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16 pages, 616 KB  
Review
Minimally Invasive Interventions for Childhood Caries: A Scoping Review of Their Applicability in Public Health and Community Settings
by Giovanna Lima Fortunato, Gabriel Pereira Nunes, Isabela dos Santos de Deus, Priscila Toninatto Alves de Toledo, Guilherme Assumpção Silva, Cristina Antoniali Silva, Aimée Maria Guiotti and Daniela Atili Brandini
Healthcare 2026, 14(9), 1155; https://doi.org/10.3390/healthcare14091155 (registering DOI) - 25 Apr 2026
Abstract
Background/Objectives: Dental caries is one of the most prevalent chronic diseases in childhood, disproportionately affecting socially vulnerable populations. This scoping review aimed to analyze the clinical effects of selected minimally invasive materials and approaches, specifically mouthrinses, fluoride varnishes, silver diamine fluoride, and glass [...] Read more.
Background/Objectives: Dental caries is one of the most prevalent chronic diseases in childhood, disproportionately affecting socially vulnerable populations. This scoping review aimed to analyze the clinical effects of selected minimally invasive materials and approaches, specifically mouthrinses, fluoride varnishes, silver diamine fluoride, and glass ionomer-based interventions, for the prevention and management of dental caries in pediatric patients, with emphasis on public health and community-based settings. Methods: This scoping review followed the Population, Concept, and Context (PCC) framework. Electronic searches were conducted up to 23 January 2026, using tailored strategies for mouthrinses, fluoride varnishes, silver diamine fluoride (SDF), and glass ionomer cements (GICs). Randomized clinical trials (RCTs) were included. Data extraction and qualitative synthesis focused on clinical outcomes and applicability in public health contexts. Results: Fifty-five RCTs were included. Fluoride- or chlorhexidine-based mouthrinses showed potential in controlling cariogenic biofilm, with evidence primarily based on microbiological outcomes. Fluoride varnishes were associated with enamel remineralization and control of early white spot lesions, particularly in supervised programs. SDF was reported to achieve high caries’ arrest rates in cavitated dentin lesions of primary teeth, while its preventive effect on sound surfaces appeared comparable to other fluoride-based interventions. GICs were associated with acceptable clinical performance as pit-and-fissure sealants and in atraumatic restorative treatment. Conclusions: Minimally invasive dentistry (MID) approaches show promise for the prevention and management of childhood dental caries in public health and community-based settings. However, these findings should be interpreted with caution due to the heterogeneity of interventions and outcome measures, the predominance of short-term and surrogate (microbiological) outcomes, and the absence of a formal risk-of-bias assessment. As a scoping review, the synthesis is narrative in nature, which limits the ability to draw definitive conclusions. Further studies with standardized clinical outcomes and longer follow-up are needed to strengthen the evidence. Full article
(This article belongs to the Special Issue Current Advances in Oral Health Promotion)
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20 pages, 601 KB  
Systematic Review
Environmental Performance of Sparkling Wine Production Across the Value Chain—A Systematic Review of LCA Studies
by Beatriz Gaspar, Miguel Ferreira, José Ferreira, Idalina Domingos and António Ferreira
Appl. Sci. 2026, 16(9), 4220; https://doi.org/10.3390/app16094220 (registering DOI) - 25 Apr 2026
Abstract
This systematic review examines the application of life cycle assessment (LCA) to evaluate the environmental performance of sparkling wine production across its value chain. Following PRISMA 2020 guidelines, a structured search in Scopus and Web of Science identified 17 relevant studies published between [...] Read more.
