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Separations, Volume 12, Issue 2

2025 February - 37 articles

Cover Story: Lignin and hemicellulose are selectively separated from soy products (meal, flakes, and hulls) using imidazolium ionic liquids. Special emphasis is placed on hulls, which currently are strictly considered as waste products. Hemicellulose and lignin components are cleanly isolated from each other. Fourier-transform infrared spectroscopy and pyrolysis–gas chromatography/mass spectrometry characterization of degraded lignin identified the H-, G-, and S-components of lignin building blocks. As much as 19% of soybean hull is composed of lignin. View this paper
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Articles (37)

  • Article
  • Open Access
1 Citations
1,697 Views
21 Pages

Experimental Study on Brine Storage for Overwintering by Using Salinity-Gradient Solar Pond in Zabuye Salt Lake, Tibet

  • Qian Wu,
  • Yunsheng Wang,
  • Jintao Zhang,
  • Ke Zhang,
  • Juntao Li,
  • Zhikui He,
  • Lingzhong Bu,
  • Jiangjiang Yu and
  • Zhen Nie

Known as the “white oil”, lithium is a key raw material to support strategic emerging industries and future industrial development. Zabuye Salt Lake is the only one in Tibet, China that has so far realized the industrialization of lithium...

  • Article
  • Open Access
3 Citations
1,996 Views
13 Pages

Trimethylamine-N-oxide (TMAO) is associated with various chronic diseases. TMAO is a downstream oxidative metabolite of trimethylamine (TMA) that is generated by the gut microbiota from dietary choline, carnitine, and betaine. Current analytical meth...

  • Review
  • Open Access
12 Citations
11,928 Views
43 Pages

The increasing global demand for critical minerals, driven by rapid population growth and the widespread adoption of low-carbon technologies, electric vehicles, and clean energy systems, highlights the urgent need for sustainable resource management....

  • Review
  • Open Access
29 Citations
8,368 Views
23 Pages

A Review of Hydrogel Application in Wastewater Purification

  • Lilyan Alsaka,
  • Lina Alsaka,
  • Ali Altaee,
  • Syed Javaid Zaidi,
  • John Zhou and
  • Tayma Kazwini

Hydrogels have garnered considerable interest in water purification owing to their distinctive physicochemical characteristics, including high porosity, modifiable surface chemistry, and superior water retention capacity. This paper provides a thorou...

  • Article
  • Open Access
7 Citations
2,280 Views
16 Pages

Research on the Flow Field Characteristics of the Industrial Elliptical Cyclone Separator

  • Yongli Zhang,
  • Kangshuo Li,
  • Kaixuan Zhang,
  • Guangfei Zhu,
  • Zhanpeng Sun and
  • Jianfang Shi

A new type of elliptical cyclone separator has been proposed recently, but the flow field characteristics within the industrial device still need to be further investigated. In this paper, the characteristics of the flow field and particle motion ins...

  • Article
  • Open Access
1,473 Views
15 Pages

Exploring the Photocatalytic Efficiency of Heterostructured TiO2 Nanobelts for Emerging Liquid Contaminants in Different Water Matrices

  • Humaira Asghar,
  • Daphne Hermosilla,
  • Antonio Gascó,
  • Valter Maurino and
  • Muhammad Ahsan Iqbal

This study reports the development of shape-controlled TiO2 (B)/anatase heterostructures for the degradation of emerging environmental pollutants, including phenol, methomyl (insecticides), and diclofenac sodium (drug), under UV-visible-light irradia...

  • Article
  • Open Access
1,722 Views
20 Pages

In this paper, the separation characteristics of mist remover in a wet flue gas desulfurization system are numerically simulated, and the separation mechanism in the channel of mist remover is analyzed considering the influence of droplets on wall re...

  • Article
  • Open Access
6 Citations
7,760 Views
10 Pages

Detection of Honey Adulteration by Liquid Chromatography—High-Resolution Mass Spectrometry: Results from an EU Coordinated Action

  • Viviana Paiano,
  • Andreas Breidbach,
  • Carolin Lörchner,
  • Tereza Ždiniaková,
  • Olivier De Rudder,
  • Alain Maquet,
  • Lourdes Alvarellos and
  • Franz Ulberth

Honey, a sweet and nutritious food produced by honeybees, is extensively consumed by humans due to its potential health benefits. Unfortunately, the adulteration of honey with inexpensive sugar syrups is a prevalent issue. Verifying the authenticity...

  • Article
  • Open Access
1,822 Views
14 Pages

We have designed, built, and characterized an inexpensive gas chromatograph with photoionization detection using readily commercially available components. These include a home carbonation CO2 cylinder for the carrier gas, headspace sampling using a...

