Search Results (31)

High-quality drilled holes are critical in thin fabric-reinforced composites used in many industrial applications; however, the influence of woven architecture on drilling performance without a backup plate remains insufficiently defined. This paper introduces the first comprehensive experimental and statistical framework for evaluating unsupported drilling of thin woven glass fiber-reinforced polymer (GFRP) laminates. The framework integrates the effect of support opening width, fiber weight fraction (wf), feed per tooth, and fabric architecture to quantify their combined effects on delamination, cutting forces, and surface roughness. The samples consisted of vacuum mold-pressed GFRP laminates. Drilling tests were conducted on plain and twill-woven plates, and hole quality was evaluated using thrust force, delamination factor, and surface roughness (Sa). A statistical DOE and multifactorial ANOVA were applied to quantify the effects of the main parameters. For plain-woven GFRP, the best results were obtained with a 65 mm support opening width, 45% fiber wf, and 0.04 mm/tooth feed. Plain-woven laminates exhibited lower average surface roughness (Sa ≈ 5.0–6.5 µm) than twill-woven laminates (Sa ≈ 6.0–7.0 µm). The study demonstrates how fabric architecture and drilling parameters jointly influence hole quality in thin GFRP composites, providing practical guidance for manufacturing applications. Full article

A non-destructive method for determining the properties of laminated composite materials made of twill-weave glass fibre fabric is considered. To determine the elastic characteristics of the composite monolayer, a combined numerical–experimental method is used. The method combines the results of experimental tests and numerical modelling methods using optimization techniques. Firstly, the method for determining the properties is tested in a virtual experiment to determine the influence of the elastic characteristics of the material that do not affect the frequency response. The adequacy of the approximation equations and the influence of elastic constants on frequency response are evaluated using Analysis of Variance (ANOVA). Using the results obtained, the properties of the elastic characteristics of layered composite plates made of twill-weave glass fibre fabric using vacuum infusion are determined. To compare the properties obtained from the dynamic calculation, a series of static measurements of tensile samples were carried out. The results showed that the elastic modulus from the static test and the flexural test do not coincide by 4% and 23%, respectively. The technique demonstrates high accuracy and applicability for the non-destructive determination of dynamic material properties in engineering practice. Full article

Direct-writing submicron copper circuits on glass with laser precision—without lithography, vacuum deposition, or etching—represents a transformative step in next-generation microfabrication. We present a high-resolution, maskless method for metallizing glass using ultrashort pulse Bessel beam laser processing, followed by silver ion activation and electroless copper plating. The laser-modified glass surface hosts nanoscale chemical defects that promote the in situ reduction of Ag⁺ to metallic Ag⁰ upon exposure to AgNO₃ solution. These silver seeds act as robust catalytic and adhesion sites for subsequent copper growth. Using this approach, we demonstrate circuit traces as narrow as 0.7 µm, featuring excellent uniformity and adhesion. Compared to conventional redistribution-layer (RDL) and under-bump-metallization (UBM) techniques, this process eliminates multiple lithographic and vacuum-based steps, significantly reducing process complexity and production time. The method is scalable and adaptable for applications in transparent electronics, fan-out packaging, and high-density interconnects. Full article

The discontinuation of commercially available saline and hypertonic saline wound dressings for the veterinary market has restricted options available to veterinary practitioners treating contaminated and infected wounds. Clinicians may manufacture their own homemade solutions in clinics or field settings to treat equine or livestock species; however, information is limited on whether autoclave sterilization is necessary or sufficient to eliminate bacterial growth in isotonic and concentrated salt solutions and how long they may subsequently be stored prior to use. The purpose of this study was to assess sterility of saline (0.9%) and hypertonic saline (20%) solutions manufactured three ways (1—autoclaved glass bottle that was autoclaved again following solution preparation; 2—autoclaved glass bottle, not autoclaved again following preparation; 3—non-autoclaved plastic bottle, not autoclaved following preparation). Solutions were stored two different ways (1—solution in sealed bottle or 2—soaked gauze in vacuum-sealed plastic packets). Products were assessed for bacterial growth at four time points (baseline, one week, one month, six months). At each time point, samples of each solution were plated on Luria–Bertani (LB) agar plates and assessed for bacterial growth at 24 h. Vacuum-sealed soaked gauze was placed in antibiotic-free growth media for 24 h, and then media were plated on LB agar plates and assessed for bacterial growth at 24 h. If bacterial growth was detected, qualitative culture with sensitivity was performed to identify bacterial isolates. No bacterial growth was detected in stored solutions for any preparation method, concentration or time point assessed. Bacterial growth was detected from 0.9% saline-soaked gauze at 1 week, 1 month and 6 months in all container types for at least one time point. Bacterial culture revealed Ralstonia, Bacillus, Sphingomonas and Staphylococcus species. Environmental controls (water, containers, salt, biosafety cabinet and benchtop) were submitted for culture to identify the source of contamination, yielding light mixed growth from tap water and no growth from any other locations. These findings provide clinicians with practical information to guide preparation and storage of homemade saline-based products for wound care. Full article

