March 2003 - 16 articles
A sample (0.85 mL, 6.5 mmol) of formic acid-acetic anhydride mixture (FAM), prepared from Ac2O and formic acid as described in the literature [1], was added to the alcohol 1 [2](255 mg, 0.79 mmol) at 10 ºC.[...]
Acetic anhydride (0.53 mL, 5.61 mmol) and N,N-dimethylaminopyridine (17 mg, 0.14 mmol) were added to a stirred solution of the alcohol 1 (442 mg, 1.31 mmol) in freshly distilled triethylamine (1.3 mL) [1].[...]
A sample (0.10 mL, 1.27 mmol) of formic acid-acetic anhydride mixture (FAM), prepared from Ac2O and formic acid as described in the literature [1], was added to the alcohol 1 [2] (83 mg, 0.25 mmol) at 10 ºC.[...]
A sample (0.03 mL, 0.45 mmol) of formic acid-acetic anhydride mixture (FAM), prepared from Ac2O and formic acid as described in the literature [1], was added to the alcohol 1 [2] (29 mg, 0.09 mmol) at 10 ºC.[...]
To a stirred solution of a mixture of E/Z isomers 1 (174 mg, 0.52 mmol, 45:55 ratio) in acetone (8 mL) was added a mixture of KMnO4 (260 mg, 1.64 mmol) and anhydrous MgSO4 (230 mg) at 10 ºC [1].[...]
To a stirred solution of a mixture of E/Z isomers 1 (81 mg, 0.22 mmol, 45:55 ratio) in acetone (5 mL) was added a mixture of KMnO4 (122 mg, 0.77 mmol) and anhydrous MgSO4 (120 mg) at 10 ºC [1].[...]
of 2
Get Alerted
Add your email address to receive forthcoming issues of this journal.
