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Keywords = tribology

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27 pages, 2823 KB  
Article
Effects of Post-Heat Treatment on Mechanical and Tribological Properties of 3D-Printed PLA and PEEK Structures
by Yunxiang Deng and Li Chang
Polymers 2026, 18(2), 253; https://doi.org/10.3390/polym18020253 (registering DOI) - 16 Jan 2026
Abstract
In the present study, post-heat treatment was applied to improve the mechanical and tribological performance of 3D-printed polymer components. Two polymers, i.e., polylactic acid (PLA) and polyether ether ketone (PEEK), were used as base materials. Re-entrant structures were incorporated into printed specimens to [...] Read more.
In the present study, post-heat treatment was applied to improve the mechanical and tribological performance of 3D-printed polymer components. Two polymers, i.e., polylactic acid (PLA) and polyether ether ketone (PEEK), were used as base materials. Re-entrant structures were incorporated into printed specimens to mitigate friction-induced vibrations (FIV). The results showed that the heat-treatment process effectively enhanced the mechanical properties of both materials by increasing their elastic modulus and yield strength. Specifically, the tensile and compressive strengths of heat-treated PLA increased from 44.14 MPa to 47.66 MPa and from 68 MPa to 82 MPa, respectively. A similar trend was observed for heat-treated PEEK, with tensile strength increasing from 75.53 MPa to 84.91 MPa and compressive strength from 106 MPa to 123 MPa. Furthermore, the increased stiffness enabled the re-entrant structures to more effectively reduce FIV during the sliding process of specimens. However, heat treatment produced contrasting effects on the wear performance of the two polymers. The specific wear rate of the heat-treated PLA sample with the re-entrant structure increased from 2.36 × 10−5 mm3/(N · m) to 4.5 × 10−4 mm3/(N · m), while it decreased for the PEEK sample from 3.18 × 10−6 mm3/(N · m) to 6.2 × 10−7 mm3/(N · m). Microscopic observations revealed that this difference was due to the variations in the brittleness of the treated materials, which influenced wear-debris formation and the development of the transfer film on the steel counterface. These findings demonstrate that post-heat treatment is an effective method for tailoring and optimizing the mechanical behavior of printed polymers while also emphasizing the necessity of systematically evaluating its influence on the tribological performance of printed engineering parts subjected to different sliding conditions. Full article
18 pages, 6562 KB  
Article
Optimal CeO2 Doping for Synergistically Enhanced Mechanical, Tribological, and Thermal Properties in Zirconia Ceramics
by Feifan Chen, Yongkang Liu, Zhenye Tang, Xianwen Zeng, Yuwei Ye and Hao Chen
Materials 2026, 19(2), 362; https://doi.org/10.3390/ma19020362 - 16 Jan 2026
Abstract
CeO2 doping is a well-established strategy for enhancing the properties of zirconia (ZrO2) ceramics, with the prior literature indicating an optimal doping range of around 10–15 wt.% for specific attributes. Building upon this foundation, this study provides a systematic investigation [...] Read more.
CeO2 doping is a well-established strategy for enhancing the properties of zirconia (ZrO2) ceramics, with the prior literature indicating an optimal doping range of around 10–15 wt.% for specific attributes. Building upon this foundation, this study provides a systematic investigation into the concurrent evolution of mechanical, tribological, and thermophysical properties across a broad compositional spectrum (0–20 wt.% CeO2). The primary novelty lies in the holistic correlation of these often separately examined properties, revealing their interdependent trade-offs governed by microstructural development. The 15Ce-ZrO2 composition, consistent with the established optimal range, achieved a synergistic balance: hardness increased by 27.6% to 310 HV1, the friction coefficient was minimized to 0.205, and the wear rate was reduced to 1.81 × 10−3 mm3/(N m). Thermally, it exhibited a 72.2% reduction in the thermal expansion coefficient magnitude at 1200 °C and a low thermal conductivity of 0.612 W/(m·K). The enhancement mechanisms are consistent with solid solution strengthening, grain refinement, and likely enhanced phonon scattering, potentially from point defects such as oxygen vacancies commonly associated with aliovalent doping in oxide ceramics, while performance degradation beyond 15 wt.% is linked to CeO2 agglomeration and duplex microstructure formation. This work provides a relatively comprehensive insight into the dataset and mechanism, which is conducive to the fine design of multifunctional ZrO2 bulk ceramics. It is not limited to determining the optimal doping level, but also aims to clarify the comprehensive performance map, providing reference significance for the development of advanced ceramic materials with synergistically optimized hardness, wear resistance, and thermal properties. Full article
(This article belongs to the Section Advanced and Functional Ceramics and Glasses)
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13 pages, 5889 KB  
Article
Metallic Structures and Tribological Properties of Ti-15mass%Nb Alloy After Gas Nitriding and Quenching Process
by Yoshikazu Mantani, Riho Takahashi, Tomoyuki Homma and Eri Akada
Metals 2026, 16(1), 98; https://doi.org/10.3390/met16010098 - 16 Jan 2026
Abstract
This study aimed to experimentally investigate the differences in metallic structures owing to the gas nitriding and quenching process (GNQP) temperature of the Ti-15mass%Nb alloy and differences in the tribological properties of the surface layer. The GNQP heating temperature was 1023 K or [...] Read more.
