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Keywords = cold/hot rolling

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25 pages, 3479 KB  
Article
Generalization of Machine Learning Surrogates Across Building Orientation and Roof Solar Absorptance in Naturally Ventilated Dwellings
by Cintia Monreal Jiménez, Angel Jiménez-Godoy, Guillermo Barrios, Robert Jäckel, Alberto Ramos Blanco and Geydy Gutiérrez-Urueta
Buildings 2026, 16(6), 1245; https://doi.org/10.3390/buildings16061245 - 21 Mar 2026
Viewed by 530
Abstract
This study develops an interpretable machine learning (ML) surrogate to predict hourly indoor air temperature and discomfort indicators for a representative Mexican social-housing prototype in San Luis Potosí (cold semi-arid, Köppen–Geiger BSk). A four-zone EnergyPlus model with constant window opening (50%) and no [...] Read more.
This study develops an interpretable machine learning (ML) surrogate to predict hourly indoor air temperature and discomfort indicators for a representative Mexican social-housing prototype in San Luis Potosí (cold semi-arid, Köppen–Geiger BSk). A four-zone EnergyPlus model with constant window opening (50%) and no internal gains was used to generate a parametric dataset spanning 24 building orientations, seven roof solar absorptance levels, and two neighborhood configurations (surrounded vs. corner). Zone-specific bagged-tree regression models were trained in MATLAB using weather predictors, temporal indicators, and weather-memory features (including outdoor temperature lags and rolling averages). Orientation and roof absorptance were included as explicit design predictors, enabling the surrogate model to generalize across the full combinatorial design space rather than requiring a separate model for each configuration. Interpretability was assessed with SHAP values. Evaluated on orientation–absorptance combinations deliberately held out during training, the surrogate achieved high accuracy across zones of the house (R2 = 0.98–0.99; RMSE = 0.31–0.67 °C) with stable, near-zero-centered residuals. When propagated into adaptive-comfort metrics computed directly relative to the monthly neutral temperature Tn, ML predictions preserved the main cold and hot discomfort degree-hour patterns across the full design space. The proposed surrogate enables rapid, physically consistent comfort-oriented screening of roof finishes and orientation choices in naturally ventilated social housing. Full article
(This article belongs to the Section Building Energy, Physics, Environment, and Systems)
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46 pages, 5499 KB  
Review
Duplex-Phase Fe-Mn-Al-C Low-Density Steels: A Review on Their Alloy Design, Processing, Mechanical and Application Performances
by Peng Chen, Yan Lin, Liu-Jiang Yue, Rong Chen, Yi Wang, Ting-Jun Zhang and Xiao-Wu Li
Materials 2026, 19(5), 953; https://doi.org/10.3390/ma19050953 - 1 Mar 2026
Viewed by 525
Abstract
Duplex-phase low-density steels are attracting interest for lightweight structural applications, as reducing vehicle mass is an effective route to lower fuel consumption and emissions. This review summarizes recent progress in alloy design, processing, microstructure control, and performance of duplex-phase low-density steels. The roles [...] Read more.
Duplex-phase low-density steels are attracting interest for lightweight structural applications, as reducing vehicle mass is an effective route to lower fuel consumption and emissions. This review summarizes recent progress in alloy design, processing, microstructure control, and performance of duplex-phase low-density steels. The roles of major alloying elements are discussed in terms of phase stability and precipitation tendency, followed by an overview of typical processing routes from melting to hot and cold rolling and subsequent heat treatments used to tailor phase fractions and defect structures. Strengthening mechanisms are reviewed with emphasis on precipitation control, including the beneficial contribution of fine intragranular κ′ precipitates and the ductility penalty associated with coarse intergranular κ* films, as well as the use of B2-based particles for high specific strength. Deformation behavior is then discussed in terms of transformation-/twinning-induced plasticity (TRIP/TWIP), planar versus wavy slip, and strain partitioning between ferrite and austenite. Finally, key challenges are outlined, including quantitative interface-based mechanism description, gaps in service property data, stable industrial production and compositional uniformity, and the development of forming and welding windows for engineering implementation. Full article
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21 pages, 19547 KB  
Article
Study on the Rolling Forming Process of Mg/Al Composite Foils with Low Edge Cracking
by Guang Feng, Zhaopeng Li, Ning Wang, Zhongxiang Li and Shaoyong Du
Materials 2026, 19(4), 694; https://doi.org/10.3390/ma19040694 - 11 Feb 2026
Viewed by 841
Abstract
Edge cracking is prone to occur during the rolling of Mg/Al composite foils. Herein, a hybrid hot–cold rolling process was adopted to fabricate 30 μm thick Mg/Al composite foils with low edge cracking. AZ31B magnesium alloy and 5052 aluminum alloy sheets, both with [...] Read more.
