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Keywords = beam-end defect

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25 pages, 5308 KB  
Article
An Integrated Physics-Based and Data-Driven Framework for Defect Prediction in Advanced Nanoimprint Lithography Toward Inorganic Semiconductor Patterning
by Jean Chien and Eric Lee
Micromachines 2026, 17(6), 674; https://doi.org/10.3390/mi17060674 - 29 May 2026
Viewed by 265
Abstract
Advanced nanoimprint lithography (NIL) is promising for inorganic semiconductor patterning because it enables high-resolution replication with a relatively simple process flow; however, yield loss increasingly originates from spatially distributed, subcritical distortions accumulated across coating, exposure, etching, and imprinting. In this study, we propose [...] Read more.
Advanced nanoimprint lithography (NIL) is promising for inorganic semiconductor patterning because it enables high-resolution replication with a relatively simple process flow; however, yield loss increasingly originates from spatially distributed, subcritical distortions accumulated across coating, exposure, etching, and imprinting. In this study, we propose an integrated physics-based and data-driven framework for pre-manufacturing defect-risk prediction in NIL. The framework combines an NDA-safe layout database, a physics-based process twin, and a stochastic risk prediction model using a physics-augmented convolutional neural network with conformal uncertainty calibration. Starting from binary design layouts, the process twin sequentially captures resist thickness variations during spin coating, proximity-induced dose redistribution and development-induced pattern deformation during electron-beam lithography (EBL), density-sensitive pattern transfer during reactive ion etching (RIE), and three-dimensional resist filling during imprinting, thereby generating physically consistent parameter maps for downstream learning. The results demonstrate an end-to-end virtual inspection flow that converts layouts into spatially resolved risk maps before fabrication. In addition, patterns with similar contour extent but different local density exhibit distinctly different risk distributions, indicating that manufacturability is governed not only by nominal geometry but also by local pattern environment. These findings support pre-manufacturing virtual inspection as a physically interpretable route for early yield-risk screening in advanced NIL. Full article
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31 pages, 9088 KB  
Article
MaxI-Net: A 3D AI Framework for CBCT-Based Maxillofacial Defect Reconstruction and Patient-Specific Implant Generation with Biomechanical Validation
by Mamta Juneja, Maanya Kharbanda, Nitin Pandey, Agrima Sudhir, Aditya Poddar, Harleen Kaur, Prashant Prakash, Manoj Kumar Jaiswal, Prashant Jindal and Philip Breedon
Bioengineering 2026, 13(6), 619; https://doi.org/10.3390/bioengineering13060619 - 26 May 2026
Viewed by 585
Abstract
Maxillofacial defects impair facial aesthetics and oral function, arising from trauma, tumor resection, or congenital anomalies; however, reconstruction using Computer-Aided Design (CAD) and autologous grafts remains complex and time-intensive, and is associated with donor-site morbidity. Although deep learning (DL) has advanced automated reconstruction, [...] Read more.
Maxillofacial defects impair facial aesthetics and oral function, arising from trauma, tumor resection, or congenital anomalies; however, reconstruction using Computer-Aided Design (CAD) and autologous grafts remains complex and time-intensive, and is associated with donor-site morbidity. Although deep learning (DL) has advanced automated reconstruction, existing models often address isolated tasks, lack integrated multi-scale feature learning, and rely on small datasets. This study proposes the Maxillofacial Implant-generation Network (MaxI-Net), a fast, resource-efficient three-dimensional DL framework for end-to-end maxillofacial defect reconstruction and patient-specific implant generation, with a completion step of cavity filling within the assembly. The model employs a 3D encoder–bottleneck-decoder architecture integrating hybrid dilated convolutions, residual connections, squeeze-and-excitation (SE) blocks, and 3D Convolutional Block Attention Modules (CBAM) with multi-scale feature fusion. It was trained on 921 Cone Beam-Computed Tomography (CBCT) scans, augmented to 11,973 maxillary defect pairs, using Dice loss and Adam optimisation with Automatic Mixed Precision, and benchmarked against UNet, UNETR, SegResNet, and SwinUNETR. MaxI-Net achieved the following: superior Dice Similarity Coefficient (DSC) = 0.778; 95th percentile Hausdorff Distance (HD95) = 3.453 mm; DSC Standard Deviation (SD) = 0.094; 95% confidence interval (CI) for mean DSC: 0.775–0.782). It was statistically validated against all competing architectures via pairwise Wilcoxon signed-rank tests, with significant DSC improvements confirmed across all comparators (p < 0.001) and rank-biserial effect sizes ranging from r = 0.250 against the closest competitor SegResNet* with high efficiency (0.06 s/volume; 9.6 min/epoch). Internal cavity filling of the generated implants was performed as a brief manual post-processing step in Autodesk Fusion 360 prior to biomechanical validation. Biomechanical validation using a finite element analysis (FEA) of polyether–ether–ketone (PEEK) implants (~26.53 g) showed 41% stress reduction under physiological loads (100–400 N), predicting a ~9.2-year lifespan. Full article
