Search Results (104)

This paper presents a K-band four-channel phased array beamformer with temperature compensation in 65 nm CMOS for 5G and satellite communications. The beamformer includes a four-way power divider/combiner, four RF channels, and digital control circuits. Each RF channel comprises a receive chain, a transmit chain, and a pair of receive/transmit (TX/RX) single-pole double-throw (SPDT) switches. The receive chain consists of a low-noise amplifier (LNA), a six-bit reflective-type phase shifter (RTPS), a drive amplifier (DA), two temperature-compensation attenuators (TCAs), and a six-bit attenuator (ATT); the transmit chain integrates a power amplifier (PA), two TCAs, a six-bit RTPS, a DA, and a six-bit ATT. Measurements show the chip exhibits 0–4.5 dB gain, noise figure (NF) < 7.8 dB, root mean square (RMS) phase error < 3.5°, and RMS gain error < 0.4 dB in receive mode operating in 19–23 GHz. In transmit mode operating in 21–23 GHz, it provides 6–10 dB gain range, RMS phase error < 3.4°, RMS gain error < 0.25 dB, and output power at 1 dB compression point (OP1dB) > 6.5 dBm. In addition, the receive and transmit gain variations are within 0.8 dB and 0.4 dB, respectively, when temperature ranges from −55 °C to 85 °C. With a compact footprint of 3.5 × 4.8 mm², the beamformer consumes 110 mW (receive) and 190 mW (transmit) DC power per channel. Full article

Inverse pole figure mapping is a common orientation visualization method used in electron backscatter diffraction (EBSD) software to display crystal orientations. Although this technique has been routinely used in commercial EBSD software, the coloring algorithm employed to map the orientation and construct the color key (standard stereographic triangle) has not been reported in the literature. This paper presents a simple algorithm to color the standard stereographic triangles of the 11 Laue groups by mapping the Maxwell color triangle to the curved standard stereographic triangles using nonlinear shape functions commonly employed in finite element methods. Detailed procedures are given to illustrate how the mapping is performed and how it is used to construct inverse pole figure maps from Euler angles. Color coding of the seven different standard stereographic triangles is demonstrated using a computer program written in C++. It is shown that the simple color-coding algorithm presented in this paper can be conveniently utilized to display orientation data in inverse pole figure maps, which is a critical part of designing customized EBSD software. It also provides a method to adjust the color center within the curved triangles to more uniformly distribute the color, which is not available in commercial EBSD software. The algorithm can also be used to design orientation representation software for other applications, e.g., crystal plasticity simulations, where representation of orientation data is also a routine task. Full article

Laser slicing has emerged as a promising low-kerf and low-damage technique for SiC wafer fabrication; however, its effects on the crystal integrity, near-surface modification, and charge-transport properties require further clarification. Here, a heavily N-doped 4° off-axis 4H-SiC wafer was sliced using an ultraviolet (UV) picosecond laser, and both laser-irradiated and laser-sliced surfaces were comprehensively characterized. X-ray diffraction and pole figure measurements confirmed that the 4H stacking sequence and macroscopic crystal orientation were preserved after slicing. Raman spectroscopy, including analysis of the folded transverse-optical and longitudinal-optical phonon–plasmon coupled modes, enabled dielectric function fitting and determination of the plasmon frequency, yielding a free-carrier concentration of ~3.1 × 10¹⁸ cm⁻³. Hall measurements provided consistent carrier density, mobility, and resistivity, demonstrating that the laser slicing process did not degrade bulk electrical properties. Multi-scale Atomic Force Microscopy (AFM), Angle-Resolved X-Ray Photoelectron Spectroscopy (ARXPS), Secondary Ion Mass Spectrometry (SIMS), and Transmission Electron Microscopy (TEM)/Selected Area Electron Diffraction (SAED) analyses revealed the formation of a near-surface thin amorphous/polycrystalline modified layer and an oxygen-rich region, with significantly increased roughness and thicker modified layers on the hilly regions of the sliced surface. These results indicate that UV laser slicing maintains the intrinsic crystalline and electrical properties of 4H-SiC while introducing localized nanoscale surface damage that must be minimized by optimizing the slicing parameters and the subsequent surface-finishing processes. Full article

