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Search Results (647)

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Keywords = uniaxial tensile strength

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10 pages, 2384 KiB  
Article
Effects of Grain Size on Mechanical Properties of Nanopolycrystalline Fe-Al Alloy
by Xiaoming Liu, Kun Gao, Long Huang, Peng Chen and Jing Yang
Processes 2025, 13(8), 2462; https://doi.org/10.3390/pr13082462 - 4 Aug 2025
Viewed by 11
Abstract
FeAl intermetallic compounds exhibit high application potential in high-voltage transmission lines to withstand external forces such as powerlines’ own gravity and wind force. The ordered crystal structure in FeAl intermetallic compounds endows materials with high strength, but the remarkable brittleness at room temperature [...] Read more.
FeAl intermetallic compounds exhibit high application potential in high-voltage transmission lines to withstand external forces such as powerlines’ own gravity and wind force. The ordered crystal structure in FeAl intermetallic compounds endows materials with high strength, but the remarkable brittleness at room temperature restricts engineering applications. This contradiction is essentially closely related to the deformation mechanism at the nanoscale. Here, we performed molecular dynamics simulations to reveal anomalous grain size effects and deformation mechanisms in nanocrystalline FeAl intermetallic material. Models with grain sizes ranging from 6.2 to 17.4 nm were systematically investigated under uniaxial tensile stress. The study uncovers a distinctive inverse Hall-Petch relationship governing flow stress within the nanoscale regime. This behavior stems from high-density grain boundaries promoting dislocation annihilation over pile-up. Crucially, the material exhibits anomalous ductility at ultra-high strain rates due to stress-induced phase transformation dominating the plastic deformation. The nascent FCC phase accommodates strain through enhanced slip systems and inherent low stacking fault energy with the increasing phase fraction paralleling the stress plateau. Nanoconfinement suppresses the propagation of macroscopic defects while simultaneously suppressing room-temperature brittle fracture and inhibiting the rapid phase transformation pathways at extreme strain rates. These findings provide new theoretical foundations for designing high-strength and high-toughness intermetallic nanocompounds. Full article
(This article belongs to the Section Materials Processes)
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23 pages, 8489 KiB  
Article
Validation of the Pull-Back Method for Dynamic Tensile Strength Characterization in Unidirectional Reinforced Concrete
by Xinlu Yu, Junfeng Zhang and Junhui Gu
Appl. Sci. 2025, 15(15), 8369; https://doi.org/10.3390/app15158369 - 28 Jul 2025
Viewed by 244
Abstract
The pull-back method for determining dynamic tensile strength assumes one-dimensional stress wave propagation and material homogeneity. This study validates these assumptions for unidirectional reinforced concrete (UDRC) through experiments and numerical simulations. Split Hopkinson pressure bar tests were conducted on plain concrete, plain UDRC, [...] Read more.
The pull-back method for determining dynamic tensile strength assumes one-dimensional stress wave propagation and material homogeneity. This study validates these assumptions for unidirectional reinforced concrete (UDRC) through experiments and numerical simulations. Split Hopkinson pressure bar tests were conducted on plain concrete, plain UDRC, and deformed UDRC specimens containing a central 6 mm steel bar. Ultra-high-speed digital image correlation at 500,000 fps enabled precise local strain rate measurements (3 s−1 to 55 s−1) at fracture locations. Finite element simulations revealed that while reinforcement induces localized multi-axial stresses near the steel–concrete interface, the bulk concrete maintains predominantly uniaxial stress conditions. Experimental results showed less than 1% variation in pull-back velocity between specimen types. Statistical analysis confirmed a unified strain rate-strength relationship: σspall=4.1+4.7log10(ε˙)MPa, independent of reinforcement configuration (ANCOVA: p=0.2182 for interaction term). The dynamic tensile strength is governed by concrete matrix properties rather than reinforcement type. These findings are the first to experimentally and numerically validate the pull-back method’s applicability to UDRC systems, establishing that dynamic tensile failure is matrix-dominated and enabling simplified one-dimensional analysis for reinforced concrete under impact. Full article
(This article belongs to the Section Civil Engineering)
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29 pages, 8597 KiB  
Article
Study on the Damage Mechanisms in the Forming Process of High-Strength Steel Laser Tailor Welded Blanks Based on the Johnson–Cook Damage Model
by Xianping Sun, Huaqiang Li, Song Gao and Qihan Li
Materials 2025, 18(15), 3497; https://doi.org/10.3390/ma18153497 - 25 Jul 2025
Viewed by 613
Abstract
This paper, based on the Johnson–Cook damage model, investigates the damage mechanism of high-strength steel tailor welded blanks (TWBs) (Usibor1500P and Ductibor500) during the forming process. Initially, specimens with varying notch sizes were designed and fabricated to perform uniaxial tensile tests to determine [...] Read more.
