Search Results (973)

Spruce wood is a natural polymeric material, consisting of cellulose, lignin, hemicelluloses and other secondary components, which gives it a unique chemical footprint and architecture. Varnishes are used in musical instruments to protect the wood against humidity variations, wood being a hygroscopic material, but also to protect the wood from dirt. The varnishes used both to protect the wood from resonance and to ensure a special aesthetic appearance are either polymeric varnishes (nitrocellulose, oil-based) or volatile solvents (spirit). In this study, the color changes, the surface morphology and the chemical spectrum produced by three types of varnishes, applied in 5, 10 and 15 layers, on resonance spruce plates were analyzed. The results revealed significant changes in the color parameters: the lightness decreased by approximately 17% after the first layer, by 50% after 5 layers, by 65% after 10 layers and by 70% after 15 layers. The color parameters are most influenced by the anatomical quality of spruce wood (annual ring width and earlywood/latewood ratio) in the case of oil-based varnishes and least influenced in the case of nitrocellulose varnishes. The chemical fingerprint was determined by FTIR spectrum analysis, which revealed that the most pronounced absorptions were the double band 2926–2858 cm⁻¹, corresponding to aliphatic methylene and methyl groups (asymmetric and symmetrical C-H stretch), and the bands at 1724 cm⁻¹ (oil-based varnish), 1722 cm⁻¹ (nitrocellulose varnish) and 1708 cm⁻¹ (spirit varnish), all assigned to non-conjugated carbonyl groups in either carboxylic acids, esters aldehydes or ketones. The novelty of the study lies in the comparative analysis of three types of varnishes used in the musical instrument industry, applied to samples of spruce resonance wood with different macroscopic characteristics in three different layer thicknesses. Full article

Robotic timber joinery demands integrated, adaptive methods to compensate for the inherent dimensional variability of wood. We introduce a seamless robotic workflow to enhance the measurement accuracy of the Workpiece Coordinate System (WCS). The approach leverages a Zivid 3D camera mounted in an eye-in-hand configuration on a KUKA industrial robot. The proposed algorithm applies a geometric method that strategically crops the point cloud and fits planes to the workpiece surfaces to define a reference frame, calculate the corresponding transformation between coordinate systems, and measure the cross-section of the workpiece. This enables reliable toolpath generation by dynamically updating WCS and effectively accommodating real-world geometric deviations in timber components. The workflow includes camera-to-robot calibration, point cloud acquisition, robust detection of workpiece features, and precise alignment of the WCS. Experimental validation confirms that the proposed method is efficient and improves milling accuracy. By dynamically identifying the workpiece geometry, the system successfully addresses challenges posed by irregular timber shapes, resulting in higher accuracy for timber joints. This method contributes to advanced manufacturing strategies in robotic timber construction and supports the processing of diverse workpiece geometries, with potential applications in civil engineering for building construction through the precise fabrication of structural timber components. Full article

Construction wood has a high economic value, and its construction waste also has multiple consumption values. Natural wood has many advantages, such as thermal, environmental, and esthetic properties; however, wood sourced from artificial fast-growing forests is found to be deficient in mechanical strength. This shortcoming makes it less competitive in certain applications, leading many markets to remain dominated by non-renewable materials. To address this issue, various modification methods have been explored, with a focus on enhancing the plasticity and strength of wood. Studies have shown that hydrogen bonds in the internal structure of wood have a significant impact on its operational performance. Whether it is organic modification, inorganic modification, or a combination thereof, these methods will lead to a change in the shape of the hydrogen bond network between the components of the wood or will affect the process of its breaking and recombination, while increasing the formation of hydrogen bonds and related molecular synergistic effects and improving the overall operational performance of the wood. These modification methods not only increase productivity and meet the needs of efficient use and sustainable environmental protection but also elevate the wood industry to a higher level of technological advancement. This paper reviews the role of hydrogen bonding in wood modification, summarizes the mechanisms by which organic, inorganic, and composite modification methods regulate hydrogen bond networks, discusses their impacts on wood mechanical properties, dimensional stability, and environmental sustainability, and provides an important resource for future research and development. Full article