This paper concerns measurements and CFD simulations of vacuum-insulated glazing (VIG), which consists of two glass panes separated by a narrow gap from which air has been removed. Distancers, e.g., in the form of small balls, are inserted into this gap every few centimeters to prevent the glass from deflecting. In the first part, simulations of two-pane VIG thermal transmittance with the Ansys Fluent program are described, resulting in thermal transmittance of VIG without the network of distancers equal to 2.18 W/(m²K) and with the distancers equal to 2.29 W/(m²K). The influence of the supports on the thermal transmittance of VIG is also determined. The CFD results show that the supporting balls increase the two-pane VIG thermal transmittance by about 0.15% with respect to the glazing without the distancers. Then, VIG is analyzed both numerically and tested in two measurement stands. Firstly, the tests are performed in a guarded hot-plate apparatus, according to the EN ISO 8302 standard. The two-pane glazing with one low-emissivity coating has a measured thermal transmittance equal to 1.75 W/(m²K). Other measurements were undertaken in the calorimetric chamber equipped with the hot-box apparatus. The results of the numerical assessment are then compared to the measurements of the existing three-pane vacuum-insulated glazing with two low-emissivity coatings, the same as simulated. The procedure follows the EN ISO 8990 standard. Measurement results of 1.10 W/(m²K) are compared to the simulation results of VIG thermal transmittance equal to 1.09 W/(m²K). A satisfactory agreement is reached. Additionally, this paper considers a new correction coefficient to thermal transmittance according to standard EN 673 in order to achieve a proper calculation of vacuum-insulated glazing in the center-of-glass region. The authors propose to use an adjustment coefficient of 1.05 when calculating the thermal transmittance of vacuum-insulated glazing without taking into account convection in the vacuum space and the thermal influence of distancers. Full article

This paper continues the mathematical research of the novel glass tube collectors for water heating. The subject of this research is a vacuum solar collector composed of a glass tube and a selective (using the SnAl₂O₃ coating) flat absorber plate. Water heating is performed using gravitational driving force and single-stage direct flow. The thermal performance with the geometric optimization (absorber width and glass tube thickness) of the presented solar collector type was determined using the specially designed iterative calculation algorithm (phase 1) and the double multi-criteria analysis (phase 2). Different operational (absorber temperature, ambient temperature and wind speed), geometric (mass, surface occupation, total surface occupation and volume occupation), economic (manufacturing costs and exploitation costs) and ecological (embodied energy and greenhouse gas emission) indicators were taken into account. The results showed that the useful heat power has an increasing trend if the flat absorber plate width increases, while the thermal efficiency has a decreasing trend. It was also determined that the glass tube thickness and the thermal performance of the solar collector are oppositely dependent. The main conclusion of this paper is that the optimal performance of such non-conventional solar systems is achieved when the absorber plate width is between 85 and 90 mm. Full article

The aim of this study was to compare the mechanical properties of carbon-fiber-reinforced polymer (CFRP) composites produced using three popular technologies. The tests were performed on composites produced from prepregs in an autoclave, the next variant is composites produced using the infusion method, and the third variant concerns composites produced using the vacuum-assisted hand lay-up method. For each variant, flat plates with dimensions of 1000 mm × 1000 mm were produced while maintaining similar material properties and fabric arrangement configuration. Samples for testing were cut using a plotter in the 0° and 45° directions. Non-destructive tests (NDTs) were carried out using the active thermography method, demonstrating the correctness of the composites, i.e., the absence of structural defects for all variants. Static peel strength tests were carried out for samples with different directional orientations. The tests were carried out at temperatures of +25 °C and +80 °C. At room temperature, similar strengths were demonstrated, which for the 0° orientation were 619 MPa, 599 MPa and 536 MPa for the autoclave, vacuum and infusion variants, respectively. However, at a temperature of +80 °C, only the composite produced in the autoclave maintained the stability of its properties, showing a strength of 668 MPa. Meanwhile, in the case of the composite produced by the infusion method, a decrease in strength at an elevated temperature of 46.5% was demonstrated, while for the composite produced by the hand lay-up method, there was a decrease of 46.2%. For the last two variants, differential scanning calorimetry (DSC) analysis of epoxy resins constituting the composite matrices was carried out, showing a glass transition temperature value of 49.91 °C for the infusion variant and 56.07 °C for the vacuum variant. In the three-point static bending test, the highest strength was also demonstrated for the 0ᵒ orientation, and the bending strength was 1088 MPa for the autoclave variant, 634 MPa for the infusion variant and 547 MPa for the vacuum variant. The fatigue strength tests in tension at 80% of the static strength for the infusion variant showed an average fatigue life of 678.788 × 10³ cycles for the autoclave variant, 176.620 × 10³ cycles for the vacuum variant and 159.539 × 10³ cycles for the infusion variant. Full article

