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Keywords = aerospace thermal test

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13 pages, 3081 KiB  
Review
Surface Air-Cooled Oil Coolers (SACOCs) in Turbofan Engines: A Comprehensive Review of Design, Performance, and Optimization
by Wiktor Hoffmann and Magda Joachimiak
Energies 2025, 18(15), 4052; https://doi.org/10.3390/en18154052 - 30 Jul 2025
Viewed by 257
Abstract
Surface Air-Cooled Oil Coolers (SACOCs) can become a critical component in managing the increasing thermal loads of modern turbofan engines. Installed within the bypass duct, SACOCs utilize high-mass flow bypass air for convective heat rejection, reducing reliance on traditional Fuel-Oil Heat Exchangers. This [...] Read more.
Surface Air-Cooled Oil Coolers (SACOCs) can become a critical component in managing the increasing thermal loads of modern turbofan engines. Installed within the bypass duct, SACOCs utilize high-mass flow bypass air for convective heat rejection, reducing reliance on traditional Fuel-Oil Heat Exchangers. This review explores SACOC design principles, integration challenges, aerodynamic impacts, and performance trade-offs. Emphasis is placed on the balance between thermal efficiency and aerodynamic penalties such as pressure drop and flow distortion. Experimental techniques, including wind tunnel testing, are discussed alongside numerical methods, and Conjugate Heat Transfer modeling. Presented studies mostly demonstrate the impact of fin geometry and placement on both heat transfer and drag. Optimization strategies and Additive Manufacturing techniques are also covered. SACOCs are positioned to play a central role in future propulsion systems, especially in ultra-high bypass ratio and hybrid-electric architectures, where traditional cooling strategies are insufficient. This review highlights current advancements, identifies limitations, and outlines research directions to enhance SACOC efficiency in aerospace applications. Full article
(This article belongs to the Special Issue Heat Transfer Analysis: Recent Challenges and Applications)
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19 pages, 2633 KiB  
Article
Influence of Mullite and Halloysite Reinforcement on the Ablation Properties of an Epoxy Composite
by Robert Szczepaniak, Michał Piątkiewicz, Dominik Gryc, Paweł Przybyłek, Grzegorz Woroniak and Joanna Piotrowska-Woroniak
Materials 2025, 18(15), 3530; https://doi.org/10.3390/ma18153530 - 28 Jul 2025
Viewed by 273
Abstract
This paper explores the impact of applying a powder additive in the form of halloysite and mullite on the thermal protection properties of a composite. The authors used CES R70 epoxy resin with CES H72 hardener, modified by varying the amount of powder [...] Read more.
This paper explores the impact of applying a powder additive in the form of halloysite and mullite on the thermal protection properties of a composite. The authors used CES R70 epoxy resin with CES H72 hardener, modified by varying the amount of powder additive. The composite samples were exposed to a mixture of combustible gases at a temperature of approximately 1000 °C. The primary parameters analyzed during this study were the temperature on the rear surface of the sample and the ablative mass loss of the tested material. The temperature increase on the rear surface of the sample, which was exposed to the hot stream of flammable gases, was measured for 120 s. Another key parameter considered in the data analysis was the ablative mass loss. The charred layer of the sample played a crucial role in this process, as it helped block oxygen diffusion from the boundary layer of the original material. This charred layer absorbed thermal energy until it reached a temperature at which it either oxidized or was mechanically removed due to the erosive effects of the heating factor. The incorporation of mullite reduced the rear surface temperature from 58.9 °C to 49.2 °C, and for halloysite, it was reduced the rear surface temperature to 49.8 °C. The ablative weight loss dropped from 57% to 18.9% for mullite and to 39.9% for halloysite. The speed of mass ablation was reduced from 77.9 mg/s to 25.2 mg/s (mullite) and 52.4 mg/s (halloysite), while the layer thickness loss decreased from 7.4 mm to 2.8 mm (mullite) and 4.4 mm (halloysite). This research is innovative in its use of halloysite and mullite as functional additives to enhance the ablative resistance of polymer composites under extreme thermal conditions. This novel approach not only contributes to a deeper understanding of composite behavior at high temperatures but also opens up new avenues for the development of advanced thermal protection systems. Potential applications of these materials include aerospace structures, fire-resistant components, and protective coatings in environments exposed to intense heat and flame. Full article
(This article belongs to the Section Advanced Composites)
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15 pages, 4749 KiB  
Article
Selective Laser Melting of a Ti-6Al-4V Lattice-Structure Gear: Design, Topology Optimization, and Experimental Validation
by Riad Ramadani, Snehashis Pal, Aleš Belšak and Jožef Predan
Appl. Sci. 2025, 15(14), 7949; https://doi.org/10.3390/app15147949 - 17 Jul 2025
Viewed by 341
Abstract
The manufacture of lightweight components is one of the most important requirements in the automotive and aerospace industries. Gears, on the other hand, are among the heaviest parts in terms of their total weight. Accordingly, a spur gear was considered, the body of [...] Read more.