This paper, based on the Johnson–Cook damage model, investigates the damage mechanism of high-strength steel tailor welded blanks (TWBs) (Usibor1500P and Ductibor500) during the forming process. Initially, specimens with varying notch sizes were designed and fabricated to perform uniaxial tensile tests to determine their mechanical properties. Then, the deformation process of the notched specimens was simulated using finite element software, revealing the distribution and variation of stress triaxiality at the fracture surface. By combining both experimental and simulation data, the parameters of the Johnson–Cook (J–C) damage model were calibrated, and the effects of temperature, strain rate, and stress triaxiality on material fracture behavior were further analyzed. Based on finite element analysis, the relevant coefficients for stress triaxiality, strain rate, and temperature were systematically calibrated, successfully establishing a J–C fracture criterion for TWB welds, Usibor1500P, and Ductibor500 high-strength steels. Finally, the calibrated damage model was further validated through the Nakajima-type bulge test, and the simulated Forming Limit Diagram (FLD) closely matched the experimental data. The results show that the analysis based on the J–C damage model can effectively predict the fracture behavior of tailor welded blanks (TWB) during the forming process. This study provides reliable numerical predictions for the damage behavior of high-strength steel laser-customized welded sheets and offers a theoretical basis for engineering design and material performance optimization. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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17 pages, 3279 KiB  
Article
Rapid Assessment of Ti-6Al-4V Fatigue Limit via Infrared Thermography
by Chiara Colombo, Antonio Salerno, Arthur Teyssiéras and Carlo Alberto Biffi
Metals 2025, 15(8), 825; https://doi.org/10.3390/met15080825 - 23 Jul 2025
Viewed by 261
Abstract
The experimental tests needed for the estimation of the fatigue limit generally require extensive time and many specimens. A valid but not standardized alternative is the thermographic analysis of the self-heating phenomenon. The present work is aimed at using Infrared thermography to determine [...] Read more.
The experimental tests needed for the estimation of the fatigue limit generally require extensive time and many specimens. A valid but not standardized alternative is the thermographic analysis of the self-heating phenomenon. The present work is aimed at using Infrared thermography to determine the fatigue limit in two kinds of Ti-6Al-4V samples obtained by hot rolling: (1) with the standard dog-bone shape (unnotched specimen) and (2) with two opposed semicircular notches at the sides (notched specimen). Uniaxial tensile experiments are performed on unnotched samples, and the surface temperature variation during loading is monitored. The stress corresponding to the end of the thermoelastic stage gives a rough indication of the fatigue limit. Then, fatigue tests at different sinusoidal loads are performed, and the thermographic signal is monitored and processed. The results obtained using lock-in thermography in dissipative mode, e.g., analyzing the second harmonic, showed a sudden change in slope when the applied stress exceeded a certain limit. This slope change is related to the fatigue limit. In addition, the ratio between the fatigue limits obtained for notched and unnotched specimens, e.g., the fatigue strength reduction factor, is consistent with literature values based on the selected geometry. Full article
(This article belongs to the Special Issue Fracture Mechanics of Metals (2nd Edition))
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12 pages, 732 KiB  
Article
Umbilical Cord Tensile Strength Under Varying Strain Rates
by Maria Antonietta Castaldi, Pietro Villa, Alfredo Castaldi and Salvatore Giovanni Castaldi
Bioengineering 2025, 12(8), 789; https://doi.org/10.3390/bioengineering12080789 - 22 Jul 2025
Viewed by 248
Abstract
The tensile strength of the umbilical cord (UC) is influenced by its composition—including collagen, elastin, and hyaluronan—contributing to its unique biomechanical properties. This experimental in vitro study aimed to evaluate the UC’s mechanical behavior under varying strain rates and to characterize its viscoelastic [...] Read more.
