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17 pages, 453 KB  
Article
Sustainable Fashion in China: Consumers’ Second-Hand Clothing Intentions and Market Evolution
by Zhiyi Zhang
Sustainability 2025, 17(24), 10997; https://doi.org/10.3390/su172410997 - 8 Dec 2025
Viewed by 956
Abstract
As global attention on environmental sustainability grows, the fashion industry is shifting towards circular models, with the second-hand clothing market emerging as a key pathway to sustainable development. In China, this market is rapidly evolving, with millennials and Generation Z showing strong interest [...] Read more.
As global attention on environmental sustainability grows, the fashion industry is shifting towards circular models, with the second-hand clothing market emerging as a key pathway to sustainable development. In China, this market is rapidly evolving, with millennials and Generation Z showing strong interest in environmentally friendly and personalized fashion. This study investigates Chinese consumers’ motivations and barriers to purchasing second-hand clothing and examines the diversity of China’s sustainable fashion ecosystem. Using a mixed-methods approach of semi-structured interviews and surveys, the findings reveal that environmental awareness, economic affordability, and social influence drive purchase intentions, while hygiene concerns, societal perceptions, and trust in platforms act as barriers. The study also compares the roles of online platforms, offline vintage stores, and upcycling fashion brands, highlighting their complementarity across economic, cultural, and social dimensions. Online platforms offer efficiency and convenience, vintage stores build brand loyalty through cultural narratives, and upcycling brands merge creativity with sustainability. It also reflects on the cultural context shaping second-hand fashion adoption in China. The study suggests enhancing trust in platforms, promoting education, and leveraging social media campaigns to support future market development. Full article
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25 pages, 3215 KB  
Review
Waste Polypropylene in Asphalt Pavements: A State-of-the-Art Review Toward Circular Economy
by Nannan Yang, Congying Du, Ye Tang, Zhiqi Li, Song Xu and Xiong Xu
Sustainability 2025, 17(24), 10954; https://doi.org/10.3390/su172410954 - 8 Dec 2025
Viewed by 483
Abstract
With the rapid increase in plastic consumption, waste polypropylene (WPP) has become one of the major components of municipal solid waste, posing significant environmental and resource challenges. According to statistics, polypropylene accounts for approximately 19.1% of the total global plastic waste, posing significant [...] Read more.
With the rapid increase in plastic consumption, waste polypropylene (WPP) has become one of the major components of municipal solid waste, posing significant environmental and resource challenges. According to statistics, polypropylene accounts for approximately 19.1% of the total global plastic waste, posing significant environmental challenges. In recent years, the recycling and reuse of WPP in asphalt pavement materials have received increasing attention due to its excellent mechanical properties, thermal stability, and low cost. This review systematically summarizes the physicochemical properties and recycling technologies of WPP, including mechanical, chemical, and energy recovery routes. Furthermore, the modification mechanisms, preparation methods, and performance characteristics of WPP-modified asphalt binders and mixtures are comprehensively discussed, focusing on their high-temperature stability, compatibility, low-temperature cracking resistance, and anti-moisture damage. Research indicates that WPP modification significantly enhances high-temperature rutting resistance, and thermo-chemical modifiers have successfully enabled the application of WPP in warm-mix asphalt. This review uniquely integrates recent advances in thermo-mechanochemical upcycling with mixture-level performance, bridging molecular design and field application. However, critical challenges, including poor compatibility, insufficient storage stability, and the lack of a unified assessment for the high variability of WPP raw materials, still need to be addressed. Finally, this review primarily focuses on the recycling technologies of WPP, its modification mechanisms in asphalt binders, and the resulting impact on the pavement performance of WPP-modified mixtures. Full article
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10 pages, 1593 KB  
Article
Upcycling Medical Tablet Blister Waste into High-Performance Triboelectric Nanogenerators for Sustainable Energy Harvesting
by Vikram Lakshmi Suneetha, Velpula Mahesh, Khanapuram Uday Kumar and Rajaboina Rakesh Kumar
Nanoenergy Adv. 2025, 5(4), 19; https://doi.org/10.3390/nanoenergyadv5040019 - 1 Dec 2025
Viewed by 325
Abstract
The increasing accumulation of medical waste, especially discarded pharmaceutical blister packs, poses both environmental risks and missed opportunities for resource recovery. In this work, we demonstrate, for the first time, the direct upcycling of tablet blister waste into a potential frictional layer in [...] Read more.