This systematic review examines the application of life cycle assessment (LCA) to evaluate the environmental performance of sparkling wine production across its value chain. Following PRISMA 2020 guidelines, a structured search in Scopus and Web of Science identified 17 relevant studies published between 2015 and 2025. The results show that environmental hotspots are consistently associated with viticultural inputs (fertilizers, pesticides, and fuel use), energy consumption in winery operations, packaging—particularly glass bottle production—and distribution. Carbon footprint values typically range from 0.9 to 1.9 kg CO2eq per bottle, with packaging accounting for up to 55–60% of total impact. Methodologically, most studies adopt an attributional LCA approach, apply partial system boundaries, and focus primarily on climate change, limiting comparability and completeness. Conversely, sparkling wine-specific stages, such as secondary fermentation and aging, remain underrepresented. Overall, the findings reveal substantial methodological heterogeneity across studies, particularly in functional units, system boundaries, and impact assessment methods. However, processes specific to sparkling wine production remain underrepresented, limiting the accuracy of environmental characterization for these systems. This review highlights the need for harmonized cradle-to-grave LCA frameworks, bottle-based functional units, and broader impact categories to improve the robustness and comparability of LCA applications in sparkling wine production. Full article
(This article belongs to the Section Food Science and Technology)
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40 pages, 1639 KB  
Review
Antenna Performance and Effects of Concealment Within Building Structures: A Comprehensive Review
by Mirza Farrukh Baig and Ervina Efzan Mhd Noor
Technologies 2026, 14(5), 259; https://doi.org/10.3390/technologies14050259 (registering DOI) - 25 Apr 2026
Abstract
The rapid expansion of wireless communication in urban environments requires antenna systems that balance high electromagnetic performance with stringent aesthetic and security constraints. This review examines recent advances in concealed antenna technologies integrated into building structures, with a focus on performance variation, material-induced [...] Read more.
The rapid expansion of wireless communication in urban environments requires antenna systems that balance high electromagnetic performance with stringent aesthetic and security constraints. This review examines recent advances in concealed antenna technologies integrated into building structures, with a focus on performance variation, material-induced attenuation, and emerging concealment strategies. Techniques such as transparent conductors on glass, structural embedding within walls, and camouflage-based designs are shown to significantly influence resonance behavior, radiation efficiency, and pattern characteristics compared to free-space operation. Despite these challenges, optimized solutions including transparent conductive oxide arrays, wideband embedded antenna geometries, and metasurface-enhanced window structures can partially recover performance while maintaining optical transparency above 70%. Material loading effects are found to induce resonant frequency shifts of approximately 10–44%, depending on dielectric properties and environmental conditions. Transparent antenna arrays achieve gains ranging from 0.34 to 13.2 dBi, while signal-transmissive wall systems demonstrate transmission improvements of up to 22 dB relative to untreated building materials. These technologies enable a wide range of applications, including 5G and beyond-5G cellular networks across sub-6 GHz and millimeter-wave bands, as well as Internet of Things systems and smart city infrastructure. However, key challenges remain, including the need for comprehensive characterization of building material electromagnetic properties, optimization of multilayer structural environments, and the development of standardized design and evaluation methodologies. This review provides a unified framework for understanding the tradeoffs associated with antenna concealment and identifies critical research directions for the development of building-integrated wireless systems in next-generation communication networks. Full article
(This article belongs to the Section Information and Communication Technologies)
22 pages, 1371 KB  
Article
Analytic Hierarchy Process-Based Multi-Criteria Optimization of Functionally Graded Thermoplastic Architectures for Enhanced Viscoelastic Energy Dissipation
by Raja Subramani
J. Compos. Sci. 2026, 10(5), 229; https://doi.org/10.3390/jcs10050229 (registering DOI) - 25 Apr 2026
Abstract
Functionally graded multi-material thermoplastic architectures provide a promising route for tailoring viscoelastic energy dissipation through controlled phase contrast and interfacial interactions. However, rational selection of optimal material compositions remains challenging due to competing requirements among stiffness, damping efficiency, thermal stability, and processability. The [...] Read more.