Edge cracking is prone to occur during the rolling of Mg/Al composite foils. Herein, a hybrid hot–cold rolling process was adopted to fabricate 30 μm thick Mg/Al composite foils with low edge cracking. AZ31B magnesium alloy and 5052 aluminum alloy sheets, both with an initial thickness of 0.5 mm, were chosen as research materials. Numerical simulations of composite pass were conducted at 300–450 °C with reduction ratios of 25–40%, and the optimal parameters were identified as 400 °C and a 35% reduction ratio. Based on this, multi-pass rolling experiments were performed: composite pass was heated at 400 °C for 10 min with 35% reduction ratio, hot rolling passes at 300 °C for 1–3 min, and subsequent cold rolling with 15% reduction ratio. After 21 rolling passes, 30 μm thick Mg/Al composite foils with low edge cracking were successfully prepared. Interface and metallographic characterizations demonstrated that the diffusion layer thickness varied slightly during hot rolling and increased moderately during cold rolling. For the magnesium alloy, hot rolling improved microstructural uniformity and reduced shear bands, while cold rolling caused decreased uniformity and the gradual emergence of shear bands. The research results provide a reference for the preparation of high-quality Mg/Al composite foils. Full article
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30 pages, 4895 KB  
Article
Technological and Chemical Drivers of Zinc Coating Degradation in DX51d+Z140 Cold-Formed Steel Sections
by Volodymyr Kukhar, Andrii Kostryzhev, Oleksandr Dykha, Oleg Makovkin, Ihor Kuziev, Roman Vakulenko, Viktoriia Kulynych, Khrystyna Malii, Eleonora Butenko, Natalia Hrudkina, Oleksandr Shapoval, Sergiu Mazuru and Oleksandr Hrushko
Metals 2026, 16(2), 146; https://doi.org/10.3390/met16020146 - 25 Jan 2026
Viewed by 741
Abstract
This study investigates the technological and chemical causes of early zinc-coating degradation on cold-formed steel sections produced from DX51D+Z140 galvanized coils. Commercially manufactured products exhibiting early corrosion symptoms were used in this study. The entire processing route, which included strip preparation, cold rolling, [...] Read more.
This study investigates the technological and chemical causes of early zinc-coating degradation on cold-formed steel sections produced from DX51D+Z140 galvanized coils. Commercially manufactured products exhibiting early corrosion symptoms were used in this study. The entire processing route, which included strip preparation, cold rolling, hot-dip galvanizing, passivation, multi-roll forming, storage, and transportation to customers, was analyzed with respect to the residual surface chemistry and process-related deviations that affect the coating integrity. Thirty-three specimens were examined using electromagnetic measurements of coating thickness. Statistical analysis based on the Cochran’s and Fisher’s criteria confirmed that the increased variability in zinc coating thickness is associated with a higher susceptibility to localized corrosion. Surface and chemical analysis revealed chloride contamination on the outer surface, absence of detectable Cr(VI) residues indicative of insufficient passivation, iron oxide inclusions beneath the zinc coating originating from the strip preparation, traces of organic emulsion residues impairing wetting and adhesion, and micro-defects related to deformation during roll forming. Early zinc coating degradation was shown to result from the cumulative action of multiple technological (surface damage during rolling, variation in the coating thickness) and environmental (moisture during storage and transportation) parameters. On the basis of the obtained results, a methodology was proposed to prevent steel product corrosion in industrial conditions. Full article
(This article belongs to the Special Issue Corrosion Behavior and Surface Engineering of Metallic Materials)
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12 pages, 8403 KB  
Article
Effects of Two-Way Cold Rolling and Subsequent Annealing on the Microstructure and Tensile Properties of Low-Carbon Steel with Different Initial Microstructures
by Toshio Ogawa, Hidetomo Hayashi and Hiroyuki Dannoshita
Materials 2026, 19(3), 466; https://doi.org/10.3390/ma19030466 - 24 Jan 2026
Viewed by 479
Abstract
We investigated the effects of two-way cold rolling and subsequent annealing on the microstructure and tensile properties of low-carbon steel with different initial microstructures. Two types of hot-rolled sheet specimens were prepared: specimen P, consisting of ferrite and pearlite, and specimen M, consisting [...] Read more.