(This article belongs to the Special Issue Artificial Intelligence (AI) in Bioengineering: Second Edition)
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17 pages, 4116 KB  
Article
Degradation Mechanism, Performance Impact, and Maintenance Strategies for Expansion Devices of Large-Span Railway Bridges
by Yunchao Ye, Aiguo Yan, Pengcheng Yin, Jinbao Liang and Zhiqiang Zhu
Infrastructures 2026, 11(1), 30; https://doi.org/10.3390/infrastructures11010030 - 19 Jan 2026
Viewed by 519
Abstract
To ensure the coordinated interaction between the beam and track of large-span bridges and achieve smooth rail transition at beam joints, rail expansion regulators and beam-end expansion devices are essential at bridge ends. However, these devices are structurally fragile, making them a weak [...] Read more.
To ensure the coordinated interaction between the beam and track of large-span bridges and achieve smooth rail transition at beam joints, rail expansion regulators and beam-end expansion devices are essential at bridge ends. However, these devices are structurally fragile, making them a weak link in the seamless track system. This study selected a long-span railway bridge and its expansion devices as research objects, summarized typical in-service diseases of beam-end expansion devices (e.g., adjustable sleeper offset, sleeper skewing, and expansion device jamming), and constructed a train–track–bridge coupled model incorporating these devices. The model was used to analyze the structural performance and train operation safety under defective conditions. Based on the analysis findings, a maintenance evaluation method for the beam-end region was proposed. Criteria include adjustable sleeper offset, lateral displacement difference between adjacent beam-ends, horizontal rotation angle of adjacent beams, vertical rotation angle of beam-ends, and longitudinal expansion amount of beam-end expansion devices in order to address the corresponding issues and achieve sustainable maintenance and operation of bridge structures. Full article
(This article belongs to the Special Issue Sustainable Bridge Engineering)
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17 pages, 3222 KB  
Article
Residual Temperature Prediction in Selective Laser Melting by Deep Neural Networks
by Nikolaos Papadimitriou, Emmanuel Stathatos and George-Christopher Vosniakos
Metals 2025, 15(10), 1119; https://doi.org/10.3390/met15101119 - 9 Oct 2025
Viewed by 1019
Abstract
Selective laser melting (SLM) builds metal parts layer by layer by locally melting powder with a fine laser beam, generating complex, geometry-dependent temperature gradients that govern density, microstructure, defects, and residual stresses. Resolving these gradients with high-fidelity finite-element (FE) models is prohibitively slow [...] Read more.
Selective laser melting (SLM) builds metal parts layer by layer by locally melting powder with a fine laser beam, generating complex, geometry-dependent temperature gradients that govern density, microstructure, defects, and residual stresses. Resolving these gradients with high-fidelity finite-element (FE) models is prohibitively slow because the temperature field must be evaluated at dense points along every scan track across multiple layers, while the laser spot is orders of magnitude smaller than typical layer dimensions. This study replaces FE analysis with a deep neural network that predicts the end-of-build temperature field orders of magnitude faster. A benchmark part containing characteristic shape features is introduced to supply diverse training cases, and a novel control-volume-based geometry-abstraction scheme encodes arbitrary workpiece shapes into compact, learnable descriptors. Thermal simulation data from the benchmark train the network, which then predicts the residual temperature field of an unseen, geometrically dissimilar part with a mean absolute error of ~10 K and a mean relative error of ~1% across 500–1300 K. The approach thus offers a rapid, accurate surrogate for FE simulations, enabling efficient temperature-driven optimization of SLM process parameters and part designs. Full article
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18 pages, 8651 KB  
Article
Interlaminar Fracture Toughness Analysis for Reliability Improvement of Wind Turbine Blade Spar Elements Based on Pultruded Carbon Fiber-Reinforced Polymer Plate Manufacturing Method
by Hakgeun Kim, Yunjung Jang, Sejin Lee, Chanwoong Choi and Kiweon Kang
Materials 2025, 18(2), 357; https://doi.org/10.3390/ma18020357 - 14 Jan 2025
Cited by 1 | Viewed by 2308
Abstract
The key structural components of a wind turbine blade, such as the skin, spar cap, and shear web, are fabricated from fiber-reinforced composite materials. The spar, predominantly manufactured via resin infusion—a process of resin injection and curing in carbon fibers—is prone to initial [...] Read more.