The increasing accumulation of medical waste, especially discarded pharmaceutical blister packs, poses both environmental risks and missed opportunities for resource recovery. In this work, we demonstrate, for the first time, the direct upcycling of tablet blister waste into a potential frictional layer in triboelectric nanogenerators (TENGs). The polymer structure of blister packs, combined with Silicone rubber as a counter frictional layer, enabled the fabrication of durable TENG devices (TS-TENGs). Systematic electrical testing revealed that the TS-TENG achieved an open-circuit voltage of approximately 300 V, a short-circuit current of about 40 μA, and a peak power density of 3.54 W/m2 at an optimal load resistance of 4 MΩ. The devices maintained excellent stability over 10,000 mechanical cycles, confirming their durability. Practical demonstrations included powering 240 LEDs, four LED lamps, and portable electronic devices, such as calculators and hygrometers, through capacitor charging. This study shows that not only can tablet blister waste be used as a triboelectric material but it also presents a sustainable method to reduce pharmaceutical waste while advancing self-powered systems. The approach offers a scalable and low-cost means to integrate medical waste management with renewable energy technologies. Full article
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16 pages, 831 KB  
Article
Stakeholders’ Perception and Adoption of Upcycling for Material Utilisation Plans in Road Construction: The Case of South Africa
by Salome Naicker, Mohamed Mostafa Hassan Mostafa and Paul Terkumbur Adeke
Buildings 2025, 15(23), 4314; https://doi.org/10.3390/buildings15234314 - 27 Nov 2025
Viewed by 329
Abstract
Transportation infrastructure underpins national mobility and economic growth, yet material sourcing for road construction imposes significant environmental and financial costs. As South Africa advances towards road construction, upcycling the reuse of reclaimed materials in higher-value applications offers opportunities to reduce waste and improve [...] Read more.
Transportation infrastructure underpins national mobility and economic growth, yet material sourcing for road construction imposes significant environmental and financial costs. As South Africa advances towards road construction, upcycling the reuse of reclaimed materials in higher-value applications offers opportunities to reduce waste and improve circular resource efficiency. This study assesses stakeholders’ perception and adoption of upcycling in the Material Utilisation Plans (MUPs) for road construction. A mixed-methods approach combined nine semi-structured interviews and thirty-two survey responses from professionals involved in the National Route 3 upgrade project. Thematic analysis identified key qualitative themes, while quantituative data from a five-point Likert scale were examined through descriptive statistics, reliability, and correlation analysis. Respondents supported existing downcycling practices (mean = 3.682, SD = 1.088) and expressed readiness to adopt upcycling for pavement surfacing, base, subbase, and subgrade (mean > 3.00, SD < 1.30). Major barriers included client specifications, limited awareness and material cost constraints. Reliability analysis (Cronbach’s α = 0.64–0.88) confirmed internal consistency across qualitative themes. Also, there was a positive correlation between reclaimed materials and cost, design specifications, and optimised cost (r > 0.30, p < 0.05), while downcycling correlated negatively with costs (r = −0.400, p < 0.05). This study provides new empirical evidence on the systemic barriers hindering upcycling adoption in South African road projects and offers a validated mixed-method framework linking perceptual, technical, and economic dimensions of material reuse. It recommends integrating upcycling criteria into design, testing, and procurement processes, shifting from compliance-based recycling to performance-based circular material management in national road infrastructure. Full article
(This article belongs to the Special Issue Advances in Road Pavements)
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21 pages, 1165 KB  
Article
Upcycling of Citrus Waste by Natural Deep Eutectic Solvents: Green Extraction of Bioactive Compounds with Antioxidant and Regenerative Properties on Human Keratinocytes
by Alessia Silla, Angela Punzo, Rossana Comito, Emanuele Porru, Greta Gozzi, Maria Cristina Barbalace, Matteo Perillo, Antonello Lorenzini, Marco Malaguti, Silvana Hrelia and Cristiana Caliceti
Nutrients 2025, 17(23), 3692; https://doi.org/10.3390/nu17233692 - 25 Nov 2025
Viewed by 471
Abstract
Background: The citrus processing industry generates over 40 million tons of waste annually, representing a significant environmental challenge. Citrus by-products are rich in bioactive compounds with proven health benefits. This study aims to upcycle citrus waste by developing green extracts and evaluating their [...] Read more.