We investigated the effects of two-way cold rolling and subsequent annealing on the microstructure and tensile properties of low-carbon steel with different initial microstructures. Two types of hot-rolled sheet specimens were prepared: specimen P, consisting of ferrite and pearlite, and specimen M, consisting of martensite. The hot-rolled sheets were cold-rolled in two directions and subsequently annealed. Two-way cold rolling promoted shear-band formation compared with one-way cold rolling. Furthermore, the two-way cold-rolled specimens showed higher strain homogeneity than the one-way cold-rolled specimens. When annealed below the Ac1 temperature, two-way cold rolling accelerated recrystallization in specimen P, but not in specimen M. In the intercritically annealed specimen P, two-way cold rolling increased the average size of recrystallized ferrite grains while reducing their aspect ratio. In addition, the strength–ductility balance of the two-way cold-rolled specimen P was similar to that of the one-way cold-rolled specimen P. In contrast, in the intercritically annealed specimen M, two-way cold rolling reduced the average size and the aspect ratio of recrystallized ferrite grains. As a result, the strength–ductility balance of the two-way cold-rolled specimen M was improved by approximately 15% compared with that of the one-way cold-rolled specimen. This improvement was attributed to the formation of fine and equiaxed recrystallized ferrite grains. The present findings provide a basis for applying two-way cold rolling as a microstructure-control strategy in high-strength steels. Full article
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15 pages, 5772 KB  
Article
Study on Formation Mechanism of Edge Cracks and Targeted Improvement in Hot-Rolled Sheets of Grain-Oriented Electrical Steel
by Weidong Zeng, Hui Tang, Xiaoyong Tang, Jiaming Wang, Zhongyu Piao and Fangqin Dai
Metals 2026, 16(1), 96; https://doi.org/10.3390/met16010096 - 15 Jan 2026
Viewed by 632
Abstract
Edge cracks in hot-rolled sheets of industrial grain-oriented electrical steel significantly affect the yield rate and pose substantial challenges to cold rolling fabrication. Eliminating such structural defects through hot rolling requires a thorough understanding of their formation mechanism. This study investigates the formation [...] Read more.