Deadwood is essential for the forest ecosystem productivity and stability. A growing body of evidence indicates that deadwood-inhabiting microbes are effective decomposition agents, yet little is known about how changes in microbial communities during the initial deadwood decay. In a small forest area, we performed dense sampling from the top, middle, and bottom portions of two representative Pinus massoniana cultivars logs to track deadwood xylem microbiota shift during the initial deadwood decay. We found xylem mycobiota varied dramatically during the initial deadwood decay. Deadwood microbes might largely originate from the endophytic microbes of living trees during the initial deadwood decay. Notably, bark type is an important driving factor for xylem mycobiota changes during the initial deadwood decay. Ten upregulated metabolites were screened out by a univariate analysis approach. Moreover, our correlation analysis suggests that enriched microbes at class level was significantly correlated with the upregulated metabolites during the initial deadwood decay. Our work provides new insights into the process of mycobiota and metabolite changes during the initial deadwood decay. Full article

The development of sustainable and functional nanocomposites has attracted considerable attention in recent years due to their broad spectrum of potential applications, including wood preservation. Also, a global goal is to reuse the large volumes of waste for environmental issues. In this context, the aim of the study was to obtain soda lignin particles, to graft ZnO nanoparticles onto their surface and to apply these hybrids, embedded into a biodegradable polymer matrix, as protection/preservation coating for oak wood. The organic–inorganic hybrids were characterized in terms of compositional, structural, thermal, and morphological properties that confirm the efficacy of soda lignin extraction and ZnO grafting by physical adsorption onto the decorating support and by weak interactions and coordination bonding between the components. The developed solution based on poly(3-hydroxybutyrate-co-3-hydroxyvalerate) and lignin-ZnO was applied to oak wood specimens by brushing, and the improvement in hydrophobicity (evaluated by water absorption that decreased by 48.8% more than wood, humidity tests where the treated sample had a humidity of 4.734% in comparison with 34.911% for control, and contact angle of 97.8° vs. 80.5° for untreated wood) and UV and fungal attack protection, while maintaining the color and aspect of specimens, was sustained. L.ZnO are well dispersed into the polymer matrix, ensuring a smooth and less porous wood surface. According to the results, the obtained wood coating using both a biodegradable polymeric matrix and a waste-based preservative can be applied for protection against weathering degradation factors, with limited water uptake and swelling of the wood, UV shielding, reduced wood discoloration and photo-degradation, effective protection against fungi, and esthetic quality. Full article

The structural analysis of shelterbelts forms the foundation of their planning and management, yet the scientific and effective quantification of shelterbelt structures requires further investigation. This study developed an innovative heterogeneous analytical framework, integrating three key methodologies: the LeWoS algorithm for wood–leaf separation, TreeQSM for structural reconstruction, and 3D alpha-shape spatial quantification, using terrestrial laser scanning (TLS) technology. This framework was applied to three typical farmland shelterbelts in the Ulan Buh Desert oasis, enabling the first precise quantitative characterization of structural components during the leaf-on stage. The results showed the following to be true: (1) The combined three-algorithm method achieved ≥90.774% relative accuracy in extracting structural parameters for all measured traits except leaf surface area. (2) Branch length, diameter, surface area, and volume decreased progressively from first- to fourth-order branches, while branch angles increased with ascending branch order. (3) The trunk, branch, and leaf components exhibited distinct vertical stratification. Trunk volume and surface area decreased linearly with height, while branch and leaf volumes and surface areas followed an inverted U-shaped distribution. (4) Horizontally, both surface area density (Scd) and volume density (Vcd) in each cube unit exhibited pronounced edge effects. Specifically, the Scd and Vcd were greatest between 0.33 and 0.60 times the shelterbelt’s height (H, i.e., mid-canopy). In contrast, the optical porosity (Op) was at a minimum of 0.43 H to 0.67 H, while the volumetric porosity (Vp) was at a minimum at 0.25 H to 0.50 H. (5) The proposed volumetric stratified porosity (Vsp) metric provides a scientific basis for regional farmland shelterbelt management strategies. This three-dimensional structural analytical framework enables precision silviculture, with particular relevance to strengthening ecological barrier efficacy in arid regions. Full article