The manufacture of lightweight components is one of the most important requirements in the automotive and aerospace industries. Gears, on the other hand, are among the heaviest parts in terms of their total weight. Accordingly, a spur gear was considered, the body of which was configured as a lattice structure to make it lightweight. In addition, the structure was optimized by topology optimization using ProTOP software. Subsequently, the gear was manufactured by a selective laser melting process by using a strong and lightweight material, namely Ti-6Al-4V. This study defeated the problems of manufacturing orientation, surface roughness, support structure, and bending due to the high thermal gradient in the selective laser melting process. To experimentally investigate the benefits of such a lightweight gear body structure, a new test rig with a closed loop was developed. This rig enabled measurements of strains in the gear ring, hub, and tooth root. The experimental results confirmed that a specifically designed and selectively laser-melted, lightweight cellular lattice structure in the gear body can significantly influence strain. This is especially significant with respect to strain levels and their time-dependent variations in the hub section of the gear body. Full article
(This article belongs to the Section Additive Manufacturing Technologies)
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39 pages, 3629 KiB  
Review
Radiative Heat Transfer Properties of Fiber–Aerogel Composites for Thermal Insulation
by Mohanapriya Venkataraman, Sebnem Sözcü and Jiří Militký
Gels 2025, 11(7), 538; https://doi.org/10.3390/gels11070538 - 11 Jul 2025
Viewed by 537
Abstract
Fiber–aerogel composites have gained significant attention as high-performance thermal insulation materials due to their unique microstructure, which suppresses conductive, convective, and radiative heat transfer. At room temperature, silica aerogels in particular exhibit ultralow thermal conductivity (<0.02 W/m·K), which is two to three times [...] Read more.
Fiber–aerogel composites have gained significant attention as high-performance thermal insulation materials due to their unique microstructure, which suppresses conductive, convective, and radiative heat transfer. At room temperature, silica aerogels in particular exhibit ultralow thermal conductivity (<0.02 W/m·K), which is two to three times lower than that of still air (0.026 W/m·K). Their brittle skeleton and high infrared transparency, however, restrict how well they insulate, particularly at high temperatures (>300 °C). Incorporating microscale fibers into the aerogel matrix enhances mechanical strength and reduces radiative heat transfer by increasing scattering and absorption. For instance, it has been demonstrated that adding glass fibers reduces radiative heat transmission by around 40% because of increased infrared scattering. This review explores the fundamental mechanisms governing radiative heat transfer in fiber–aerogel composites, emphasizing absorption, scattering, and extinction coefficients. We discuss recent advancements in fiber-reinforced aerogels, focusing on material selection, structural modifications, and predictive heat transfer models. Recent studies indicate that incorporating fiber volume fractions as low as 10% can reduce the thermal conductivity of composites by up to 30%, without compromising their mechanical integrity. Key analytical and experimental methods for determining radiative properties, including Fourier transform infrared (FTIR) spectroscopy and numerical modeling approaches, are examined. The emissivity and transmittance of fiber–aerogel composites have been successfully measured using FTIR spectroscopy; tests show that fiber reinforcement at high temperatures reduces emissivity by about 15%. We conclude by outlining the present issues and potential avenues for future research to optimize fiber–aerogel composites for high-temperature applications, including energy-efficient buildings (where long-term thermal stability is necessary), electronics thermal management systems, and aerospace (where temperatures may surpass 1000 °C), with a focus on improving the materials’ affordability and scalability for industrial applications. Full article
