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Search Results (12,009)

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Keywords = surface heating

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17 pages, 3157 KiB  
Article
Research on Online Traceability Methods for the Causes of Longitudinal Surface Crack in Continuous Casting Slab
by Junqiang Cong, Qiancheng Lv, Zihao Fan, Haitao Ling and Fei He
Materials 2025, 18(15), 3695; https://doi.org/10.3390/ma18153695 - 6 Aug 2025
Abstract
In the casting and rolling production process, surface longitudinal cracks are a typical casting defect. Tracing the causes of longitudinal cracks online and controlling the key parameters leading to their formation in a timely manner can enhance the stability of casting and rolling [...] Read more.
In the casting and rolling production process, surface longitudinal cracks are a typical casting defect. Tracing the causes of longitudinal cracks online and controlling the key parameters leading to their formation in a timely manner can enhance the stability of casting and rolling production. To this end, the influencing factors of longitudinal cracks were analyzed, a data integration storage platform was constructed, and a tracing model was established using empirical rule analysis, statistical analysis, and intelligent analysis methods. During the initial production phase of a casting machine, longitudinal cracks occurred frequently. The tracing results using the LightGBM-SHAP method showed that the relative influence of the narrow left wide inner heat flow ratio of the mold was significant, followed by the heat flow difference on the wide symmetrical face of the mold and the superheat of the molten steel, with weights of 0.135, 0.066, and 0.048, respectively. Based on the tracing results, we implemented online emergency measures. By controlling the cooling intensity of the mold, we effectively reduced the recurrence rate of longitudinal cracks. Root cause analysis revealed that the total hardness of the mold-cooling water exceeded the standard, reaching 24 mg/L, which caused scaling on the mold copper plates and uneven cooling, leading to the frequent occurrence of longitudinal cracks. After strictly controlling the water quality, the issue of longitudinal cracks was brought under control. The online application of the tracing method for the causes of longitudinal cracks has effectively improved efficiency in resolving longitudinal crack problems. Full article
(This article belongs to the Special Issue Advanced Sheet/Bulk Metal Forming)
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20 pages, 11969 KiB  
Article
Spatiotemporal Variability of Cloud Parameters and Their Climatic Impacts over Central Asia Based on Multi-Source Satellite and ERA5 Data
by Xinrui Xie, Liyun Ma, Junqiang Yao and Weiyi Mao
Remote Sens. 2025, 17(15), 2724; https://doi.org/10.3390/rs17152724 - 6 Aug 2025
Abstract
As key components of the climate system, clouds exert a significant influence on the Earth’s radiation budget and hydrological cycle. However, studies focusing on cloud properties over Central Asia are still limited, and the impacts of cloud variability on regional temperature and precipitation [...] Read more.
As key components of the climate system, clouds exert a significant influence on the Earth’s radiation budget and hydrological cycle. However, studies focusing on cloud properties over Central Asia are still limited, and the impacts of cloud variability on regional temperature and precipitation remain poorly understood. This study uses reanalysis and multi-source remote sensing datasets to investigate the spatiotemporal characteristics of clouds and their influence on regional climate. The cloud cover increases from the southwest to the northeast, with mid and low-level clouds predominating in high-altitude regions. All clouds have shown a declining trend during 1981–2020. According to satellite data, the sharpest decline in total cloud cover occurs in summer, while reanalysis data show a more significant reduction in spring. In addition, cloud cover changes influence the local climate through radiative forcing mechanisms. Specifically, the weakening of shortwave reflective cooling and the enhancement of longwave heating of clouds collectively exacerbate surface warming. Meanwhile, precipitation is positively correlated with cloud cover, and its spatial distribution aligns with the cloud water path. The cloud phase composition in Central Asia is dominated by liquid water, accounting for over 40%, a microphysical characteristic that further impacts the regional hydrological cycle. Full article
(This article belongs to the Section Atmospheric Remote Sensing)
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14 pages, 4016 KiB  
Article
Failure Mechanism of Pre-Stressed CFRP Beam Under Laser Ablation
by Yuting Zhao, Ruokun Zhang and Zhuhua Tan
Polymers 2025, 17(15), 2153; https://doi.org/10.3390/polym17152153 - 6 Aug 2025
Abstract
This paper focuses on the failure mechanism of a pre-stressed CFRP cantilever beam under laser ablation. During testing, a mass was applied to the CFRP cantilever beam to achieve a pre-stressed state, and the laser power densities varied from 500 to 1500 W·cm [...] Read more.