Edge cracks in hot-rolled sheets of industrial grain-oriented electrical steel significantly affect the yield rate and pose substantial challenges to cold rolling fabrication. Eliminating such structural defects through hot rolling requires a thorough understanding of their formation mechanism. This study investigates the formation mechanism of edge cracks in hot-rolled sheets, which are characterized by coarse strip-like grains with typical thicknesses ranging from 20 μm to 100 μm. Coarse, strip-shaped grains have low fracture stress, which is the cause of edge cracks. They originate from abnormally developed columnar grains in continuous casting slabs after reheating, which is unavoidable in industrial large-scale production. Inadequate fragmentation and insufficient recrystallization during rough rolling result in residual coarse grains of intermediate slabs, and their preferential deformation and outward protrusion lead to the formation of grooves. In the subsequent finishing rolling process, deformed coarse grains near the grooves undergo further elongation, developing into distinct strip-like structures. Based on the above mechanistic understanding, the edge microstructure under various rolling parameters was investigated, and targeted improvement measures for edge cracks were proposed. It is concluded that the edge quality can be significantly enhanced through increasing the total width reduction, additional rough rolling passes, and the implementation of edge heating during rough rolling. Quantitative analysis demonstrates that increasing the rolling passes from D to E significantly reduces the fraction of band structure from 64% to 48% and the average width of elongated grains from 43.5 μm to 38.4 μm. Full article
(This article belongs to the Section Metal Casting, Forming and Heat Treatment)
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21 pages, 10735 KB  
Article
Effect of Annealing Temperature on the Microstructure, Texture, and Properties of Hot-Rolled Ferritic Stainless Steel with Preferential α-Fiber Orientation
by Rongxun Piao, Jinhui Zhang, Gang Zhao and Junhai Wang
Materials 2026, 19(2), 293; https://doi.org/10.3390/ma19020293 - 11 Jan 2026
Viewed by 752
Abstract
For hot-rolled ferritic stainless steels with preferential α-fiber texture, the strong α-fiber texture is retained after annealing, greatly affecting the texture and plastic formability during the subsequent cold-rolling process. For optimizing the texture of hot-rolled steels toward the favorable γ-fiber type, it is [...] Read more.
For hot-rolled ferritic stainless steels with preferential α-fiber texture, the strong α-fiber texture is retained after annealing, greatly affecting the texture and plastic formability during the subsequent cold-rolling process. For optimizing the texture of hot-rolled steels toward the favorable γ-fiber type, it is essential to control the annealing temperature in the annealing process. To investigate the evolution of the microstructure, texture, and properties of hot-rolled ferritic stainless steel with preferential α-fiber orientation, a series of annealing tests was performed at the lab scale at 800, 840, 880, 910, 930, and 950 °C for 3 min. The microstructure, texture, and grain boundary characteristics of the tested samples were analyzed using optical microscopy (OM) and electron back-scattered diffraction (EBSD). The mechanical properties and plastic strain ratio (r-value) were determined through universal tensile testing. The results show that at temperatures above 840 °C, more than 93% of recrystallization occurs, leading to significant microstructural refinement. The α-fiber texture intensity typically diminishes with rising temperature, whereas the γ-fiber texture initially weakens during the early stages of recrystallization (below 840 °C) and subsequently exhibits a slight increase at higher temperatures. The improved formability of the material is mainly attributed to microstructural refinement and texture refinement, as reflected by the I(γ)/I(α) texture intensity ratio. At an annealing temperature of 930 °C, the I(γ)/I(α) ratio peaks at 0.85, static toughness is maximized, the strain-hardening exponent (n) reaches a high value of 0.28, and the maximum average plastic strain ratio (r¯) is 0.96. This result represents the optimum balance between mechanical properties and formability, making it suitable for subsequent cold-rolling. Full article
(This article belongs to the Special Issue Processing of Metals and Alloys)
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18 pages, 788 KB  
Article
Organic Chromium Sources as a Strategy to Improve Performance, Carcass Traits, and Economic Return in Lambs Finishing at Heavier Weights
by Alejandro Rivera-Villegas, Alejandra Ríos, Oliver Yaotzin Sánchez-Barbosa, Octavio Carrillo-Muro, Pedro Hernández-Briano, Alejandro Plascencia, Octavio Martínez-Guerrero and Rosalba Lazalde-Cruz
Agriculture 2025, 15(24), 2559; https://doi.org/10.3390/agriculture15242559 - 11 Dec 2025
Viewed by 720
Abstract
Thirty-six Dorper × Katahdin intact male lambs [44.0 ± 0.27 kg initial body weight (BW)] were used in a randomized complete block design to evaluate the effects of supplementing different organic chromium (OrCr) sources on growth performance, dietary energetics, carcass traits, meat quality, [...] Read more.