(This article belongs to the Special Issue Synthesis and Application of Aerogel (2nd Edition))
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50 pages, 8944 KiB  
Review
Fire-Resistant Coatings: Advances in Flame-Retardant Technologies, Sustainable Approaches, and Industrial Implementation
by Rutu Patel, Mayankkumar L. Chaudhary, Yashkumar N. Patel, Kinal Chaudhari and Ram K. Gupta
Polymers 2025, 17(13), 1814; https://doi.org/10.3390/polym17131814 - 29 Jun 2025
Viewed by 1502
Abstract
Fire-resistant coatings have emerged as crucial materials for reducing fire hazards in various industries, including construction, textiles, electronics, and aerospace. This review provides a comprehensive account of recent advances in fire-resistant coatings, emphasizing environmentally friendly and high-performance systems. Beginning with a classification of [...] Read more.
Fire-resistant coatings have emerged as crucial materials for reducing fire hazards in various industries, including construction, textiles, electronics, and aerospace. This review provides a comprehensive account of recent advances in fire-resistant coatings, emphasizing environmentally friendly and high-performance systems. Beginning with a classification of traditional halogenated and non-halogenated flame retardants (FRs), this article progresses to cover nitrogen-, phosphorus-, and hybrid-based systems. The synthesis methods, structure–property relationships, and fire suppression mechanisms are critically discussed. A particular focus is placed on bio-based and waterborne formulations that align with green chemistry principles, such as tannic acid (TA), phytic acid (PA), lignin, and deep eutectic solvents (DESs). Furthermore, the integration of nanomaterials and smart functionalities into fire-resistant coatings has demonstrated promising improvements in thermal stability, char formation, and smoke suppression. Applications in real-world contexts, ranging from wood and textiles to electronics and automotive interiors, highlight the commercial relevance of these developments. This review also addresses current challenges such as long-term durability, environmental impacts, and the standardization of performance testing. Ultimately, this article offers a roadmap for developing safer, sustainable, and multifunctional fire-resistant coatings for future materials engineering. Full article
(This article belongs to the Special Issue Flame-Retardant Polymer Composites II)
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13 pages, 2262 KiB  
Article
Application of Bioinspired Structural Ceramics with High-Temperature Electrical Insulation and High Adhesion in K-Type Coaxial Thermocouples
by Zhenyin Hai, Yue Chen, Zhixuan Su, Yemin Wang, Shigui Gong, Yihang Zhang, Shanmin Gao, Chengfei Zhang, Zhangquan Wang, Hongwei Ji, Chenyang Xue and Zhichun Liu
Materials 2025, 18(12), 2901; https://doi.org/10.3390/ma18122901 - 19 Jun 2025
Viewed by 346
Abstract
Surface erosion of the coaxial thermocouple probe initiates continuous bridging of thermoelectric materials on the insulation layer surface, forming new temperature measurement junctions. This inherent ability to measure continuous self-erosion ensures the operational reliability of the coaxial thermocouples in high-temperature ablative environments. However, [...] Read more.