Functionally graded multi-material thermoplastic architectures provide a promising route for tailoring viscoelastic energy dissipation through controlled phase contrast and interfacial interactions. However, rational selection of optimal material compositions remains challenging due to competing requirements among stiffness, damping efficiency, thermal stability, and processability. The absence of a quantitative decision framework often limits systematic design of architected polymer systems. This study proposes an Analytic Hierarchy Process (AHP)-based multi-criteria decision model to identify the optimal rigid–elastic thermoplastic composition for enhanced damping performance. Nine performance criteria were considered, including storage modulus, loss factor, damping bandwidth, interfacial adhesion strength, elongation at break, impact resistance, glass transition temperature, thermal stability, and printability. Fourteen alternative material configurations combining different rigid phases, elastomeric interlayers, filler contents, and layer thickness ratios were evaluated. Pairwise comparison matrices were constructed based on experimentally measured thermomechanical data and literature-reported values, and consistency ratios were maintained below 0.1 to ensure decision reliability. Numerical results indicate that a graded PLA/soft-TPU/PLA architecture with optimized layer thickness ratio achieved the highest global priority weight (0.431), outperforming the baseline PLA/TPU system by approximately ~25–30% in overall performance index. Sensitivity analysis confirmed ranking robustness across variations in damping and stiffness weighting factors. The proposed framework establishes a systematic methodology for polymer material selection and multi-material architectural optimization, enabling data-driven design of thermoplastic systems with tunable viscoelastic performance. Full article
(This article belongs to the Section Composites Manufacturing and Processing)
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30 pages, 10532 KB  
Article
Data-Driven Multi-Objective Optimization of Building Envelope Retrofits for Senior Apartments in Beijing
by Lai Fan, Mengying Li and Yang Shi
Buildings 2026, 16(9), 1682; https://doi.org/10.3390/buildings16091682 (registering DOI) - 24 Apr 2026
Abstract
Aging populations have intensified the demand for thermally comfortable and energy-efficient housing, particularly for elderly residents whose diminished thermoregulatory capacity renders them disproportionately vulnerable to indoor temperature fluctuations. Existing senior apartments in cold-climate regions frequently fail to meet age-specific thermal comfort standards, yet [...] Read more.
Aging populations have intensified the demand for thermally comfortable and energy-efficient housing, particularly for elderly residents whose diminished thermoregulatory capacity renders them disproportionately vulnerable to indoor temperature fluctuations. Existing senior apartments in cold-climate regions frequently fail to meet age-specific thermal comfort standards, yet systematic retrofit optimization frameworks explicitly tailored to elderly occupants remain scarce. This study presents a data-driven multi-objective optimization framework for building envelope retrofitting, which is validated using on-site temperature measurements from a representative 1980s brick–concrete senior apartment building in Beijing. The framework integrates Latin Hypercube Sampling (LHS) for design space exploration, a Long Short-Term Memory (LSTM) surrogate model for simultaneous prediction of three performance objectives, and Non-dominated Sorting Genetic Algorithm II (NSGA-II) for Pareto-optimal solution generation, with final selection performed via a weighted Mahalanobis distance-based Technique for Order Preference by Similarity to an Ideal Solution (TOPSIS). Optimization targets—annual energy consumption, indoor thermal discomfort hours, and retrofit cost—are parameterized using the age-sensitive comfort thresholds specified in GB 50340-2016. The LSTM surrogate achieved R2 values of 0.91–0.93 across all objectives with training–testing differences below 0.02. The optimal retrofit package—Polyvinyl Chloride (PVC) Low Emissivity (Low-E) double-glazed windows (5 + 6A + 5), glass fiber roof insulation (65.25 mm), and Extruded Polystyrene (XPS) external wall insulation (65.39 mm)—reduces annual energy consumption by 47.1% (from 40,867 to 21,626 kWh) and annual thermal discomfort hours by 62.4% (from 2454 °C·h to 923 °C·h). SHapley Additive exPlanations (SHAP)-based sensitivity analysis further identifies wall U-value and roof thickness as the dominant performance drivers. A reproducible and computationally efficient pathway is provided by the proposed framework for evidence-based envelope retrofit decision-making in existing senior residential buildings. Full article
(This article belongs to the Special Issue Human Comfort and Building Energy Efficiency)
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20 pages, 4678 KB  
Article
An Investigation into the Friction Stir Spot Welding Behavior of 3D-Printed Glass Fiber-Reinforced Polylactic Acid
by Emre Kanlı, Oğuz Koçar and Nergizhan Anaç
Polymers 2026, 18(9), 1041; https://doi.org/10.3390/polym18091041 (registering DOI) - 24 Apr 2026
Abstract
The production of fiber-reinforced polymer composites using 3D printing technology offers significant potential and opportunities for industrial applications. However, current dimensional limitations in 3D printing necessitate the use of joining techniques to obtain larger components. Recently, innovative strategies such as friction stir spot [...] Read more.
