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Keywords = durable characteristics

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38 pages, 15791 KiB  
Article
Experimental and Statistical Evaluations of Recycled Waste Materials and Polyester Fibers in Enhancing Asphalt Concrete Performance
by Sara Laib, Zahreddine Nafa, Abdelghani Merdas, Yazid Chetbani, Bassam A. Tayeh and Yunchao Tang
Buildings 2025, 15(15), 2747; https://doi.org/10.3390/buildings15152747 - 4 Aug 2025
Abstract
This research aimed to evaluate the impact of using brick waste powder (BWP) and varying lengths of polyester fibers (PFs) on the performance properties of asphalt concrete (AC) mixtures. BWP was utilized as a replacement for traditional limestone powder (LS) filler, while PFs [...] Read more.
This research aimed to evaluate the impact of using brick waste powder (BWP) and varying lengths of polyester fibers (PFs) on the performance properties of asphalt concrete (AC) mixtures. BWP was utilized as a replacement for traditional limestone powder (LS) filler, while PFs of three lengths (3 mm, 8 mm, and 15 mm) were introduced. The study employed the response surface methodology (RSM) for experimental design and analysis of variance (ANOVA) to identify the influence of BWP and PF on the selected performance indicators. These indicators included bulk density, air voids, voids in the mineral aggregate, voids filled with asphalt, Marshall stability, Marshall flow, Marshall quotient, indirect tensile strength, wet tensile strength, and the tensile strength ratio. The findings demonstrated that BWP improved moisture resistance and the mechanical performance of AC mixes. Moreover, incorporating PF alongside BWP further enhanced these properties, resulting in superior overall performance. Using multi-objective optimization through RSM-based empirical models, the study identified the optimal PF length of 5 mm in combination with BWP for achieving the best AC properties. Validation experiments confirmed the accuracy of the predicted results, with an error margin of less than 8%. The study emphasizes the intriguing prospect of BWP and PF as sustainable alternatives for improving the durability, mechanical characteristics, and cost-efficiency of asphalt pavements. Full article
(This article belongs to the Special Issue Advanced Studies in Asphalt Mixtures)
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18 pages, 914 KiB  
Review
Advances in Surgical Management of Malignant Gastric Outlet Obstruction
by Sang-Ho Jeong, Miyeong Park, Kyung Won Seo and Jae-Seok Min
Cancers 2025, 17(15), 2567; https://doi.org/10.3390/cancers17152567 - 4 Aug 2025
Abstract
Malignant gastric outlet obstruction (MGOO) is a serious complication arising from advanced gastric or pancreatic head cancer, significantly impairing patients’ quality of life by disrupting oral intake and inducing severe gastrointestinal symptoms. With benign causes such as peptic ulcer disease on the decline, [...] Read more.
Malignant gastric outlet obstruction (MGOO) is a serious complication arising from advanced gastric or pancreatic head cancer, significantly impairing patients’ quality of life by disrupting oral intake and inducing severe gastrointestinal symptoms. With benign causes such as peptic ulcer disease on the decline, malignancies now account for 50–80% of gastric outlet obstruction (GOO) cases globally. This review outlines the pathophysiology, evolving epidemiology, and treatment modalities for MGOO. Therapeutic approaches include conservative management, endoscopic stenting, surgical gastrojejunostomy (GJ), stomach partitioning gastrojejunostomy (SPGJ), and endoscopic ultrasound-guided gastroenterostomy (EUS-GE). While endoscopic stenting offers rapid symptom relief with minimal invasiveness, it has higher rates of re-obstruction. Surgical options like GJ and SPGJ provide more durable palliation, especially for patients with longer expected survival. SPGJ, a modified surgical technique, demonstrates reduced incidence of delayed gastric emptying and may improve postoperative oral intake and survival compared to conventional GJ. EUS-GE represents a promising, minimally invasive alternative that combines surgical durability with endoscopic efficiency, although long-term data remain limited. Treatment selection should consider patient performance status, tumor characteristics, prognosis, and institutional resources. This comprehensive review underscores the need for individualized, multidisciplinary decision-making to optimize symptom relief, nutritional status, and overall outcomes in patients with MGOO. Full article
(This article belongs to the Special Issue Advances in the Treatment of Upper Gastrointestinal Cancer)
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23 pages, 9258 KiB  
Article
Uniaxial Mechanical Behavior and Constitutive Modeling of Early-Age Steel Fiber-Reinforced Concrete Under Variable-Temperature Curing Conditions
by Yongkang Xu, Quanmin Xie, Hui Zhou, Yongsheng Jia, Zhibin Zheng and Chong Pan
Materials 2025, 18(15), 3642; https://doi.org/10.3390/ma18153642 (registering DOI) - 2 Aug 2025
Viewed by 55
Abstract
In high geothermal tunnels (>28 °C), curing temperature critically affects early-age concrete mechanics and durability. Uniaxial compression tests under six curing conditions, combined with CT scanning and machine learning-based crack analysis, were used to evaluate the impacts of curing age, temperature, and fiber [...] Read more.