This study aimed to experimentally investigate the differences in metallic structures owing to the gas nitriding and quenching process (GNQP) temperature of the Ti-15mass%Nb alloy and differences in the tribological properties of the surface layer. The GNQP heating temperature was 1023 K or 1223 K, and the holding time was set to 1 h. In the X-ray diffraction profiles, the diffraction peak of the (101¯1) plane of the hexagonal close-packed phase exhibited a shift toward lower angles, following the sequence AN:α, AQ:α′, and GNQP:α-TiN0.3. In both the 1023 K and 1223 K GNQP specimens, the α″ phase exhibited lower values than the α′ phase; nonetheless, it still exhibited larger values than the annealed α phase. Based on transmission electron microscopy observations, the high core hardness of the 1223 K GNQP specimen was attributed to solid-solution strengthening caused by nitrogen diffusion or to strain hardening associated with the diffusion and was not attributed to the influence of precipitation phases, such as the ω phase. In the friction and wear tests, both the 1023 K and 1223 K GNQP specimens exhibited narrower wear track widths, clearly demonstrating that the GNQP enhanced the wear resistance. Moreover, the TiO2 layer was effective in maintaining a low coefficient of friction. Full article
(This article belongs to the Section Crystallography and Applications of Metallic Materials)
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21 pages, 4628 KB  
Article
Effect of Inclined Angles and Contouring Parameters on Upskin Surface Characteristics of Parts Made by Laser Powder-Bed Fusion
by Nismath Valiyakath Vadakkan Habeeb and Kevin Chou
Coatings 2026, 16(1), 119; https://doi.org/10.3390/coatings16010119 - 16 Jan 2026
Abstract
Surface finish plays a critical role in the tribological performance of additively manufactured engineering components. In exploring part characteristics in laser powder-bed fusion (L-PBF), this study investigates the effect of contouring strategies on the upskin surface of inclined specimens (30°, 45°, and 60°) [...] Read more.
Surface finish plays a critical role in the tribological performance of additively manufactured engineering components. In exploring part characteristics in laser powder-bed fusion (L-PBF), this study investigates the effect of contouring strategies on the upskin surface of inclined specimens (30°, 45°, and 60°) made with L-PBF, using post- and pre-contouring strategies with various levels of process parameters. The surface data of fabricated inclined specimens were acquired by white-light interferometry, followed by a quantitative analysis using surface images. The results show that post-contouring leads to better surface finishes, with the lowest Sa of 8.68 µm attained at the highest laser power (195 W) and the slowest scan speed (500 mm/s) on 30°-inclined specimens, likely due to increased remelting and less step-edges. In contrast, pre-contouring produces distinct surface textures on the upskin of L-PBF specimens, resulting in a rougher surface morphology, with a maximum Sa of 33.39 µm also from 30°-inclined specimens at the lowest power (100 W) and the highest speed (2000 mm/s), suggesting an insufficient remelting of surface defects. In comparative analysis, in general, post-contouring yields smoother upskin surfaces, with a 17%–30% reduction in Sa, than those from equivalent pre-contouring conditions, highlighting the potential of scan sequences for optimizing L-PBF to improve the surface finish of inclined structures. Full article
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9 pages, 3593 KB  
Proceeding Paper
Experimental Study on the Impact of Variable Concentration of Graphite Nanoparticles on the Tribological Behaviour of 15W40 Lubricating Oil
by Sonia Dangi, Sumit Chaudhary, Shadab Ahmad, Yebing Tian, Ramesh Chandra Singh, Mohammad Yusuf and Hussameldin Ibrahim
Eng. Proc. 2024, 76(1), 112; https://doi.org/10.3390/engproc2024076112 - 15 Jan 2026
Abstract
An experiment examined the impact of 0.2% to 1.0% w/w graphite nanoparticles in 15W40 lubricating oil on tribological and rheological behaviour. Analysis, conducted with a pin-on-disc machine and four-ball tester, revealed improved tribological properties and a 30% reduction in friction coefficient [...] Read more.