Surface erosion of the coaxial thermocouple probe initiates continuous bridging of thermoelectric materials on the insulation layer surface, forming new temperature measurement junctions. This inherent ability to measure continuous self-erosion ensures the operational reliability of the coaxial thermocouples in high-temperature ablative environments. However, the fabrication of a high-temperature electrical insulation layer and a high-adhesion insulating layer in the coaxial thermocouples remains a challenge. Inspired by calcium carbonate/oxalate crystals in jujube leaves that strengthen the leaves, a bioinspired structural ceramic (BSC) mimicking these needle-like crystals is designed. This BSC demonstrates excellent high-temperature insulation (with insulation impedance of 2.55 kΩ at 1210 °C) and adhesion strength (35.3 Newtons). The BSC is successfully used as the insulating layer in a K-type coaxial thermocouple. The generation rules for surface junctions are systematically studied, revealing that stable and reliable measurement junctions can be created when the sandpaper grit does not exceed 600#. Static test results show that the K-type coaxial thermocouple ranges from 200 °C to 1200 °C with an accuracy of 1.1%, a drift rate better than 0.0137%/h, and hysteresis better than 0.81%. Dynamic test results show that the response time is 1.08 ms. The K-type coaxial thermocouple can withstand a high-temperature flame impact for 300 s at 1200 °C, as well as over forty cycles of high-power laser thermal shock, while maintaining good response characteristics. Therefore, the K-type coaxial thermocouple designed in this study provides an ideal solution for long-term temperature monitoring of the thermal components of aerospace engines under extremely high-temperature, high-speed, and strong thermal shock conditions. Full article
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13 pages, 3556 KiB  
Article
High-Temperature Tensile Grain Evolution and Mechanical Properties of Additively Manufactured TA15 Aerospace Titanium Alloy
by Pengfei Li, Zhenkun Dong, Qingtao Yang, Hao Xu, Dehai Kong and Minghui Hu
Metals 2025, 15(6), 677; https://doi.org/10.3390/met15060677 - 18 Jun 2025
Cited by 1 | Viewed by 355
Abstract
This study investigates the grain characteristics and high-temperature tensile properties of an additively manufactured (AM) TA15 titanium alloy. Directed energy deposition (DED) was utilized for its high material efficiency and design flexibility to explore the alloy’s applicability in aerospace manufacturing, where TA15 is [...] Read more.
This study investigates the grain characteristics and high-temperature tensile properties of an additively manufactured (AM) TA15 titanium alloy. Directed energy deposition (DED) was utilized for its high material efficiency and design flexibility to explore the alloy’s applicability in aerospace manufacturing, where TA15 is valued for its excellent high-temperature performance. A comparative analysis between DED and hot-rolled TA15 alloys was conducted at 25 °C and 600 °C to examine the influence of grain size and crystallographic texture on mechanical behavior. The AM TA15 alloy exhibited superior tensile properties at both temperatures compared to its hot-rolled counterpart. Microstructural analysis revealed finer grain size, stronger α-phase diffraction intensity, and altered grain boundary misorientation in the AM alloy after high-temperature testing, accompanied by improved plasticity. These findings highlight the potential of thermal process optimization and microstructural tailoring to enhance the high-temperature performance of AM TA15, offering valuable insights for the fabrication of critical aerospace components. Full article
(This article belongs to the Special Issue Machining, Grinding, and Laser Processing of Metallic Materials)
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16 pages, 5105 KiB  
Article
On the Effect of the Cell Size and Beam Radius on the Compressive Strength and Residual Stresses of Ti-6Al-4V BCC Lattice Sandwich Structures Manufactured by L-PBF
by Gaetano Pollara, Dina Palmeri, Roberto Licari and Antonio Barcellona
J. Manuf. Mater. Process. 2025, 9(6), 192; https://doi.org/10.3390/jmmp9060192 - 10 Jun 2025
Viewed by 545
Abstract
Lattice structures offer the possibility to obtain lightweight components with additional functionalities, improving their shock absorption and thermal exchange properties. Recently, a body-centered cubic (BCC) lattice structure has been used to fabricate metal lattice sandwich panels (MLSPs) for aerospace applications. MLSPs are made [...] Read more.
