Search Results (1,574)

With Aligned Formable Fibre Technology (AFFT^™), fibers are reformatted into highly oriented epoxy prepreg tapes, enabling the structural reuse of recycled composite waste. The present study investigates whether discontinuous fiber laminates produced with AFFT^™ can be characterized and optimized with the same finite-element workflows long established for continuous fiber composites and whether the resulting structures meet demanding stiffness targets. Initially, various manufacturing methods were adopted, including vacuum bagging, compression molding at 7 bar to simulate autoclave conditions, and compression molding at 90 bar, comprising the three most reasonable manufacturing processes for AFFT^™ laminates. Experimentally measured orthotropic properties were introduced into a finite-element model representing an idealized bicycle top tube, which was chosen as a case study. A genetic algorithm screened candidate stacking sequences, minimizing the combined bending-and-torsion deflection. The best lay-ups reduced deformation by more than 30% compared to a quasi-isotropic baseline, showing that well-oriented short fibers can significantly contribute to the stiffness of composites. Tubes produced with the optimized lay-up were tested in three-point bending tests, and the measured stiffness matched simulations within 5%. These results confirm a key point for sustainable engineering: despite the absence of continuous fibers, conventional simulation strategies accurately predict the performance of AFFT^™ laminates and can be used as the basis for effective genetic optimization. This validation is significant: it enables the design of stiff, high-performance structures from recycled materials using established, cost-effective methods. By proving that optimization strategies developed for traditional continuous fiber composites apply to AFFT^™, this study offers a trusted and accessible pathway to scale circular economy solutions in next-generation composite products. Full article

Non-destructive and destructive test methods are applied to wood to characterize this heterogeneous natural material. There have been multiple studies to characterize and investigate the change after the treatment (impregnation, thermal modification, etc.). In terms of thermal modification, there have been few studies on thermo–vacuum treatment, which is performed in a continuous vacuum atmosphere. With this method, the objective was to attempt to reduce the strength decrease after the thermal treatment. The aim of this study was to estimate the flexural properties of thermo–vacuum-treated Scots pine wood with destructive and acoustic-based non-destructive test methods. Wood was treated at 180 °C and 360 mm Hg. Both treated and untreated samples were cut into small specimens to ensure they were free of defects and were tested with acoustic-based non-destructive (longitudinal vibration and stress wave) and static bending test methods. The results show a decrease in equilibrium moisture content, demonstrating the efficiency of the treatment. When the results were compared with destructive test results, higher correlations (R² > 0.858) were found when estimating the modulus of elasticity (MOE) for both the untreated and treated wood, while lower correlations (R² < 0.440) were found for the modulus of rupture (MOR). When an additional equation was developed, stronger correlations (R² > 0.8986) were obtained between the non-destructive and destructive test results. Full article

External leakage from valve stem packings is a critical safety and reliability issue in high-pressure hydrogen systems. This work aims to quantify how packing geometry and polymer selection influence stem sealing in a PN650 needle valve (316L body and stem). Two geometries were compared: a conical V-ring (chevron style) stack and a flat three-disc stack. Two polymer material sets were assessed: Vespel^® polyimide (SP-1/SP-21) and a glass-filled PTFE sealing element combined with a virgin PEEK back-up ring. Four assemblies (one per geometry/material combination) were first screened by hydrostatic pressure hold testing up to 1500 bar and by helium mass spectrometer leak measurements under vacuum. All assemblies sustained the hydrostatic overpressure hold with negligible decay. Vacuum helium screening produced leak rates between 3.7 × 10⁻¹⁰ and 9.5 × 10⁻¹⁰ mbar·l·s⁻¹, with the conical V-ring geometry consistently outperforming the disc stack. A more demanding helium test at 700 bar with external vacuum yielded leak rates of 3.6–3.7 × 10⁻⁸ mbar·l·s⁻¹, for conical assemblies. Based on the screening results and practical industrial considerations, the PTFE/PEEK conical configuration was selected for endurance testing and completed 2500 open/close cycles in 650 bar hydrogen without gland readjustment. Post-cycling checks confirmed continued tightness, including a qualitative helium pressure hold result near 700 bar and 0 bubbles in 10 min in the seat tightness test. Microscopy/EDX revealed limited wear with minor metallic transfer. The proposed multi-stage workflow provides a pragmatic route for the early qualification of stem packings for high-pressure hydrogen valves. Full article