Hole quality in composite materials is gaining interest in aerospace, automotive, and marine industries, especially for structural applications. This paper aims to investigate the quality of holes performed without a backup plate, in thin plates of glass fiber-reinforced polymer (GFRP). The samples were manufactured by two different technologies: vacuum bagging and an innovative method named vacuum mold pressing. Three experiments were designed choosing the control factors that affect the maximum cutting force, delamination factor, and surface roughness of drilled holes in composite materials based on twill fabric layers. Quality analysis of the hole features was performed by microscopy investigations. The effects of the main factors on the targets are investigated using the statistical design of experiments, considering control factors, such as support opening width, weight fraction (wf), feed per tooth, and hole area. The results showed that the feed per tooth and hole area had a more significant influence on the delamination factors and surface roughness (Sa). The best quality of the holes drilled in twill-based GFRP was achieved for a lower feed rate of 0.04 mm/tooth and used a support opening width of 55 mm. Full article

This paper presents an analytical method for the dimensioning and selection of the four glass tube collector types: single-glazed with an air layer, single-glazed with a vacuum layer, double-glazed with an air layer, and double-glazed with a vacuum layer. In the first part of the paper (dimensioning phase), the iterative thermal resistance calculation algorithms were developed for all glass tube collector types, whereby the iterative thermal resistance calculation algorithm of the single-glazed tube collector with an air layer was experimentally tested and validated. The second part of the paper (selection phase) uses a multi-criteria decision-making method to determine the optimal glass tube collector design. Unlike other papers, three indicator groups are taken into account in this case: geometric (mass, surface occupation, total surface occupation, volume occupation), economic (manufacturing and exploitation costs), and ecological (embodied energy and greenhouse gas emission). The proposed method is characterized by simple and fast calculations with satisfactory accuracy, which avoids high investment costs (experimental research), approximation and discretization of physical models (numerical research), and a large number of input parameters with boundary conditions (theoretical research). It should be noted that, with certain additions and changes, it can also be applied to other solar thermal collectors, so the authors believe such tools are handy for the global scientific public. Full article

In this paper, we present a new processing method, called MOSES—Impacts, for the detection of micrometer-sized damage on glass plate surfaces. It extends existing methods by a separation of damaged areas, called impacts, to support state-of-the-art recycling systems in optimizing their parameters. These recycling systems are used to repair process-related damages on glass plate surfaces, caused by accelerated material fragments, which arise during a laser–matter interaction in a vacuum. Due to a high number of impacts, the presented MOSES—Impacts algorithm focuses on the separation of connected impacts in two-dimensional images. This separation is crucial for the extraction of relevant features such as centers of gravity and radii of impacts, which are used as recycling parameters. The results show that the MOSES—Impacts algorithm effectively separates impacts, achieves a mean agreement with human users of (82.0 ± 2.0)%, and improves the recycling of glass plate surfaces by identifying around 7% of glass plate surface area as being not in need of repair compared to existing methods. Full article

In order to enhance the sensitivity of wafer-level vacuum-packaged electric field sensors, this paper proposed a vertical-resonant MEMS electric field sensor based on TGV (Through Glass Via) technology. The microsensor is composed of the electric field sensing cover, the drive cover, and the SOI-based microstructures between them. TGV technology is innovatively used to fabricate the electric field sensing cover and the vertically-driven cover. The external electric field is concentrated and transmitted to the area below the silicon plate in the center of the electric field sensing cover through a metal plate and a metal pillar, reducing the coupling capacitance between the silicon plate and the packaging structure, thereby achieving the enhanced transmission of the electric field. The sensitivity-enhanced mechanism of the sensor is analyzed, and the key parameters of the sensor are optimized through finite element simulation. The fabrication process is designed and realized. A prototype is tested to characterize its performance. The experimental results indicate that the sensitivity of the sensor is 0.82 mV/(kV/m) within the electrostatic electric field ranging from 0–50 kV/m. The linearity of the sensor is 0.65%. Full article