Background: The citrus processing industry generates over 40 million tons of waste annually, representing a significant environmental challenge. Citrus by-products are rich in bioactive compounds with proven health benefits. This study aims to upcycle citrus waste by developing green extracts and evaluating their biological activities for cosmeceutical applications. Methods: Three NaDES formulations—choline chloride–urea (ChCl: U), choline chloride–citric acid (ChCl: CA), and betaine–urea (Bet: U)—were optimized to extract polyphenols from orange and lemon waste using roller agitation. Extracts were characterized by HPLC–ESI–MS/MS. Biological activities were assessed in human keratinocytes (HaCaT). Antioxidant activity was measured using a chemiluminescent assay that detects intracellular H2O2 production. The wound-healing potential was evaluated using scratch assays, and cytokine release (IL-6, IL-8, IL-1β, IL-10) was assessed by ELISA. DNA damage protection was evaluated by quantifying 53BP1 foci following genotoxic exposure (neocarzinostatin). Results: All NaDES extracts showed high polyphenol content, with hesperidin being the primary compound. Pretreatment with the extracts for 24 h significantly reduced intracellular H2O2 levels, confirming their antioxidant efficacy. In scratch assays, extracts enhanced wound closure; notably, the Bet: U-derived orange extract achieved complete closure within 48 h. All extracts increased IL-6 and IL-8 release, consistent with an early pro-regenerative response. Pretreatment with the Bet: U orange extract lowered the number of cells with high 53BP1 foci after genotoxic stress, indicating partial DNA damage protection. Conclusions: These findings highlight citrus by-product extracts as sustainable bioactive ingredients with great potential for skin repair and anti-aging formulations, promoting responsible cosmeceutical innovation. Full article
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31 pages, 627 KB  
Review
Ecological Paradox in the Reuse of Internal Combustion Engines from Scrapped Vehicles for Electric Power Generation—Circular Economy Potential Versus Emission Certification Barriers
by Łukasz Warguła, Adil Kadirov, Damir Aimukhanov, Dariusz Ulbrich, Piotr Kaczmarzyk, Damian Bąk and Bartosz Wieczorek
Sustainability 2025, 17(23), 10435; https://doi.org/10.3390/su172310435 - 21 Nov 2025
Viewed by 1083
Abstract
Concepts such as reuse, repurposing, upcycling, remanufacturing, and re-powering can be applied to the reuse of combustion engines from passenger cars and trucks in stationary or mobile machines, such as power generators. Technical, economic, environmental, and research analyses indicate that such solutions may [...] Read more.