An experiment examined the impact of 0.2% to 1.0% w/w graphite nanoparticles in 15W40 lubricating oil on tribological and rheological behaviour. Analysis, conducted with a pin-on-disc machine and four-ball tester, revealed improved tribological properties and a 30% reduction in friction coefficient compared to fresh 15W40. Wear was negligible, and extreme-pressure performance increased by approximately 20%. SEM morphology confirmed the presence of graphite nanoparticles on the tribo-pair surface, indicating enhanced lubricant performance. Full article
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40 pages, 4627 KB  
Review
Friction Stir Processing: An Eco-Efficient Route to High-Performance Surface Architectures in MMCs
by Sachin Kumar Sharma, Saša Milojević, Lokesh Kumar Sharma, Sandra Gajević, Yogesh Sharma, Mohit Sharma, Stefan Čukić and Blaža Stojanović
Processes 2026, 14(2), 306; https://doi.org/10.3390/pr14020306 - 15 Jan 2026
Viewed by 32
Abstract
Friction Stir Processing (FSP) has emerged as an advanced solid-state surface engineering technique for tailoring high-performance surface architectures in metal matrix composites (MMCs). By combining localized thermo-mechanical deformation with controlled material flow, FSP enables grain refinement, homogeneous dispersion of reinforcement, and strong interfacial [...] Read more.
Friction Stir Processing (FSP) has emerged as an advanced solid-state surface engineering technique for tailoring high-performance surface architectures in metal matrix composites (MMCs). By combining localized thermo-mechanical deformation with controlled material flow, FSP enables grain refinement, homogeneous dispersion of reinforcement, and strong interfacial bonding without melting or altering bulk properties. This review critically examines the role of FSP in enhancing the mechanical, tribological, and corrosion performance of composites, with emphasis on process–structure–property relationships. Key strengthening mechanisms, including grain boundary strengthening, load transfer, particle pinning, and defect elimination, are systematically discussed, along with their implications for wear resistance, fatigue life, and durability. Special attention is given to corrosion and tribo-corrosion behavior, highlighting electrochemical mechanisms such as micro-galvanic interactions, passive film stability, and interfacial chemistry. Furthermore, the eco-efficiency, industrial viability, and sustainability advantages of FSP are evaluated in comparison with conventional surface modification techniques. The review concludes by identifying critical challenges and outlining future research directions for the scalable, multifunctional, and sustainable design of composite surfaces. Full article
(This article belongs to the Section Materials Processes)
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31 pages, 4459 KB  
Review
Prospects and Challenges for Achieving Superlubricity in Porous Framework Materials (MOFs/POFs): A Review
by Ruishen Wang, Xunyi Liu, Sifan Huo, Mingming Liu, Jiasen Zhang, Yuhong Liu, Yanhong Cheng and Caixia Zhang
Lubricants 2026, 14(1), 42; https://doi.org/10.3390/lubricants14010042 - 15 Jan 2026
Viewed by 146
Abstract
Metal–organic frameworks (MOFs) and porous organic frameworks (POFs) have been extensively explored in recent years as lubricant additives for various systems due to their structural designability, pore storage capacity, and tunable surface chemistry. These materials are utilized to construct low-friction, low-wear interfaces and [...] Read more.