The production of fiber-reinforced polymer composites using 3D printing technology offers significant potential and opportunities for industrial applications. However, current dimensional limitations in 3D printing necessitate the use of joining techniques to obtain larger components. Recently, innovative strategies such as friction stir spot welding (FSSW) have attracted considerable attention for joining polymer composites due to their ability to produce strong joints with relatively low heat input (solid-state welding). Nevertheless, it is important to understand how the fibers present in fiber-reinforced polymer composites influence material flow and welding performance during the FSSW process. In this study, glass fiber-reinforced polylactic acid (PLA-GF) composite samples produced using a 3D printer were joined by means of FSSW. Five different tool rotational speeds (900, 1200, 1500, 1800, and 2100 rpm) and three different plunge rates (10, 20, and 30 mm/min) were employed during the welding process. Mechanical tests were performed on the welded joints to investigate the relationship between the welding parameters and the resulting mechanical properties. In addition, microstructural analyses were conducted to examine the formation of welding defects. The results revealed that three distinct zones were formed in the material after the FSSW process: the stir zone, mixed zone, and shoulder zone. Defects were observed in the mixed zone of the samples exhibiting relatively lower mechanical properties. The highest tensile force was achieved at a plunge rate of 20 mm/min and a rotational speed of 900 rpm. The highest bending force, on the other hand, was obtained at a plunge rate of 30 mm/min and a tool rotational speed of 2100 rpm. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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20 pages, 2217 KB  
Article
Assessing Climate Benefits and Circularity of Using Glass Waste in Concrete and New Glass Production
by Madumita Sadagopan, Abdinasir Kadawo, Habib Loubani, Nada Al-Hellali, Nitin Harale and Agnes Nagy
Materials 2026, 19(9), 1750; https://doi.org/10.3390/ma19091750 (registering DOI) - 24 Apr 2026
Abstract
Flat glass waste from building demolition is an underused resource with potential to reduce the climate impact of construction materials. This study compares two recycling pathways for flat glass waste: the first is closed-loop recycling into new glass, and the second is the [...] Read more.
Flat glass waste from building demolition is an underused resource with potential to reduce the climate impact of construction materials. This study compares two recycling pathways for flat glass waste: the first is closed-loop recycling into new glass, and the second is the use of glass in concrete as a replacement for cement. The comparison is based on life cycle, circularity assessment and experimental evaluation of concrete performance. Recycling flat glass into new glass can reduce emissions by 945 kg CO2eq per ton of recycled glass when the production mix contains 65 percent recycled content. However, only between 1 and 3% percent of demolition flat glass is suitable for this process because of contamination and quality limitations. As a result, the practical climate benefit of demolition glass in new glass production is limited to about 38 kg CO2eq per ton of demolition glass. Concrete offers a much larger waste sink. Replacing 20% of cement with milled glass powder results in emission savings of 776 kg CO2eq per ton of glass. A concrete mix containing 33% glass shows the same compressive strength as a reference mix. Full article
(This article belongs to the Special Issue Life-Cycle Assessment of Sustainable Concrete)
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19 pages, 3061 KB  
Article
Design and Manufacturing of Artificial Composite Stone Using Waste Limestone and Glass-Based Reinforcements
by Şükrü Çetinkaya
Polymers 2026, 18(9), 1040; https://doi.org/10.3390/polym18091040 - 24 Apr 2026
Abstract
Artificial composite stones have recently attracted attention as multifunctional materials for construction and defense-related applications. In this study, a novel composite stone was developed using waste limestone as the primary mineral filler, combined with an unsaturated polyester resin matrix and reinforced with glass [...] Read more.