Concepts such as reuse, repurposing, upcycling, remanufacturing, and re-powering can be applied to the reuse of combustion engines from passenger cars and trucks in stationary or mobile machines, such as power generators. Technical, economic, environmental, and research analyses indicate that such solutions may be justified; however, their implementation is limited by homologation and emission regulations. In most countries, there are no specific rules governing emissions from power generator engines, while in the European Union, such engines are categorized as mobile generators (portable or trailer-mounted) subject to Stage V (Reg. 2016/1628/EU), stationary generators (permanently installed) subject to the MCP Directive (2015/2193/EU), and emergency generators (limited operation) partially exempt from MCP but requiring registration. Consequently, engines recovered from road vehicles do not meet formal or technical emission compliance requirements for power generators and can only be used under conditional approval for research, experimental, or temporary purposes. This reveals a paradox of modern environmental policy: although reusing functional engines from dismantled vehicles could embody the principles of a circular economy, restrictive emission standards (Stage V, MCP, NSPS) effectively prevent such technological recycling. Addressing this issue requires legislative action and the development of simplified testing methods for used engines in new applications. This article is the first to systematically demonstrate that current Stage V, MCP and NSPS emission frameworks create a regulatory paradox that prevents the circular-economy reuse of functional automotive engines, and it proposes a dedicated secondary type-approval pathway enabling their legal and environmentally controlled application in power generators. Full article
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33 pages, 6615 KB  
Review
Upcycled Orange Peel Ingredients: A Scoping Review on Phytochemical Composition, Extraction Techniques, and Biorefinery Strategies
by Ana A. Vilas-Boas, Daniela Magalhães, Ricardo Gómez-García, Débora A. Campos, Marta Correia and Manuela Pintado
Foods 2025, 14(21), 3766; https://doi.org/10.3390/foods14213766 - 3 Nov 2025
Viewed by 2674
Abstract
Background/Objectives: Orange peels (OP), a major by-product of the juice industry, are rich in bioactive compounds (phenolic compounds, pectin, carotenoids, and essential oils). Its valorization represents a promising route to reduce food waste and foster a circular bioeconomy. This review aimed to [...] Read more.
Background/Objectives: Orange peels (OP), a major by-product of the juice industry, are rich in bioactive compounds (phenolic compounds, pectin, carotenoids, and essential oils). Its valorization represents a promising route to reduce food waste and foster a circular bioeconomy. This review aimed to map scientific progress in OP upcycling, focusing on the extraction of bioactive ingredients for human nutrition and integrated biorefinery approaches aligned with zero-waste principles. Methods: A bibliometric analysis and a scoping review were conducted covering studies published between 2003 and 2023. Scopus database and VOSviewer was usedto identify research trends, hotspots, and gaps. Conventional and emerging green extraction methods were critically compared, and integrated biorefinery strategies for maximizing OP valorization were systematically assessed. Results: The analysis revealed an exponential rise in OP research over the past decade, reflecting growing interest in sustainable food waste valorization. Polyphenol- and pectin-rich extracts are currently the focus of research and applications, driven by their high economic and nutritional value. Innovative multi-extraction and zero-waste biorefinery models have emerged, yet most remain at low technological readiness levels. Carotenoids and other bioactive compounds remain underexplored, and challenges persist regarding standardization and scalability. Conclusions: OP valorization is shifting towards integrated green extraction and biorefinery frameworks that address clean-label demands, promote circular economy goals, and align with the Sustainable Development Goals. Future research should prioritize (i) standardized protocols, (ii) scalable green extraction technologies, (iii) the inclusion of underutilized compounds such as carotenoids, and (iv) regulatory pathways to accelerate industrial translation. Full article
(This article belongs to the Special Issue Potential Health Benefits of Plant Food-Derived Bioactive Compounds)
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32 pages, 4896 KB  
Review
Catalyst Design and Engineering for Enhanced Microplastic Degradation and Upcycling—A Review
by Chunxiang Zhu, Ge Zeng and Pu-Xian Gao
Catalysts 2025, 15(10), 984; https://doi.org/10.3390/catal15100984 - 14 Oct 2025
Viewed by 1568
Abstract
Microplastics (MPs), defined as synthetic polymer particles ranging from 1 μm to 5 mm, originate from various sources, including synthetic textiles, tire wear, degraded plastic waste, etc. Their small size and chemical stability make them challenging to remove, collect and degrade, posing significant [...] Read more.