Metal–organic frameworks (MOFs) and porous organic frameworks (POFs) have been extensively explored in recent years as lubricant additives for various systems due to their structural designability, pore storage capacity, and tunable surface chemistry. These materials are utilized to construct low-friction, low-wear interfaces and investigate the potential for superlubricity. This paper systematically reviews the tribological behavior and key mechanisms of MOFs/POFs in oil-based, water-based, and solid coating systems. In oil-based systems, MOFs/POFs primarily achieve friction reduction and wear resistance through third-body particles, layer slip, and synergistic friction-induced chemical/physical transfer films. However, limitations in achieving superlubricity stem from the multi-component heterogeneity of boundary films and the dynamic evolution of shear planes. In water-based systems, MOFs/POFs leverage hydrophilic functional groups to induce hydration layers, promote polymer thickening, and soften gels through interfacial anchoring. Under specific conditions, a few cases exhibit superlubricity with coefficients of friction entering the 10−3 range. In solid coating systems, two-dimensional MOFs/COFs with controllable orientation leverage interlayer weak interactions and incommensurate interfaces to reduce potential barriers, achieving structural superlubricity at the 10−3–10−4 level on the micro- and nano-scales. However, at the engineering scale, factors such as roughness, contamination, and discontinuities in the lubricating film still constrain performance, leading to amplified energy dissipation and degradation. Finally, this paper discusses key challenges in achieving superlubricity with MOFs/POFs and proposes future research directions, including the design of shear-plane structures. Full article
(This article belongs to the Special Issue Superlubricity Mechanisms and Applications)
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20 pages, 5426 KB  
Review
Morphological Diversity and Interparticle Interactions of Lubricating Grease Thickeners: Current Insights and Research Approaches
by Maciej Paszkowski, Ewa Kadela and Agnieszka Skibińska
Lubricants 2026, 14(1), 41; https://doi.org/10.3390/lubricants14010041 - 15 Jan 2026
Viewed by 113
Abstract
The study systematizes the current state of knowledge on the morphological diversity of dispersed-phase particles in the most widely used lubricating greases, encompassing their shape, size, surface structure, and overall geometry. The extensive discussion of the diversity of grease thickener particles is supplemented [...] Read more.
The study systematizes the current state of knowledge on the morphological diversity of dispersed-phase particles in the most widely used lubricating greases, encompassing their shape, size, surface structure, and overall geometry. The extensive discussion of the diversity of grease thickener particles is supplemented with their microscopic images. Particular emphasis is placed on the influence of thickener particle morphology, the degree of their aggregation, and interparticle interactions on the rheological, mechanical, and tribological properties of grease formulations. The paper reviews recent advances in investigations of grease microstructure, with special emphasis on imaging techniques—ranging from dark-field imaging, through scanning electron microscopy, to atomic force microscopy—together with a discussion of their advantages and limitations in the assessment of particle morphology. A significant part of the work is devoted to rheological studies, which enable an indirect evaluation of the structural state of grease by analyzing its response to shear and deformation, thereby allowing inferences to be drawn about the micro- and mesostructure of lubricating greases. The historical development of rheological research on lubricating greases is also presented—from simple flow models, through the introduction of the concepts of viscoelasticity and structural rheology, to modern experimental and modeling approaches—highlighting the close relationships between rheological properties and thickener structure, manufacturing processes, composition, and in-service behavior of lubricating greases, particularly in tribological applications. It is indicated that contemporary studies confirm the feasibility of tailoring the microstructure of grease thickeners to specific lubrication conditions, as their characteristics fundamentally determine the rheological and tribological properties of the entire system. Full article
(This article belongs to the Special Issue Rheology of Lubricants in Lubrication Engineering)
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24 pages, 4253 KB  
Article
Performance Evaluation of a Halbach Permanent Magnet Axial Protection Bearing Under Vertical Magnetic Levitation Flywheel Rotor Drop
by Dengke Li, Jun Ye, Gang Chen, Lai Hu, Zixi Wang, Taishun Qian, Jiahao Zhang, Mengchen Zi and Chao Liang
Lubricants 2026, 14(1), 40; https://doi.org/10.3390/lubricants14010040 - 15 Jan 2026
Viewed by 100
Abstract
This study addresses the issues with traditional rolling protection bearings in vertical magnetic levitation flywheel energy storage systems (FESSs), which are prone to impact, wear, and temperature rise under abnormal conditions, such as drops. It designed a permanent magnet axial protection bearing based [...] Read more.