Artificial composite stones have recently attracted attention as multifunctional materials for construction and defense-related applications. In this study, a novel composite stone was developed using waste limestone as the primary mineral filler, combined with an unsaturated polyester resin matrix and reinforced with glass powder and chopped glass fibers. The influence of binder content and reinforcement type on physico-mechanical and microstructural behavior was investigated. Experimental characterization included water absorption, compressive strength, abrasion resistance, acid resistance, and optical microscopy. The results demonstrated that fine fillers improved matrix densification and reduced porosity, while short glass fiber reinforcement enhanced load-bearing capacity. Abrasion resistance and durability were found to depend on binder content and particle packing characteristics. Overall, the developed composite material exhibits promising mechanical performance, low water absorption, and improved durability, suggesting its potential as a candidate material for applications requiring environmental resistance, including potential use in defense-related camouflage applications. Full article
(This article belongs to the Special Issue Application of Polymers in Cementitious Materials)
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14 pages, 3746 KB  
Article
Percolation-Driven NO2 Sensing in Structurally Tuned Sn/SnO Nanoparticles at Room Temperature with Parts-per-Billion Sensitivity
by Wilfredo Otaño, Adrian Camacho, Wilanyi Alvarez, Wanda Rivera, Francisco Bezares, Danilo Barrionuevo and Victor M. Pantojas
Sensors 2026, 26(9), 2651; https://doi.org/10.3390/s26092651 - 24 Apr 2026
Abstract
Monitoring air quality is crucial for understanding and improving public health. There is interest in developing ultra-sensitive, low-power, cost-effective sensors. This work demonstrates that structural modulation of Sn nanoparticles through controlled deposition and oxidation enables a transition from metallic to semiconducting percolative networks, [...] Read more.
Monitoring air quality is crucial for understanding and improving public health. There is interest in developing ultra-sensitive, low-power, cost-effective sensors. This work demonstrates that structural modulation of Sn nanoparticles through controlled deposition and oxidation enables a transition from metallic to semiconducting percolative networks, significantly enhancing NO2 sensing performance at room temperature. The proposed percolation-driven sensing mechanism provides a new framework for understanding charge transport and gas interaction in nanostructured metal oxide systems. The nanoparticles are deposited near the percolation threshold for electrical conduction and, upon exposure to air, consist of a tin core and an amorphous Sn3O4 surface. Post-deposition heating in air at 320 °C for two hours forms SnO and Sn3O4 on top of the gold electrodes and polycrystalline SnO in the tetragonal litharge phase, known as Romarchite, on the glass between the electrodes. Both as-deposited and heat-treated sensors were capable of detecting NO2 at room temperature, with a limit of detection in the parts-per-billion range. A percolation model is used to explain their operating currents, in which NO2 reacts at nanoparticle gaps and intra-grain boundaries to form charge-depletion regions that primarily determine their resistance. Heat treatment has also been found to cause disproportionation of SnO, resulting in tin-rich precipitates and increasing the operating current to the milliampere range. These precipitates, although oxidized on their surfaces when exposed to air, may serve as bridges that reduce the total resistance of the percolating paths. Full article
(This article belongs to the Special Issue Nano/Micro-Structured Materials for Gas Sensor)
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12 pages, 2592 KB  
Article
Cerium-Doped ZnO Thin Films for Photocatalysts
by Pavlina Bancheva-Koleva, Stephan Kozhukharov, Christian Girginov, Ivo Banchev, Plamen Petkov, Tamara Petkova and Georgi Avdeev
Materials 2026, 19(9), 1739; https://doi.org/10.3390/ma19091739 - 24 Apr 2026
Abstract
In this work, Ce-doped ZnO thin films at various contents of cerium were deposited on glass substrates by thermal vacuum evaporation to study the influence of Ce concentration on their optical, structural, morphological, and photocatalytic behavior. Pure ZnO and Ce-doped ZnO films doped [...] Read more.