Mechanical testing of glass-fibre-reinforced composite (GFRP) plates made of twill fabric and a thermoplastic recyclable infusion resin is presented. The considered thermoplastic resin, ELIUM^®, is made of poly-methylmethacrylate and can be infused with properly tuned vacuum techniques, in the same manner as all liquid resin. Tensile, flexural, and drop-dart impact tests were carried out to assess the mechanical properties of the composites considering different fabrication conditions, such as the different degassing pressure before infusion and three different infusion vacuum pressures. The work reports a methodology to infuse ELIUM resin at a relatively high vacuum pressure of 0.8 bar. X-ray microtomography analysis showed that the produced laminates are free of defects, differently from what was reported in the literature, where void problems related to a vacuum infusion pressure higher than 0.3–0.5 bar were pointed out. Vacuum pressure values influence the mechanical characteristics of the laminate: when higher vacuum pressures are adopted, the mechanical properties of the GFRP laminates are enhanced and higher values of elastic modulus and strength are obtained. On the other hand, degassing the resin before infusion does not influence the mechanical properties of the laminates. A maximum bending and tensile strength of 420 and 305 MPa were reached by using the vacuum infusion of 0.8 bar with an elastic modulus of 18.5 and 20.6 GPa, respectively. The density of the produced laminates increases at higher vacuum infusion pressure up to a maximum value of 1.81 g/cm³ with the fibre volume fraction of each laminate. Full article

The VIG (Vacuum Insulated Glazing) unit, composite glazing in which the space between glass panes is filled with vacuum, is one of the most advanced technologies. The key elements of the construction of VIG plates are the support pillars. Therefore, an important issue is the analysis of their mechanical properties, such as Young’s modulus and their variability over a long period of time. Machine learning (ML) methods are undergoing tremendous development these days. Among the many different techniques included in AI, neural networks (NN) and extreme gradient boosting (XGB) algorithms deserve special attention. In this study, to train selected methods of machine learning, numerical data developed in the VIG plate modelling process using Abaqus program were used. The test method proposed in this article is based on the VIG plate subjected to forced vibrations of specific frequencies and then the reading of the dynamic response of the composite plate. Such collected and pre-developed experimental data were used to obtain the mechanical parameters of the steel elements located inside the analysed vacuum glazing. In the future, the proposed research methods can be used to analyse the mechanical properties of other types of composite panels. Full article

An experimental study has been carried out to assess the effectiveness of infrared thermography in wrinkle detection in composite GFRP (Glass Fiber Reinforced Plastic) structures by infrared active thermography. Wrinkles in composite GFRP plates with different weave patterns (twill and satin) have been manufactured with the use of the vacuum bagging method. The different localization of defects in laminates has been taken into account. Transmission and reflection measurement techniques of active thermography have been verified and compared. The section of a turbine blade with a vertical axis of rotation containing post-manufacturing wrinkles has been prepared to verify active thermography measurement techniques in the real structure. In the turbine blade section, the influence of a gelcoat surface on the effectiveness of thermography damage detection has also been taken into account. Straightforward thermal parameters applied in structural health monitoring systems allow an effective damage detection method to be built. The transmission IRT setup allows not only for damage detection and localization in composite structures but also for accurate damage identification. The reflection IRT setup is convenient for damage detection systems coupled with nondestructive testing software. In considered cases, the type of fabric weave has negligible influence on the quality of damage detection results. Full article

This paper presents an easy and low-cost flame treatment method to improve the bonding performance of GF/EP (Glass Fiber-Reinforced Epoxy) pultrusion plates, which are using widely for large size wind blades. In order to explore the effect of flame treatment on the bonding performance of the precast GF/EP pultruded sheet vs. the infusion plate, the GF/EP pultruded sheets were treated with different flame treatment cycles and were embedded in the fiber fabrics during the vacuum-assisted resin infusion process (VARI). The bonding shear strengths were measured by tensile shear tests. It is found that after 1, 3, 5, and 7 flame treatments, the tensile shear strength between the GF/EP pultrusion plate and infusion plate increased by 8.0%, 13.3%, 22.44%, and −2.1%, respectively. This indicates that the maximum tensile shear strength can be obtained after five times of flame treatment. In addition, DCB and ENF tests were also adopted to characterize the fracture toughness of the bonding interface with the optimal flame treatment. It is found that the optimal treatment gives increments of 21.84% and 78.36% for G I C and G II C, respectively. Finally, the surficial topography of the flame-treated GF/EP pultruded sheets were characterized by optical microscopy, SEM, contact angle test, FTIR, and XPS. The results show that flame treatment plays an impact on the interfacial performance through the combination of physical meshing locking and chemical bonding mechanism. Proper flame treatment would remove the weak boundary layer and mold release agent on the surface of the GF/EP pultruded sheet, etch the bonding surface and improve the oxygen-containing polar groups, such as C–O and O–C=O, to improve the surface roughness and surface tension coefficient of pultruded sheet to enhance the bonding performance. Excessive flame treatment destroys the integrity of epoxy matrix on bonding surface which results into the exposure of the glass fiber, and the carbonization of release agent and resin on the surface loosen the surficial structure, which reduces the bonding properties. Full article