  • Article
  • Open Access
5 Citations
4,435 Views
12 Pages

Recycling of Multilayer Flexible Packaging Waste Through Delamination with Recoverable Switchable Hydrophilicity Solvents

  • Roberta Mastroddi,
  • Chiara Samorì,
  • Martina Vagnoni,
  • Chiara Gualandi,
  • Paola Galletti and
  • Emilio Tagliavini

Multilayer flexible packaging wastes (MFPWs) consist of complex materials composed of multiple plastic films, which are often laminated with aluminum foil, and they constitute a large portion of packaging waste. The use of several polymeric layers is...

  • Article
  • Open Access
2 Citations
3,334 Views
15 Pages

Besides the well-known hallucinogenic ketamine, various novel ketamine derivatives are available on the illicit drug market, sold as designer drugs. Minor chemical changes to the parent compound aim to circumvent existing narcotic drug laws while mim...

  • Article
  • Open Access
1,030 Views
13 Pages

Investigations into Effects of Inclined Channels on the Forced Foam Drainage

  • Yumeng Deng,
  • Miao Jin,
  • Lisha Dong,
  • Jiakun Tan and
  • Chao Ni

Gangue particle entrainment during flotation remains a significant challenge in mineral processing. Previous studies have shown that incorporating inclined plates into the froth zone can reduce the recovery of fine gangue particles. However, the effe...

  • Article
  • Open Access
3 Citations
1,348 Views
20 Pages

In Situ N-Doped Low-Corrosion Porous Carbon Derived from Biomass for Efficient CH4/N2 Separation

  • Huihui Wang,
  • Yuqiong Zhao,
  • He Lian,
  • Qi Wang,
  • Zhihong Shang and
  • Guojie Zhang

The separation of CH4 and N2 is essential for the effective use of low-concentration coalbed methane (CBM). In this study, a series of nitrogen-doped porous carbons were synthesized using an in situ nitrogen doping method combined with K2CO3 activati...

  • Review
  • Open Access
1 Citations
4,422 Views
19 Pages

Techniques and Methods for Fatty Acid Analysis in Lipidomics: Exploring Pinus cembroides Kernels as a Sustainable Food Resource

  • Luis Ricardo León-Herrera,
  • Luis Miguel Contreras-Medina,
  • Ana Angélica Feregrino-Pérez,
  • Christopher Cedillo,
  • Genaro Martín Soto-Zarazúa,
  • Miguel Angel Ramos-López,
  • Samuel Tejeda,
  • Eduardo Amador-Enríquez and
  • Enrique Montoya-Morado

The large-scale conversion of forests to agriculture has caused biodiversity loss, climate change, and disrupted dietary fatty acid balances, with adverse public health effects. Wild edibles like pine nuts, especially Pinus cembroides, provide sustai...

  • Article
  • Open Access
4 Citations
1,873 Views
15 Pages

Synthesis of Zeolitic Imidazolate Framework-8 from Waste Electrodes via Ball Milling for Efficient Uranium Removal

  • Minhua Su,
  • Jinyao Zhu,
  • Ruoning Wu,
  • Jiaqi Pan,
  • Jingran Yang,
  • Jiaxue Zhao,
  • Diyun Chen,
  • Changzhong Liao,
  • Kaimin Shih and
  • Shengshou Ma

Developing a cost-effective approach for the remediation of wastewater containing uranyl [U(VI)] ions is essentially important to ecosystems and human health. In this study, a Zn-based ZIF-8 framework was fabricated from wasted batteries through an e...

  • Article
  • Open Access
5 Citations
1,923 Views
11 Pages

Exploring Chicken Feathers as a Cost-Effective Adsorbent for Aqueous Dye Removal

  • Marcela Caovilla,
  • Carolina E. Demaman Oro,
  • Rúbia Mores,
  • Luciana D. Venquiaruto,
  • Marcelo L. Mignoni,
  • Marco Di Luccio,
  • Helen Treichel,
  • Rogério Marcos Dallago and
  • Marcus V. Tres

This study explored the use of chicken feathers, a low-cost and abundant agricultural byproduct, as a sorbent for the removal of reactive yellow dye from aqueous solutions. The dual potential of feathers as both adsorbents and sorbents, attributed to...

  • Article
  • Open Access
2 Citations
1,096 Views
13 Pages

Preparation, Characterization, and Mechanism of SMS Titanium–Manganese Nanocomposite for Antimony Removal from Water

  • Yannan Lv,
  • Wenqing Wen,
  • Shenrui Han,
  • Kaixin Li,
  • Ziyu Fu,
  • Fansong Mu and
  • Meng Luo

This study investigates the synthesis of SMS-Ti-Mn (SMS-Ti-Mn stands for spent mushroom substrate activated carbon-Ti-Mn) nanocomposites and their application in removing the heavy metal antimony from water. In the process of antimony mining and smel...