In this work, Ce-doped ZnO thin films at various contents of cerium were deposited on glass substrates by thermal vacuum evaporation to study the influence of Ce concentration on their optical, structural, morphological, and photocatalytic behavior. Pure ZnO and Ce-doped ZnO films doped with 2% and 5% Ce were characterized by SEM, XRD, AFM, UV–VIS spectroscopy, and ellipsometry. The XRD analysis confirmed that all the films retained the hexagonal wurtzite structure, while Ce incorporation induced lattice strain and reduced crystallite size, particularly at higher doping levels. SEM and AFM studies showed that films with 2% Ce exhibited smaller grain size and lower roughness, whereas 5% Ce-doped films showed grain growth and increased roughness. Pure ZnO films displayed high transparency (>90%), whereas Ce incorporation caused a red shift in the absorption edge and narrowing of the optical band gap due to defect-related states and lattice distortion. Photocatalytic experiments revealed that Ce doping improved charge carrier separation and increased the number of oxygen vacancies. Among all samples, the 2% Ce-doped ZnO film demonstrated the highest photocatalytic efficiency. These findings highlight the importance of controlled Ce doping in tuning the microstructure, optical properties, and photocatalytic performance of ZnO thin films, making them suitable for environmental remediation and optoelectronic applications. Full article
20 pages, 5623 KB  
Article
Synergistic Effects of Bioactive Glass on the Physicochemical Properties and In Vitro Bioactivity of 3D-Printed PCL Scaffolds
by Bo Yang, Runhua Wang, Guang Yang, Zejia Zhang and Xiaohong Chen
Materials 2026, 19(9), 1740; https://doi.org/10.3390/ma19091740 - 24 Apr 2026
Abstract
Polycaprolactone (PCL) is widely utilized in bone tissue engineering due to its excellent biocompatibility and processability; however, its inherent bioinertness and hydrophobicity significantly restrict its clinical osteogenic efficacy. To overcome these limitations, we incorporated sol–gel synthesized silicate-based bioactive glass (BG) into a PCL [...] Read more.
Polycaprolactone (PCL) is widely utilized in bone tissue engineering due to its excellent biocompatibility and processability; however, its inherent bioinertness and hydrophobicity significantly restrict its clinical osteogenic efficacy. To overcome these limitations, we incorporated sol–gel synthesized silicate-based bioactive glass (BG) into a PCL matrix and fabricated a series of composite scaffolds with varying BG contents via direct ink writing (DIW) 3D printing. Rheological characterization confirmed that all ink formulations exhibited shear-thinning behavior, with viscosity increasing monotonically with BG content. DSC analysis revealed that BG incorporation progressively reduced the crystallinity of PCL from 51.47% to 36.23%. We systematically evaluated the physicochemical properties, mechanical resilience, and in vitro degradation behavior of these scaffolds. The results indicated that BG incorporation significantly improved the surface hydrophilicity, with the contact angle decreasing from 104.8 ± 2.81° to 69.8 ± 2.91°. Furthermore, as the BG content increased, the porosity and mechanical strength exhibited an initial increase followed by a subsequent decrease, yet all values remained within the range of human cancellous bone. Notably, cellular assays revealed that the introduction of 58SBG enhanced cell–matrix interactions; the PCL/BG scaffolds promoted superior cell attachment and more extensive morphological spreading compared to pure PCL. Among all groups, the PCL/30BG composite scaffold demonstrated the most optimal balance of mechanical integrity and biological response. Consequently, the PCL/30BG scaffold developed in this study exhibits immense potential as a bone graft substitute, providing a promising approach for clinical bone defect repair strategies. Full article
(This article belongs to the Section Advanced Composites)
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25 pages, 5717 KB  
Article
An End-to-End Foundation Model-Based Framework for Robust LAI Retrieval Under Cloud Cover
by Xiangfeng Gu, Wenyuan Li and Shikang Guan
Remote Sens. 2026, 18(9), 1308; https://doi.org/10.3390/rs18091308 - 24 Apr 2026
Abstract
Leaf Area Index is a crucial biophysical variable, and its accurate estimation is essential for understanding vegetation dynamics. However, cloud cover significantly restricts optical remote sensing, hindering the generation of spatially continuous Leaf Area Index products. Remote sensing foundation models offer novel solutions [...] Read more.