The key structural components of a wind turbine blade, such as the skin, spar cap, and shear web, are fabricated from fiber-reinforced composite materials. The spar, predominantly manufactured via resin infusion—a process of resin injection and curing in carbon fibers—is prone to initial defects, such as pores, wrinkles, and delamination. This study suggests employing the pultrusion technique for spar production to consistently obtain a uniform cross-section and augment the reliability of both the manufacturing process and the design. In this context, this study introduces carbon fiber-reinforced polymer (CFRP/CFRP) and glass fiber-reinforced polymer (GFRP/CFRP) test specimens, which mimic the bonding structure of the spar cap, utilizing pultruded CFRP in accordance with ASTM standards to analyze the delamination traits of the spar. Delamination tests—covering Mode I (double cantilever beam), Mode II (end-notched flexure), and mixed mode (mixed-mode bending)—were performed to gauge displacement, load, and crack growth length. Through this crack growth mechanism, the interlaminar fracture toughness derived was examined, and the stiffness and strength changes compared to CFRP based on the existing prepreg manufacturing method were analyzed. In addition, the interlaminar fracture toughness for GFRP, which is a material in contact with the spar structure, was analyzed, and through this, it was confirmed that the crack behavior has less deviation compared to a single CFRP material depending on the stiffness difference between the materials when joining dissimilar materials. This means that the higher the elasticity of the high-stiffness material, the higher the initial crack resistance, but the crack growth behavior shows non-uniform characteristics thereafter. This comparison provides information for predicting interlaminar delamination damage within the interior and bonding area of the spar and skin and provides insight for securing the reliability of the design life. Full article
(This article belongs to the Section Advanced Composites)
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12 pages, 4594 KB  
Article
Monitoring of Directed Energy Deposition Laser Beam of Nickel-Based Superalloy via High-Speed Mid-Wave Infrared Coaxial Camera
by Marco Mazzarisi, Andrea Angelastro, Sabina Luisa Campanelli, Vito Errico, Paolo Posa, Andrea Fusco, Teresa Colucci, Alexander John Edwards and Simona Corigliano
J. Manuf. Mater. Process. 2024, 8(6), 294; https://doi.org/10.3390/jmmp8060294 - 18 Dec 2024
Cited by 3 | Viewed by 3558
Abstract
Directed Energy Deposition Laser Beam (DED-LB) is a promising additive manufacturing technique that uses a laser source and a powder stream to build or repair metal components. Repair applications offer significant economic and environmental benefits but are more challenging to develop, especially for [...] Read more.
Directed Energy Deposition Laser Beam (DED-LB) is a promising additive manufacturing technique that uses a laser source and a powder stream to build or repair metal components. Repair applications offer significant economic and environmental benefits but are more challenging to develop, especially for components that are difficult to process due to their intricate geometries and materials. Process conditions can change precipitously, and it is essential to implement monitoring systems that ensure high process stability and, consequently, superior end-product quality. In the present work, a mid-wave infrared coaxial camera was used to monitor the melt pool geometry. To simulate the challenging repair process conditions of the DED-LB process, experimental tests were carried out on substrates with different thicknesses. The stability of the deposition process on nickel-based superalloys was analyzed by means of MATLAB algorithms. Thus, the effect of open-loop and closed-loop monitoring with back control on laser power on the process conditions was assessed and quantified. Metallographic analysis of the produced samples was carried out to validate the analyses performed by the monitoring system. The occurrence of production defects (lack of fusion and porosity) related to parameters not directly controllable by monitoring systems, such as penetration depth and dilution, was determined. Full article
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9 pages, 4539 KB  
Communication
Fabrication of Circular Defects in 2-Dimensional Photonic Crystal Lasers with Convex Edge Structure
by Rubing Zuo, Yuki Adachi, Yuto Kudo, Hanqiao Ye, Tetsuya Yagi, Masato Morifuji, Hirotake Kajii, Akihiro Maruta and Masahiko Kondow
Photonics 2024, 11(9), 853; https://doi.org/10.3390/photonics11090853 - 10 Sep 2024
Viewed by 1670
Abstract
We have developed circular defects in 2-dimensional photonic crystal lasers that allow current injection for interconnected optical communications. However, when cleaving the sample to measure the output light, the output light intensity changes due to the cleaving position. In a previous study, we [...] Read more.