  • Article
  • Open Access
4 Citations
1,437 Views
12 Pages

The use of ionic liquids in biomass pretreatment for ethanol production has seen increased attention in recent years. In this work, 1-butyl-3-methylimidazolium chloride ([Bmim]Cl), 1-allyl-3-methylimidazolium chloride ([Amim]Cl), and 1-ethyl-3-methyl...

  • Article
  • Open Access
3 Citations
5,367 Views
18 Pages

Investigation of Impurities in Peptide Pools

  • Gaby Bosc-Bierne and
  • Michael G. Weller

Peptide pools are important research tools in different biomedical fields. They consist of a complex mixture of defined peptides, which places high demands on the production and quality control of these products. Previously it has been shown that the...

  • Article
  • Open Access
1 Citations
1,781 Views
22 Pages

Critical Insights into Untargeted GC-HRMS Analysis: Exploring Volatile Organic Compounds in Italian Ambient Air

  • Marina Cerasa,
  • Catia Balducci,
  • Benedetta Giannelli Moneta,
  • Serena Santoro,
  • Mattia Perilli and
  • Vladimir Nikiforov

This study critically examines the workflow for untargeted analysis of volatile organic compounds (VOCs) in ambient air, from sampling strategies to data interpretation by using GC-HRMS. While untargeted approaches are well-established in liquid chro...

  • Article
  • Open Access
1,565 Views
18 Pages

Optimizing Quercetin Extraction from Taraxacum mongolicum Using Ionic Liquid–Enzyme Systems and Network Pharmacology Analysis

  • Jingwei Hao,
  • Yifan Sun,
  • Nan Dong,
  • Yingying Pei,
  • Xiangkun Zhou,
  • Yi Zhou and
  • Heming Liu

Quercetin in Taraxacum mongolicum was extracted by ultrasound-assisted extraction in synergy with an ionic liquid–enzyme complex system, and the antioxidant function of quercetin was investigated based on network pharmacology. From 1-butyl-3-me...

  • Review
  • Open Access
6 Citations
5,020 Views
20 Pages

Research Progress in Tritium Processing Technologies: A Review

  • Ziqian Zhao,
  • Yandong Sun,
  • Qi Chen,
  • Tianchi Li,
  • Fang Liu,
  • Taihong Yan and
  • Weifang Zheng

Recent advancements in tritium separation technologies have significantly improved efficiency, particularly through the integration of vapor phase catalytic exchange (VPCE), liquid phase catalytic exchange (LPCE), and combined electrolysis catalytic...

  • Review
  • Open Access
8 Citations
7,111 Views
29 Pages

Production of Algae-Derived Biochar and Its Application in Pollutants Adsorption—A Mini Review

  • Luyang Li,
  • Jinfeng Wang,
  • Weiming Sun,
  • Xinhong Peng and
  • Xinhua Qi

Developing algae cultivation for food, chemicals, and bio-energy generates a significant amount of algal waste/residue after utilization. Meanwhile, harmful algal blooms caused by abnormal proliferation of various algae produce a large amount of alga...

  • Article
  • Open Access
1 Citations
1,416 Views
13 Pages

Cyclone separation is a widely utilized separation technique, which enables the self-rotation behaviors of particles in the internal flow field, in order to realize high-performance separation of mixtures. Oily sludges are solid wastes generated by t...

  • Technical Note
  • Open Access
3 Citations
1,753 Views
23 Pages

The gradual increase in water scarcity due to depletion and/or inadequate use of water resources has affected the automotive sector. In this context, possibilities for water reuse in the pre-treatment tunnel in an automotive painting process were stu...

  • Article
  • Open Access
3,114 Views
16 Pages

Effect of Washing Process on the Release of Microplastics from Polyester Fabrics

  • Tanja Pušić,
  • Nino Dimitrov,
  • Ana Šaravanja,
  • Ivona Vidić Štrac and
  • Tihana Dekanić

Microplastics (MP), consisting of particles under 5 mm in size, and fibrous microplastics (FMPs), which originate from textiles and are shed during the washing process, are acknowledged as a new and expanding category of pollutants. This study aimed...

  • Article
  • Open Access
1 Citations
1,918 Views
20 Pages

Strengthened Effect of Surface-Active Ionic Liquids on Curcumin Solubility and Extraction Performance of Curcuminoids

  • Dan Li,
  • Yuxin Qin,
  • Jingxing Li,
  • Subhan Mahmood,
  • Jianqin Shi,
  • Yu Cao and
  • Shun Yao

As a kind of bioactive component in the rhizome of natural plant Curcuma longa L. (turmeric), curcumin is almost insoluble in water at neutral and acidic pH, which limits its further utilization and development. At the same time, traditional extracti...