This paper focuses on the failure mechanism of a pre-stressed CFRP cantilever beam under laser ablation. During testing, a mass was applied to the CFRP cantilever beam to achieve a pre-stressed state, and the laser power densities varied from 500 to 1500 W·cm−2. Corresponding scanning electron microscope (SEM) tests were also performed on the ablation zone and fracture surface to analyze the failure mechanism. The results showed that the CFRP beam failed in compression at the bottom surface, which was due to a decrease in local stiffness and strength caused by heat softening, rather than by ablation damage on the top surface. The failure time decreased from 19.64 s to 6.52 s as the power density (500–1500 W·cm−2) and pre-stress loading (300–750 N·cm) increased, indicating that pre-stress loading has a more significant influence on the failure time of CFRP beams compared to power density. Full article
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11 pages, 2177 KiB  
Article
Early Signs of Tool Damage in Dry and Wet Turning of Chromium–Nickel Alloy Steel
by Tanuj Namboodri, Csaba Felhő and István Sztankovics
J 2025, 8(3), 28; https://doi.org/10.3390/j8030028 - 6 Aug 2025
Abstract
Machining chromium–nickel alloy steel is challenging due to its material properties, such as high strength and toughness. These properties often lead to tool damage and degradation of tool life, which overall impacts the production time, cost, and quality of the product. Therefore, it [...] Read more.
Machining chromium–nickel alloy steel is challenging due to its material properties, such as high strength and toughness. These properties often lead to tool damage and degradation of tool life, which overall impacts the production time, cost, and quality of the product. Therefore, it is essential to investigate early signs of tool damage to determine the effective machining conditions for chromium–nickel alloy steel, thereby increasing tool life and improving product quality. In this study, the early signs of tool wear were observed in a physical vapor deposition (PVD) carbide-coated tool (Seco Tools, Björnbacksvägen, Sweden) during the machining of X5CrNi18-10 steel under both dry and wet conditions. A finish turning operation was performed on the outer diameter (OD) of the workpiece with a 0.4 mm nose radius tool. At the early stage, the tool was examined from the functional side (f–side) and the passive side (p–side). The results indicate that dry machining leads to increased coating removal, more heat generation, and visible damage, such as pits and surface scratches. By comparison, wet machining helps reduce heat and wear, thereby improving tool life and machining quality. These findings suggest that a coolant must be used when machining chromium–nickel alloy steel with a PVD carbide-coated tool. Full article
(This article belongs to the Section Engineering)
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18 pages, 9049 KiB  
Article
Study on the Wear Performance of 20CrMnTi Gear Steel with Different Penetration Gradient Positions
by Yingtao Zhang, Shaokui Wei, Wuxin Yang, Jiajian Guan and Gong Li
Materials 2025, 18(15), 3685; https://doi.org/10.3390/ma18153685 - 6 Aug 2025
Abstract
This study investigates the wear performance of 20CrMnTi steel, a commonly used material for spiral bevel gears, after heat treatment, with a focus on the microstructural evolution and wear behavior in both the surface and gradient direction of the carburized layer. The results [...] Read more.