Thirty-six Dorper × Katahdin intact male lambs [44.0 ± 0.27 kg initial body weight (BW)] were used in a randomized complete block design to evaluate the effects of supplementing different organic chromium (OrCr) sources on growth performance, dietary energetics, carcass traits, meat quality, and economic return. Treatments (n = 9 lambs/treatment) were (1) Control (no Cr), (2) chromium-enriched yeast (Cr-Yeast), (3) chromium–methionine (Cr-Met), and (4) chromium–propionate (Cr-Pr). All Cr sources were provided at 1.2 mg elemental Cr/lamb/d for 45 d. Lambs received a high-energy finishing diet (78:22 concentrate/forage; steam-rolled corn-based). Dry matter intake was not affected (p = 0.583; 1.27 ± 0.034 kg/d). Compared with Control, Cr-Pr increased final BW (+5%; p = 0.025) and average daily gain (+66%; p = 0.034), and improved feed efficiency (+59%; p = 0.045) and observed-to-expected net energy ratio (+22%; p = 0.042); Cr-Met and Cr-Yeast showed intermediate responses. No differences were observed (p > 0.05) in longissimus lumborum muscle area, cold carcass weight, dressing percentage, cooling loss, or zoometric traits. Rib and rump fat thickness decreased with Cr-Met (−15 and −12%; p = 0.024 and p = 0.048) and with Cr-Pr (−19 and −13%; p = 0.024 and p = 0.048), and all OrCr sources reduced omental (−6 to −25%; p = 0.034), mesenteric (≈−7%; p = 0.042), visceral (−12 to −16%; p = 0.034), and perirenal fat (−25 to −39%; p = 0.028). Empty body weight and hot carcass weight increased with Cr-Pr (p = 0.029 and p = 0.031, respectively). Cr-Yeast and Cr-Pr increased muscle proportion (+5 to +7%; p = 0.003) and reduced carcass fat (−20 to −27%; p = 0.018), improving the muscle/fat ratio (+42 to +50%; p = 0.045). Cr-Pr improved water-holding capacity (+27%; p = 0.014) without affecting pH24h, purge loss, cooking loss, or Warner–Bratzler shear force (p > 0.05). Cr-Pr reduced cost per kg of gain (−31%; p < 0.001) and increased income (+188% live; +105% carcass; p < 0.001), whereas Cr-Met and Cr-Yeast provided moderate benefits. In conclusion, OrCr supplementation improved dietary energy utilization, growth, carcass traits, and meat quality, enhancing profitability in lambs finished at heavier weights, with Cr-Pr producing the greatest responses. Full article
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28 pages, 13303 KB  
Article
Effect of Processing History on the Microstructure and Magnetic Properties of Ultra-Low Carbon Si + Sb Non-Oriented Electrical Steels
by Fernando Hernández-Navarro, Armando Salinas-Rodríguez, Rogelio Deaquino-Lara, Javier Aguilar-Carrillo, Iván A. Reyes-Domínguez, Lizangela Guerra-Fuentes, Ma. de J. Soria-Aguilar, Francisco R. Carrillo-Pedroza, Josefina García-Guerra, Verónica E. Salazar-Muñoz and Emmanuel J. Gutiérrez-Castañeda
Solids 2025, 6(4), 65; https://doi.org/10.3390/solids6040065 - 27 Nov 2025
Cited by 1 | Viewed by 1447
Abstract
In this work, different processing routes were investigated to evaluate the effects of hot rolling temperature, annealing before cold rolling (ABCR), and one- or two-stage cold rolling and annealing schedules to obtain more efficient electrical steels. The correlation between processing variables, microstructure, thickness, [...] Read more.