This study investigated the effects of black chokeberry (Aronia melanocarpa) (Michx.) Elliott powder addition (0.1–0.4%) on the quality attributes of cheese snacks produced from a blended camel–goat–cow milk base (60:20:20) using microwave vacuum drying. The snacks were evaluated for chemical composition, colour parameters, texture profile and water activity in order to assess how black chokeberry incorporation influences their physicochemical and sensory-related properties. Chemical analysis showed that the high protein content of the dried cheese matrix was maintained across all formulations, while fat, carbohydrate and energy values varied within a relatively narrow range, without a clear dose-dependent trend attributable solely to black chokeberry addition. Black chokeberry powder induced concentration-dependent colour changes, with decreased lightness and increased redness and overall colour difference, indicating visually noticeable shifts that may enhance product differentiation. Texture profile analysis revealed a significant reduction in fracturability at intermediate inclusion levels, suggesting a less brittle structure, whereas other texture parameters showed non-linear but statistically non-significant variations due to limited replication. All snacks exhibited very low water activity, consistent with shelf-stable, low-moisture products. A preliminary sensory test with untrained assessors indicated that black chokeberry-enriched snacks, particularly at around 0.3%, were generally well accepted, although the small panel size limits the strength of these conclusions. Overall, the findings suggest that small additions of black chokeberry powder can be used to develop visually attractive, high-protein cheese snacks with promising textural and sensory characteristics, while more comprehensive studies are needed to characterise their antioxidant properties, detailed nutritional profile and long-term stability. Full article

Ti₃C₂T_x/Al6061 composites were fabricated via vacuum induction melting, with systematic analysis conducted on their microstructure, mechanical properties, and wear behavior. Findings indicate that Ti₃C₂T_x addition significantly refined the composite grain size. Uniformly dispersed Ti₃C₂T_x particles promoted heterogeneous nucleation, reducing the average grain size by 44.7% compared to the matrix at the optimal 2 wt.% addition. Strong interfacial bonding ensured efficient load transfer, resulting in a 48.4% increase in tensile strength for the 2 wt.% Ti₃C₂T_x/Al6061 composites compared to the matrix alloy, while elongation decreased by 11.7%. Tribological analysis revealed that the wear rate of 2 wt.% Ti₃C₂T_x/Al6061 composites increases with applied load but remained substantially lower than Al6061 under all tested conditions. This excellent wear resistance is attributed to the synergistic effect of the protective mechanically mixed-layers formation and the inherent self-lubrication property of Ti₃C₂T_x during sliding contact. With increasing load, the friction coefficient and tendency for microcracking on the worn surface of the composite increased, and the dominant wear mechanisms transitioned from abrasive and adhesive wear to delamination wear. Full article

The structural segmentation of wind turbine blades offers advantages in transportation, manufacturing, and maintenance; however, it introduces interfaces that may compromise load transfer and fatigue performance. This study presents the experimental and numerical validation of a composite coupling system designed for small wind turbine blades compliant with IEC 61400-2 requirements. A 2 m representative section extracted from the mid-span region of a 9 m blade was manufactured using vacuum-assisted resin infusion and tested under static loading conditions. A detailed finite element model based on classical laminate theory and orthotropic material properties was developed to predict structural response. Experimental measurements showed a maximum tip deflection of 15 mm under the applied load, compared to 13.76 mm predicted numerically, corresponding to a deviation of 8.9%. Surface strain measurements obtained from eight strain gauges installed across the blade–coupling interface indicated maximum mean values of +632.4 με in tension and −664.2 με in compression, with no evidence of localized strain amplification at the instrumented locations. These findings demonstrate that fully composite permanent segmentation can preserve stiffness continuity while maintaining strain levels below reported fatigue initiation thresholds, supporting the structural feasibility of segmented blade architectures for small wind turbine applications. Full article