Societies are aiming to have a higher ecological consciousness in wastewater treatment operations and achieve a more sustainable future. With this said, global demands for larger quantities of resources and the consequent waste generated will inevitably lead to the exhaustion of current municipal wastewater treatment works. The utilization of biosolids (particularly microbial proteins) from wastewater treatment operations could generate a sustainable bio-adhesive for the wood industry, reduce carbon footprint, mitigate health concerns related to the use of carcinogenic components, and support a more circular economic option for wastewater treatment. A techno-economic analysis for three 10 MGD wastewater treatment operations producing roughly 11,300 dry pounds of biosolids per day, in conjunction with co-feedstock defatted soy flour protein at varying ratios (i.e., 0%, 15%, and 50% wet weight), was conducted. Aspen Capital Cost Estimator V12 was used to design and estimate installed equipment additions for wastewater treatment plant integration into an urban biorefinery process. Due to the mechanical attributes and market competition, the chosen selling prices of each adhesive per pound were set for analysis as USD 0.75 for Plant Option P1, USD 0.85 for Plant Option P2, and USD 1.00 for Plant Option P3. Over a 20-year life, each plant option demonstrated economic viability with high NPVs of USD 107.9M, USD 178.7M, and USD 502.2M and internal rates of return (IRRs) of 24.0%, 29.0%, and 44.2% respectively. The options examined have low production costs of USD 0.14 and USD 0.19 per pound, minimum selling prices of USD 0.42–USD 0.51 per pound, resulting in between 2- and 4-year payback periods. Sensitivity analysis shows the effects biosolid production fluctuations, raw material market price, and adhesive selling price have on economics. The results proved profitable even with large variations in the feedstock and raw material prices, requiring low market selling prices to reach the hurdle rate of examination. This technology is economically enticing, and the positive environmental impact of waste utilization encourages further development and analysis of the bio-adhesive process. Full article

This paper describes the process of drying sewage sludge mixtures with the addition of various components: straw chaff, wood sawdust, ash, bark, wood chips, and walnut shells. The tests were conducted in two series: summer and autumn (with maximum insolation of 24.1 and 29.8 MJ∙m⁻², respectively). Using a set of sensors with which the experimental station was equipped, the parameters of the environment (temperature, humidity, and insolation) and the parameters of the dried mixtures (temperature and humidity) were measured. Based on the results obtained, the influence of external factors on the parameters, time, and drying effect of the respective mixtures was analyzed. With the initial moisture content of the mixtures ranging from 41 to 79%, a final moisture content of 6 to 49% was obtained, depending on the components and drying conditions. It was found that the drying rate was most influenced by the amount of solar energy and the associated outdoor (maximum 29 °C and 19 °C) and indoor (maximum 33 °C and 24 °C) air temperatures, and in the second series, there was an additional effect of the temperature of the mixtures (maximum 30 °C), upon which the intensity of water evaporation depended. Straw chaff and walnut shells proved to be the best additives, for which the highest drying rates were obtained (max. 50 to 60% humidity drop). The possibility of using dried materials for agricultural and energy purposes was indicated. This approach is in line with the principles of sustainable development. Full article

Wood is a green and renewable bio-based building material, but its hygroscopicity affects its dimensional stability, limiting its use in construction. Chemical modification can improve its properties, yet its effectiveness depends on wood permeability and traditional modifiers. This study first used a deep eutectic solvent (DES) to boost the permeability of North American alder wood. Then, methyl trimethoxysilane was impregnated under supercritical carbon dioxide (SCI), pressure (PI), vacuum (VI), and atmospheric pressure (AI) conditions. DES treatment damaged the cell structure, increasing wood permeability. Silane was deposited and polymerized in the cell lumen, chemically bonding with cell-wall components, filling walls and pits, and thickening walls. The VI group had the highest absolute density (0.59 g/cm³, +36.6%) and the lowest moisture absorption (4.4%, −33.3%). The AI group had the highest ASE (25%). The PI group showed the highest surface hardness (RL, 2592 N) and a water contact angle of 131.9°, much higher than natural wood. Overall, the VI group had the best performance. Silane reacts with cellulose, hemicellulose, and lignin in wood via hydrolysis and hydroxyl bonding, forming stable bonds that enhance the treated wood’s hydrophobicity, dimensional stability, and surface hardness. Full article