The tensile strength of the umbilical cord (UC) is influenced by its composition—including collagen, elastin, and hyaluronan—contributing to its unique biomechanical properties. This experimental in vitro study aimed to evaluate the UC’s mechanical behavior under varying strain rates and to characterize its viscoelastic response. Twenty-nine UC specimens, each 40 mm in length, were subjected to uniaxial tensile testing and randomly assigned to three traction speed groups: Group A (n = 10) at 8 mm/min, Group B (n = 7) at 12 mm/min, and Group C (n = 12) at 16 mm/min. Four different parameters were analyzed: the ultimate tensile strength and its corresponding elongation, the elastic modulus defined as the slope of the linear initial portion of the stress–strain plot, and the elongation at the end of the test (at break). While elongation and elongation at break did not differ significantly between groups (one-way ANOVA), Group C showed a significantly higher ultimate tensile strength (p = 0.047). A linear relationship was observed between test speed and stiffness (elastic modulus), with the following regression equation: y = 0.3078e4.425x. These findings confirm that the UC exhibits nonlinear viscoelastic properties and strain-rate-dependent stiffening, resembling non-Newtonian behavior. This novel insight may have clinical relevance during operative deliveries, where traction speed is often overlooked but may play a role in preserving cord integrity and improving neonatal outcomes. Full article
(This article belongs to the Section Biosignal Processing)
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22 pages, 13284 KiB  
Article
Mechanical Properties of CuZr Amorphous Metallic Nanofoam at Various Temperatures Investigated by Molecular Dynamics Simulation
by Yuhang Zhang, Hongjian Zhou and Xiuming Liu
Materials 2025, 18(14), 3423; https://doi.org/10.3390/ma18143423 - 21 Jul 2025
Viewed by 438
Abstract
Metallic nanofoams with amorphous structures demonstrate exceptional properties and significant potential for diverse applications. However, their mechanical properties at different temperatures are still unclear. By using molecular dynamics simulation, this study investigates the mechanical responses of representative CuZr amorphous metallic nanofoam (AMNF) under [...] Read more.
Metallic nanofoams with amorphous structures demonstrate exceptional properties and significant potential for diverse applications. However, their mechanical properties at different temperatures are still unclear. By using molecular dynamics simulation, this study investigates the mechanical responses of representative CuZr amorphous metallic nanofoam (AMNF) under uniaxial tension and compression at various temperatures. Our results reveal that the mechanical properties, such as Young’s modulus, yield stress, and maximum stress, exhibit notable temperature sensitivity and tension–compression asymmetry. Under tensile loading, the Young’s modulus, yield strength, and peak stress exhibit significant reductions of approximately 30.5%, 33.3%, and 32.9%, respectively, as the temperature increases from 100 K to 600 K. Similarly, under compressive loading, these mechanical properties experience even greater declines, with the Young’s modulus, yield strength, and peak stress decreasing by about 34.5%, 38.0%, and 41.7% over the same temperature range. The tension–compression asymmetry in yield strength is temperature independent. Interestingly, the tension–compression asymmetry in elastic modulus becomes more pronounced at elevated temperatures, which is attributed to the influence of surface energy effects. This phenomenon is further amplified by the increased disparity in surface-area-to-volume ratio variations between tensile and compressive loading at higher temperatures. Additionally, as the temperature rises, despite material softening, the structural resistance under large tensile strains improves due to delayed ligament degradation and more uniform deformation distribution, delaying global failure. Full article
(This article belongs to the Section Mechanics of Materials)
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22 pages, 3727 KiB  
Article
Johnson–Cook Constitutive Model Parameters Estimation of 22MnB5 Hot Stamping Steel for Automotive Application Produced via the TSCR Process
by Yuxin Song, Yaowen Xu and Gengwei Yang
Metals 2025, 15(7), 811; https://doi.org/10.3390/met15070811 - 20 Jul 2025
Viewed by 2813
Abstract
In the industrial practice of metal forming, the consistent and reasonable characterization of the material behavior under the coupling effect of strain, strain rate, and temperature on the material flow stress is very important for the design and optimization of process parameters. The [...] Read more.