Lattice structures offer the possibility to obtain lightweight components with additional functionalities, improving their shock absorption and thermal exchange properties. Recently, a body-centered cubic (BCC) lattice structure has been used to fabricate metal lattice sandwich panels (MLSPs) for aerospace applications. MLSPs are made of two external skins and a lattice core and can be produced thanks to laser powder bed fusion technology (LPBF), which is characterized by its superior printing accuracy with respect to other additive manufacturing processes for metals. Since few studies can be found in the literature on Ti-6Al-4V MLSPs, further work is needed to evaluate the mechanical response of these panels. Moreover, due to their design complexity and to avoid a costly experimental campaign, numerical simulation could be used to encourage the industrial application of these structures. In this paper, different cell configurations were printed and tested in compression to study the influence of the cell’s geometrical parameters, i.e., the cell size and beam radius, on the mechanical response of MLSPs. Numerical simulations of the LPBF of these geometries were also carried out to understand how the residual stresses can be varied by varying the cell configuration. A geometrical evaluation was carried out to quantitatively express the influence of the beam radius and cell size on the resulting volume fraction, which strongly influences the mechanical behavior and residual stress profiles of MLSPs. From the analysis, we found that the C2-R0.35 sample resulted in the configuration with the highest compressive strength, while C3-R0.25 showed the lowest and most uniform residual stress profile. Full article
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19 pages, 2560 KiB  
Article
Investigation of the Combustion Products of Ionic Liquid-Based Green Propellants Using Infrared Spectroscopy
by Jacob Oberndorfer, Philipp Teuffel, Sophie C. Stölzle, Dominic Freudenmann and Christoph U. Kirchberger
Aerospace 2025, 12(6), 507; https://doi.org/10.3390/aerospace12060507 - 3 Jun 2025
Viewed by 367
Abstract
In rocketry today, conventional hypergolic propellant combinations typically use hydrazine-derived fuels and oxidizers based on nitrogen tetroxide. Due to their high toxicity and consequently expensive handling, safer alternatives, so-called “green hypergolics”, are currently being developed. The ionic liquid-based fuels [EMIM][SCN], HIP_11 and HIM_30, [...] Read more.
In rocketry today, conventional hypergolic propellant combinations typically use hydrazine-derived fuels and oxidizers based on nitrogen tetroxide. Due to their high toxicity and consequently expensive handling, safer alternatives, so-called “green hypergolics”, are currently being developed. The ionic liquid-based fuels [EMIM][SCN], HIP_11 and HIM_30, paired with highly concentrated hydrogen peroxide as an oxidizer, are three candidates for such green hypergolics, which are currently under research at the German Aerospace Center (DLR). These combinations have been shown to exhibit reliable hypergolic ignition. For a better understanding of the reaction process and to assess the risks in working with these propellants, it is desirable to determine their combustion products. A test setup was designed to extract the gaseous combustion products from hypergolic drop tests. The gas samples were analyzed using Fourier-transform infrared spectroscopy and the gaseous combustion products were determined from the infrared spectra. Additional tests with varied oxidizer concentration or alternative fuels were conducted to further investigate detailed aspects of the findings. It was concluded that [EMIM][SCN], HIP_11 and HIM_30 produce very similar sets of combustion products with hydrogen peroxide, including water vapor, carbon dioxide, carbon monoxide, hydrogen cyanide and sulfur dioxide. Finally, the combustion products were compared to the substances produced when thermally decomposing the fuels. This confirmed that the previously detected substances were caused by a reaction between hydrogen peroxide and the fuels, rather than by their thermal decomposition due to heating. Full article
(This article belongs to the Section Astronautics & Space Science)
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19 pages, 10561 KiB  
Article
Environmental Effects of Moisture and Elevated Temperatures on the Mode I and Mode II Interlaminar Fracture Toughness of a Toughened Epoxy Carbon Fibre Reinforced Polymer
by Anna Williams, Ian Hamerton and Giuliano Allegri
Polymers 2025, 17(11), 1503; https://doi.org/10.3390/polym17111503 - 28 May 2025
Cited by 1 | Viewed by 628
Abstract
The use of composite materials within extreme environments is an exciting frontier in which a wealth of cutting-edge developments have taken place recently. Although there is vast knowledge of composites’ behaviour in standard room temperature and humidity, there is a great need to [...] Read more.