We have developed circular defects in 2-dimensional photonic crystal lasers that allow current injection for interconnected optical communications. However, when cleaving the sample to measure the output light, the output light intensity changes due to the cleaving position. In a previous study, we proposed a new end face structure called a convex edge structure. In this paper, we design the electron beam lithography patterns to fabricate this structure. With this design, it is possible to eliminate the effect of different cleaving positions and ensure that the cleavage tolerance is larger than the cleavage position error. We also develop the fabrication technology for this structure, fabricate samples, and measure the output light experimentally. The optical properties of the fabricated sample are similar to well-fabricated samples with normal cleavage edge faces. We are assured that these results contribute to future work such as accurate manufacturing and improving the end face configuration to obtain higher outputs. Full article
(This article belongs to the Special Issue Photonic Crystals: Physics and Devices, 2nd Edition)
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18 pages, 6929 KB  
Article
Stiffness-Based Evaluation of Hinge Joints in Prefabricated Assembled Multi-Girder Bridges under Operational Conditions
by Zhiqiang Shang, Fengzong Gong, Zhufeng Shao, Jose Matos, Gongfeng Xin and Ye Xia
Sensors 2024, 24(13), 4255; https://doi.org/10.3390/s24134255 - 30 Jun 2024
Cited by 5 | Viewed by 1954
Abstract
Presently, the prevailing approaches to assessing hinge joint damage predominantly rely on predefined damage indicators or updating finite element models (FEMs). However, these methods possess certain limitations. The damage indicator method requires high-quality monitoring data and demonstrates variable sensitivities of distinct indicators to [...] Read more.
Presently, the prevailing approaches to assessing hinge joint damage predominantly rely on predefined damage indicators or updating finite element models (FEMs). However, these methods possess certain limitations. The damage indicator method requires high-quality monitoring data and demonstrates variable sensitivities of distinct indicators to damage. On the other hand, the FEM approach mandates a convoluted FEM update procedure. Hinge joint damage represents a major kind of defect in prefabricated assembled multi-girder bridges (AMGBs). Therefore, effective damage detection methods are imperative to identify the damage state of hinge joints. To this end, a stiffness-based method for the performance evaluation of hinge joints of AMGBs is proposed in this paper. The proposed method estimates hinge joint stiffness by solving the characteristic equations of the multi-beam system. In addition, this study introduces a method for determining baseline joint stiffness using design data and FEM. Subsequently, a comprehensive evaluation framework for hinge joints is formulated, coupling a finite element model with the baseline stiffness, thereby introducing a damage indicator rooted in stiffness ratios. To verify the effectiveness of the proposed method, strain and displacement correlations are analyzed using actual bridge monitoring data, and articulation joint stiffness is identified. The results underscore the capability of the proposed method to accurately pinpoint the location and extent of hinge joint damage. Full article
(This article belongs to the Section Fault Diagnosis & Sensors)
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18 pages, 13299 KB  
Article
Study on the Nonlinear Stability and Parametric Analysis of a Tensile–Beam Cable Dome
by Jianchen Guo, Mingmin Ding, Libin Wang, Yangjie Ruan and Bin Luo
Symmetry 2023, 15(9), 1690; https://doi.org/10.3390/sym15091690 - 2 Sep 2023
Cited by 2 | Viewed by 2086
Abstract
To reveal the stable bearing capacity of a new semi-rigid dome structure, the tensile–beam cable dome (TBCD), a detailed numerical simulation and analysis of a 60 m model TBCD is conducted. Then, the effects of factors such as the prestress level, original imperfection [...] Read more.