Phase-change materials (PCMs) are capable of storing or releasing a substantial amount of thermal energy within a small volume through the latent heat of fusion during phase transitions of melting and solidification, i.e., from solid to liquid or vice versa, in a near isothermal process. However, commonly used organic PCMs, such as paraffin wax, exhibit very low thermal conductivity, contributing to an adverse increase in overall thermal resistance and, thus, a slow thermal response. This limitation often becomes a bottleneck for the system from a thermal performance standpoint. To mitigate this issue, the present work explores the fabrication of heat sinks incorporating nano-structured graphitic foams, including carbon foam (CF) and expanded graphite (EG), as well as micro-structured metal foams such as open-cell copper foam (OCCF), all impregnated with a paraffin-based PCM with a melting temperature near 37 °C. This study focuses on applying passive thermal management strategies to design efficient heat sinks capable of maintaining the temperatures of battery modules and electronic circuits within an acceptable thermal safety threshold for small satellites and spacecrafts, exemplified by the OPTIMUS and Pumpkin battery modules designed for CubeSats with a nominal cross-sectional area of almost 4″ × 4″. Temperature responses and average overall thermal resistances for fabricated heat sinks are accordingly assessed and compared in a vacuum chamber to simulate space conditions. Furthermore, the impact of operating pressure on the thermal performances of various heat sinks will be investigated by executing the same tests in both atmospheric and vacuum conditions. The findings demonstrate a superior thermal performance of composite heat sinks integrating carbon foam and copper foam into the paraffin PCM compared to the baseline PCM heat sink under both vacuum and atmospheric operating pressure conditions. Full article

Practical development of terahertz technology requires higher power radiation sources. The sheet electron beam vacuum device is an effective solution of increasing the output power of terahertz radiation sources, but faces the difficulty of stable transmission of the beam. In this paper, a compact quadrupole permanent magnet (QPM) focusing system for terahertz sheet beam devices is designed, and a practical focusing system is constructed into a prototype for beam transmission verification. In the experiment, 16 pieces of high-performance NdFeB permanent magnets were adopted with a total weight of about 10 kg. The magnetic field test of the system was carried out and the results show that the system can provide a uniform high-intensity magnetic field of over 0.95 T within an axial length of 20 mm. With the tested QPM magnetic field configuration, PIC simulation of the sheet beam transmission was implemented, indicating that a sheet electron beam with a 20 kV voltage and 15 mA current can travel through a beam tunnel of a cross-section 0.1 mm × 0.05 mm, with a transmission ratio of 98.5%. Full article

This study examines the effect of vanadium addition on the microstructure and mechanical properties of low-cost powder metallurgy Ti-4Al-2Fe-3Cu alloys. Alloys with and without 6 wt.% V were fabricated by hot extrusion of blended elemental powders followed by vacuum heat treatment. Microstructural analysis revealed that the base alloy exhibits a coarse lamellar α/β structure, while vanadium addition promotes a refined basketweave morphology with a significantly higher β-phase fraction, increasing from 28.1% to 46.2%. Energy-dispersive spectroscopy confirmed preferential partitioning of Fe, Cu, and V into the β phase. Mechanical testing showed that the addition of 6 wt.% V markedly enhances strength, increasing yield strength and ultimate tensile strength from 1122 MPa and 1214 MPa to 1291 MPa and 1349 MPa, respectively, while maintaining comparable tensile ductility (~3.5%). The strength improvement is attributed to α-plate refinement, increased β-phase fraction, and solid-solution strengthening of the β phase. These results demonstrate that vanadium addition is an effective approach for improving the strength of low-cost PM titanium alloys without compromising ductility. Full article