In this work, different processing routes were investigated to evaluate the effects of hot rolling temperature, annealing before cold rolling (ABCR), and one- or two-stage cold rolling and annealing schedules to obtain more efficient electrical steels. The correlation between processing variables, microstructure, thickness, and magnetic properties was established from the analysis of 3D surface plots. It was found that the lowest core loss values (3.4 W/kg) were obtained when steel is processed by hot rolling (800 °C), ABCR (880 °C–180 min), first cold rolling (up to 0.25 mm), first annealing (850 °C–10 min), second cold rolling (up to 0.2 mm), and second annealing (850 °C–10 min). The better combination between thickness and grain size leads to the enhancement of the magnetic properties, which affects the way eddy and hysteresis losses contribute to the total core losses. Full article
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14 pages, 4753 KB  
Article
Finding Optimal Thermo-Mechanical Processing for a TNTZ-O Beta-Titanium Alloy
by Vasile Danut Cojocaru, Anna Nocivin, Doina Raducanu, Claudia Ioana Cojocaru, Raluca Elena Irimescu and Mihai Bogdan Galbinasu
Materials 2025, 18(23), 5281; https://doi.org/10.3390/ma18235281 - 23 Nov 2025
Viewed by 646
Abstract
A titanium-based alloy, with niobium, tantalum and zirconium as its main alloying elements, and a small amount of oxygen, was subjected to a thermo-mechanical processing program consisting of hot and cold rolling interspersed with different solution treatments applied above the β-transus temperature. The [...] Read more.
A titanium-based alloy, with niobium, tantalum and zirconium as its main alloying elements, and a small amount of oxygen, was subjected to a thermo-mechanical processing program consisting of hot and cold rolling interspersed with different solution treatments applied above the β-transus temperature. The objective was to analyze the correlation between structure, processing methods and resulting mechanical properties in order to find an appropriate optimized processing path to obtain suitable mechanical characteristics for application in hard tissue implantology. By using microstructural analysis, such as X-ray diffraction and scanning electron microscopy, a series of microstructural features were analyzed. The enthalpy of mixing—ΔHmix—and the atom size difference parameter—δ—were determined, through which the β-solid solution stability was estimated. Tensile tests were performed, through which the main mechanical characteristics were determined: a yield strength (0.2%) and ultimate tensile strength of around 550 MPa and 650 MPa, respectively, with a low Young’s modulus of 56–58 GPa and an improved elongation to fracture value of 17–18%, associated with a good mechanical osteo-compatibility parameter. Full article
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14 pages, 8937 KB  
Article
Microstructure Evolution and Mechanical Properties of Fe-25Ni-15Cr Alloy During Cumulative Cold-Drawing Deformation Process
by Yunfei Zhang, Zhen Zhang, Wei Chen, Zhongjie Tian, Xueliang An, Yang Zhang and Zhongwu Zhang
Nanomaterials 2025, 15(22), 1717; https://doi.org/10.3390/nano15221717 - 13 Nov 2025
Viewed by 650
Abstract
In this study, we fabricated Fe-25Ni-15Cr alloy rods via vacuum induction melting, electroslag remelting, forging, hot rolling, and annealing. We systemically investigated the influence of varying cold-drawing deformation levels (10–60%) on microstructure evolution and mechanical properties, which were characterized by a variety of [...] Read more.
In this study, we fabricated Fe-25Ni-15Cr alloy rods via vacuum induction melting, electroslag remelting, forging, hot rolling, and annealing. We systemically investigated the influence of varying cold-drawing deformation levels (10–60%) on microstructure evolution and mechanical properties, which were characterized by a variety of multi-scale characterization techniques, including optical microscopy, scanning electron microscopy, X-ray diffraction, and transmission electron microscopy. The results show that when the cumulative deformation amount is less than 30%, the hardness, tensile strength, and yield strength increase significantly with the increase in deformation amount, while the elongation continues to decline; when the cumulative deformation amount exceeds 30%, the rates of increase in hardness and strength decrease significantly; and when the deformation amount increases to 50%, dislocation density accumulates preferentially at the grain boundaries and forms a cellular substructure, while the texture orientation gradually stabilizes from random distribution to the <111> direction. This alloy rod exhibits three strengthening mechanisms during cold drawing: grain refinement, second-phase precipitation, and work hardening. A predictive model for tensile strength is derived through theoretical calculations. This work has guiding significance for establishing a cold-drawing process window without intermediate annealing. Full article
(This article belongs to the Section Synthesis, Interfaces and Nanostructures)
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8 pages, 219 KB  
Editorial
Advanced Stainless Steel—From Making, Shaping, Treating to Products
by Chao Chen, Zhixuan Xue and Wangzhong Mu
Materials 2025, 18(20), 4730; https://doi.org/10.3390/ma18204730 - 15 Oct 2025
Cited by 2 | Viewed by 1221
Abstract
Stainless steels have undergone more than a century of continuous development, during which various advanced grades—such as lean duplex, super austenitic, and high-nitrogen stainless steels—have been introduced. Despite remarkable progress, the manufacturing of stainless steel remains a complex process that spans multiple critical [...] Read more.