To reveal the stable bearing capacity of a new semi-rigid dome structure, the tensile–beam cable dome (TBCD), a detailed numerical simulation and analysis of a 60 m model TBCD is conducted. Then, the effects of factors such as the prestress level, original imperfection size, original imperfection distribution, and addition of hoop tension rods on the stability of the TBCD model are investigated. The results show that the unstable loads of the TBCD are arranged from small to large in the following order: doubly nonlinearity with an original imperfection, geometry nonlinearity with an original imperfection, geometry nonlinearity without an original imperfection, and eigen buckling. In this case, the effects of geometry nonlinearity, material nonlinearity, and original imperfections must be comprehensively analyzed. The unstable mode of the TBCD depends on the loading form. Torsional buckling of the overall structure occurs under the symmetric load of ‘Full live + full dead’, while local out-of-plane buckling appears with the asymmetric load of ‘Half live + full dead’. With 2–3 times the loading integrations, the innermost tension beams change from stretch bending to pressurized bending, which causes the overall TBCD to become unstable. A small prestress level clearly decreases the stability of the TBCD, while a relatively large prestress level has little effect. When the original imperfection is greater than 1/400 of the span, the stability of the TBCD is problematic. Comprehensively considering the impact of multiple defects is needed when analyzing the buckling of the TBCD. Adding hoop tension beams between the top ends of rods can effectively improve the integrity and stability of the TBCD. Full article
(This article belongs to the Special Issue Advances in Structural Mechanics and Symmetry/Asymmetry)
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8 pages, 5932 KB  
Communication
Intra-Cavity Cascaded Pumped 946/1030 nm Dual-Wavelength Vortex Laser Using a Spot-Defect Mirror
by Yashuai Yang, Yongliang Li, Xinyi Zhu, Chi Wang and Chao Yang
Photonics 2023, 10(5), 554; https://doi.org/10.3390/photonics10050554 - 10 May 2023
Cited by 5 | Viewed by 2658
Abstract
Due to their unique properties, vortex lasers have high application value in frontier fields such as optical micromanipulation, super-resolution imaging, quantum entanglement, and optical communication. In this study, we demonstrated a 946/1030 nm Laguerre-Gaussian (LG01) mode dual-wavelength vortex laser by using [...] Read more.
Due to their unique properties, vortex lasers have high application value in frontier fields such as optical micromanipulation, super-resolution imaging, quantum entanglement, and optical communication. In this study, we demonstrated a 946/1030 nm Laguerre-Gaussian (LG01) mode dual-wavelength vortex laser by using an intracavity cascade pumped structure and a spot-defect output mirror. Using a coaxial linear cavity structure, the 808 nm laser diode (LD) was used to end-pump the Nd:YAG crystal to generate a 946 nm laser and then use it to directly pump the Yb:YAG crystal in the cavity to generate a 1030 nm laser, and finally a 946/1030 nm dual-wavelength laser came out. By making a spot defect in the center of the output mirror to suppress the oscillation of the fundamental Gaussian mode laser and carefully adjusting the position of the laser crystals, the LG01 mode dual-wavelength vortex laser was output in single handedness. When the pump power was 40 W, the total output was 664 mW (356 and 308 mW at 946 and 1030 nm LG01 mode vortex lasers), and the total optical-optical conversion efficiency was 1.7%; the output power fluctuations of 946 and 1030 nm LG01 mode vortex lasers within 1 h were 3.43% and 3.13%, respectively; the beam quality factors M2 of 946 and 1030 nm LG01 mode vortex lasers were 2.35 and 2.40, respectively. It was proved that the generated dual-wavelength vortex laser had the wavefront phase expiϕ by the self-interference method. Full article
(This article belongs to the Special Issue Advances and Application of Structured Light)
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12 pages, 8408 KB  
Article
Femtosecond Laser Surface Cleaning for Diamond Segmented Drill Bit Manufacturing
by Attila Zsolt Kenéz, Éva Lublóy, Gyula Bagyinszki and Tamás Földes
Crystals 2023, 13(4), 672; https://doi.org/10.3390/cryst13040672 - 13 Apr 2023
Cited by 3 | Viewed by 2514
Abstract
Microsecond and nanosecond lasers have been studied in the past for laser cleaning applications and, today, femtosecond lasers are also being used successfully for removing paint, rust, and surface contamination. For diamond segmented drill bits, it may be also necessary to improve the [...] Read more.