In high geothermal tunnels (>28 °C), curing temperature critically affects early-age concrete mechanics and durability. Uniaxial compression tests under six curing conditions, combined with CT scanning and machine learning-based crack analysis, were used to evaluate the impacts of curing age, temperature, and fiber content. The test results indicate that concrete exhibits optimal development of mechanical properties under ambient temperature conditions. Specifically, the elastic modulus increased by 33.85% with age in the room-temperature group (RT), by 23.35% in the fiber group (F), and decreased by 26.75% in the varying-temperature group (VT). A Weibull statistical damage-based constitutive model aligned strongly with the experimental data (R2 > 0.99). Fractal analysis of CT-derived cracks revealed clear fractal characteristics in the log(Nr)–log(r) curves, demonstrating internal damage mechanisms under different thermal histories. Full article
(This article belongs to the Section Construction and Building Materials)
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15 pages, 3579 KiB  
Article
Dual-Control-Gate Reconfigurable Ion-Sensitive Field-Effect Transistor with Nickel-Silicide Contacts for Adaptive and High-Sensitivity Chemical Sensing Beyond the Nernst Limit
by Seung-Jin Lee, Seung-Hyun Lee, Seung-Hwa Choi and Won-Ju Cho
Chemosensors 2025, 13(8), 281; https://doi.org/10.3390/chemosensors13080281 - 2 Aug 2025
Viewed by 48
Abstract
In this study, we propose a bidirectional chemical sensor platform based on a reconfigurable ion-sensitive field-effect transistor (R-ISFET) architecture. The device incorporates Ni-silicide Schottky barrier source/drain (S/D) contacts, enabling ambipolar conduction and bidirectional turn-on behavior for both p-type and n-type configurations. Channel polarity [...] Read more.
In this study, we propose a bidirectional chemical sensor platform based on a reconfigurable ion-sensitive field-effect transistor (R-ISFET) architecture. The device incorporates Ni-silicide Schottky barrier source/drain (S/D) contacts, enabling ambipolar conduction and bidirectional turn-on behavior for both p-type and n-type configurations. Channel polarity is dynamically controlled via the program gate (PG), while the control gate (CG) suppresses leakage current, enhancing operational stability and energy efficiency. A dual-control-gate (DCG) structure enhances capacitive coupling, enabling sensitivity beyond the Nernst limit without external amplification. The extended-gate (EG) architecture physically separates the transistor and sensing regions, improving durability and long-term reliability. Electrical characteristics were evaluated through transfer and output curves, and carrier transport mechanisms were analyzed using band diagrams. Sensor performance—including sensitivity, hysteresis, and drift—was assessed under various pH conditions and external noise up to 5 Vpp (i.e., peak-to-peak voltage). The n-type configuration exhibited high mobility and fast response, while the p-type configuration demonstrated excellent noise immunity and low drift. Both modes showed consistent sensitivity trends, confirming the feasibility of complementary sensing. These results indicate that the proposed R-ISFET sensor enables selective mode switching for high sensitivity and robust operation, offering strong potential for next-generation biosensing and chemical detection. Full article
(This article belongs to the Section Electrochemical Devices and Sensors)
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20 pages, 10391 KiB  
Article
Sustainable Substitution of Petroleum-Based Processing Oils with Soybean-Derived Alternatives in Styrene–Butadiene Rubber: Effects on Processing Behavior and Mechanical Properties
by Yang-Wei Lin, Tsung-Yi Chen, Chen-Yu Chueh, Yi-Ting Chen, Tsunghsueh Wu and Hsi-Ming Hsieh
Polymers 2025, 17(15), 2129; https://doi.org/10.3390/polym17152129 - 1 Aug 2025
Viewed by 204
Abstract
This study evaluates the replacement of petroleum-based naphthenic oil with four types of soybean-derived alternatives—virgin soybean oil (SBO), epoxidized SBO (ESBO), expired SBO, and recycled SBO—in styrene–butadiene rubber (SBR) composites. The materials were tested in both staining rubber (SR) and non-staining rubber (NSR) [...] Read more.