This study addresses the issues with traditional rolling protection bearings in vertical magnetic levitation flywheel energy storage systems (FESSs), which are prone to impact, wear, and temperature rise under abnormal conditions, such as drops. It designed a permanent magnet axial protection bearing based on a Halbach array, utilizing N42SH permanent magnet material. The five-layer Halbach array achieved a maximum axial magnetic force of 86 KN and a maximum air gap magnetic flux density of 2.2 T, meeting the application requirements. Simulation results, combined with rotor drop dynamics and thermal analysis, show that under an 8000 rpm drop condition, the permanent magnet bearing reduces radial and axial contact forces by approximately 60% and 54%, respectively, and wear by around 70%. Additionally, the maximum system temperature decreases from 109 °C to 74 °C, with a 32% reduction in temperature rise. Friction experimental analysis indicates that low frequency, low load, and moderate temperatures improve friction stability and reduce wear. Overall, the permanent magnet axial protective bearing effectively mitigates drop impact, reduces friction heat and wear, and enhances the safety and reliability of the flywheel energy storage system under abnormal working conditions, providing valuable theoretical support and a design reference for engineering applications. Full article
(This article belongs to the Special Issue High Performance Machining and Surface Tribology)
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35 pages, 16491 KB  
Article
Laser Surface Texturing of AA1050 Aluminum to Enhance the Tribological Properties of PTFE Coatings with a Taguchi-Based Analysis
by Timur Canel, Sinan Fidan, Mustafa Özgür Bora, Satılmış Ürgün, Demet Taşkan Ürgün and Mehmet İskender Özsoy
Lubricants 2026, 14(1), 39; https://doi.org/10.3390/lubricants14010039 - 15 Jan 2026
Viewed by 105
Abstract
Fiber laser surface texturing was applied to AA1050 aluminum to improve friction and wear performance of PTFE coatings. A Taguchi L16 design varied texture geometry (square, diamond, hexagon, circle), scanned area ratio (20% to 80%), and laser power (40 to 100 W) prior [...] Read more.
Fiber laser surface texturing was applied to AA1050 aluminum to improve friction and wear performance of PTFE coatings. A Taguchi L16 design varied texture geometry (square, diamond, hexagon, circle), scanned area ratio (20% to 80%), and laser power (40 to 100 W) prior to primer plus PTFE topcoat deposition (25 to 35 µm). Dry reciprocating sliding against a 6 mm 100Cr6 ball was conducted at 20 N, 1 Hz, and 50 m, and wear track geometry was measured by non-contact profilometry. The non-textured reference exhibited an average COF of 0.143, whereas the lowest mean COF was achieved with diamond 60% and 40 W (0.095) and the highest with hexagon 60% and 100 W (0.156); hexagon 20% and 60 W matched the reference. ANOVA indicated scanned area ratio as the dominant contributor to COF (39.72%), followed by geometry (35.07%) and power (25.21%). Profilometry confirmed reduced coating penetration for optimized textures: the reference wear track was approximately 1240 µm wide and 82 µm deep, compared with 930 µm and 34 µm for square 80% and 40 W, 997 µm and 39 µm for diamond 60% and 40 W, and 965 µm and 36 µm for hexagon 40% and 40 W. Full article
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19 pages, 6631 KB  
Article
Research on the Influence of Ore Particle Shape on the Load Behavior of Charge and Wear of Ball Mill Liners Based on Rocky-DEM
by Zixin Yin and Xiangyi Pan
Lubricants 2026, 14(1), 37; https://doi.org/10.3390/lubricants14010037 - 15 Jan 2026
Viewed by 108
Abstract
This study investigates the influence of ore particle shape on the wear behavior of ball mill liners using the Rocky-DEM software. A simulation model of a laboratory-scale ball mill was established to analyze the wear patterns of liners under three different ore particle [...] Read more.
This study investigates the influence of ore particle shape on the wear behavior of ball mill liners using the Rocky-DEM software. A simulation model of a laboratory-scale ball mill was established to analyze the wear patterns of liners under three different ore particle shapes: polyhedron, ellipsoid, and sphere. The results indicate that while the overall motion patterns of the charge showed minor differences across particle shapes, significant variations were observed in flowability, with the polyhedral system exhibiting the lowest fluidity. Particle shape had a negligible impact on translational velocity but a substantial effect on rotational velocity. Regarding liner wear, the polyhedral system generated significantly higher wear compared to the spherical and ellipsoidal systems. The polyhedral system also exhibited the highest shear stress, identifying shear stress as the core factor dominating liner wear. The wear-time curves for individual liners in both radial and axial directions displayed a stepwise increase, suggesting that wear is primarily concentrated in the toe region. Full article
(This article belongs to the Special Issue Tribology in Ball Milling: Theory and Applications)
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23 pages, 5255 KB  
Article
Analysis of Wear Behavior Between Tire Rubber and Silicone Rubber
by Juana Abenojar, Miguel Angel Martínez and Daniel García-Pozuelo
Appl. Sci. 2026, 16(2), 878; https://doi.org/10.3390/app16020878 - 14 Jan 2026
Viewed by 100
Abstract
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire [...] Read more.