The use of composite materials within extreme environments is an exciting frontier in which a wealth of cutting-edge developments have taken place recently. Although there is vast knowledge of composites’ behaviour in standard room temperature and humidity, there is a great need to understand their performance in ‘hot/wet’ conditions, as these are the conditions of their envisaged applications. One of the key failure mechanisms within composites is interlaminar fracture, commonly referred to as delamination. The environmental effects of moisture and elevated temperatures on interlaminar fracture toughness are therefore essential design considerations for laminated aerospace-grade composite materials. IM7/8552, a toughened epoxy/carbon fibre reinforced polymer, was experimentally characterised in both ‘Dry’ and ‘Wet’ conditions at 23 °C and 90 °C. A moisture uptake study was conducted during the ‘Wet’ conditioning of the material in a 70 °C/85% relative humidity environment. Dynamic mechanical thermal analysis was carried out to determine the effect of moisture on the glass transition temperature of the material. Mode I initiation and propagation fracture properties were determined using double cantilevered beam specimens and Mode II initiation fracture properties were deduced using end-notched flexure specimens. The effects of precracking and the methodology of high-temperature testing are discussed in this report. Mode I interlaminar fracture toughness, GIC, was found to increase with elevated temperatures and moisture content, with GIC=0.205kJ/m2 in ‘Dry 23 °C’ conditions increasing by 26% to GIC=0.259kJ/m2 in ‘Wet 90 °C’ conditions, demonstrating that the material exhibited its toughest behaviour in ‘hot/wet’ conditions. Increased ductility due to matrix softening and fibre bridging caused by temperature and moisture were key contributors to the elevated GIC values. Mode II interlaminar fracture toughness, GIIC, was observed to decrease most significantly when moisture or elevated temperature was applied individually, with the combination of ‘hot/wet’ conditions resulting in an 8% drop in GIIC, with GIIC=0.586kJ/m2 in ‘Dry 23 °C’ conditions and GIIC=0.541kJ/m2 in ‘Wet 90 °C’ conditions. The coupled effect of fibre-matrix interface degradation and increased plasticity due to moisture resulted in a relatively small knockdown on GIIC compared to GIC in ‘hot/wet’ conditions. Fractographic studies of the tested specimens were conducted using scanning electron microscopy. Noteworthy surface topography features were observed on specimens of different fracture modes, moisture saturation levels, and test temperature conditions, including scarps, cusps, broken fibres and river markings. The qualitative features identified during microscopy are critically examined to extrapolate the differences in quantitative results in the various environmental conditions. Full article
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13 pages, 3608 KiB  
Article
Symmetrical Configuration Design and Experimental Study of a Repeatable Stowing Deployment Flexible Solar Array
by Lei Cheng, Aoxiang Zhang, Qifeng Cui, Desheng Wan, Zhexiao Ye and Peng Yue
Symmetry 2025, 17(6), 822; https://doi.org/10.3390/sym17060822 - 25 May 2025
Viewed by 440
Abstract
Compared with the traditional rigid solar wings, flexible solar arrays are characterized by light weight and high stowing/deployment ratio, and the repeatable stowing/deployment flexible solar arrays have become one of the hotspots of solar arrays research in the aerospace field. As integrated rigid–flexible [...] Read more.
Compared with the traditional rigid solar wings, flexible solar arrays are characterized by light weight and high stowing/deployment ratio, and the repeatable stowing/deployment flexible solar arrays have become one of the hotspots of solar arrays research in the aerospace field. As integrated rigid–flexible structures, flexible solar arrays face risks of repeatable stowing/deployment function failure due to the nonlinear force-heat coupling effects. This paper takes symmetry as the core design concept, and through the introduction of rotationally symmetric sector layout, material stacking, and the stowing/deployment mechanism, the thermal response of flexible solar arrays under extreme thermal environments was systematically investigated, which significantly improves thermal distribution uniformity of the flexible solar arrays and provides a new way of solving the problem of repeatable stowing/deployment of flexible solar arrays. Furthermore, we propose a high- and low-temperature unfolding test method for fan-shaped flexible solar arrays, which verifies the reliability of symmetric fan-shaped arrays in high and low temperatures during the working process of repeatable stowing/deployment and the safety of the stowing/deployment process, as well as providing a reference for the subsequent design and test of flexible solar arrays of other configurations. Full article
(This article belongs to the Special Issue Symmetry in Aerospace Sciences and Applications)
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26 pages, 7824 KiB  
Article
Microstructural Synergy of ZrC-NbC Reinforcements and Its Coupled Effects on Mechanical and Dynamic Properties of Titanium Matrix Composites
by Juan Wang, Haijun Zhang, Baiqing Zhou and Zhong Yang
Metals 2025, 15(6), 573; https://doi.org/10.3390/met15060573 - 22 May 2025
Viewed by 407
Abstract
In aerospace applications, titanium matrix composites (TMCs) must balance high strength, thermal stability, and vibration resistance. This study investigates the microstructural evolution and multi-property correlations in single-phase ZrC-reinforced (TMC1) and dual-phase ZrC-NbC-co-reinforced (TMC2) TMCs via SEM/TEM, XRD, tensile testing, and ANSYS simulations. The [...] Read more.