Leaf Area Index is a crucial biophysical variable, and its accurate estimation is essential for understanding vegetation dynamics. However, cloud cover significantly restricts optical remote sensing, hindering the generation of spatially continuous Leaf Area Index products. Remote sensing foundation models offer novel solutions to this challenge. This study presents an end-to-end framework based on the fine-tuned Prithvi foundation model for direct LAI retrieval from cloud-contaminated 30 m Harmonized Landsat and Sentinel-2 imagery. By mapping inputs directly to Hi-GLASS reference labels, the proposed architecture processes cloud contamination and vegetation signals simultaneously and circumvents the error propagation inherent in cascaded retrieval pipelines. Results demonstrate that the end-to-end LAI retrieval model significantly outperforms cascaded variants, achieving a superior R2 (0.78) and lower RMSE (0.57). Furthermore, predictive accuracy exhibits a distinct U-shaped trajectory relative to the temporal mean cloud fraction, reaching an inflection point at 50–60% occlusion, which highlights the model’s implicit regularization capacity under severe atmospheric interference. This work establishes that direct feature learning with foundation models offers a more robust and streamlined pathway for generating continuous biophysical products from imperfect optical observations, prioritizing quantitative fidelity over artificial perceptual sharpness. Full article
(This article belongs to the Section Remote Sensing in Agriculture and Vegetation)
15 pages, 3175 KB  
Article
Comparative Study on Injection Molding and Performance of Glass Fiber-Reinforced PET and PA6 Thermoplastic Insulators
by Yao Wang, Yuliang Fu, Xiaofei Chen, Zehao Zhang and Weiqi Qin
Materials 2026, 19(9), 1729; https://doi.org/10.3390/ma19091729 - 24 Apr 2026
Abstract
In ultra-high-voltage GIS and GIL systems, epoxy resin insulators are still the mainstream choice. However, as a thermosetting material, epoxy resin is difficult to recycle after disposal, which limits its environmental benefits. Thermoplastic insulators, due to their recyclability, are potential alternatives. This study [...] Read more.
In ultra-high-voltage GIS and GIL systems, epoxy resin insulators are still the mainstream choice. However, as a thermosetting material, epoxy resin is difficult to recycle after disposal, which limits its environmental benefits. Thermoplastic insulators, due to their recyclability, are potential alternatives. This study focuses on 30% glass fiber-reinforced PET and PA6 materials. Their injection molding behavior, hydraulic pressure performance, and insulation performance were systematically analyzed using Moldflow, ANSYS, and COMSOL, respectively. For injection molding, Moldflow simulations were conducted for filling, packing, and cooling stages. Melt temperature was varied from 260 to –310 °C (PET) and 250–300 °C (PA6), while mold temperature was varied from 80 to –130 °C (PET) and 70–120 °C (PA6). An optimization objective function, Y = Δp/20 + Δx/0.5 + Δs/1.8, was developed to determine optimal processing parameters. Based on this function, the optimal parameters identified are: PET at 290 °C melt temperature and 120 °C mold temperature; PA6 at 250 °C melt temperature and 70 °C mold temperature. For hydraulic testing, Moldflow–ANSYS coupled simulations were performed under 2.4 MPa pressure with the compliance criteria of bulk stress < 90 MPa and insert-contact stress < 20 MPa. PA6 passed within a processing window of melt temperature < 270 °C and mold temperature < 120 °C. PET failed under all tested conditions, with insert-contact stress ranging from 24.25 to 27.55 MPa, consistently exceeding the 20 MPa threshold. In terms of insulation performance, this paper utilizes COMSOL to study the electric field distribution of thermoplastic insulators in SF6 GIS/GIL and provides optimization suggestions for insulator geometry design. This study systematically compares the injection molding processes and hydraulic pressure performance of PET and PA6 thermoplastic insulators. These results provide important process insights and design guidance for evaluating thermoplastic materials as potential alternatives to epoxy resin in GIS/GIL applications. Full article
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11 pages, 4795 KB  
Article
Microhardness Recovery and Micromorphology of Demineralized Dentin Restored with Modified Glass Hybrid Material
by Ivan Šalinović, Maja Bilić-Prcić, Maria Bota, Anja Ivica and Ivana Miletić
Materials 2026, 19(9), 1733; https://doi.org/10.3390/ma19091733 - 24 Apr 2026
Abstract
This study evaluated how the addition of 5 wt% bioactive glass and 15 wt% short glass fibers to EQUIA Forte HT affects the microhardness, micromorphology, and elemental composition of demineralized dentin. Class I cavities in 28 human third molars were demineralized with 37% [...] Read more.