In the industrial practice of metal forming, the consistent and reasonable characterization of the material behavior under the coupling effect of strain, strain rate, and temperature on the material flow stress is very important for the design and optimization of process parameters. The purpose of this work was to establish an appropriate constitutive model to characterize the rheological behavior of a hot-formed steel plate (22MnB5 steel) produced through the TSCR (Thin Slab Casting and Rolling) process under practical deformation temperatures (150–250 °C) and strain rates (0.001–3000 s−1). Subsequently, the material flow behavior was modeled and predicted using the Johnson–Cook flow stress constitutive model. In this study, uniaxial tensile tests were conducted on 22MnB5 steel at room temperature under varying strain rates, along with elevated-temperature tensile tests at different strain rates, to obtain the engineering stress–strain curves and analyze the mechanical properties under various conditions. The results show that during room-temperature tensile testing within the strain rate range of 10−3 to 300 s−1, the 22MnB5 steel exhibited overall yield strength and tensile strength of approximately 1500 MPa, and uniform elongation and fracture elongation of about 7% and 12%, respectively. When the strain rate reached 1000–3000 s−1, the yield strength and tensile strength were approximately 2000 MPa, while the uniform elongation and fracture elongation were about 6% and 10%, respectively. Based on the experimental results, a modified Johnson–Cook constitutive model was developed and calibrated. Compared with the original model, the modified Johnson–Cook model exhibited a higher coefficient of determination (R2), indicating improved fitting accuracy. In addition, to predict the material’s damage behavior, three distinct specimen geometries were designed for quasi-static strain rate uniaxial tensile testing at ambient temperature. The Johnson–Cook failure criterion was implemented, with its constitutive parameters calibrated through integrated finite element analysis to establish the damage model. The determined damage parameters from this investigation can be effectively implemented in metal forming simulations, providing valuable predictive capabilities regarding workpiece material performance. Full article
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33 pages, 167102 KiB  
Article
Influence of Mineralogical and Petrographic Properties on the Mechanical Behavior of Granitic and Mafic Rocks
by Muhammad Faisal Waqar, Songfeng Guo, Shengwen Qi, Malik Aoun Murtaza Karim, Khan Zada, Izhar Ahmed and Yanjun Shang
Minerals 2025, 15(7), 747; https://doi.org/10.3390/min15070747 - 17 Jul 2025
Viewed by 363
Abstract
This study investigates the impact of mineralogical and petrographic characteristics on the mechanical behavior of granitic and mafic rocks from the Shuangjiangkou (Sichuan Province) and Damiao complexes (Hebei Province) in China. The research methodology combined petrographic investigation, comprising optical microscopy and Scanning Electron [...] Read more.