Isothermal hot compression tests were performed on an Al-4.8Cu-0.25Mg-0.32Mn-0.17Si alloy using a Gleeble-3500 thermomechanical simulator within the temperature range of 350–510 °C and strain rate range of 0.001–10 s⁻¹, achieving a true strain of 0.9. The constitutive equation and hot processing maps were established to predict the flow behavior of the alloy. The hot deformation mechanisms were investigated through microstructural characterization using inverse pole figure (IPF), grain boundary (GB), and grain orientation spread (GOS) analysis. The results demonstrate that both dynamic recovery (DRV) and dynamic recrystallization (DRX) occur during hot deformation. At high lnZ values (high strain rates and low deformation temperatures), discontinuous dynamic recrystallization (DDRX) dominates. Under middle lnZ conditions (low strain rate or high deformation temperature), both continuous dynamic recrystallization (CDRX) and DDRX are the primary mechanisms. Conversely, at low lnZ values (low strain rates and high temperatures), CDRX and geometric dynamic recrystallization (GDRX) become predominant. The DRX process in the Al-Cu-Mg alloy is controlled by the deformation temperature and strain rate. Full article

Improving the isotropic magnetic properties of FeSi electrical steels has traditionally focused on enhancing their crystallographic texture and microstructural morphology. Strengthening the cube texture within a ferritic matrix of optimal grain size is known to reduce core losses and increase magnetic induction. However, conventional cold rolling followed by annealing remains insufficient to optimise the magnetic performance of thin FeSi strips fully. This study explores an alternative approach based on grain boundary migration driven by temperature gradients combined with deformation gradients, either across the sheet thickness or between neighbouring grains, in thin, weakly deformed non-oriented (NO) electrical steel sheets. The concept relies on deformation-induced grain growth supported by rapid heat transport to promote the preferential formation of coarse grains with favourable orientations. Experimental material consisted of vacuum-degassed FeSi steel with low silicon content. Controlled deformation was introduced by temper rolling at room temperature with 2–40% thickness reductions, followed by rapid recrystallisation annealing at 950 °C. Microstructure, texture, and residual strain distributions were analysed using inverse pole figure (IPF) maps, kernel average misorientation (KAM) maps, and orientation distribution function (ODF) sections derived from electron backscattered diffraction (EBSD) data. This combined thermomechanical treatment produced coarse-grained microstructures with an enhanced cube texture component, reducing coercivity from 162 A/m to 65 A/m. These results demonstrate that temper rolling combined with dynamic annealing can surpass the limitations of conventional processing routes for NO FeSi steels. Full article

TbCu₇-type Sm-based compounds can be produced in bulk and potentially surpass Nd₂Fe₁₄B as permanent magnets. However, as the processes to prepare anisotropic magnetic particles are limited, the full potential of TbCu₇-type Sm-based compounds cannot be exploited. In this study, metastable TbCu₇-type phases of anisotropic Sm–Fe–N ultrafine particles were prepared using the low-oxygen induction thermal plasma (LO-ITP) process. X-ray diffraction analysis revealed that the obtained TbCu₇-type Sm–Fe alloy nanoparticles exhibited a c/a value of 0.8419, with an Fe/Sm atomic ratio of ~8.5. After nitrogenation, the obtained Sm–Fe–N nanoparticles were aligned under an external magnetic field, indicating that each alloy particle exhibited anisotropic magnetic properties. A substantially high degree of alignment of 91 ± 2% was achieved, quantitatively estimated via pole figure measurements. Numerical analysis following Sm–Fe nanoparticle formation showed that, compared with Fe condensation, Sm condensation persisted even at low temperatures, because of a significant difference in vapor pressure between Sm and Fe. Though this led to a relatively large compositional distribution of Sm within particles with a Sm concentration of 9–12 at%, the preparation of single-phase TbCu₇-type Sm–Fe–N particles could be facilitated by optimizing several parameters during the LO-ITP process. Full article

This article presents a low-noise amplifier (LNA) with high image rejection ratio (IRR) operating in the 5G millimeter-wave band using a 65 nm CMOS process. The circuit adopts an inter-stage notch filtering structure composed of a transformer and a switched capacitor array to achieve image suppression and impedance matching with no die area overhead. By adjusting the values of the switch capacitor array, the transmission zeros are positioned in the stopband while the poles are placed in the passband, thereby realizing image rejection. Furthermore, the number and distribution of poles under the both real and complex impedance conditions are analyzed. Moreover, the quality factor (Q) of the zero is derived to establish the relationship between Q and the image rejection ratio, guiding the optimization of both gain and IRR of the circuit design. Measurement results demonstrate that the LNA exhibits a gain of 18 dB and a noise figure (NF) of 4.4 dB at 40 GHz, with a corresponding IRR of 53.4 dB when the intermediate frequency (IF) is 6 GHz. The circuit demonstrates a 3 dB bandwidth from 36.3 to 40.7 GHz, with an IRR greater than 42 dB across this frequency range. The power consumption is 25.4 mW from a 1 V supply, and the pad-excluded core area of the entire chip is 0.13 mm². Full article