Stainless steels have undergone more than a century of continuous development, during which various advanced grades—such as lean duplex, super austenitic, and high-nitrogen stainless steels—have been introduced. Despite remarkable progress, the manufacturing of stainless steel remains a complex process that spans multiple critical stages, including stainless steelmaking, solidification and casting, continuous casting, heat treatment, electroslag and vacuum arc remelting, as well as both hot and cold rolling operations. Ensuring excellent corrosion resistance and mechanical performance of the final products continues to be a central focus of research and production. The current Special Issue (SI) entitled ‘Advanced Stainless Steel—from Making, Shaping, Treating to Products’ has collected eight research papers focusing on various aspects of steel production, e.g., inclusions in steelmaking and continuous casting processes, continuous casting processes and the quality of stainless steel casting, heat treatment, corrosion of steels, and fatigue of steels. This summary aims to contribute to the state-of-the-art of the development of steel production. Full article
(This article belongs to the Special Issue Advanced Stainless Steel—from Making, Shaping, Treating to Products)
25 pages, 13748 KB  
Article
Differential Corrosion Behavior of High-Aluminum 304 Stainless Steel in Molten Nitrate Salts: The Roles of Rolling and Heat Treatment
by Weijie Tang, Kan Zhou, Zhenguo Li, Lifu Xin, Dexian Huang, Faqi Zhan, Penghui Yang, Haicun Yu and Peiqing La
Materials 2025, 18(19), 4513; https://doi.org/10.3390/ma18194513 - 28 Sep 2025
Cited by 2 | Viewed by 1048
Abstract
The high material cost has restricted the development of concentrated solar power (CSP) systems. In this study, a low-cost alternative material was developed by adding aluminum to 304 stainless steel to form a protective oxide film, thereby enhancing its corrosion resistance to molten [...] Read more.
The high material cost has restricted the development of concentrated solar power (CSP) systems. In this study, a low-cost alternative material was developed by adding aluminum to 304 stainless steel to form a protective oxide film, thereby enhancing its corrosion resistance to molten salt. Three material variants were tested: untreated hot-rolled plates after solution treatment and cold-rolled high-aluminum 304 stainless steel (High-Al304SS) after solution treatment and annealing treatment. After all samples were immersed in a NaNO3-KNO3 mixed salt at 600 °C for 480 h, corrosion products including NaFeO2, CrO2, Mn2O4, and NiCr2O4 were formed. The phase composition was determined by XRD, and the surface and cross-section of the corrosion layer were analyzed by SEM and EDS surface and point analysis. The corrosion rate of the samples was calculated by the weight loss method. Notably, an Al2O3-Cr2O3 composite oxide film was formed on the sample surface, effectively inhibiting corrosion. The high defect density and grain boundary energy introduced by the cold-rolling process, as well as the precipitation of the second phase during annealing, accelerated the corrosion process of the samples. However, the hot-rolled samples after solution treatment exhibited excellent corrosion resistance (64.43 μm/year) and, through further process optimization, are expected to become an ideal low-cost alternative material for 347H stainless steel (23 μm/year) in CSP systems. Full article
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15 pages, 3956 KB  
Article
Novel Alloy Designed Electrical Steel for Improved Performance in High-Frequency Electric Machines
by Carl Slater, Xiyun Ma, Gwendal Lagorce, Juliette Soulard and Claire Davis
Metals 2025, 15(10), 1066; https://doi.org/10.3390/met15101066 - 23 Sep 2025
Cited by 1 | Viewed by 1302
Abstract
The increase in electrification and desire for greater electrical motor efficiency under a range of operating conditions for different products (e.g., household appliances, automotive and aerospace) is driving innovative motor designs and demands for higher performing electrical steels. Improvements in the magnetic, electrical [...] Read more.