This study evaluates the replacement of petroleum-based naphthenic oil with four types of soybean-derived alternatives—virgin soybean oil (SBO), epoxidized SBO (ESBO), expired SBO, and recycled SBO—in styrene–butadiene rubber (SBR) composites. The materials were tested in both staining rubber (SR) and non-staining rubber (NSR) systems to assess processing characteristics, mechanical performance, and environmental durability. Among the alternatives, SBO demonstrated the best overall performance, improving processability and tensile strength by over 10%, while ESBO enhanced ozone resistance by 35% due to its epoxide functionality. Expired and recycled SBOs maintained essential mechanical properties within 90% of virgin SBO values. The full replacement of CH450 with SBO in tire prototypes resulted in burst strength exceeding 1000 kPa and stable appearance after 5000 km of road testing. To validate industrial relevance, the developed green tire was exhibited at the 2025 Taipei International Cycle Show, attracting interest from international buyers and stakeholders for its eco-friendly composition and carbon footprint reduction potential, thereby demonstrating both technical feasibility and commercial viability. Full article
(This article belongs to the Special Issue Functional Polymers and Their Composites for Sustainable Development)
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23 pages, 4322 KiB  
Article
Fly-Ash-Based Microbial Self-Healing Cement: A Sustainable Solution for Oil Well Integrity
by Lixia Li, Yanjiang Yu, Qianyong Liang, Tianle Liu, Guosheng Jiang, Guokun Yang and Chengxiang Tang
Sustainability 2025, 17(15), 6989; https://doi.org/10.3390/su17156989 (registering DOI) - 1 Aug 2025
Viewed by 157
Abstract
The cement sheath is critical for ensuring the long-term safety and operational efficiency of oil and gas wells. However, complex geological conditions and operational stresses during production can induce cement sheath deterioration and cracking, leading to reduced zonal isolation, diminished hydrocarbon recovery, and [...] Read more.
The cement sheath is critical for ensuring the long-term safety and operational efficiency of oil and gas wells. However, complex geological conditions and operational stresses during production can induce cement sheath deterioration and cracking, leading to reduced zonal isolation, diminished hydrocarbon recovery, and elevated operational expenditures. This study investigates the development of a novel microbial self-healing well cement slurry system, employing fly ash as microbial carriers and sustained-release microcapsules encapsulating calcium sources and nutrients. Systematic evaluations were conducted, encompassing microbial viability, cement slurry rheology, fluid loss control, anti-channeling capability, and the mechanical strength, permeability, and microstructural characteristics of set cement stones. Results demonstrated that fly ash outperformed blast furnace slag and nano-silica as a carrier, exhibiting superior microbial loading capacity and viability. Optimal performance was observed with additions of 3% microorganisms and 3% microcapsules to the cement slurry. Microscopic analysis further revealed effective calcium carbonate precipitation within and around micro-pores, indicating a self-healing mechanism. These findings highlight the significant potential of the proposed system to enhance cement sheath integrity through localized self-healing, offering valuable insights for the development of advanced, durable well-cementing materials tailored for challenging downhole environments. Full article
(This article belongs to the Section Environmental Sustainability and Applications)
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13 pages, 3341 KiB  
Article
Regulation of Electrochemical Activity via Controlled Integration of NiS2 over Co3O4 Nanomaterials for Hydrogen Evolution Reaction
by Mrunal Bhosale, Rutuja U. Amate, Pritam J. Morankar and Chan-Wook Jeon
Coatings 2025, 15(8), 887; https://doi.org/10.3390/coatings15080887 - 30 Jul 2025
Viewed by 181
Abstract
Electrochemical water splitting represents a sustainable approach for hydrogen production, yet efficient hydrogen evolution reaction (HER) catalysts operating in alkaline environments remain critically needed. Herein, we report the fabrication of Co3O4–NiS2 nanocomposites synthesized through a facile coprecipitation and [...] Read more.