In aerospace applications, titanium matrix composites (TMCs) must balance high strength, thermal stability, and vibration resistance. This study investigates the microstructural evolution and multi-property correlations in single-phase ZrC-reinforced (TMC1) and dual-phase ZrC-NbC-co-reinforced (TMC2) TMCs via SEM/TEM, XRD, tensile testing, and ANSYS simulations. The in situ reaction (Ti + ZrC/NbC → TiC + Zr/Nb) and NbC-induced grain boundary pinning drive microstructural optimization in TMC2, achieving 30% higher reinforcement homogeneity and 5 μm grain refinement from 15 μm to 10 μm. TMC2’s tensile strength reaches 1210 MPa, a 15% increase over TMC1, with an elongation at a break of 4.74%, 2.2 times that of TMC1. This performance stems from synergistic Hall–Petch strengthening and nano-TiC dispersion strengthening. Modal simulations show TMC2 exhibits a first-mode natural frequency of 98.5 kHz, 1.1% higher than TMC1’s 97.4 kHz, with maximum displacement reduced by 2.3%. These improvements correlate with TMC2’s elevated elastic modulus (125 GPa vs. 110 GPa) and uniform mass/stiffness distribution. The ZrC-NbC synergy establishes a microstructural framework for the concurrent enhancement of static and dynamic properties, offering critical insights for a high-performance TMC design in extreme environments. Full article
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21 pages, 8395 KiB  
Article
Deep Artificial Neural Network Modeling of the Ablation Performance of Ceramic Matrix Composites in the Hydrogen Torch Test
by Jayanta Bhusan Deb, Christopher Varela, Fahim Faysal, Yiting Wang, Chiranjit Maiti and Jihua Gou
J. Compos. Sci. 2025, 9(5), 239; https://doi.org/10.3390/jcs9050239 - 13 May 2025
Viewed by 748
Abstract
In recent years, there has been increasing interest in new materials such as ceramic matrix composites (CMCs) for power generation and aerospace propulsion applications through hydrogen combustion. This study employed a deep artificial neural network (DANN) model to predict the ablation performance of [...] Read more.