This study investigates the impact of mineralogical and petrographic characteristics on the mechanical behavior of granitic and mafic rocks from the Shuangjiangkou (Sichuan Province) and Damiao complexes (Hebei Province) in China. The research methodology combined petrographic investigation, comprising optical microscopy and Scanning Electron Microscopy–Energy-Dispersive X-ray Spectroscopy (SEM-EDS) methods, with methodical geotechnical characterization to establish quantitative relationships between mineralogical composition and engineering properties. The petrographic studies revealed three lithologic groups: fine-to-medium-grained Shuangjiangkou granite (45%–60% feldspar, 27%–35% quartz, 10%–15% mica), plagioclase-rich anorthosite (more than 90% of plagioclase), and intermediate mangerite (40%–50% of plagioclase, 25%–35% of perthite). The uniaxial compressive strength tests showed great variations: granite (127.53 ± 15.07 MPa), anorthosite (167.81 ± 23.45 MPa), and mangerite (205.12 ± 23.87 MPa). Physical properties demonstrated inverse correlations between mechanical strength and both water absorption (granite: 0.25%–0.42%; anorthosite: 0.07%–0.44%; mangerite: 0.10%–0.25%) and apparent porosity (granite: 0.75%–0.92%; anorthosite: 0.20%–1.20%; mangerite: 0.29%–0.69%), with positive correlations to specific gravity (granite: 1.88–3.03; anorthosite: 2.67–2.90; mangerite: 2.43–2.99). Critical petrographic features controlling mechanical behavior include the following: (1) mica content in granite creating anisotropic properties, (2) extensive feldspar alteration through sericitization increasing microporosity and reducing intergranular cohesion, (3) plagioclase micro-fracturing and alteration to clinozoisite–sericite assemblages in anorthosite creating weakness networks, and (4) mangerite’s superior composition of >95% hard minerals with minimal sheet mineral content and limited alteration. Failure mode analysis indicated distinct patterns: granite experiencing shear-dominated failure (30–45° diagonal planes), anorthosite demonstrated tensile fracturing with vertical splitting, and mangerite showed catastrophic brittle failure with extensive fracture networks. These findings provide quantitative frameworks that relate petrographic features to engineering behavior, offering valuable insights for rock mass assessment and engineering design in similar crystalline rock terrains. Full article
(This article belongs to the Special Issue Characterization of Geological Material at Nano- and Micro-scales)
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27 pages, 5072 KiB  
Article
Study on the Mechanical Properties of Optimal Water-Containing Basalt Fiber-Reinforced Concrete Under Triaxial Stress Conditions
by Kaide Liu, Songxin Zhao, Yaru Guo, Wenping Yue, Chaowei Sun, Yu Xia, Qiyu Wang and Xinping Wang
Materials 2025, 18(14), 3358; https://doi.org/10.3390/ma18143358 - 17 Jul 2025
Viewed by 210
Abstract
In response to the high-performance requirements of concrete materials under complex triaxial stress states and water-containing environments in marine engineering, this study focuses on water-containing basalt fiber-reinforced concrete (BFRC). Uniaxial compression and splitting tensile tests were conducted on specimens with different fiber contents [...] Read more.
In response to the high-performance requirements of concrete materials under complex triaxial stress states and water-containing environments in marine engineering, this study focuses on water-containing basalt fiber-reinforced concrete (BFRC). Uniaxial compression and splitting tensile tests were conducted on specimens with different fiber contents (0.0%, 0.05%, 0.10%, 0.15%, and 0.20%) to determine the optimal fiber content of 0.1%. The compressive strength of the concrete with this fiber content increased by 13.5% compared to the control group without fiber, reaching 36.90 MPa, while the tensile strength increased by 15.9%, reaching 2.33 MPa. Subsequently, NMR and SEM techniques were employed to analyze the internal pore structure and micro-morphology of BFRC. It was found that an appropriate amount of basalt fiber (content of 0.1%) can optimize the pore structure and form a reticular three-dimensional structure. The pore grading was also improved, with the total porosity decreasing from 7.48% to 7.43%, the proportion of harmless pores increasing from 4.03% to 4.87%, and the proportion of harmful pores decreasing from 1.67% to 1.42%, thereby significantly enhancing the strength of the concrete. Further triaxial compression tests were conducted to investigate the mechanical properties of BFRC under different confining pressures (0, 3, and 6 MPa) and water contents (0%, 1%, 2%, and 4.16%). The results showed that the stress–strain curves primarily underwent four stages: initial crack compaction, elastic deformation, yielding, and failure. In terms of mechanical properties, when the confining pressure increased from 0 MPa to 6 MPa, taking dry sandstone as an example, the peak stress increased by 54.0%, the elastic modulus increased by 15.7%, the peak strain increased by 37.0%, and the peak volumetric strain increased by 80.0%. In contrast, when the water content increased from 0% to 4.16%, taking a confining pressure of 0 MPa as an example, the peak stress decreased by 27.4%, the elastic modulus decreased by 43.2%, the peak strain decreased by 59.3%, and the peak volumetric strain decreased by 106.7%. Regarding failure characteristics, the failure mode shifted from longitudinal splitting under no confining pressure to diagonal shear under confining pressure. Moreover, as the confining pressure increased, the degree of failure became more severe, with more extensive cracks. However, when the water content increased, the failure degree was relatively mild, but it gradually worsened with further increases in water content. Based on the CDP model, a numerical model for simulating the triaxial compression behavior of BFRC was developed. The simulation results exhibited strong consistency with the experimental data, thereby validating the accuracy and applicability of the model. Full article
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19 pages, 40657 KiB  
Article
Development and Analysis of a Sustainable Interlayer Hybrid Unidirectional Laminate Reinforced with Glass and Flax Fibres
by York Schwieger, Usama Qayyum and Giovanni Pietro Terrasi
Polymers 2025, 17(14), 1953; https://doi.org/10.3390/polym17141953 - 16 Jul 2025
Viewed by 257
Abstract
In this study, a new fibre combination for an interlayer hybrid fibre-reinforced polymer laminate was investigated to achieve pseudo-ductile behaviour in tensile tests. The chosen high-strain fibre for this purpose was S-Glass, and the low-strain fibre was flax. These materials were chosen because [...] Read more.