This study investigates the wear performance of 20CrMnTi steel, a commonly used material for spiral bevel gears, after heat treatment, with a focus on the microstructural evolution and wear behavior in both the surface and gradient direction of the carburized layer. The results show that the microstructure composition in the gradient direction of the carburized layer gradually transitions from martensite and residual austenite to a martensite–bainite mixed structure, and eventually transforms to fully bainitic in the matrix. With the extension of carburizing time, both the effective carburized layer depth and the hardened layer depth significantly increase. Wear track morphology analysis reveals that the wear track depth gradually becomes shallower and narrower, and the wear rate increases significantly with increasing load. However, the friction coefficient shows little sensitivity to changes in carburizing time and load. Further investigations show that as the carburized layer depth increases, the carbon concentration and hardness of the samples gradually decrease, resulting in an increase in the average wear rate and a progressive worsening of wear severity. After the wear tests, different depths of plowing grooves, spalling, and fish-scale-like features were observed in the wear regions. Additionally, with the increase in load and carburized layer depth, both the width and depth of the wear tracks significantly increased. The research results provide a theoretical basis for optimizing the surface carburizing process of 20CrMnTi steel and improving its wear resistance. Full article
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14 pages, 5840 KiB  
Article
Paint Removal Performance and Sub-Surface Microstructural Evolution of Ti6Al4V Alloy Using Different Process Parameters of Continuous Laser Cleaning
by Haoye Zeng, Biwen Li, Liangbin Hu, Yun Zhang, Ruiqing Li, Chaochao Zhou and Pinghu Chen
Coatings 2025, 15(8), 916; https://doi.org/10.3390/coatings15080916 (registering DOI) - 6 Aug 2025
Abstract
Laser cleaning technology has been increasingly applied in the removal of damaged protective coatings from aircraft components due to its environmental friendliness and high efficiency. Appropriate laser cleaning process parameters improve cleaning efficiency while preventing substrate damage. In this study, a Gaussian continuous-wave [...] Read more.
Laser cleaning technology has been increasingly applied in the removal of damaged protective coatings from aircraft components due to its environmental friendliness and high efficiency. Appropriate laser cleaning process parameters improve cleaning efficiency while preventing substrate damage. In this study, a Gaussian continuous-wave laser was used to remove the 120 μm coating on the surface of Ti6Al4V alloy. The influence of laser power (100 W to 200 W) and scanning speed (520 mm/min to 610 mm/min) on the paint removal effect was explored based on paint removal rate, surface roughness, microstructural evolution, and the hardness’ change in the direction of heat transfer. The results reveal that optimal paint removal parameters are achieved at a laser power of 100 W with a scanning speed of 550 mm/min. The surface roughness of the sample after paint removal (55 nm) is similar to that of the original substrate (56 nm). Through EBSD analysis, the influence of laser thermal accumulation on the microstructure of the substrate is relatively small. The average hardness of the cross-section after cleaning was 347 HV, which was only 3.41% higher than that of the original substrate. This confirms that parameter-controlled laser cleaning can effectively remove ~120 μm thick paint layers without inflicting damage on the substrate. Full article
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23 pages, 3831 KiB  
Article
Estimating Planetary Boundary Layer Height over Central Amazonia Using Random Forest
by Paulo Renato P. Silva, Rayonil G. Carneiro, Alison O. Moraes, Cleo Quaresma Dias-Junior and Gilberto Fisch
Atmosphere 2025, 16(8), 941; https://doi.org/10.3390/atmos16080941 (registering DOI) - 5 Aug 2025
Abstract
This study investigates the use of a Random Forest (RF), an artificial intelligence (AI) model, to estimate the planetary boundary layer height (PBLH) over Central Amazonia from climatic elements data collected during the GoAmazon experiment, held in 2014 and 2015, as it is [...] Read more.