Microsecond and nanosecond lasers have been studied in the past for laser cleaning applications and, today, femtosecond lasers are also being used successfully for removing paint, rust, and surface contamination. For diamond segmented drill bits, it may be also necessary to improve the mechanical properties of the laser-welded joint, i.e., to increase the tensile strength and toughness. Therefore, in this study, we investigated the possibility of using femtosecond lasers to clean the surface before laser welding to see what effect it has on the mechanical properties of the joint. The end surface of the thin-walled tube was pretreated to remove grease and oil before laser-beam welding a powder metallurgical segment onto it and the results are compared to an untreated sample. The laser-welded seams were investigated by micro-computer tomography, break-out test, and optical microscopy. Any defects in the seams were analyzed and, according to the results obtained in this study, no cracks were found by computer tomography, a shade of grey diagram shows, and all the pre-treated samples had a higher absorption than the untreated sample. Four of the six treating parameters had a significant effect, +30% on average, and two treating parameters had a positive effect, +13.5% on average, compared to the untreated sample. In addition, the break-out values showed that only one treating parameter had a significantly, +19%, higher effect than the other treating parameters. This test showed different results from the micro-CT scan. The optimal process parameters for oil and grease removal are discussed in the conclusion. Full article
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17 pages, 31185 KB  
Review
Research Progress of Laser Additive Manufacturing Nickel-Based Alloy Metal Matrix Composites
by Zhiqiang Wang, Shuang Gao, Shuijin Li, Weiguang Zhang, Liang Lan, Yifu Jiang and Bo He
Metals 2023, 13(1), 129; https://doi.org/10.3390/met13010129 - 9 Jan 2023
Cited by 14 | Viewed by 5977
Abstract
Nickel-based alloy metal matrix composite (NAMMC) is a new type of composite material which is expected to replace traditional Nickel-base superalloy used in the manufacture of important hot-end components in aerospace, naval ships and industrial gas turbine engines due to its excellent high [...] Read more.
Nickel-based alloy metal matrix composite (NAMMC) is a new type of composite material which is expected to replace traditional Nickel-base superalloy used in the manufacture of important hot-end components in aerospace, naval ships and industrial gas turbine engines due to its excellent high temperature strength, superior thermal fatigue resistance, high oxidation resistance and thermal corrosion resistance. However, these outstanding properties make it hard to process these materials with conventional manufacturing methods such as forging and machining owing to posing problems of high cost and energy consumptions. Laser additive manufacturing (AM) with a high degree of machining freedom and a high-energy-density laser beam as heat source has been used for processing NAMMC hot-end components with superior performance and complicated structure. Nevertheless, some manufacturing defects of poor bonding, high residual stress, cracking, pore etc. still exist in laser AM NAMMC parts. Therefore, this paper reviews research progress of laser AM NAMMC at present. The control method of manufacturing defect and the effect of reinforcements on the microstructure and mechanical properties of NAMMC are summarized. In addition, the challenges and prospects of laser AM NAMMC in the future are also discussed. Full article
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17 pages, 4227 KB  
Article
Towards Tough Thermoplastic Adhesive Tape by Microstructuring the Tape Using Tailored Defects
by Ahmed Wagih, Hassan A. Mahmoud, Ran Tao and Gilles Lubineau
Polymers 2023, 15(2), 259; https://doi.org/10.3390/polym15020259 - 4 Jan 2023
Cited by 5 | Viewed by 3212
Abstract
This paper presents a strategy towards achieving thermoplastic adhesive tapes with high toughness by microstructuring conventional tapes using tailored defects. Toughened tape was manufactured using two layers of a conventional tape where the bondline between the two adhesive layers was microstructured by embedding [...] Read more.
This paper presents a strategy towards achieving thermoplastic adhesive tapes with high toughness by microstructuring conventional tapes using tailored defects. Toughened tape was manufactured using two layers of a conventional tape where the bondline between the two adhesive layers was microstructured by embedding tailored defects with specific size and gap between them using PTFE film. Mode I toughness of the toughened tape was characterized experimentally. A high-fidelity finite element model was implemented to describe the toughening mechanisms using double cantilever beam simulations and end notch flexural tests. The model considers for the plasticity of the adhesive layer, the decohesion at the adherend–adhesive and adhesive–adhesive interfaces and progressive damage inside the adhesive layer. The adhesive–adhesive interface with the tailored defects inside the adhesive layer enables crack migration between adherend–adhesive interfaces, crack propagation at adhesive–adhesive interface, backward crack propagation under the defect, and plastic deformation of the adhesive ligament. The maximum toughness improvement of the tape with tailored defects of equal width and gap between two successive defects of 2 mm reached 278% and 147% for mode I and II, respectively, compared to conventional tape. Full article
(This article belongs to the Section Polymer Applications)
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20 pages, 9029 KB  
Article
External Illumination Enables Coaxial Sensing of Surface and Subsurface Molten Pool Geometry in LPBF
by Leonardo Caprio, Ali Gökhan Demir and Barbara Previtali
Metals 2022, 12(10), 1762; https://doi.org/10.3390/met12101762 - 20 Oct 2022
Cited by 6 | Viewed by 3410
Abstract
Laser powder bed fusion (LPBF) attracts the attention of high-end manufacturing sectors for its capability of depositing free-form components with elevated mechanical properties. However, due to the intrinsic nature of the feedstock material and the interaction with the laser beam, the process is [...] Read more.