Microplastics (MPs), defined as synthetic polymer particles ranging from 1 μm to 5 mm, originate from various sources, including synthetic textiles, tire wear, degraded plastic waste, etc. Their small size and chemical stability make them challenging to remove, collect and degrade, posing significant adverse effects to both ecosystems and human health. While efforts to develop sustainable alternatives and removal methods are ongoing, effective solutions remain limited. Catalytic degradation and upcycling present a promising route to mitigate MP pollution by enabling efficient breakdown into less harmful molecules and potential upcycling into valuable products with lower energy requirements. This review provides a comprehensive overview of recent advances in catalyst design and development specifically for MP degradation, highlighting photochemical, thermal, biological, electrochemical, and hybrid approaches. Key challenges, reaction mechanisms, and future directions are discussed, offering a timely reference for researchers in this emerging field. Full article
(This article belongs to the Special Issue Feature Papers in "Industrial Catalysis" Section, 2nd Edition)
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13 pages, 2897 KB  
Article
Thermal Performance of Silica-Coated Wood Particles
by Elif Yurttaş, Mariem Zouari, Silvo Hribernik and Matthew Schwarzkopf
J. Compos. Sci. 2025, 9(10), 556; https://doi.org/10.3390/jcs9100556 - 10 Oct 2025
Viewed by 810
Abstract
Wood is one of the most widely used sustainable lignocellulosic materials, with numerous applications in consumer goods and the construction sector. Despite its positive properties, such as a high strength-to-weight ratio, thermal insulation, and low density, wood’s natural thermal degradation can limit its [...] Read more.
Wood is one of the most widely used sustainable lignocellulosic materials, with numerous applications in consumer goods and the construction sector. Despite its positive properties, such as a high strength-to-weight ratio, thermal insulation, and low density, wood’s natural thermal degradation can limit its potential applications. In composite applications like wood–plastic composites, the particle morphology and surface topography must be preserved to support intimate polymer–wood contact and mechanical interlocking. This study investigated the efficacy of a thin silica coating for thermal protection, which was applied via an in situ sol–gel method using the precursor tetraethoxysilane (TEOS). The wood particles and treatments were characterized using particle size analysis, physisorption, FTIR, SEM, XRD, and TGA analyses. After treatment, the specific and microporous surface area of wood particles increased by 118% and 97%, respectively, an effect of the porosity of silica itself. FTIR spectra of the silica-treated wood displayed peaks corresponding to Si stretching, and SEM micrographs confirmed a successful silica coating formation. TGA showed that the silica coating increased the temperatures needed to degrade the underlying hemicellulose and cellulose by 16 °C for all treatment levels. This particle-scale coating provided a promising method for producing thermally protected, functionalizable wood fillers for composites that maintain the filler geometry and potential mechanical interlocking, offering an attractive upcycling pathway for wood residues. Full article
(This article belongs to the Section Composites Modelling and Characterization)
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19 pages, 1201 KB  
Article
Sustainable Fashion in Slovenia: Circular Economy Strategies, Design Processes, and Regional Innovation
by Tanja Devetak and Alenka Pavko Čuden
Sustainability 2025, 17(19), 8890; https://doi.org/10.3390/su17198890 - 6 Oct 2025
Cited by 1 | Viewed by 1350
Abstract
This study investigates sustainability-oriented design and production practices in Slovenia, focusing on brand-led approaches grounded in local innovation, cultural heritage and community engagement. Through mapping of Slovenian fashion enterprises, the research identifies and analyzes core sustainability and circularity strategies including zero- and low-waste [...] Read more.
This study investigates sustainability-oriented design and production practices in Slovenia, focusing on brand-led approaches grounded in local innovation, cultural heritage and community engagement. Through mapping of Slovenian fashion enterprises, the research identifies and analyzes core sustainability and circularity strategies including zero- and low-waste design, recycling, upcycling and the development of adaptable, long-lasting garments. Further attention is given to participatory design methods involving consumers, the strategic social media use for community building and service-based circular economy models such as lifetime garment repair. Technological and production innovations, localized supply chains and small-scale production models are assessed for their role in reducing environmental impact and advancing sustainable supply chain management. The study also analyzes initiatives to shorten the fashion loop, including dematerialization and production minimization, as pathways to reduce resource consumption. Methodologically, the study combines empirical fieldwork, participant observation and literature review to deliver a comprehensive analysis of Slovenia’s sustainable fashion sector. The findings contribute to the global discourse on regional and place-based sustainability in fashion demonstrating how design-driven, small- and medium-sized enterprises can integrate circular economy principles, cultural continuity and collaborative innovation to foster environmentally responsible and socially embedded fashion. Full article
(This article belongs to the Special Issue Sustainable Product Design, Manufacturing and Management)
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29 pages, 618 KB  
Review
End-of-Life Strategies for Wind Turbines: Blade Recycling, Second-Life Applications, and Circular Economy Integration
by Natalia Cieślewicz, Krzysztof Pilarski and Agnieszka A. Pilarska
Energies 2025, 18(19), 5182; https://doi.org/10.3390/en18195182 - 29 Sep 2025
Cited by 2 | Viewed by 4007
Abstract
Wind power is integral to the transformation of energy systems towards sustainability. However, the increasing number of wind turbines approaching the end of their service life presents significant challenges in terms of waste management and environmental sustainability. Rotor blades, typically composed of thermoset [...] Read more.