This study investigates the use of a Random Forest (RF), an artificial intelligence (AI) model, to estimate the planetary boundary layer height (PBLH) over Central Amazonia from climatic elements data collected during the GoAmazon experiment, held in 2014 and 2015, as it is a key metric for air quality, weather forecasting, and climate modeling. The novelty of this study lies in estimating PBLH using only surface-based meteorological observations. This approach is validated against remote sensing measurements (e.g., LIDAR, ceilometer, and wind profilers), which are seldom available in the Amazon region. The dataset includes various meteorological features, though substantial missing data for the latent heat flux (LE) and net radiation (Rn) measurements posed challenges. We addressed these gaps through different data-cleaning strategies, such as feature exclusion, row removal, and imputation techniques, assessing their impact on model performance using the Root Mean Square Error (RMSE), Mean Absolute Error (MAE), and r2 metrics. The best-performing strategy achieved an RMSE of 375.9 m. In addition to the RF model, we benchmarked its performance against Linear Regression, Support Vector Regression, LightGBM, XGBoost, and a Deep Neural Network. While all models showed moderate correlation with observed PBLH, the RF model outperformed all others with statistically significant differences confirmed by paired t-tests. SHAP (SHapley Additive exPlanations) values were used to enhance model interpretability, revealing hour of the day, air temperature, and relative humidity as the most influential predictors for PBLH, underscoring their critical role in atmospheric dynamics in Central Amazonia. Despite these optimizations, the model underestimates the PBLH values—by an average of 197 m, particularly in the spring and early summer austral seasons when atmospheric conditions are more variable. These findings emphasize the importance of robust data preprocessing and higtextight the potential of ML models for improving PBLH estimation in data-scarce tropical environments. Full article
(This article belongs to the Special Issue Applications of Artificial Intelligence in Atmospheric Sciences)
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21 pages, 4392 KiB  
Article
Visualization of Kinetic Parameters of a Droplet Nucleation Boiling on Smooth and Micro-Pillar Surfaces with Inclined Angles
by Yi-Nan Zhang, Guo-Qing Huang, Lu-Ming Zhao and Hong-Xia Chen
Energies 2025, 18(15), 4152; https://doi.org/10.3390/en18154152 - 5 Aug 2025
Abstract
The evaporation dynamics of droplets on smooth and inclined micro-pillar surfaces were experimentally investigated. The surface temperature was increased from 50 °C to 120 °C, with the inclination angles being 0°, 30°, 45°, and 60° respectively. The dynamic parameters, including contact area, nucleation [...] Read more.
The evaporation dynamics of droplets on smooth and inclined micro-pillar surfaces were experimentally investigated. The surface temperature was increased from 50 °C to 120 °C, with the inclination angles being 0°, 30°, 45°, and 60° respectively. The dynamic parameters, including contact area, nucleation density, bubble stable diameter, and droplet asymmetry, were recorded using two high-speed video cameras, and the corresponding evaporation performance was analyzed. Experimental results showed that the inclination angle had a significant influence on the evaporation of micro-pillar surfaces than smooth surfaces as well as a positive correlation between the enhancement performance of the micro-pillars and increasing inclination angles. This angular dependence arises from surface inclination-induced tail elongation and the corresponding asymmetry of droplets. With definition of the one-dimensional asymmetry factor (ε) and volume asymmetry factor (γ), it was proven that although the asymmetric thickness of the droplets reduces the nucleation density and bubble stable diameter, the droplet asymmetry significantly increased the heat exchange area, resulting in a 37% improvement in the evaporation rate of micro-pillar surfaces and about a 15% increase in its enhancement performance to smooth surfaces when the inclination angle increased from 0°to 60°. These results indicate that asymmetry causes changes in heat transfer conditions, specifically, a significant increase in the wetted area and deformation of the liquid film, which are the direct enhancement mechanisms of inclined micro-pillar surfaces. Full article
(This article belongs to the Special Issue Advancements in Heat Transfer and Fluid Flow for Energy Applications)
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15 pages, 2970 KiB  
Article
A Study on the Heat Dissipation Effects During the Meshing Process of Involute Gears with Variable Tooth Thickness
by Huicheng Zhang, Yongping Liu and Junhai Guo
Machines 2025, 13(8), 686; https://doi.org/10.3390/machines13080686 - 5 Aug 2025
Abstract
The involute gear with variable tooth thickness lacks established methods for calculating meshing heat and studying oil-jet lubrication and cooling effects. This study aims to theoretically estimate the meshing heat generated during the engagement process of involute gears with variable tooth thickness. To [...] Read more.