Methods for the improvement of regional lignocellulosic resources (wood and agriculture waste) were studied and analyzed using blends with optimized compositions and a selective pretreatment of the blends using microwaves to enhance their thermochemical conversion and energy production efficiency. A batch-size pilot device was used to provide the thermochemical conversion of biomass blends of different compositions, analyzing the synergy of the effects of thermal and chemical interaction between the components on the yield and thermochemical conversion of volatiles, responsible for producing heat energy at various stages of flame formation. To control the thermal decomposition of the biomass, improving the flame characteristics and the produced heat, a selective pretreatment of blends using microwaves (2.45 GHz) was achieved by varying the temperature of microwave pretreatment. Assessing correlations between changes in the main characteristics of pretreated blends (elemental composition and heating value) on the produced heat and composition of products suggests that selective MW pretreatment of biomass blends activates synergistic effects of thermal and chemical interaction, enhancing the yield and combustion of volatiles with a correlating increase in produced heat energy, thus promoting the wider use of renewable biomass resources for sustainable energy production by limiting the use of fossil fuels for heat-energy production and the formation of GHG emissions. Full article

In the case of forest inventory, heterogeneous areas are particularly challenging due to variability in vegetation structure. This is especially true in Galicia (northwest Spain), where land is highly fragmented, complicating the planning and management of single-species plantations such as Pinus radiata. This study proposes a cost-effective strategy using open-access tools and data to characterize and estimate wood volume in these plantations. Two stratification approaches—classical and cluster-based—were compared to a modeling method based on Principal Component Analysis (PCA). Data came from open-access national LiDAR point clouds, acquired using manned aerial vehicles under the Spanish National Aerial Orthophoto Plan (PNOA). Moreover, two volume estimation methods were applied: one from the Xunta de Galicia (XdG) and another from Spain’s central administration (4IFN). A Generalized Linear Model (GLM) was also fitted using PCA-derived variables with logarithmic transformation. The results show that although overall volume estimates are similar across methods, cluster-based stratification yielded significantly lower absolute errors per hectare (XdG: 28.04 m³/ha vs. 44.07 m³/ha; 4IFN: 25.64 m³/ha vs. 38.22 m³/ha), improving accuracy by 7% over classical stratification. Moreover, it does not require precise field parcel locations, unlike PCA modeling. Both official volume estimation methods tended to overestimate stock by about 10% compared to PCA. These results confirm that clustering offers a practical, low-cost alternative that improves estimation accuracy by up to 18 m³/ha in fragmented forest landscapes. Full article

We designed detachable steel sleeves to reinforce wooden joints and improve their integrity under earthquake action and investigated their mechanical properties. Monotonic bending tests were performed on a half-tenon pure wooden joint and a joint strengthened by a detachable steel sleeve. More obvious tenon pulling-out failure was observed in the pure wood joint; in comparison, only slight extrusion fracture of wooden beams and extrusion deformation of steel sleeves occurred in the wood joint reinforced by a detachable steel sleeve. Our test results showed that the initial rotational stiffness of the strengthened joint, JG1, was increased by 495.4% compared with that of the unstrengthened joint, JG0. The yield bending moment increased by 425.9%, and the ultimate bending moment increased by 627.5%, which indicated that the mechanical performance was significantly improved when the joint was reinforced by a detachable steel sleeve. Numerical simulations of different components were performed with finite element analysis software to analyze the mechanical performance of the reinforced joint. It was found that the stiffness and ultimate flexural performance of the joint could be increased by setting stiffeners on the steel sleeve and connecting the wooden column with self-tapping screws. The results of the tests were compared with those obtained through finite element analysis, and a high degree of accuracy was achieved, which could provide a theoretical basis for the reinforcement of timber structural buildings. Full article