Wind power is integral to the transformation of energy systems towards sustainability. However, the increasing number of wind turbines approaching the end of their service life presents significant challenges in terms of waste management and environmental sustainability. Rotor blades, typically composed of thermoset polymer composites reinforced with glass or carbon fibres, are particularly problematic due to their low recyclability and complex material structure. The aim of this article is to provide a system-level review of current end-of-life strategies for wind turbine components, with particular emphasis on blade recycling and decision-oriented comparison, and its integration into circular economy frameworks. The paper explores three main pathways: operational life extension through predictive maintenance and design optimisation; upcycling and second-life applications; and advanced recycling techniques, including mechanical, thermal, and chemical methods, and reports qualitative/quantitative indicators together with an indicative Technology Readiness Level (TRL). Recent innovations, such as solvolysis, microwave-assisted pyrolysis, and supercritical fluid treatment, offer promising recovery rates but face technological and economic as well as environmental compliance limitations. In parallel, the review considers deployment maturity and economics, including an indicative mapping of cost and deployment status to support decision-making. Simultaneously, reuse applications in the construction and infrastructure sectors—such as concrete additives or repurposed structural elements—demonstrate viable low-energy alternatives to full material recovery, although regulatory barriers remain. The study also highlights the importance of systemic approaches, including Extended Producer Responsibility (EPR), Digital Product Passports and EU-aligned policy/finance instruments, and cross-sectoral collaboration. These instruments are essential for enhancing material traceability and fostering industrial symbiosis. In conclusion, there is no universal solution for wind turbine blade recycling. Effective integration of circular principles will require tailored strategies, interdisciplinary research, and bankable policy support. Addressing these challenges is crucial for minimising the environmental footprint of the wind energy sector. Full article
(This article belongs to the Collection Feature Papers in Energy, Environment and Well-Being)
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27 pages, 3871 KB  
Article
A Cascade Approach to Valorizing Camellia oleifera Abel Shell: Ultrasound-Assisted Extraction Coupled with Resin Purification for High-Efficiency Production of Multifunctional Polyphenols
by Jingyi Chen, Wei Li, Tao Liang, Yuting Yang, Rui Zhou, Rui Li, Daiyu Xie, Dayan Xiang, Shiling Feng, Tao Chen, Lijun Zhou and Chunbang Ding
Antioxidants 2025, 14(10), 1192; https://doi.org/10.3390/antiox14101192 - 29 Sep 2025
Cited by 1 | Viewed by 864
Abstract
Camellia oleifera Abel shell is an abundant lignocellulosic byproduct of the Chinese woody oil industry, which is currently underutilized. To achieve its high-value utilization, this study developed an innovative cascade process integrating ultrasound-assisted extraction and macroporous resin purification for the efficient preparation of [...] Read more.