The involute gear with variable tooth thickness lacks established methods for calculating meshing heat and studying oil-jet lubrication and cooling effects. This study aims to theoretically estimate the meshing heat generated during the engagement process of involute gears with variable tooth thickness. To achieve this, a heat calculation model is derived based on the corresponding tooth surface equations. The impact of oil-jet lubrication parameters—jet velocity, pitch cone angle, face width ratio, and axial displacement—on the gear surface temperature and internal gearbox environment is systematically studied. Numerical simulations of the temperature field are validated through experimental measurements. The results indicate that an oil-jet velocity of 15 m/s combined with a pitch cone angle of 4° significantly reduces both gear surface and internal flow field temperatures. Additionally, smaller face width ratios and axial displacements effectively lower the internal temperature of the gearbox. These findings offer a theoretical basis for calculating meshing heat and designing oil-jet lubrication systems for variable-tooth-thickness involute gears. Full article
(This article belongs to the Section Machine Design and Theory)
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26 pages, 5455 KiB  
Article
Features of Thermal Stabilization of PVC Modified with Microstructured Titanium Phosphate
by Irina N. Vikhareva, Anton Abramian, Dragan Manojlović and Oleg Bol’shakov
Polymers 2025, 17(15), 2140; https://doi.org/10.3390/polym17152140 - 5 Aug 2025
Abstract
Poly(vinyl chloride) (PVC) undergoes thermal degradation during processing and operation, which necessitates the use of effective thermal stabilizers. The purpose of this work is to comprehensively evaluate the potential of new hierarchically structured titanium phosphates (TiP) with controlled morphology as thermal stabilizers of [...] Read more.
Poly(vinyl chloride) (PVC) undergoes thermal degradation during processing and operation, which necessitates the use of effective thermal stabilizers. The purpose of this work is to comprehensively evaluate the potential of new hierarchically structured titanium phosphates (TiP) with controlled morphology as thermal stabilizers of plasticized PVC, focusing on the effect of morphology and Ti/P ratio on their stabilizing efficiency. The thermal stability of the compositions was studied by thermogravimetric analysis (TGA) in both inert (Ar) and oxidizing (air) atmospheres. The effect of TiP concentration and its synergy with industrial stabilizers was analyzed. An assessment of the key degradation parameters is given: the temperature of degradation onset, the rate of decomposition, exothermic effects, and the carbon residue yield. In an inert environment, TiPMSI/TiPMSII microspheres demonstrated an optimal balance by increasing the temperature of degradation onset and the residual yield while suppressing the rate of decomposition. In an oxidizing environment, TiPR rods and TiPMSII microspheres provided maximum stability, enhancing resistance to degradation onset and reducing the degradation rate by 10–15%. Key factors of effectiveness include ordered morphology (spheres, rods); the Ti-deficient Ti/P ratio (~0.86), which enhances HCl binding; and crystallinity. The stabilization mechanism of titanium phosphates is attributed to their high affinity for hydrogen chloride (HCl), which catalyzes PVC chain scission, a catalyst for the destruction of the PVC chain. The unique microstructure of titanium phosphate provides a high specific surface area and, as a result, greater activity in the HCl neutralization reaction. The formation of a sol–phosphate framework creates a barrier to heat and oxygen. An additional contribution comes from the inhibition of oxidative processes and the possible interaction with unstable chlorallyl groups in PVC macromolecules. Thus, hierarchically structured titanium phosphates have shown high potential as multifunctional PVC thermostabilizers for modern polymer materials. Potential applications include the development of environmentally friendly PVC formulations with partial or complete replacement of toxic stabilizers, the optimization of thermal stabilization for products used in aggressive environments, and the use of hierarchical TiP structures in flame-resistant and halogen-free PVC-based compositions. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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19 pages, 29727 KiB  
Review
A Review of Methods for Increasing the Durability of Hot Forging Tools
by Jan Turek and Jacek Cieślik
Materials 2025, 18(15), 3669; https://doi.org/10.3390/ma18153669 - 4 Aug 2025
Abstract
The article presents a comprehensive review of key issues and challenges related to enhancing the durability of hot forging tools. It discusses modern strategies aimed at increasing tool life, including modifications to tool materials, heat treatment, surface engineering, tool and die design, die [...] Read more.