Background: Aorto-esophageal fistula is a rare but life-threatening condition most often linked to thoracic aortic aneurysms and significant upper gastrointestinal bleeding. Thoracic endovascular aortic repair (TEVAR) is a crucial, life-saving procedure, but delayed complications, such as secondary esophageal fistulas caused by endograft erosion, can develop. Prompt recognition and multidisciplinary management are vital for survival. Case Presentation: We describe a 57-year-old patient with cardiovascular comorbidities and a saccular thoracic aortic aneurysm, who initially presented with massive hematemesis, melena, and hemodynamic instability. Imaging showed an aorto-esophageal fistula. Emergency treatment included placing a fully covered esophageal stent followed by TEVAR. Three weeks later, he experienced fever, chest pain, and worsening dysphagia. Laboratory tests indicated elevated inflammatory markers and hypoalbuminemia. Computed tomography revealed a new retrocardial esophageal fistula at T9, caused by mechanical erosion from the thoracic endograft. Endoluminal vacuum-assisted closure (EndoVAC) therapy was performed, leading to clinical improvement and the return of esophageal function. Conclusions: This case highlights a rare instance of a delayed secondary esophageal fistula after TEVAR beneath a preexisting stent, likely due to chronic contact between the endograft and esophagus. Despite advancements in endoscopic therapy, secondary fistulas after TEVAR are associated with high morbidity. Early diagnosis, aggressive infection management, structured nutritional support, and a multidisciplinary approach are essential. Extraluminal or intraluminal vacuum-assisted closure offers a promising minimally invasive option for managing complex esophageal defects. Full article

This study evaluated Salmonella behavior during Sardinian fermented sausage (SFS) production through a challenge test on experimentally inoculated raw meat. The objectives were to (i) determine the survival and reduction kinetics of Salmonella during fermentation and ripening and (ii) evaluate the relationship between pathogen behavior and the evolution of key chemical-physical parameters (pH, water activity). Three batches of SFS were produced, and the meat mixture was inoculated with a three-strain Salmonella cocktail (reference and field strains) to 10² CFU/g. After 20 days of ripening, sausages were vacuum-packed and stored under refrigerated conditions (+4 ± 2 °C). For each batch, triplicate samples were collected and analyzed at different production stages (mixing, after overnight rest, and 24 h after stuffing) and during shelf life (days 6, 21, 30, and 40). Analyses included Salmonella detection and enumeration by direct plating, aerobic colony count, Enterobacteriaceae, staphylococci, lactic acid bacteria, molds and yeasts, as well as pH, water activity, and gross composition. Salmonella counts increased by approximately one log unit after stuffing, before the onset of acidification. During fermentation and ripening, pathogen levels declined but remained detectable, even after prolonged refrigerated storage. These findings indicate that although ripening, and particularly fermentation, significantly (p < 0.05) reduce Salmonella levels, complete inactivation is not achieved. The study highlights the importance of controlling initial contamination levels, validating fermentation and ripening conditions, and the application of additional post-process hurdles to ensure product safety. Full article

TC4/Al₃Ti metal–intermetallic laminated (MIL) composites were fabricated by the vacuum hot-pressing process at 650 °C. The microstructure characteristics, i.e., grain boundary distribution, crystallographic orientation and Kernel Average Misorientation (KAM) map, were analyzed using EBSD. Meanwhile, the distribution of local strain and the fracture behavior of TC4/Al₃Ti MIL composites during tensile process were determined by Digital Image Correlation (DIC) and in situ tensile experiments, respectively. Results show that the TC4/Al₃Ti interfaces are well bonded and exhibit a distinct wavy morphology. The obvious Kirkendall pores and centerline are observed within the central region of the Al₃Ti layer. The texture components of (10-10) <0001> and (11-20) <10-10> are predominant in the TC4 layers; (100) <001> and (110) <001> are observed in the Al₃Ti layer. Additionally, the average geometrically necessary dislocation (GNDs) density is 2.53 × 10¹⁴ m⁻² in the TC4 layer, whereas it is 1.74 × 10¹⁴ m⁻² in the Al₃Ti layer. In the tensile test, the fracture resistance of TC4/Al₃Ti MIL composites is significantly improved by the plastic deformation of the TC4 layers and the suppression of crack-tip instability. It is found that the extrinsic toughening mechanisms contain crack deflection, crack blunting, crack bridging, multiple cracking modes, and the plastic deformation of ductile TC4 layers in TC4/Al₃Ti MIL composites. The real-time observation technique may provide more complete insights into the relationship between fracture behavior and enhanced toughness. Full article