This study evaluated how the addition of 5 wt% bioactive glass and 15 wt% short glass fibers to EQUIA Forte HT affects the microhardness, micromorphology, and elemental composition of demineralized dentin. Class I cavities in 28 human third molars were demineralized with 37% phosphoric acid and restored with: (1) Filtek Universal composite, (2) EQUIA Forte HT, (3) EQUIA Forte HT + 5wt% BAG, or (4) EQUIA Forte HT + 15wt% short glass fibers. After 4 weeks of storage in phosphate-buffered saline at 37 °C, the teeth were cut in half, obtaining two samples from each tooth (n = 14). Vickers microhardness (HV0.1) was measured on demineralized dentin 50–100 μm apical to the restoration interface. Representative specimens (n = 2) were examined using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). Data were analyzed with one-way ANOVA (α = 0.05). Unmodified EQUIA Forte HT showed the highest mean dentin microhardness recovery (25.06 ± 1.42 HV0.1), followed by composite (17.31 ± 0.66 HV0.1), BAG-modified (23.74 ± 1.37 HV0.1) and fiber-reinforced (22.15 ± 1.06 HV0.1) groups (p < 0.001, all pairwise comparisons p ≤ 0.039). Glass hybrids showed prominent Ca/P peaks; modified groups had elevated Si (BAG) and Al (fibers). SEM revealed smoother surfaces with fewer cracks in modified materials. Unmodified EQUIA Forte HT produced the highest short-term microhardness recovery, while BAG and fiber additions altered surface morphology and elemental composition but slightly reduced early hardness. Full article
(This article belongs to the Section Biomaterials)
30 pages, 1113 KB  
Article
Influence of Combined Waste-Based Materials on Fine-Grained Concrete Properties
by Giedrius Girskas, Modestas Kligys and Jurgita Malaiškienė
Processes 2026, 14(9), 1364; https://doi.org/10.3390/pr14091364 - 24 Apr 2026
Abstract
This study investigates the influence of waste-based materials, namely drinking water treatment sludge (DWTS) and expanded glass production waste (EGPW), on the properties of fine-grained concrete when used as partial Portland cement replacements. Fine-grained concrete mixtures containing different proportions of DWTS and EGPW [...] Read more.
This study investigates the influence of waste-based materials, namely drinking water treatment sludge (DWTS) and expanded glass production waste (EGPW), on the properties of fine-grained concrete when used as partial Portland cement replacements. Fine-grained concrete mixtures containing different proportions of DWTS and EGPW were evaluated in terms of hydration behavior, microstructural development, mechanical performance, durability, and dimensional stability. Density, ultrasonic pulse velocity, water absorption, flexural and compressive strengths, drying shrinkage, and porosity parameters were determined, while frost resistance was assessed and predicted based on porosity characteristics. Hydration kinetics were analyzed using X-ray diffraction and semi-adiabatic calorimetry. The results showed that increasing EGPW content enhanced cement hydration processes and promoted matrix densification through pozzolanic reactions, resulting in reduced water absorption and improved mechanical properties. In contrast, DWTS exhibited an inhibiting effect on hydration due to its inert nature and high Fe2O3 content, acting primarily as a micro-filler; however, when combined with EGPW at moderate dosages, DWTS contributed positively to flexural strength and slightly reduced drying shrinkage. The combined use of DWTS and EGPW enabled the formation of a balanced pore structure and improved the durability of fine-grained concrete. Among the tested mixtures, ED-3 (7.5% EGPW + 5% DWTS) provided the most favorable balance between hydration activation and binder reduction, while the highest frost resistance was achieved by the ED-4 mixture, reaching approximately 603 predicted freeze–thaw cycles. Overall, the results indicate that properly optimized combinations of EGPW and DWTS can significantly enhance the performance and durability of fine-grained concrete while controlling drying shrinkage. Full article
(This article belongs to the Special Issue Recycling and Value-Added Utilization of Secondary Resources)
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