In this study, a new fibre combination for an interlayer hybrid fibre-reinforced polymer laminate was investigated to achieve pseudo-ductile behaviour in tensile tests. The chosen high-strain fibre for this purpose was S-Glass, and the low-strain fibre was flax. These materials were chosen because of their relatively low environmental impact compared to carbon/carbon and carbon/glass hybrids. An analytical model was used to find an ideal combination of the two materials. With that model, the expected stress–strain relation could also be predicted analytically. The modelling was based on preliminary tensile tests of the two basic components investigated in this research: unidirectional laminates reinforced with either flax fibres or S-Glass fibres. Hybrid specimens were then designed, produced in a heat-assisted pressing process, and subjected to tensile tests. The strain measurement was performed using distributed fibre optic sensing. Ultimately, it was possible to obtain repeatable pseudo-ductile stress–strain behaviour with the chosen hybrid when the specimens were subjected to quasi-static uniaxial tension in the direction of the fibres. The intended damage-mode, consisting of a controlled delamination at the flax-fibre/glass-fibre interface after the flax fibres failed, followed by a load transfer to the glass fibre layers, was successfully achieved. The pseudo-ductile strain averaged 0.52% with a standard deviation of 0.09%, and the average load reserve after delamination was 145.5 MPa with a standard deviation of 48.5 MPa. The integrated fibre optic sensors allowed us to monitor and verify the damage process with increasing strain and load. Finally, the analytical model was compared to the measurements and was partially modified by neglecting the Weibull strength distribution of the high-strain material. Full article
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15 pages, 1602 KiB  
Article
Correlation Analysis of Macro–Micro Parameters of Sandstone Based on PFC3D
by Guohua Zhang, Qingqing Liu, Yubo Li, Zibo Li, Ke Jing and Tao Qin
Appl. Sci. 2025, 15(14), 7878; https://doi.org/10.3390/app15147878 - 15 Jul 2025
Viewed by 199
Abstract
To address the issue of the low compression–tension ratio in the traditional parallel bond model (PBM), this study proposes an improved PBM incorporating a random distribution strategy of strong–weak contact groups. An L27(312) orthogonal experimental design was employed to [...] Read more.
To address the issue of the low compression–tension ratio in the traditional parallel bond model (PBM), this study proposes an improved PBM incorporating a random distribution strategy of strong–weak contact groups. An L27(312) orthogonal experimental design was employed to construct 27 sets of numerical simulation schemes. Combined with Pearson correlation coefficient analysis and multivariate regression, the influence of twelve microscopic parameters on seven of the macroscopic mechanical properties of sandstone was systematically investigated, including elastic modulus (E), Poisson’s ratio (v), uniaxial compressive strength (σc), internal friction angle (φ), cohesion (c), crack damage stress ratio (σcd/σc), and compressive–tensile strength ratio (σc/σt). Based on these analyses, a quantitative relationship model between the macro and micro parameters was established and validated through numerical simulation and experimental comparison. The proposed method provides a theoretical foundation for the mechanical modeling of sandstone and the inversion of microscopic parameters. Full article
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23 pages, 8675 KiB  
Article
Research on the Deterioration Mechanism of PPF Mortar-Masonry Stone Structures Under Freeze–Thaw Conditions
by Jie Dong, Hongfeng Zhang, Zhenhuan Jiao, Zhao Yang, Shaohui Chu, Jinfei Chai, Song Zhang, Lunkai Gong and Hongyu Cui
Buildings 2025, 15(14), 2468; https://doi.org/10.3390/buildings15142468 - 14 Jul 2025
Viewed by 296
Abstract
Significant progress has been made in the low-temperature toughness and crack resistance of polypropylene fiber-reinforced composites. However, there is still a gap in the research on damage evolution under freeze–thaw cycles and complex stress ratios. To solve the problem of durability degradation of [...] Read more.