In order to conduct an in-depth and exhaustive investigation into the mechanical properties of steel tubes filled with wood, a thin-walled steel–wood composite column was elaborately designed. The damage progression, failure mode, and mechanical performance of this column under eccentric compression were systematically investigated through both experimental research and finite element simulations. The impacts of different numbers of bolts on the mechanical properties of the composite column were minutely analyzed, and the test results of composite columns were compared with the pure steel pipe column under the same experimental conditions. It was clearly observed that the pure thin-walled steel pipe specimen was highly susceptible to elastic instability under eccentric compression, and the high-strength and high-ductility potential of structural steel was not fully developed. However, after filling with wood and applying bolt restraints, the greater the number of bolts in the specimen of thin-walled steel–wood composite column under the identical eccentricity condition, the higher the ultimate load-bearing capacity. Specifically, the ultimate load-bearing capacity of the columns filled with wood increased by 77.78–114% in comparison with that of the pure steel pipe column. Through a meticulous comparison between the test and finite element analysis results, the error was ascertained to be in the range of 4.9–11.1%. In addition, filling the thin-walled steel tube with wood and restraining it with bolts can effectively enhance the lateral deformation resistance of the specimens, and the reduction rate of lateral deflection exceeded 50%. Moreover, the greater the number of filling bolts, the smaller the strain of components subjected to the eccentric compression occurred, and the better the mechanical properties. Full article

Heat treatment is a widely employed method for modifying solid wood and has also been extended to veneer-type woods. Owing to the thinness and ease of handling of veneers, the regulation of protective media in heat treatment has not been highly regarded by the industry and is scarcely reported in research. In light of this, in this paper, rubber wood (Hevea brasiliensis) veneer is taken as the research subject to investigate the influences of heat treatment with hot air (HTHA) and heat treatment with superheated steam (HTSS) at different temperatures on the chemical properties, longitudinal tensile strength, color values, hygroscopicity, thermal degradation performance and microstructure of the wood. The results show that heat treatment alters the chemical properties of wood. Both heat treatments reduce the content of hemicellulose and other components in the veneer, and the characteristic peak of lignin in HTSS is slightly enhanced. The crystallinity of the veneer slightly increases after heat treatment, and the increase in HTSS is greater than that in HTHA. Through scanning electron microscopy, it is observed that heat treatment can effectively remove starch granules in rubber wood veneer, with HTSS being superior to HTHA, and the removal effect increases with the rise in temperature. The longitudinal tensile strength of the veneer decreased by 0.69%, 3.87%, and 24.98% respectively at 135~155 °C HTHA, and by 3.25%, 7.00%, and 18.47% respectively at 135~155 °C HTSS. Both heat treatments reduced the lightness of the veneer and increased the chroma index. At 155 °C, the color difference value of the veneer treated by HTSS was smaller than that treated by HTHA. The effects of heat treatment on the moisture absorption performance of the veneer were different. The equilibrium moisture content of the veneer treated at 135 °C HTHA and 135~155 °C HTSS was lower than that of the untreated material, indicating an improvement in moisture absorption stability. The maximum moisture sorption hysteresis of untreated material is 3.39%. The maximum moisture sorption hysteresis of 135 °C HTHA is not much different from that of untreated material. The values of 145 °C and 155 °C HTHA increase by 8.85% and 9.14% respectively. The values of 135 °C, 145 °C, and 155 °C HTSS increase by 22.42%, 25.37%, and 19.47% respectively. The moisture absorption hysteresis of the veneer increases after heat treatment, and the effect of HTSS improvement is more significant. From the TG and DTG curves, it can be seen that the residual mass percentage of the veneer after heat treatment is higher than that of the untreated material. The residual mass percentage of HTHA at 135 °C, 145 °C, and 155 °C increased by 3.13%, 3.07%, and 2.06% respectively, and that of HTSS increased by 5.14%, 7.21%, and 6.08% respectively. Full article

Wood–textile composites (WTCs), consisting of polypropylene and woven willow wood, have potential for both interior and exterior applications. However, their basic materials are not inherently resistant to outdoor weathering. This study examines the impact of various climatic conditions on the material behavior of WTCs. The composite and its components were aged under different scenarios, including kiln-drying, frost, standard and tropical climate, and artificial weathering and water storage, and analyzed for dimensional stability, chemical changes (FTIR), mechanical damage (µ-CT), and mechanical performance. While kiln-drying, frost, and tropical climates had only minor effects, water storage caused swelling-related damage, resulting in a 45% decrease in Young’s modulus but increased elongation at break (+88%) and impact strength (+75%). Artificial weathering led to significant degradation: tensile strength declined by 28%, Young’s modulus by 49%, and impact strength by 26%. In the medium term, this degradation compromises the integrity of the composite. The results highlight the need for effective stabilization measures—such as polymer modification or structural protection—to ensure the long-term durability of WTCs in outdoor use. Full article