Electrochemical water splitting represents a sustainable approach for hydrogen production, yet efficient hydrogen evolution reaction (HER) catalysts operating in alkaline environments remain critically needed. Herein, we report the fabrication of Co3O4–NiS2 nanocomposites synthesized through a facile coprecipitation and subsequent thermal treatment method. Detailed characterization via physicochemical techniques confirmed the successful formation of a hybrid Co3O4–NiS2 heterostructure with tunable compositional and morphological characteristics. Among the synthesized catalysts (Co–Ni–1, Co–Ni–2, and Co–Ni–3), the Co–Ni–2 sample demonstrated optimal structural integration, displaying interconnected nanosheet morphologies and balanced elemental distribution. Remarkably, Co–Ni–2 achieved exceptional HER performance in 1 M KOH electrolyte, requiring an ultralow overpotential of only 84 mV at 10 mA cm−2 and exhibiting a favorable Tafel slope of 67.5 mV dec−1. Electrochemical impedance spectroscopy and electrochemical surface area measurements further substantiated the superior electrocatalytic kinetics, rapid charge transport, and abundant active site accessibility in the optimized Co–Ni–2 composite. Additionally, Co–Ni–2 demonstrated outstanding durability with negligible activity decay over 5000 cycles. This study not only highlights the strategic synthesis of Co3O4–NiS2 nanostructures but also provides valuable insights for designing advanced, stable, and efficient non-noble electrocatalysts for sustainable hydrogen generation. Full article
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28 pages, 6625 KiB  
Article
Short- and Long-Term Mechanical and Durability Performance of Concrete with Copper Slag and Recycled Coarse Aggregate Under Magnesium Sulfate Attack
by Yimmy Fernando Silva, Claudia Burbano-Garcia, Eduardo J. Rueda, Arturo Reyes-Román and Gerardo Araya-Letelier
Appl. Sci. 2025, 15(15), 8329; https://doi.org/10.3390/app15158329 (registering DOI) - 26 Jul 2025
Viewed by 244
Abstract
Sustainability in the construction sector has become a fundamental objective for mitigating escalating environmental challenges; given that concrete is the most widely used man-made material, extending its service life is therefore critical. Among durability concerns, magnesium sulfate (MgSO4) attack is particularly [...] Read more.
Sustainability in the construction sector has become a fundamental objective for mitigating escalating environmental challenges; given that concrete is the most widely used man-made material, extending its service life is therefore critical. Among durability concerns, magnesium sulfate (MgSO4) attack is particularly deleterious to concrete structures. Therefore, this study investigates the short- and long-term performance of concrete produced with copper slag (CS)—a massive waste generated by copper mining activities worldwide—employed as a supplementary cementitious material (SCM), together with recycled coarse aggregate (RCA), obtained from concrete construction and demolition waste, when exposed to MgSO4. CS was used as a 15 vol% cement replacement, while RCA was incorporated at 0%, 20%, 50%, and 100 vol%. Compressive strength, bulk density, water absorption, and porosity were measured after water curing (7–388 days) and following immersion in a 5 wt.% MgSO4 solution for 180 and 360 days. Microstructural characteristics were assessed using scanning electron microscopy (SEM), X-ray diffraction (XRD), thermogravimetric analysis with its differential thermogravimetric derivative (TG-DTG), and Fourier transform infrared spectroscopy (FTIR) techniques. The results indicated that replacing 15% cement with CS reduced 7-day strength by ≤10%, yet parity with the reference mix was reached at 90 days. Strength losses increased monotonically with RCA content. Under MgSO4 exposure, all mixtures experienced an initial compressive strength gain during the short-term exposures (28–100 days), attributed to the pore-filling effect of expansive sulfate phases. However, at long-term exposure (180–360 days), a clear strength decline was observed, mainly due to internal cracking, brucite formation, and the transformation of C–S–H into non-cementitious M–S–H gel. Based on these findings, the combined use of CS and RCA at low replacement levels shows potential for producing environmentally friendly concrete with mechanical and durability performance comparable to those of concrete made entirely with virgin materials. Full article
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17 pages, 2815 KiB  
Article
Research on the Structural Design and Mechanical Properties of T800 Carbon Fiber Composite Materials in Flapping Wings
by Ruojun Wang, Zengyan Jiang, Yuan Zhang, Luyao Fan and Weilong Yin
Materials 2025, 18(15), 3474; https://doi.org/10.3390/ma18153474 - 24 Jul 2025
Viewed by 246
Abstract
Due to its superior maneuverability and concealment, the micro flapping-wing aircraft has great application prospects in both military and civilian fields. However, the development and optimization of lightweight materials have always been the key factors limiting performance enhancement. This paper designs the flapping [...] Read more.