Significant progress has been made in the low-temperature toughness and crack resistance of polypropylene fiber-reinforced composites. However, there is still a gap in the research on damage evolution under freeze–thaw cycles and complex stress ratios. To solve the problem of durability degradation of traditional rubble masonry in cold regions, this paper focuses on the study of polypropylene fiber-mortar-masonry blocks with different fiber contents. Using acoustic emission and digital image technology, the paper conducts a series of tests on the scaled-down polypropylene fiber-mortar-masonry structure, including uniaxial compressive tests, three-point bending tests, freeze–thaw cycle tests, and tests with different stress ratios. Based on the Kupfer criterion, a biaxial failure criterion for polypropylene fiber mortar-masonry stone (PPF-MMS) was established under different freeze–thaw cycles. A freeze–thaw damage evolution model was also developed under different stress ratios. The failure mechanism of PPF-MMS structures was analyzed using normalized average deviation (NAD), RA-AF, and other parameters. The results show that when the dosage of PPF is 0.9–1.1 kg/m3, it is the optimal content. The vertical stress shows a trend of increasing first and then decreasing with the increase in the stress ratio, and when α = 0.5, the degree of strength increase reaches the maximum. However, the freeze–thaw cycle has an adverse effect on the internal structure of the specimens. Under the same number of freeze–thaw cycles, the strength of the specimens without fiber addition decreases more rapidly than that with fiber addition. The NAD evolution rate exhibits significant fluctuations during the middle loading period and near the damage failure, which can be considered precursors to specimen cracking and failure. RA-AF results showed that the specimens mainly exhibited tensile failure, but the occurrence of tensile failure gradually decreased as the stress ratio increased. Full article
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21 pages, 4000 KiB  
Article
Structure-Properties Correlations of PVA-Cellulose Based Nanocomposite Films for Food Packaging Applications
by Konstantinos Papapetros, Georgios N. Mathioudakis, Dionysios Vroulias, Nikolaos Koutroumanis, George A. Voyiatzis and Konstantinos S. Andrikopoulos
Polymers 2025, 17(14), 1911; https://doi.org/10.3390/polym17141911 - 10 Jul 2025
Viewed by 386
Abstract
Bio-nanocomposites based on poly (vinyl alcohol) (PVA) and cellulosic nanostructures are favorable for active food packaging applications. The current study systematically investigates the mechanical properties, gas permeation, and swelling parameters of PVA composites with cellulose nanocrystals (CNC) or nano lignocellulose (NLC) fibers. Alterations [...] Read more.