Camellia oleifera Abel shell is an abundant lignocellulosic byproduct of the Chinese woody oil industry, which is currently underutilized. To achieve its high-value utilization, this study developed an innovative cascade process integrating ultrasound-assisted extraction and macroporous resin purification for the efficient preparation of purified polyphenols from the shell (P-CPCS). The major constituents were identified by quadrupole/Orbitrap high-resolution mass spectrometry (HPLC-Q-Exactive-MS: Biotech Pack Co., Ltd., Beijing, China) analysis. The optimized process significantly enhanced the polyphenol yield (40.05 ± 0.58 mg GAE/g dw) and purity (57.72%), surpassing conventional methods. P-CPCS exhibited exceptional multifunctional bioactivities, including potent antioxidant capacity (with low IC50 values against DPPH, ABTS+·, and ·OH radicals), effective tyrosinase inhibition (whitening effect), and significant bacteriostatic effects against various pathogens. Furthermore, P-CPCS notably suppressed the LPS-induced inflammatory response in RAW264.7 macrophages by reducing NO overproduction. This work highlights a novel and efficient strategy for upcycling agricultural waste into a high-performance natural antioxidant, positioning P-CPCS as a promising ingredient for applications in functional foods, cosmetics, and biomaterial stabilization. Full article
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18 pages, 1182 KB  
Article
Compositional Analysis and Sustainable Valorization of the Calabrian Hazelnut cv. ‘Tonda Calabrese’ and Its Processing Derivatives
by Federica Turrini, Federica Grasso, Aseel Swaidan, Giosuè Costa, Sonia Bonacci, Antonio Procopio, Carmine Lupia, Raffaella Boggia and Stefano Alcaro
Foods 2025, 14(18), 3269; https://doi.org/10.3390/foods14183269 - 20 Sep 2025
Viewed by 1153
Abstract
Hazelnut cultivation is a strategic agricultural sector in Italy, with Calabria contributing through the native “Tonda Calabrese” cultivar, valued for its biodiversity. Despite its importance, data on the nutritional and compositional characteristics of this cultivar remain limited. In this study, hazelnuts from three [...] Read more.
Hazelnut cultivation is a strategic agricultural sector in Italy, with Calabria contributing through the native “Tonda Calabrese” cultivar, valued for its biodiversity. Despite its importance, data on the nutritional and compositional characteristics of this cultivar remain limited. In this study, hazelnuts from three different Calabrian producers were analyzed for morphological traits, proximate composition, and elemental content, using both conventional and non-destructive techniques such as CIELab color profiling and ATR-FTIR spectroscopy. The nuts showed high levels of essential micro-elements (Fe, Cu, Zn), aligning with previous findings on other cultivars, and showed no detectable pesticide residues, confirming their nutritional quality. Moreover, this study also aims to explore sustainable valorization strategies for hazelnut by-products, embracing circular economy principles in a “zero waste” approach, including oils and defatted flours. The extracted oils were evaluated for oxidative stability (peroxide value, p-anisidine, TOTOX index) and acidity, meeting Codex Alimentarius quality standards. The residual defatted flour was upcycled through eco-friendly methods, such as Ultrasound-Assisted Extraction (UAE) and Enzyme-Assisted Extraction (EAE), to isolate the polyphenol and protein fractions, respectively. Both extracts exhibited notable antioxidant activity (34.7–35.3 mmol Fe2+ eq/100 g and 64.3–82.2 mmol Fe2+ eq/100 g, respectively), suggesting their potential use as valuable ingredients for dietetic and nutraceutical applications. Full article
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17 pages, 5170 KB  
Article
Dual-Action Grouper Bone and Wakame Hydrolysates Supplement Enhances Exercise Performance and Modulates Gut Microbiota in Mice
by Huey-Jine Chai, Tsung-Kai Yi, Yi-Feng Kao, Te-Hua Liu, Tsung-Yu Tsai and Yi-Ming Chen
Nutrients 2025, 17(18), 2933; https://doi.org/10.3390/nu17182933 - 11 Sep 2025
Viewed by 883
Abstract
Background: Sustainable, dual-action ergogenic strategies are underexplored; most products target a single pathway and rarely upcycle seafood sidestreams. We therefore tested an upcycled formulation combining grouper bone hydrolysate and Undaria pinnatifida extract (GU) for ergogenic and microbiota effects in mice. We tested [...] Read more.