Due to its superior maneuverability and concealment, the micro flapping-wing aircraft has great application prospects in both military and civilian fields. However, the development and optimization of lightweight materials have always been the key factors limiting performance enhancement. This paper designs the flapping mechanism of a single-degree-of-freedom miniature flapping wing aircraft. In this study, T800 carbon fiber composite material was used as the frame material. Three typical wing membrane materials, namely polyethylene terephthalate (PET), polyimide (PI), and non-woven kite fabric, were selected for comparative analysis. Three flapping wing configurations with different stiffness were proposed. These wings adopted carbon fiber composite material frames. The wing membrane material is bonded to the frame through a coating. Inspired by bionics, a flapping wing that mimics the membrane vein structure of insect wings is designed. By changing the type of membrane material and the distribution of carbon fiber composite materials on the wing, the stiffness of the flapping wing can be controlled, thereby affecting the mechanical properties of the flapping wing aircraft. The modal analysis of the flapping-wing structure was conducted using the finite element analysis method, and the experimental prototype was fabricated by using 3D printing technology. To evaluate the influence of different wing membrane materials on lift performance, a high-precision force measurement experimental platform was built, systematic tests were carried out, and the lift characteristics under different flapping frequencies were analyzed. Through computational modeling and experiments, it has been proven that under the same flapping wing frequency, the T800 carbon fiber composite material frame can significantly improve the stiffness and durability of the flapping wing. In addition, the selection of wing membrane materials has a significant impact on lift performance. Among the test materials, the PET wing film demonstrated excellent stability and lift performance under high-frequency conditions. This research provides crucial experimental evidence for the optimal selection of wing membrane materials for micro flapping-wing aircraft, verifies the application potential of T800 carbon fiber composite materials in micro flapping-wing aircraft, and opens up new avenues for the application of advanced composite materials in high-performance micro flapping-wing aircraft. Full article
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27 pages, 7191 KiB  
Review
Advances in Nano-Reinforced Polymer-Modified Cement Composites: Synergy, Mechanisms, and Properties
by Yibo Gao, Jianlin Luo, Jie Zhang, Muhammad Asad Ejaz and Liguang Liu
Buildings 2025, 15(15), 2598; https://doi.org/10.3390/buildings15152598 - 23 Jul 2025
Viewed by 216
Abstract
Organic polymer introduction effectively enhances the toughness, bond strength, and durability of ordinary cement-based materials, and is often used for concrete repair and reinforcement. However, the entrained air effect simultaneously induced by polymer and the inhibitory action on cement hydration kinetics often lead [...] Read more.