Bio-nanocomposites based on poly (vinyl alcohol) (PVA) and cellulosic nanostructures are favorable for active food packaging applications. The current study systematically investigates the mechanical properties, gas permeation, and swelling parameters of PVA composites with cellulose nanocrystals (CNC) or nano lignocellulose (NLC) fibers. Alterations in these macroscopic properties, which are critical for food packaging applications, are correlated with structural information at the molecular level. Strong interactions between the fillers and polymer host matrix were observed, while the PVA crystallinity exhibited a maximum at ~1% loading. Finally, the orientation of the PVA nanocrystals in the uniaxially stretched samples was found to depend non-monotonically on the CNC loading and draw ratio. Concerning the macroscopic properties of the composites, the swelling properties were reduced for the D1 food simulant, while for water, a considerable decrease was observed only when high NLC loadings were involved. Furthermore, although the water vapor transmission rates are roughly similar for all samples, the CO2, N2, and O2 gas permeabilities are low, exhibiting further decrease in the 1% and 1–5% loading for CNC and NLC composites, respectively. The mechanical properties were considerably altered as a consequence of the good dispersion of the filler, increased crystallinity of the polymer matrix, and morphology of the filler. Thus, up to ~50%/~170% enhancement of the Young’s modulus and up to ~20%/~50% enhancement of the tensile strength are observed for the CNC/NLC composites. Interestingly, the elongation at break is also increased by ~20% for CNC composites, while it is reduced by ~40% for the NLC composites, signifying the favorable/unfavorable interactions of cellulose/lignin with the matrix. Full article
(This article belongs to the Special Issue Cellulose and Its Composites: Preparation and Applications)
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21 pages, 13213 KiB  
Article
Experimental Study on Mechanical Properties of European Oak and Norway Spruce Clear Wood
by Serena Gambarelli, Josipa Bošnjak, Rey Noé Fararoni Platas and Kexin Jin
Materials 2025, 18(14), 3257; https://doi.org/10.3390/ma18143257 - 10 Jul 2025
Viewed by 309
Abstract
The trends in the building industry related to sustainability and environmental footprint make timber structures more appealing than ever. Many challenges in understanding the behaviour of structural timber can be addressed by combining experimental and numerical methods. However, sophisticated numerical tools require a [...] Read more.
The trends in the building industry related to sustainability and environmental footprint make timber structures more appealing than ever. Many challenges in understanding the behaviour of structural timber can be addressed by combining experimental and numerical methods. However, sophisticated numerical tools require a complete description of the behaviour at the material level. Even though there are vast databases on the properties of different species, there are only limited studies on the mechanical response with complete stress–strain curves for all relevant directions. In order to bridge this gap, the present study investigates the mechanical response of European oak (hardwood) and Norway spruce (softwood). Uniaxial tensile and compressive tests were performed on small clear wood specimens. The behaviour was investigated for the direction parallel (longitudinal) and perpendicular to the grain (radial and tangential). Both species exhibit brittle tensile behaviour in all material directions, in contrast to the ductile performance under compression. The tensile strength lies at 70 MPa and 80 MPa for spruce and oak, respectively, whereas both species exhibit a compressive strength of approximately 50 MPa in the longitudinal direction. Due to the narrow range of the investigated density, growth-ring angle and growth-ring width, only a limited effect of these parameters was observed on the tensile behaviour in the longitudinal direction. Full article
(This article belongs to the Section Mechanics of Materials)
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20 pages, 2412 KiB  
Article
Strength Parameters and Failure Criterion of Granite After High-Temperature and Water-Cooling Treatment
by Jincai Yu, Cheng Cheng, Yuan Xie and Peng Chen
Appl. Sci. 2025, 15(13), 7481; https://doi.org/10.3390/app15137481 - 3 Jul 2025
Viewed by 319
Abstract
Granite is the main rock type in hot dry rock reservoirs, and hydraulic fracturing is always required during the process of geothermal production. It is necessary to understand the strength parameters and failure criterion of granite after high-temperature and water-cooling treatment. In this [...] Read more.
Granite is the main rock type in hot dry rock reservoirs, and hydraulic fracturing is always required during the process of geothermal production. It is necessary to understand the strength parameters and failure criterion of granite after high-temperature and water-cooling treatment. In this paper, laboratory uniaxial and triaxial compression experiments are carried out on granite samples after high-temperature and water-cooling treatment. Combined with some experimental data collected from pre-existing studies, the variation behaviors of cohesion (c), the internal friction angle (φ) and tensile strength σt are systematically studied considering the heating and cooling treatment. It is found that c and φ generally show two different types of variation behaviors with the increasing heating temperature. Tensile strength decreases in a similar way for the different granite samples with the increasing treatment temperature. Empirical equations are provided to describe these strength parameters. Finally, a modified Mohr–Coulomb failure criterion with a “tension cut-off” is established for the granite samples, considering the effects of high-temperature and water-cooling treatment. This study should be helpful for understanding the mechanical behavior of hot dry rock during hydraulic fracturing in geothermal production, and the proposed failure criterion can be applied for the numerical modeling of reservoirs. Full article
(This article belongs to the Special Issue Advances in Geotechnical and Geological Engineering)
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