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Open AccessArticle

Controlled Stepwise Synthesis and Characterization of a Ternary Multicomponent Crystal with 2-Methylresorcinol

1
Universitaet Duesseldorf, Inorganic Chemistry, Universitaetsstrasse 1, 40225 Düsseldorf, Germany
2
Solid-Chem GmbH, Universitätstrasse 136, 44799 Bochum, Germany
3
Inorganic Chemistry, Ruhr-University Bochum, Inorganic Chemistry 1, Universitaetstrasse 150, 44801 Bochum, Germany
*
Author to whom correspondence should be addressed.
Chemistry 2020, 2(1), 93-100; https://doi.org/10.3390/chemistry2010009
Received: 6 February 2020 / Revised: 27 February 2020 / Accepted: 28 February 2020 / Published: 4 March 2020
(This article belongs to the Special Issue Supramolecular Chemistry in the 3rd Millennium)
A typical approach of a multicomponent crystal design starts with a retrosynthetic analysis of the target molecule followed by a one-pot reaction of all components. To develop protocols for multicomponent crystal syntheses, controlled stepwise syntheses of a selected crystalline ternary multicomponent system 1 involving 2-methylresorcinol (MRS), tetramethyl-pyrazine (TMP), and 1,2-bis(4-pyridyl)ethane (BPE) are presented. The obtained binary cocrystals 2 (involving MRS and TMP) and 3 (involving MRS and BPE) as well as the final resulting ternary multicomponent system 1 were characterized by X-ray analysis. View Full-Text
Keywords: multicomponent cocrystal; cocrystallization mechanism; cocrystal synthesis multicomponent cocrystal; cocrystallization mechanism; cocrystal synthesis
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MDPI and ACS Style

Komisarek, D.; Schauerte, C.; Merz, K. Controlled Stepwise Synthesis and Characterization of a Ternary Multicomponent Crystal with 2-Methylresorcinol. Chemistry 2020, 2, 93-100.

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