The increase in electrification and desire for greater electrical motor efficiency under a range of operating conditions for different products (e.g., household appliances, automotive and aerospace) is driving innovative motor designs and demands for higher performing electrical steels. Improvements in the magnetic, electrical and/or mechanical properties of electrical steels are required for high-volume electric motors and recent advances include steels with increased silicon (Si) content (from <3.5 wt% Si up to 6.5 wt%). Whilst the 6.5 wt% Si steels provide increased motor performance at high frequencies, the formation of a brittle BCC B2/D03 phase means that they cannot be cold-rolled, and therefore the production route involves siliconization after the required thickness strip is produced. The advances in computationally driven alloy design, coupled with physical metallurgical understanding, allow for more adventurous alloy design for electrical steels, outside the traditional predominantly Fe-Si compositional space. Two alloys representing a new alloy family called HiPPES (High-Performing and Processable Electrical Steel), based on low cost commonly used steel alloying elements, have been developed, cast, rolled, heat-treated, and both magnetically and mechanically tested. These alloys (with nominal compositions of Fe-3.2Mn-3.61Si-0.63Ni-0.75Cr-0.15Al-0.4Mo and Fe-2Mn-4.5Si-0.4Ni-0.75Cr-0.09Al) offer improvements compared to current ≈3 wt% Si grades: in magnetic performance (>25% magnetic loss reduction at >1 kHz), and in tensile strength (>33% increase in tensile strength with similar elongation value). Most importantly, they are maintaining processability to allow for full-scale commercial production using traditional continuous casting, hot and cold rolling, and annealing. The new alloys also showed improved resilience to grain size, with the HiPPES materials showing a <5% variance in loss at frequencies greater than 400 Hz for grain sizes between 55 and 180 µm. Comparatively, a commercial M250-35A material showed a 40% increase in loss for the same range. The paper reports on the alloy design approach used, the microstructures, and the mechanical, electrical and magnetic properties of the developed novel electrical steels compared to conventional ≈3 wt% Si and 6.5 wt% Si material. Full article
(This article belongs to the Special Issue Electrical Steels)
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18 pages, 2873 KB  
Article
Systematic Study on the Thermal Performance of Casting Slab Under Varying Environmental Conditions
by Guichang Tian, Baokuan Li, Donglin Mo and Jianxiang Xu
Metals 2025, 15(9), 967; https://doi.org/10.3390/met15090967 - 29 Aug 2025
Cited by 1 | Viewed by 1156
Abstract
Accurate prediction of slab temperature during the continuous casting and rolling process is essential for optimizing reheating furnace scheduling and achieving energy savings and emission reductions in steel production. However, because of the dynamic boundary conditions caused by the complex transport processes, obtaining [...] Read more.
Accurate prediction of slab temperature during the continuous casting and rolling process is essential for optimizing reheating furnace scheduling and achieving energy savings and emission reductions in steel production. However, because of the dynamic boundary conditions caused by the complex transport processes, obtaining precise temperature data for slabs remains challenging. These difficulties lead to issues such as low hot charging rates, mixing of hot and cold slabs in reheating furnaces, and excessive heat loss from slabs after cutting. To address these challenges, this study develops a mathematical model to calculate slab temperatures during the continuous casting and rolling process, providing a foundation for production scheduling optimization. The model accounts for the coupled heat transfer effects induced by dynamic slab stacking and the stacking heat transfer effects resulting from slabs with varying cross-sectional dimensions. Validation against experimental data demonstrated the model’s accuracy and reliability. Key findings highlighted that neglecting dynamic stacking effects or simplifying slab dimensions introduces errors. These results enhance slab temperature tracking in complex processes and advance related theoretical understanding. Full article
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