This study explores the use of banana pseudostem fibers from Córdoba, Colombia, as reinforcement in polymer composites manufactured through vacuum-assisted resin transfer molding (VARTM). The fibers were decorticated, oven-dried at 40 °C, and subjected to mercerization and epoxy coating treatments. Plain-weave fabrics were produced using continuous yarns composed of 10 and 15 fibers, both treated and untreated. Experimental analyses included pull-out tests, thermogravimetric analysis, fourier-transform infrared spectroscopy, winding speed, surface twist angle, and tensile strength tests for yarns, as well as tensile load, adhesion, and permeability tests for fabrics and tensile and flexural strength tests for composites. Treated yarns exhibited a slight increase in diameter and a lower extraction (25%) compared to untreated yarns (33%). Although treated fabrics showed enhanced permeability and improved resin infiltration, untreated fabrics demonstrated superior mechanical performance, with a tensile load of 2.33 kN in comparison to 1.37 kN for treated yarns. The highest tensile strength of 76.56 MPa was achieved in composites reinforced with three layers of untreated fabric, while the best flexural strength of 86.93 MPa was observed in single-layer composites with the same configuration. These results emphasize the potential of untreated banana fiber fabrics as promising reinforcement in structural composite applications. Full article

Currently, the packaging sector must continue developing more sustainable systems to reduce the high quantities of single-use plastic waste generated. This study evaluated the production and characterization of bio-based composite trays with antimicrobial activity. Different formulations of polybutylene adipate co-terephthalate (PBAT) and polylactic acid (PLA) with polyethylene glycol (PEG) as plasticizer and citric acid as a compatibilizer/crosslinker were evaluated, in addition to the inclusion of plantain microfibers (PFs), TiO₂, and menthol as reinforcing and antimicrobial agents, respectively. The mixtures were subjected to pellet extrusion (165/175/185/190 °C and 60 rpm) and then to flat sheet extrusion (at 185/190/195/205 °C and 60 rpm), besides calendering (at 3.5–6.0 rpm). A single-screw extruder was used in both cases. The obtained sheets (0.317 ± 0.040 mm thick and 17 cm wide) were molded into 12.5 × 11.0 × 3.5 cm trays in a thermoforming machine (at 325 °C and vacuum pressure). For the resulting composite sheets and trays, measurements of mechanical strength, moisture absorption, barrier (WVTR), transmittance, and color were performed. FT-IR, DSC, TGA, SEM, and in vitro antimicrobial tests were also conducted. Based on these tests, an initial formulation with an 85/15 (w/w) PLA/PBAT ratio was defined, which was then reinforced with 3% (w/w) PF. Furthermore, the inclusion of 5% (w/w) menthol in the composite led to fungistatic activity against Botrytis cinerea, also resulting in homogeneous sheets (tensile strength 24.137 ± 1.439 MPa) and trays (compressive strength 0.113 ± 0.010 MPa). These findings can be applied to the packaging and preservation of perishable produce. Full article

We investigate the dynamical stability of circular orbits around a Kerr black hole embedded in a Dehnen-type dark matter halo. The effective spacetime metric of the combined system is constructed using the Newman–Janis algorithm, and the effective potential for test-particle motion in the equatorial plane is derived. The stability of circular orbits is analyzed through the Hessian matrix of the effective potential, while the stability strength and restoring-force distribution are employed to quantify the orbital response to small perturbations. Our results show that the presence of the dark matter halo significantly alters the spatial structure of stable circular orbits, leading to non-continuous stable regions whose location and extent depend sensitively on the halo’s characteristic density, scale radius, and the black hole spin. The innermost stable circular orbit (ISCO) is shifted relative to the vacuum Kerr case, with its position determined by the combined effects of the spin and halo parameters. Two-dimensional heatmaps, parameter scans, and three-dimensional visualizations systematically illustrate how the black hole spin and dark matter halo properties influence the ISCO and the distribution of stable orbits. Finally, we analyze the influence of the dark matter halo on the structure of the black hole event horizon. These results provide a detailed theoretical investigation of orbital dynamics around rotating black holes in dark-matter-rich environments. Full article