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire rubber and silicone VMQ, motivated by a wheel concept based on a detachable tread aimed at improving durability and sustainability rather than proposing an immediate material substitution. Wear and friction behavior were investigated under abrasive and self-friction conditions using pin-on-disk testing with an abrasive counterpart representative of asphalt, supported by optical and scanning electron microscopy. The results show that NR-SBR undergoes severe abrasive and erosive wear, characterized by deep and irregular wear tracks, pronounced fluctuations in the dynamic friction coefficient, and strong sensitivity to load and sliding speed, particularly during the initial stages of track formation. In contrast, VMQ exhibits mild abrasive wear dominated by viscoelastic deformation, leading to shallow and stable wear tracks, lower friction coefficients, and significantly reduced material loss once the contact track is fully developed. These differences are attributed to the distinct mechanical responses of the elastomers, as the higher hardness and limited strain capacity of rubber promote micro-tearing and unstable material removal, while the high elasticity of silicone enables stress redistribution and stable contact conditions under abrasive loading. UV aging increases stiffness of rubber, resulting in reduced wear and friction, while silicone remains largely unaffected after 750 h due to the stability of its Si–O–Si backbone. Self-friction tests further indicate that smooth silicone sliding against rubber yields the lowest friction values, highlighting a favorable material pairing for detachable tread concepts. Factorial design analysis confirms material type as the dominant factor influencing both wear and friction. Overall, for the specific materials and operating conditions investigated, VMQ demonstrates higher durability, greater tribological stability, and improved aging resistance compared to NR-SBR, providing experimental evidence that supports its potential for long-life, more sustainable detachable tread applications. Full article
(This article belongs to the Section Materials Science and Engineering)
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25 pages, 4121 KB  
Review
Advances in the Tribological Research of Ceramic-on-Ceramic Artificial Joints
by Menglin Zhou, Zihan Lin, Xiaolu Jiang, Jianhua Jin, Qi Wan, Li Zhang and Zhaoxian Zheng
Lubricants 2026, 14(1), 36; https://doi.org/10.3390/lubricants14010036 - 14 Jan 2026
Viewed by 62
Abstract
Ceramic-on-ceramic (CoC) bearings are widely used in total hip arthroplasty due to their extremely low wear rate, excellent chemical stability, and good biocompatibility. They are considered one of the most reliable long-term friction bearing systems. Although frictional instability, lubrication regime transitions, and microstructural [...] Read more.
Ceramic-on-ceramic (CoC) bearings are widely used in total hip arthroplasty due to their extremely low wear rate, excellent chemical stability, and good biocompatibility. They are considered one of the most reliable long-term friction bearing systems. Although frictional instability, lubrication regime transitions, and microstructural damage mechanisms have been widely reported at the experimental and retrieval-analysis levels, current clinical evidence, limited by follow-up duration and event incidence, has not demonstrated a definitive negative impact on the clinical performance of fourth-generation ceramic components, including BIOLOX® delta. Data from national arthroplasty registries consistently demonstrate excellent survivorship and low complication rates for 4th-generation ceramics in both hard-on-soft and hard-on-hard configurations. The most reported causes for revision, such as infection, dislocation, aseptic loosening, and periprosthetic fracture, are not primarily associated with ceramic-related complications, such as ceramic fracture, excessive wear, squeaking, and revision, related to bearing failure; however, these mechanisms remain highly relevant for the design and evaluation of emerging ceramic materials and next-generation implant systems, where inadequate control may potentially impact long-term clinical performance. This review summarizes recent advances in the tribological research of CoC artificial joints, focusing on clinical tribological challenges, material composition and surface characteristics, lubrication mechanisms, wear and microdamage evolution, and third-body effects. Recent progress in ceramic toughening strategies, surface engineering, biomimetic lubrication simulation, and structural optimization is also discussed. Finally, future research directions are outlined to support the performance optimization and long-term reliability assessment of CoC artificial joint systems. Full article
(This article belongs to the Special Issue Tribology of Medical Devices)
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20 pages, 5660 KB  
Article
Synthesis and Tribological Properties of Multifunctional Nitrogen-Containing Heterocyclic Dialkyl Dithiocarbamate Derivatives
by Mengxuan Wang, Ting Li, Zhongxian Li, Wenjing Hu, Junwei Wang and Jiusheng Li
Lubricants 2026, 14(1), 35; https://doi.org/10.3390/lubricants14010035 - 14 Jan 2026
Viewed by 99
Abstract
Energy conservation and efficiency enhancement necessitate continuous advancement in the development and preparation of multifunctional, high-performance lubricant additives. This paper reports three novel ashless, phosphorus-free, multifunctional nitrogen-containing heterocyclic dialkyl dithiocarbamate derivative additives (Py-2-DBDTC, PDM-DBDTC, and BZT-DBDTC). Thermal stability, oxidation resistance, and tribological properties [...] Read more.