Organic polymer introduction effectively enhances the toughness, bond strength, and durability of ordinary cement-based materials, and is often used for concrete repair and reinforcement. However, the entrained air effect simultaneously induced by polymer and the inhibitory action on cement hydration kinetics often lead to degradation in mechanical performances of polymer-modified cement-based composite (PMC). Nanomaterials provide unique advantages in enhancing the properties of PMC due to their characteristic ultrahigh specific surface area, quantum effects, and interface modulation capabilities. This review systematically examines recent advances in nano-reinforced PMC (NPMC), elucidating their synergistic optimization mechanisms. The synergistic effects of nanomaterials—nano-nucleation, pore-filling, and templating mechanisms—refine the microstructure, significantly enhancing the mechanical strength, impermeability, and erosion resistance of NPMC. Furthermore, nanomaterials establish interpenetrating network structures (A composite structure composed of polymer networks and other materials interwoven with each other) with polymer cured film (The film formed after the polymer loses water), enhancing load-transfer efficiency through physical and chemical action while optimizing dispersion and compatibility of nanomaterials and polymers. By systematically analyzing the synergy among nanomaterials, polymer, and cement matrix, this work provides valuable insights for advancing high-performance repair materials. Full article
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19 pages, 3112 KiB  
Article
Durable Superhydrophobic Composite Coating Based on Hydrangea-like SiO2 Nanoparticles with Excellent Performance in Anticorrosion, Drag Reduction, and Antifouling
by Yuhao Xue, Yamei Zhao, Xiaoqi Gu, Mengdan Huo, Kunde Yang, Mingyu Liu, Sixian Fan and Maoyong Zhi
Materials 2025, 18(15), 3443; https://doi.org/10.3390/ma18153443 - 23 Jul 2025
Viewed by 257
Abstract
Superhydrophobic coatings possess distinct wettability characteristics and hold significant potential in metal corrosion protection and underwater drag reduction. However, their practical application is often hindered by poor durability arising from the fragility of their micro/nanostructured surface roughness. In this study, a durable superhydrophobic [...] Read more.
Superhydrophobic coatings possess distinct wettability characteristics and hold significant potential in metal corrosion protection and underwater drag reduction. However, their practical application is often hindered by poor durability arising from the fragility of their micro/nanostructured surface roughness. In this study, a durable superhydrophobic coating featuring a hierarchical, hydrangea-like micro/nanostructure was successfully fabricated on an aluminum alloy substrate via a simple one-step cold-spraying technique. The coating consisted of hydrangea-shaped SiO2 nanoparticles modified with 1H,1H,2H,2H-perfluorodecyltrimethoxysilane (PFDT) to produce multiscale roughness, while epoxy resin (EP) served as the binding matrix to enhance mechanical integrity. The hydrangea-like SiO2 nanostructures were characterized by solid cores and wrinkled, petal-like outgrowths. This unique morphology not only increased the surface roughness but also provided more active sites for air entrapment, thereby enhancing the coating’s overall performance. The h-SiO2@PFDT-EP composite coating exhibited excellent superhydrophobicity, with a WCA of 170.1° ± 0.8° and a SA of 2.7° ± 0.5°. Durability was evaluated through sandpaper abrasion, tape peeling, acid and alkali immersion, artificial weathering, and salt spray tests. The results demonstrated that the coating retained stable superhydrophobic performance under various environmental stresses. Compared with bare 6061 aluminum and EP coatings, its corrosion current density was reduced by four and three orders of magnitude, respectively. Furthermore, the coating achieved a maximum drag-reduction rate of 31.01% within a velocity range of 1.31–7.86 m/s. The coating also displayed excellent self-cleaning properties. Owing to its outstanding durability, corrosion resistance, and drag-reducing capability, this one-step fabricated superhydrophobic coating showed great promise for applications in marine engineering and defense. Full article
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30 pages, 9107 KiB  
Article
Numerical Far-Field Investigation into Guided Waves Interaction at Weak Interfaces in Hybrid Composites
by Saurabh Gupta, Mahmood Haq, Konstantin Cvetkovic and Oleksii Karpenko
J. Compos. Sci. 2025, 9(8), 387; https://doi.org/10.3390/jcs9080387 - 22 Jul 2025
Viewed by 226
Abstract
Modern aerospace engineering places increasing emphasis on materials that combine low weight with high mechanical performance. Fiber metal laminates (FMLs), which merge metal layers with fiber-reinforced composites, meet this demand by delivering improved fatigue resistance, impact tolerance, and environmental durability, often surpassing the [...] Read more.
