformation fields imposed during vessel shaping. The study demonstrates that quantitative 3D analysis of pore orientation in whole vessels provides reliable criteria for identifying ceramic forming techniques and confirms previous qualitative observations. This approach offers a robust framework for technological analysis of ceramics and can be applied to both complete vessels and suitably oriented fragments. Full article
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14 pages, 4605 KB  
Article
A K-Band Four-Channel Beamformer with Temperature Compensation Based on 65 nm CMOS Process
by Cetian Wang, Yanning Liu, Xuejie Liao, Fan Zhang, Chun Deng, Ying Liu, Wenxu Sun, He Guan and Deyun Zhou
Micromachines 2026, 17(4), 462; https://doi.org/10.3390/mi17040462 - 10 Apr 2026
Cited by 1 | Viewed by 1091
Abstract
This paper presents a K-band four-channel phased array beamformer with temperature compensation in 65 nm CMOS for 5G and satellite communications. The beamformer includes a four-way power divider/combiner, four RF channels, and digital control circuits. Each RF channel comprises a receive chain, a [...] Read more.
This paper presents a K-band four-channel phased array beamformer with temperature compensation in 65 nm CMOS for 5G and satellite communications. The beamformer includes a four-way power divider/combiner, four RF channels, and digital control circuits. Each RF channel comprises a receive chain, a transmit chain, and a pair of receive/transmit (TX/RX) single-pole double-throw (SPDT) switches. The receive chain consists of a low-noise amplifier (LNA), a six-bit reflective-type phase shifter (RTPS), a drive amplifier (DA), two temperature-compensation attenuators (TCAs), and a six-bit attenuator (ATT); the transmit chain integrates a power amplifier (PA), two TCAs, a six-bit RTPS, a DA, and a six-bit ATT. Measurements show the chip exhibits 0–4.5 dB gain, noise figure (NF) < 7.8 dB, root mean square (RMS) phase error < 3.5°, and RMS gain error < 0.4 dB in receive mode operating in 19–23 GHz. In transmit mode operating in 21–23 GHz, it provides 6–10 dB gain range, RMS phase error < 3.4°, RMS gain error < 0.25 dB, and output power at 1 dB compression point (OP1dB) > 6.5 dBm. In addition, the receive and transmit gain variations are within 0.8 dB and 0.4 dB, respectively, when temperature ranges from −55 °C to 85 °C. With a compact footprint of 3.5 × 4.8 mm2, the beamformer consumes 110 mW (receive) and 190 mW (transmit) DC power per channel. Full article
(This article belongs to the Special Issue Recent Advancements in Microwave and Optoelectronics Devices)
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20 pages, 6226 KB  
Article
Designing Customized EBSD Software: Inverse Pole Figure Mapping of Crystal Orientations Using Finite Element Shape Functions
by Youliang He
Designs 2026, 10(1), 14; https://doi.org/10.3390/designs10010014 - 2 Feb 2026
Viewed by 1876
Abstract
Inverse pole figure mapping is a common orientation visualization method used in electron backscatter diffraction (EBSD) software to display crystal orientations. Although this technique has been routinely used in commercial EBSD software, the coloring algorithm employed to map the orientation and construct the [...] Read more.
Inverse pole figure mapping is a common orientation visualization method used in electron backscatter diffraction (EBSD) software to display crystal orientations. Although this technique has been routinely used in commercial EBSD software, the coloring algorithm employed to map the orientation and construct the color key (standard stereographic triangle) has not been reported in the literature. This paper presents a simple algorithm to color the standard stereographic triangles of the 11 Laue groups by mapping the Maxwell color triangle to the curved standard stereographic triangles using nonlinear shape functions commonly employed in finite element methods. Detailed procedures are given to illustrate how the mapping is performed and how it is used to construct inverse pole figure maps from Euler angles. Color coding of the seven different standard stereographic triangles is demonstrated using a computer program written in C++. It is shown that the simple color-coding algorithm presented in this paper can be conveniently utilized to display orientation data in inverse pole figure maps, which is a critical part of designing customized EBSD software. It also provides a method to adjust the color center within the curved triangles to more uniformly distribute the color, which is not available in commercial EBSD software. The algorithm can also be used to design orientation representation software for other applications, e.g., crystal plasticity simulations, where representation of orientation data is also a routine task. Full article
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25 pages, 4782 KB  
Article
Comprehensive Structural and Interfacial Characterization of Laser-Sliced SiC Wafers
by Hong Chen, Seul Lee, Minseung Kang, Hye Seon Youn, Seongwon Go, Eunsook Kang and Chae-Ryong Cho
Materials 2025, 18(24), 5615; https://doi.org/10.3390/ma18245615 - 14 Dec 2025
Cited by 3 | Viewed by 1367
Abstract
Laser slicing has emerged as a promising low-kerf and low-damage technique for SiC wafer fabrication; however, its effects on the crystal integrity, near-surface modification, and charge-transport properties require further clarification. Here, a heavily N-doped 4° off-axis 4H-SiC wafer was sliced using an ultraviolet [...] Read more.