In recent years, there has been increasing interest in new materials such as ceramic matrix composites (CMCs) for power generation and aerospace propulsion applications through hydrogen combustion. This study employed a deep artificial neural network (DANN) model to predict the ablation performance of CMCs in the hydrogen torch test (HTT). The study was conducted in three phases to increase the accuracy of the model’s predictions. Initially, to predict the thermal behavior of ceramic composites, two linear machine learning models were used known as Lasso and Ridge regression. In the second step, four decision tree-based ensemble machine learning models, namely random forest, gradient boosting regression, extreme gradient boosting regression, and extra tree regression, were used to improve the prediction accuracy metrics, including root mean square error (RMSE), mean absolute error (MAE), correlation coefficient (R2 score), and mean absolute percentage error (MAPE), relative to the previously introduced linear models. Finally, to forecast the thermal stability of CMCs with time, an optimized DANN model with two hidden layers having rectified linear unit activation function was developed. The data collection procedure involved preparing CMCs with continuous Yttria-Stabilized Zirconia (YSZ) fibers and silicon carbide (SiC) matrix using a polymer infiltration and pyrolysis (PIP) technique. The samples were exposed to a hydrogen flame at a high heat flux of 183 W/cm2 for a duration of 10 min. A good agreement between the DANN model’s predictions and experimental data with an R2 score of 0.9671, RMSE of 16.45, an MAE of 14.07, and an MAPE of 3.92% confirmed the acceptability of the developed neural network model in this study. Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2025)
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21 pages, 12040 KiB  
Article
Electrically Conductive Nanoparticle-Enhanced Epoxy Adhesives for Localised Joule Heating-Based Curing in Composite Bonding
by Karina Dragasiute, Gediminas Monastyreckis and Daiva Zeleniakiene
Polymers 2025, 17(9), 1176; https://doi.org/10.3390/polym17091176 - 25 Apr 2025
Viewed by 650
Abstract
This study investigates the application of carbon nanotube (CNT)-enhanced epoxy adhesives for localised Joule heating-based curing in composite bonding. The electrical, thermal, and mechanical properties of epoxy with 0.25–1 wt% CNT loadings were evaluated. A simple CNT alignment method using DC voltage showed [...] Read more.
This study investigates the application of carbon nanotube (CNT)-enhanced epoxy adhesives for localised Joule heating-based curing in composite bonding. The electrical, thermal, and mechanical properties of epoxy with 0.25–1 wt% CNT loadings were evaluated. A simple CNT alignment method using DC voltage showed improved electrical conductivity, greatly reducing the percolation threshold. Transient thermal analysis using finite element modelling of representative volume elements revealed that aligned CNTs led to increased localised temperatures near the CNT clusters. The model was validated with infrared thermal imaging analysis, which also showed similar non-linear heat distribution and more uniform heating under higher CNT loading. Additionally, power distribution mapping was evaluated through inverse modelling techniques, suggesting different conductivity zones and cluster distribution within the single-lap joint. The numerical and experimental results demonstrated that CNT alignment significantly enhanced localised conductivity, thereby improving curing efficiency at lower voltages. The lap shear test results showed a peak shear strength of 10.16 MPa at 0.5 wt% CNT loading, 9% higher than pure epoxy. Scanning electron microscopy analysis confirmed the formation of aligned CNT clusters, and how CNT loading affected the failure modes, transitioning from cohesive to void-rich fracture patterns at a higher wt%. These findings establish CNT-enhanced Joule heating as a viable and scalable alternative for efficient composite bonding in aerospace and structural applications. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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16 pages, 4872 KiB  
Article
Experimental Study on the Effects of Thermal Cycling and Ultraviolet Irradiation on Stable Characteristics of Carbon Fiber/Bismaleimide Polymer Composite Shells
by Zheng Zhang, Xinyue Ji, Min Sun, Libin Xiong, Guang Zhang, Wenjie Ding, Jiquan Li and Shaofei Jiang
Materials 2025, 18(9), 1942; https://doi.org/10.3390/ma18091942 - 24 Apr 2025
Viewed by 380
Abstract
Carbon fiber/epoxy composites are widely used in aerospace due to their strength and ease of fab weatherrication, but they suffer from glass transition at high temperatures. In contrast, carbon fiber/bismaleimide composites exhibit superior thermal stability, irradiation resistance, and toughness. This study investigates the [...] Read more.
Carbon fiber/epoxy composites are widely used in aerospace due to their strength and ease of fab weatherrication, but they suffer from glass transition at high temperatures. In contrast, carbon fiber/bismaleimide composites exhibit superior thermal stability, irradiation resistance, and toughness. This study investigates the effects of thermal cycling and UV irradiation on carbon fiber/bismaleimide composite shells. Anti-symmetric shells with varying ply angles were tested under two-point tensile loading. Results show that these shells maintain stability between −70 °C and 180 °C, outperforming epoxy-based composites. This research offers valuable insights for aerospace applications of such bistable shells under thermal and UV aging conditions. Full article
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