Magnetic shape memory alloys have attracted considerable attention due to their multifunctional properties. Among these materials, Ni-Mn-Ga alloys are distinguished by their ability to achieve up to 10% strain when exposed to a magnetic field, a characteristic predominantly observed in single-crystal samples. Consequently, it is essential to develop nanomaterials with a crystal structure closely resembling that of a single crystal. In this study, an epitaxial Ni-Mn-Ga thin film was fabricated using Pulsed Laser Deposition on an Al₂O₃ $\left(11\overline{2}0\right)$ single-crystal substrate. The crystal structure was characterised through X-ray diffraction methodologies, such as symmetrical $2\theta -\omega$ scans, pole figures, and reciprocal space maps. The results indicated that the sample was mainly in a slightly distorted cubic austenite phase, and some incipient martensite phase also appeared. A detailed microstructural analysis, performed by transmission electron microscopy, confirmed that certain regions of the sample exhibited an incipient transformation to the martensite phase. Regions closer to the substrate retained the austenite phase, suggesting that the constraint imposed by the substrate inhibits the phase transition. These results indicate that it is possible to grow high crystalline quality thin films of Ni-Mn-Ga by Pulsed Laser Deposition. Full article

The cube texture in alloys shows deterioration under plastic deformation. To further observe the evolution of orientation in individual grains during deformation, in-situ tensile testing was coupled with electron backscattered diffraction (EBSD). We found that the rotation of an individual grain is not only determined by its Schmid factor and size, but also by the condition of the adjacent grains. We demonstrated the interactions between grains using the EBSD data in different models, including the crystal orientation, the kernel average misorientation, the Schmid factor, the inverse pole figure, and the grain reference orientation deviation. A systematic three-factor coupled model involving the Schmid factor, grain size, and neighboring grain states is proposed. Furthermore, the mechanism by which small-sized grains induce the splitting of adjacent larger grains through the pinning effect has not been reported in highly textured polycrystalline materials to date. This characterization allows us to better understand the changes in grain shape and crystal lattice rotation, which can be used to characterize other polycrystalline alloys. Full article

Low-pass filters with bandwidths larger than several GHz are required in many applications, such as anti-aliasing filters in high-speed ADCs and pulse-shaping filters in high-speed DACs. In highly integrated applications, low area occupation and power consumption are key specifications, so inductor-less implementations are to be preferred. Furthermore, full CMOS implementations provide an advantage in terms of technology availability and cost. In this paper, we present an inductor-less CMOS biquad stage based on the super source follower topology that provides an 8 GHz cutoff frequency and a low power consumption of 0.42 mW per pole, showing remarkable performance also in terms of bandwidth and dynamic range. The availability of two separate current sources allows independent tuning of natural frequency and quality factor. The stage can be implemented in two complementary ways, exploiting NMOS and PMOS input devices, respectively, thus simplifying cascadability. The two complementary biquads have been implemented in the STMicroelectronics FDSOI 28 nm CMOS process and extensively simulated and provide stable performance under PVT variations and mismatches. The area occupation is about 387.5 μm² per biquad, one of the lowest in the literature. The figures-of-merit are remarkable, as the filters achieve excellent power efficiency, very low area occupation, and good dynamic range. Full article

Ultrasonic vibration (UV) has been employed in various plastic forming processes due to its special effect known as acoustoplasticity. Mostly, UV is applied along the longitudinal direction in experimental investigations. However, very few studies have focused on normal UV-assisted uniaxial tension, which is more similar to the loading state of sheet metal in actual forming processes. Herein, normal UV-assisted tension tests on a TA1 thin sheet are performed to study its mechanical properties and microstructure evolution. The macro-mechanical behavior is demonstrated by stress–strain curves under different ultrasonic amplitudes and strain rates. Fracture morphology and microstructure evolution are characterized by scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) to reveal the UV softening mechanism at the micro level. The results show that the stress reduction induced by UV reaches 20% when the ultrasonic amplitude is 13.9 μm. Fracture mode changes from ductile fracture to brittle fracture with increasing amplitude. Microstructure examinations show that low-angle grain boundary (LAGB) fraction, kernel average misorientation (KAM), and geometrically necessary dislocation (GND) density in the samples experiencing normal UV-assisted tension are all decreased, leading to a reduction in deformation resistance. The inverse pole figures (IPFs) further reveal that the plastic deformation mechanism of the TA1 thin sheet is diversified with the superposition of normal UV. Full article