Energy conservation and efficiency enhancement necessitate continuous advancement in the development and preparation of multifunctional, high-performance lubricant additives. This paper reports three novel ashless, phosphorus-free, multifunctional nitrogen-containing heterocyclic dialkyl dithiocarbamate derivative additives (Py-2-DBDTC, PDM-DBDTC, and BZT-DBDTC). Thermal stability, oxidation resistance, and tribological properties were investigated for the synthesized additives. All three additives demonstrated excellent thermal stability and oxidation resistance. Furthermore, their extreme-pressure properties improved by 116.33% or more compared to the base oil, while wear reduction rates also exceeded 58.32%. Under both point-to-point and point-on-flat friction conditions, the friction-reducing performance of all three additives was equally outstanding. Across a broad temperature range (25 °C–150 °C), all additives maintained their friction-reducing properties. Analysis of the worn surface morphology reveals that all three additives undergo tribochemical reactions during the friction process, forming tribofilms containing sulfur elements. Research indicates that introducing different nitrogen-containing heterocyclic structures into dialkyl dithiocarbamates can effectively enhance the adsorption capacity of the additives on metal surfaces and promote the formation of tribofilms at the friction interface, thereby significantly improving tribological performance. These systematic investigations not only provide important guidance for the molecular design and industrial application of multifunctional lubricant additives but also further advance the development of sustainable lubrication technologies. Full article
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14 pages, 5388 KB  
Article
Influence of Voltage on the Microstructure and Tribocorrosion Properties of Porous Coatings Produced by Micro-Arc Oxidation
by Laila Sulyubayeva, Daryn Baizhan, Nurbol Berdimuratov, Dastan Buitkenov, Balym Alibekova and Gulim Tleubergenova
Coatings 2026, 16(1), 104; https://doi.org/10.3390/coatings16010104 - 13 Jan 2026
Viewed by 78
Abstract
Micro-arc oxidation (MAO) coatings were produced on commercially pure titanium Grade 2 using a composite electrolyte containing sodium phosphate (Na3PO4) and sodium silicate (Na2SiO3), while varying the applied voltage. The surface morphology, phase composition, and [...] Read more.
Micro-arc oxidation (MAO) coatings were produced on commercially pure titanium Grade 2 using a composite electrolyte containing sodium phosphate (Na3PO4) and sodium silicate (Na2SiO3), while varying the applied voltage. The surface morphology, phase composition, and structural features of the coatings were examined using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The coatings exhibited a characteristic crater-like microporous surface morphology associated with the micro-arc discharge process. XRD analysis confirmed the formation of mixed TiO2 phases in the anatase and rutile modifications, with higher voltages promoting the growth of the thermodynamically stable rutile phase. Corrosion and tribological properties were evaluated in a 3.5 wt.% NaCl solution using potentiodynamic polarization and a ball-on-disc test configuration, respectively. The results revealed a substantial improvement in both corrosion resistance and wear performance compared with bare titanium. The coating formed at 300 V demonstrated the highest wear resistance due to its denser microstructure, whereas the coating produced at 350 V exhibited the lowest friction coefficient and the greatest corrosion resistance, attributed to the increased rutile content. Overall, MAO coatings fabricated in the phosphate–silicate electrolyte effectively enhance the combined operational properties of titanium and can be recommended for applications requiring improved wear and corrosion resistance. Full article
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