Laser slicing has emerged as a promising low-kerf and low-damage technique for SiC wafer fabrication; however, its effects on the crystal integrity, near-surface modification, and charge-transport properties require further clarification. Here, a heavily N-doped 4° off-axis 4H-SiC wafer was sliced using an ultraviolet (UV) picosecond laser, and both laser-irradiated and laser-sliced surfaces were comprehensively characterized. X-ray diffraction and pole figure measurements confirmed that the 4H stacking sequence and macroscopic crystal orientation were preserved after slicing. Raman spectroscopy, including analysis of the folded transverse-optical and longitudinal-optical phonon–plasmon coupled modes, enabled dielectric function fitting and determination of the plasmon frequency, yielding a free-carrier concentration of ~3.1 × 1018 cm−3. Hall measurements provided consistent carrier density, mobility, and resistivity, demonstrating that the laser slicing process did not degrade bulk electrical properties. Multi-scale Atomic Force Microscopy (AFM), Angle-Resolved X-Ray Photoelectron Spectroscopy (ARXPS), Secondary Ion Mass Spectrometry (SIMS), and Transmission Electron Microscopy (TEM)/Selected Area Electron Diffraction (SAED) analyses revealed the formation of a near-surface thin amorphous/polycrystalline modified layer and an oxygen-rich region, with significantly increased roughness and thicker modified layers on the hilly regions of the sliced surface. These results indicate that UV laser slicing maintains the intrinsic crystalline and electrical properties of 4H-SiC while introducing localized nanoscale surface damage that must be minimized by optimizing the slicing parameters and the subsequent surface-finishing processes. Full article
(This article belongs to the Section Advanced Materials Characterization)
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17 pages, 5074 KB  
Article
Dynamic Recrystallization and Microstructural Evolution During Hot Deformation of Al-Cu-Mg Alloy
by Fangyan He, Xiaolan Wu, Zhizheng Rong, Xueqin Zhang, Xiangyuan Xiong, Shengping Wen, Kunyuan Gao, Wu Wei, Li Rong, Hui Huang and Zuoren Nie
Metals 2025, 15(10), 1100; https://doi.org/10.3390/met15101100 - 1 Oct 2025
Cited by 4 | Viewed by 2388
Abstract
Isothermal hot compression tests were performed on an Al-4.8Cu-0.25Mg-0.32Mn-0.17Si alloy using a Gleeble-3500 thermomechanical simulator within the temperature range of 350–510 °C and strain rate range of 0.001–10 s−1, achieving a true strain of 0.9. The constitutive equation and hot processing [...] Read more.
Isothermal hot compression tests were performed on an Al-4.8Cu-0.25Mg-0.32Mn-0.17Si alloy using a Gleeble-3500 thermomechanical simulator within the temperature range of 350–510 °C and strain rate range of 0.001–10 s−1, achieving a true strain of 0.9. The constitutive equation and hot processing maps were established to predict the flow behavior of the alloy. The hot deformation mechanisms were investigated through microstructural characterization using inverse pole figure (IPF), grain boundary (GB), and grain orientation spread (GOS) analysis. The results demonstrate that both dynamic recovery (DRV) and dynamic recrystallization (DRX) occur during hot deformation. At high lnZ values (high strain rates and low deformation temperatures), discontinuous dynamic recrystallization (DDRX) dominates. Under middle lnZ conditions (low strain rate or high deformation temperature), both continuous dynamic recrystallization (CDRX) and DDRX are the primary mechanisms. Conversely, at low lnZ values (low strain rates and high temperatures), CDRX and geometric dynamic recrystallization (GDRX) become predominant. The DRX process in the Al-Cu-Mg alloy is controlled by the deformation temperature and strain rate. Full article
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20 pages, 5035 KB  
Article
Effect of Small Deformations on Optimisation of Final Crystallographic Texture and Microstructure in Non-Oriented FeSi Steels
by Ivan Petrišinec, Marcela Motýľová, František Kováč, Ladislav Falat, Viktor Puchý, Mária Podobová and František Kromka
Crystals 2025, 15(10), 839; https://doi.org/10.3390/cryst15100839 - 26 Sep 2025
Viewed by 884
Abstract
Improving the isotropic magnetic properties of FeSi electrical steels has traditionally focused on enhancing their crystallographic texture and microstructural morphology. Strengthening the cube texture within a ferritic matrix of optimal grain size is known to reduce core losses and increase magnetic induction. However, [...] Read more.
Improving the isotropic magnetic properties of FeSi electrical steels has traditionally focused on enhancing their crystallographic texture and microstructural morphology. Strengthening the cube texture within a ferritic matrix of optimal grain size is known to reduce core losses and increase magnetic induction. However, conventional cold rolling followed by annealing remains insufficient to optimise the magnetic performance of thin FeSi strips fully. This study explores an alternative approach based on grain boundary migration driven by temperature gradients combined with deformation gradients, either across the sheet thickness or between neighbouring grains, in thin, weakly deformed non-oriented (NO) electrical steel sheets. The concept relies on deformation-induced grain growth supported by rapid heat transport to promote the preferential formation of coarse grains with favourable orientations. Experimental material consisted of vacuum-degassed FeSi steel with low silicon content. Controlled deformation was introduced by temper rolling at room temperature with 2–40% thickness reductions, followed by rapid recrystallisation annealing at 950 °C. Microstructure, texture, and residual strain distributions were analysed using inverse pole figure (IPF) maps, kernel average misorientation (KAM) maps, and orientation distribution function (ODF) sections derived from electron backscattered diffraction (EBSD) data. This combined thermomechanical treatment produced coarse-grained microstructures with an enhanced cube texture component, reducing coercivity from 162 A/m to 65 A/m. These results demonstrate that temper rolling combined with dynamic annealing can surpass the limitations of conventional processing routes for NO FeSi steels. Full article
(This article belongs to the Special Issue Microstructure and Deformation of Advanced Alloys (2nd Edition))
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