Background: Sustainable, dual-action ergogenic strategies are underexplored; most products target a single pathway and rarely upcycle seafood sidestreams. We therefore tested an upcycled formulation combining grouper bone hydrolysate and Undaria pinnatifida extract (GU) for ergogenic and microbiota effects in mice. We tested the ergogenic and microbiota modulating effects of GU in mice versus a vehicle and a BCAA control. Methods: GU was prepared via enzymatic hydrolysis of marine by-products and administered to male ICR mice for 4 weeks. Mice were divided into five groups (n = 7/group), receiving a vehicle control, a branched-chain amino acid (BCAA) supplement, or GU at three dose levels (1X, 2X, 3X) based on human-equivalent conversion. Exercise performance was assessed via grip strength and treadmill tests. Biochemical markers of fatigue, body composition, and safety indicators were also analyzed. Gut microbiota was evaluated using 16S rRNA sequencing and constrained principal coordinates analysis (CPCoA). Results: Four weeks of GU supplementation significantly enhanced exercise performance [(treadmill time ↑ Δ = 10.2–11.7 min versus vehicle (q ≤ 0.0002), grip strength ↑ Δ = 40.4–48.5 g (q ≤ 0.05)] and lean body mass [FFM ↑ at GU-1X (Δ = +0.80%, q = 0.0123)], surpassing the commercial BCAA control. Biochemical analyses indicated reduced exercise-induced lactate accumulation [(post-exercise lactate ↓ Δ = −2.71/−2.18 mmol·L−1, q = 0.0006)]. Gut microbiota profiling revealed distinct shifts in community composition in GU-treated groups, notably with an increased abundance of beneficial taxa such as Lactobacillus and Muribaculum. These alterations reflect the prebiotic activity of seaweed-derived polysaccharides, promoting a healthier gut microbial profile. Notably, GU improved metabolic markers (aspartate aminotransferase, [AST]; lactate dehydrogenase, [LDH]) without inducing toxicity. Conclusions: These findings indicate that GU functions as a dual-action supplement, coupling amino acid-mediated muscle anabolism with microbiome modulation to enhance physical performance and metabolic health. As an upcycled marine product, it presents a sustainable and effective strategy for exercise support. Future studies should include 90-day safety, mechanistic assays, and a preregistered human pilot. Full article
(This article belongs to the Topic News and Updates on Probiotics)
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18 pages, 9239 KB  
Article
Sustainable Upcycling of Spent Battery Graphite into High-Performance PEG Anodes via Flash Joule Heating
by Yihan Luo, Jing Sun, Wenxin Chen, Shuo Lu and Ziliang Wang
Recycling 2025, 10(5), 171; https://doi.org/10.3390/recycling10050171 - 2 Sep 2025
Viewed by 1498
Abstract
The upcycling of spent lithium-ion battery graphite constitutes an essential pathway for mitigating manufacturing expenditures and alleviating ecological burdens. This study proposes an integrated strategy to upcycle spent graphite into high-performance porous expanded graphite (PEG) anodes, leveraging flash Joule heating (FJH) as a [...] Read more.
The upcycling of spent lithium-ion battery graphite constitutes an essential pathway for mitigating manufacturing expenditures and alleviating ecological burdens. This study proposes an integrated strategy to upcycle spent graphite into high-performance porous expanded graphite (PEG) anodes, leveraging flash Joule heating (FJH) as a core technique for efficient decontamination, interlayer expansion, and active etching. Results show that the binders and impurities are efficiently removed by FJH treatment, and the graphite interlayer spacing is expanded. The iron oxide, which acts as an etching reagent, can then be easily intercalated and laid into the decontaminated graphite for subsequent etching. A subsequent FJH treatment simultaneously releases oxidized intercalants and triggers in-situ metal oxide etching, yielding PEG with a rich porous architecture and enhanced specific surface area. This method successfully prepared high-performance porous expanded graphite anode material with a mesoporous structure. The resulting anode delivers a remarkable capacity retention of 419 mAh·g−1 after 600 cycles at 2C, outperforming the performance of commercial graphite anodes. This innovative approach offers a promising route for sustainable graphite reclamation. Full article
(This article belongs to the Special Issue Lithium-Ion and Next-Generation Batteries Recycling)
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