The deployment of fifth-generation (5G) and beyond-5G wireless communication systems necessitates advanced transceiver architectures to support high data rates, spectrum efficiency, and energy-efficient designs. This paper presents a highly adaptive reconfigurable receiver front-end (HARRF) designed for 5G and satellite applications, integrating a switchable low noise amplifier (LNA) and a single pole double throw (SPDT) switch. The HARRF architecture supports both X-band (8–12 GHz) and K/Ka-band (23–28 GHz) operations, enabling seamless adaptation between radar, satellite communication, and millimeter-wave (mmWave) 5G applications. The proposed receiver front-end employs a 0.15 μ$\mathrm{m}$ pseudomorphic high electron mobility transistor (pHEMT) process, optimised through a three-stage cascaded LNA topology. A switched-tuned matching network is utilised to achieve reconfigurability between X-band and K/Ka-band. Performance evaluations indicate that the X-band LNA achieves a gain of 23–27 dB with a noise figure below 7 dB, whereas the K/Ka-band LNA provides 23–27 dB gain with a noise figure ranging from 2.3–2.6 dB. The SPDT switch exhibits low insertion loss and high isolation, ensuring minimal signal degradation across operational bands. Network analysis and scattering parameter extractions were conducted using advanced design system (ADS) simulations, demonstrating superior return loss, power efficiency, and impedance matching. Comparative analysis with state-of-the-art designs shows that the proposed HARRF outperforms existing solutions in terms of reconfigurability, stability, and wideband operation. The results validate the feasibility of the proposed reconfigurable RF front-end in enabling efficient spectrum utilisation and energy-efficient transceiver systems for next-generation communication networks. Full article

This comprehensive review focuses on the most recent advances in electron backscatter diffraction (EBSD) methods in the context of materials science and includes a thorough evaluation of the sample preparation procedures unique to EBSD as well as a complete examination of the important operational parameters inherent in EBSD setups. This review highlights the importance of customizing EBSD parameters for precise microstructural imaging and enhancing understanding of material behavior. While some studies have explored grain boundary characterization, stored energy, and crystallographic orientation using EBSD, there is a clear need for more comprehensive investigations to fully leverage its capabilities. Additionally, there is a significant gap in understanding the optimal choice of the reference plane in EBSD analysis, indicating the necessity for further research to improve EBSD analyses’ accuracy and efficacy. The review seeks to present a detailed and contemporary viewpoint on the many applications, sample preparation techniques, and optimal operational considerations that jointly increase the adaptability and efficacy of EBSD in materials science research by relying on the relevant literature. Full article

The microstructure of bivalve foliated calcite is extraordinary. It consists of units formed of stacks of folia with individual folia consisting of arrowhead-ended crystal laths. We investigated the texture of the foliated microstructure, the texture of individual and arrays of folia and the texture of assemblies of foliated units of the gryphaeid oyster Hyotissa hyotis with low kV, high-resolution, electron backscatter diffraction (EBSD). We base our understanding of the foliated texture on the combined interpretation of crystallographic aspects of individual and stacks of folia with the nature of crystal organization in a folium, a foliated unit and in foliated unit aggregations. Calcite c- and a*-axes arrangement in a folium is single-crystal-like. Due to the parallel organization of adjacent laths in a folium and the stacked arrangement of folia in a foliated unit, the assembly of calcite c- and a*-axes in foliated units is graded. The result is a ring-like distribution of c- and a*-axes orientations in the pole figures; nonetheless, the orientation rings are substructured by c- and a*-axes orientation clusters. The direction of the arrowhead endings of the laths is coincident with the growth direction of the shell. The morphology of arrowheaded laths initiates the formation of planes with {105}, {106} directions and a parallel orientation to the inner shell surface. H. hyotis’s foliated microstructure has a specific texture that is not fully understood. We discuss axial, spherulitic, turbostratic-like textures the foliated microstructure and suggest that the foliated texture of H. hyotis can, to some degree, be described with a turbostratic pattern. Full article

The twin-roll casting (TRC) process has gained significant attention for aluminum sheet production due to its cost-effectiveness and high processing efficiency. However, controlling the initial grain structure of TRC strips remains challenging due to the absence of a hot rolling stage, necessitating an advanced predictive modeling approach. In this study, a cellular automaton–finite element (CA-FE) model was developed to predict the grain structure and texture of aluminum strips fabricated via TRC. Both pure Al and AA7075 alloys were cast under identical conditions using a pilot-scale horizontal twin-roll caster, and their microstructures were characterized experimentally. The developed model incorporated a Gaussian nucleation distribution function and an equivalent binary approach to account for the solidification behavior of multicomponent alloys. The CA-FE simulation results successfully reproduced the key aspects of solidification, grain structure, and texture evolution of TRC strips. The predicted temperature distribution and solid fraction evolution showed distinct differences between the alloys, with pure Al forming columnar grains and AA7075 developing a fully equiaxed structure, which closely matched the experimental findings. Additionally, texture analysis using inverse pole figures (IPFs) and pole figures (PFs) revealed a clear <001> orientation in pure Al, whereas AA7075 exhibited a random texture, both of which were well captured by the CA-FE model. The findings indicate that the developed model offers a reliable prediction of the solidification microstructure and texture evolution in TRC strips, making it a valuable tool for optimizing continuous casting processes. Full article