Modern aerospace engineering places increasing emphasis on materials that combine low weight with high mechanical performance. Fiber metal laminates (FMLs), which merge metal layers with fiber-reinforced composites, meet this demand by delivering improved fatigue resistance, impact tolerance, and environmental durability, often surpassing the performance of their constituents in demanding applications. Despite these advantages, inspecting such thin, layered structures remains a significant challenge, particularly when they are difficult or impossible to access. As with any new invention, they always come with challenges. This study examines the effectiveness of the fundamental anti-symmetric Lamb wave mode (A0) in detecting weak interfacial defects within Carall laminates, a type of hybrid fiber metal laminate (FML). Delamination detectability is analyzed in terms of strong wave dispersion observed downstream of the delaminated sublayer, within a region characterized by acoustic distortion. A three-dimensional finite element (FE) model is developed to simulate mode trapping and full-wavefield local displacement. The approach is validated by reproducing experimental results reported in prior studies, including the author’s own work. Results demonstrate that the A0 mode is sensitive to delamination; however, its lateral resolution depends on local position, ply orientation, and dispersion characteristics. Accurately resolving the depth and extent of delamination remains challenging due to the redistribution of peak amplitude in the frequency domain, likely caused by interference effects in the acoustically sensitive delaminated zone. Additionally, angular scattering analysis reveals a complex wave behavior, with most of the energy concentrated along the centerline, despite transmission losses at the metal-composite interfaces in the Carall laminate. The wave interaction with the leading and trailing edges of the delaminations is strongly influenced by the complex wave interference phenomenon and acoustic mismatched regions, leading to an increase in dispersion at the sublayers. Analytical dispersion calculations clarify how wave behavior influences the detectability and resolution of delaminations, though this resolution is constrained, being most effective for weak interfaces located closer to the surface. This study offers critical insights into how the fundamental anti-symmetric Lamb wave mode (A0) interacts with delaminations in highly attenuative, multilayered environments. It also highlights the challenges in resolving the spatial extent of damage in the long-wavelength limit. The findings support the practical application of A0 Lamb waves for structural health assessment of hybrid composites, enabling defect detection at inaccessible depths. Full article
(This article belongs to the Special Issue Metal Composites, Volume II)
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26 pages, 4303 KiB  
Article
Thermal Degradation and Microstructural Evolution of Geopolymer-Based UHPC with Silica Fume and Quartz Powder
by Raghda A. Elhefny, Mohamed Abdellatief, Walid E. Elemam and Ahmed M. Tahwia
Infrastructures 2025, 10(8), 192; https://doi.org/10.3390/infrastructures10080192 - 22 Jul 2025
Viewed by 212
Abstract
The durability and fire resilience of concrete structures are increasingly critical in modern construction, particularly under elevated-temperature exposure. With this context, the current study explores the thermal and microstructural characteristics of geopolymer-based ultra-high-performance concrete (G-UHPC) incorporating quartz powder (QP) and silica fume (SF) [...] Read more.
The durability and fire resilience of concrete structures are increasingly critical in modern construction, particularly under elevated-temperature exposure. With this context, the current study explores the thermal and microstructural characteristics of geopolymer-based ultra-high-performance concrete (G-UHPC) incorporating quartz powder (QP) and silica fume (SF) after exposure to elevated temperatures. SF was used at 15% and 30% to partially replace the precursor material, while QP was used at 25%, 30%, and 35% as a partial replacement for fine sand. The prepared specimens were exposed to 200 °C, 400 °C, and 800 °C, followed by air cooling. Mechanical strength tests were conducted to evaluate compressive and flexural strengths, as well as failure patterns. Microstructural changes due to thermal exposure were assessed using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). Among the prepared mixtures, the 30SF35QP mixture exhibited the highest compressive strength (156.0 MPa), followed by the 15SF35QP mix (146.83 MPa). The experimental results demonstrated that G-UHPC underwent varying levels of thermal degradation across the 200–800 °C range yet displayed excellent resistance to thermal spalling. At 200 °C, compressive strength increased due to enhanced geopolymerization, with the control mix showing a 29.8% increase. However, significant strength reductions were observed at 800 °C, where the control mix retained only 30.8% (32.0 MPa) and the 30SF25QP mixture retained 28% (38.0 MPa) of their original strengths. Despite increased porosity and cracking at 800 °C, the 30SF35QP mixture exhibited superior strength retention due to its denser matrix and reduced voids. The EDS results confirmed improved gel stability in the 30% SF mixtures, as evidenced by higher silicon content. These findings suggest that optimizing SF and QP content significantly enhances the fire resistance and structural integrity of G-UHPC, providing practical insights for the design of sustainable, high-performance concrete structures in fire-prone environments. Full article
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20 pages, 3201 KiB  
Article
Effect of Screw Configuration on the Recyclability of Natural Fiber-Based Composites
by Vlasta Chyzna, Steven Rowe, James Finnerty, Trevor Howard, Christopher Doran, Shane Connolly, Noel Gately, Alexandre Portela, Alan Murphy, Declan M. Devine and Declan Mary Colbert
Fibers 2025, 13(7), 98; https://doi.org/10.3390/fib13070098 - 18 Jul 2025
Viewed by 387
Abstract
The burgeoning crisis of plastic waste accumulation necessitates innovative approaches towards sustainable packaging solutions. Polylactic acid (PLA), a leading biopolymer, emerges as a promising candidate in this realm, especially for environmentally friendly packaging. PLA is renowned for its compostable properties, offering a strategic [...] Read more.