  • Article
  • Open Access
1 Citations
1,911 Views
13 Pages

Electromigration Separation of Lithium Isotopes with the Benzo-12-Crown-4-Ether (B12C4) System

  • Zhiyu Zhao,
  • Lianjing Mao,
  • Tianyu Zheng,
  • Xiao Li,
  • Chunsen Ye,
  • Pengrui Zhang,
  • Huifang Li,
  • Wei Sun and
  • Jinhe Sun

Enriched lithium isotopes (6Li and 7Li) are essential in the nuclear energy industry, where 6Li is bombarded with neutrons to produce tritium for fusion reactions, while 7Li is used as a core coolant and pH regulator. Separation of 6Li and 7Li by ele...

  • Article
  • Open Access
1 Citations
2,650 Views
13 Pages

A simple method has been developed for the simultaneous analysis of ibuprofen (acid drug), and salbutamol and atenolol (basic drugs) in urine samples at concentrations of 0.40 µg·mL−1. Simultaneous chromatographic separation has be...

  • Article
  • Open Access
1 Citations
3,679 Views
17 Pages

Green Chemistry Method for Analyzing Bisphenol A in Milk

  • Angela M. Encerrado Manriquez and
  • Wen-Yee Lee

A simple, fast, green, and sensitive method for determining Bisphenol A (BPA) levels in commercial milk was developed using a solventless sample preparation technique known as stir bar sorptive extraction, coupled with thermal desorption–gas ch...

  • Article
  • Open Access
2 Citations
1,445 Views
16 Pages

Efficient Separation of Hydroxylamine from Metal Ions by PIM-ED Process

  • Lilei Yang,
  • Zhongwei Ding,
  • Zhengtao Zhu and
  • Weidong Zhang

Selective separation of hydroxylamine (HA) from metal ions to prepare high-purity HA remains a challenge. In this study, given that HA can react with carbonyl compounds, TTA (thenoyltrifluoroacetone) was screened as a carrier to prepare the polymer i...

  • Article
  • Open Access
1 Citations
2,114 Views
14 Pages

Antimicrobial Steroids from Poisonous Mushroom Gymnopilus orientispectabilis and Their Molecular Docking Studies

  • Bowon Jung,
  • Eun Jin Heo,
  • Dieu Linh Nguyen,
  • Ui Joung Youn,
  • Ki Hyun Kim,
  • Boram Son and
  • Seulah Lee

In this study, three fungal steroids (13) were isolated from the fruiting bodies of the poisonous mushroom Gymnopilus orientispectabilis, based on bioactivity-guided isolation methods. The chemical structures of the isolates (13) were d...

  • Article
  • Open Access
1 Citations
1,230 Views
15 Pages

A comprehensive understanding of the compositions and physicochemical properties of coal-based liquids is conducive to the rapid development of multipurpose, high-performance, and high-value functional chemicals. However, because of their complex com...

  • Review
  • Open Access
7 Citations
6,292 Views
21 Pages

Plant Sample Preparation for Metabolomics, Lipidomics, Ionomics, Fluxomics, and Peptidomics

  • Walace Breno da Silva,
  • Gabriel Felipe Hispagnol,
  • Emanuel Victor dos Santos Nunes,
  • Ian Castro-Gamboa and
  • Alan Cesar Pilon

Plant metabolomics, lipidomics, ionomics, fluxomics, and peptidomics are essential approaches for exploring how plants respond to epigenetic, pathological, and environmental stimuli through comprehensive chemical profiling. Over the past decades, sig...

  • Review
  • Open Access
5 Citations
2,766 Views
24 Pages

For the past few years, biochar has emerged as a promising material for the removal of various pollutants from aquatic environments, owing to its advantageous characteristics, such as tunable porosity, abundant surface functional groups, ease of modi...

  • Article
  • Open Access
2 Citations
3,758 Views
14 Pages

Development of a Validated HPLC-UV Method for the Determination of Panthenol, Hesperidin, Rutin, and Allantoin in Pharmaceutical Gel-Permeability Study

  • Sofia Almpani,
  • Pavlina-Ioanna Agiannitou,
  • Paraskevi Kyriaki Monou,
  • Georgios Kamaris and
  • Catherine K. Markopoulou

A pressure ulcer is the necrosis of the skin and tissues due to prolonged pressure. Its prevention and treatment are of great importance not only for the health but also for the patient’s quality of life and are considered the highest priority....

  • Article
  • Open Access
4 Citations
2,370 Views
13 Pages

In this study, ZnO nanoparticles (ZnO NPs) were synthesized using a green method employing fresh Citrus aurantium L. aqueous extract (CA) as a reducing agent. After preparation, the ZnO NPs were characterized by transmission electron microscopy (TEM)...

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Separations - ISSN 2297-8739