Laser powder bed fusion (LPBF) attracts the attention of high-end manufacturing sectors for its capability of depositing free-form components with elevated mechanical properties. However, due to the intrinsic nature of the feedstock material and the interaction with the laser beam, the process is prone to defect formation and manufacturing inaccuracies. Therefore, the development of a monitoring architecture capable of measuring the geometrical features of the process tool (i.e., the melt pool generated by the laser-material interaction) is of paramount importance. This information may then be exploited to evaluate process stability. In this work, a high-speed camera was implemented coaxially in the optical chain of an LPBF system to extrapolate the geometrical features of the molten pool surface and its oscillatory behaviour, with elevated spatial and temporal resolution. A secondary light source was tested in both coaxial and off-axis configuration to dominate process emission and assess optimal illumination conditions for extracting the molten pool’s geometrical features. Preliminary results showed that the off-axis configuration of the illumination light enabled direct measurement of the molten pool surface geometry. A newly developed image processing algorithm based on illuminated images obtained via the coaxial observation frame was employed to provide automated identification of the melt pool geometry. Moreover, bright reflections of the external illumination over the melt surface could be clearly observed and used to characterise the oscillatory motion of the molten material. This information may therefore be taken as an indirect indicator of the molten pool penetration depth, hence providing information regarding the subsurface geometry. A successive experimental investigation showed the capability of the monitoring architecture to resolve the molten pool’s length, width and area with elevated acquisition frequency. Molten pool surface oscillations in the kHz range could be correlated to the penetration depth while the molten pool width measured via the high-speed imaging setup corresponded to the track width of the depositions. Hence, the methodological approach for the concurrent measurement of the molten pool’s geometry in three spatial dimensions was demonstrated and may be used to track the stability of LPBF depositions. Full article
(This article belongs to the Special Issue Additive Manufacturing of Architected Metallic Materials)
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10 pages, 8400 KB  
Article
Periodic Structural Defects in Graphene Sheets Engineered via Electron Irradiation
by Nicola Melchioni, Filippo Fabbri, Alessandro Tredicucci and Federica Bianco
Micromachines 2022, 13(10), 1666; https://doi.org/10.3390/mi13101666 - 3 Oct 2022
Cited by 6 | Viewed by 2861
Abstract
Artificially-induced defects in the lattice of graphene are a powerful tool for engineering the properties of the crystal, especially if organized in highly-ordered structures such as periodic arrays. A method to deterministically induce defects in graphene is to irradiate the crystal with low-energy [...] Read more.
Artificially-induced defects in the lattice of graphene are a powerful tool for engineering the properties of the crystal, especially if organized in highly-ordered structures such as periodic arrays. A method to deterministically induce defects in graphene is to irradiate the crystal with low-energy (<20 keV) electrons delivered by a scanning electron microscope. However, the nanometric precision granted by the focused beam can be hindered by the pattern irradiation itself due to the small lateral separation among the elements, which can prevent the generation of sharp features. An accurate analysis of the achievable resolution is thus essential for practical applications. To this end, we investigated patterns generated by low-energy electron irradiation combining atomic force microscopy and micro-Raman spectroscopy measurements. We proved that it is possible to create well-defined periodic patterns with precision of a few tens of nanometers. We found that the defected lines are influenced by electrons back-scattered by the substrate, which limit the achievable resolution. We provided a model that takes into account such substrate effects. The findings of our study allow the design and easily accessible fabrication of graphene devices featuring complex defect engineering, with a remarkable impact on technologies exploiting the increased surface reactivity. Full article
(This article belongs to the Special Issue 2D Materials for Opto-Electronics)
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