The burgeoning crisis of plastic waste accumulation necessitates innovative approaches towards sustainable packaging solutions. Polylactic acid (PLA), a leading biopolymer, emerges as a promising candidate in this realm, especially for environmentally friendly packaging. PLA is renowned for its compostable properties, offering a strategic avenue to mitigate plastic waste. However, its dependency on specific industrial composting conditions, characterized by elevated temperatures, humidity, and thermophilic microbes, limits its utility for household composting. This study aims to bridge the research gap in PLA’s recyclability and explore its feasibility in mechanical recycling processes. The research focuses on assessing the mechanical characteristics of PLA and PLA-based composites post-recycling. Specifically, we examined the effects of two extrusion methods—conical and parallel—on PLA and its composites containing 20 wt.% basalt fibers (BF). The recycling process encompassed repeated cycles of hot melt extrusion (HME), followed by mechanical grinding to produce granules. These granules were then subjected to injection moulding (IM) after 1, 3 and 5 recycling cycles. The tensile properties of the resulting IM-produced bars provided insights into the material’s durability and stability. The findings reveal that both PLA and PLA/BF composites retain their mechanical integrity through up to 5 cycles of mechanical recycling. This resilience underscores PLA’s potential for integration into existing recycling streams, addressing the dual challenges of environmental sustainability and waste management. The study contributes to the broader understanding of PLA’s lifecycle and opens new possibilities for its application in eco-friendly packaging, beyond the limits of composting. The implications of these findings extend towards enhancing the circularity of biopolymers and reducing the environmental footprint of plastic packaging. Full article
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28 pages, 3506 KiB  
Review
A Review of Electromagnetic Wind Energy Harvesters Based on Flow-Induced Vibrations
by Yidan Zhang, Shen Li, Weilong Wang, Pengfei Zen, Chunlong Li, Yizhou Ye and Xuefeng He
Energies 2025, 18(14), 3835; https://doi.org/10.3390/en18143835 - 18 Jul 2025
Viewed by 235
Abstract
The urgent demand of wireless sensor nodes for long-life and maintenance-free miniature electrical sources with output power ranging from microwatts to milliwatts has accelerated the development of energy harvesting technologies. For the abundant and renewable nature of wind in environments, flow-induced vibration (FIV)-based [...] Read more.
The urgent demand of wireless sensor nodes for long-life and maintenance-free miniature electrical sources with output power ranging from microwatts to milliwatts has accelerated the development of energy harvesting technologies. For the abundant and renewable nature of wind in environments, flow-induced vibration (FIV)-based wind energy harvesting has emerged as a promising approach. Electromagnetic FIV wind energy harvesters (WEHs) show great potential for realistic applications due to their excellent durability and stability. However, electromagnetic WEHs remain less studied than piezoelectric WEHs, with few dedicated review articles available. This review analyzes the working principle, device structure, and performance characteristics of electromagnetic WEHs based on vortex-induced vibration, galloping, flutter, wake galloping vibration, and Helmholtz resonator. The methods to improve the output power, broaden the operational wind speed range, broaden the operational wind direction range, and enhance the durability are then discussed, providing some suggestions for the development of high-performance electromagnetic FIV WEHs. Full article
(This article belongs to the Section D: Energy Storage and Application)
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