The article presents a comprehensive review of key issues and challenges related to enhancing the durability of hot forging tools. It discusses modern strategies aimed at increasing tool life, including modifications to tool materials, heat treatment, surface engineering, tool and die design, die geometry, tribological conditions, and lubrication. The review is based on extensive literature data, including recent publications and the authors’ own research, which has been implemented under industrial conditions at the modern forging facility in Forge Plant “Glinik” (Poland). The study introduces original design and technological solutions, such as an innovative concept for manufacturing forging dies from alloy structural steels with welded impressions, replacing traditional hot-work tool steel dies. It also proposes a zonal hardfacing approach, which involves applying welds with different chemical compositions to specific surface zones of the die impressions, selected according to the dominant wear mechanisms in each zone. General guidelines for selecting hardfacing material compositions are also provided. Additionally, the article presents technological processes for die production and regeneration. The importance and application of computer simulations of forging processes are emphasized, particularly in predicting wear mechanisms and intensity, as well as in optimizing tool and forging geometry. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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50 pages, 9033 KiB  
Article
Heat Pipe Integrated Cooling System of 4680 Lithium–Ion Battery for Electric Vehicles
by Yong-Jun Lee, Tae-Gue Park, Chan-Ho Park, Su-Jong Kim, Ji-Su Lee and Seok-Ho Rhi
Energies 2025, 18(15), 4132; https://doi.org/10.3390/en18154132 - 4 Aug 2025
Abstract
This study investigates a novel heat pipe integrated cooling system designed for thermal management of Tesla’s 4680 cylindrical lithium–ion batteries in electric vehicles (EVs). Through a comprehensive approach combining experimental analysis, 1-D AMESim simulations, and 3-D Computational Fluid Dynamics (CFD) modeling, the thermal [...] Read more.
This study investigates a novel heat pipe integrated cooling system designed for thermal management of Tesla’s 4680 cylindrical lithium–ion batteries in electric vehicles (EVs). Through a comprehensive approach combining experimental analysis, 1-D AMESim simulations, and 3-D Computational Fluid Dynamics (CFD) modeling, the thermal performance of various wick structures and working fluid filling ratios was evaluated. The experimental setup utilized a triangular prism chamber housing three surrogate heater blocks to replicate the heat generation of 4680 cells under 1C, 2C, and 3C discharge rates. Results demonstrated that a blended fabric wick with a crown-shaped design (Wick 5) at a 30–40% filling ratio achieved the lowest maximum temperature (Tmax of 47.0°C), minimal surface temperature deviation (ΔTsurface of 2.8°C), and optimal thermal resistance (Rth of 0.27°C/W) under 85 W heat input. CFD simulations validated experimental findings, confirming stable evaporation–condensation circulation at a 40% filling ratio, while identifying thermal limits at high heat loads (155 W). The proposed hybrid battery thermal management system (BTMS) offers significant potential for enhancing the performance and safety of high-energy density EV batteries. This research provides a foundation for optimizing thermal management in next-generation electric vehicles. Full article
(This article belongs to the Special Issue Optimized Energy Management Technology for Electric Vehicle)
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11 pages, 1539 KiB  
Article
Heat Exchange and Flow Resistance in a Heat Exchanger Based on a Minimal Surface of the Gyroid Type—Results of Experimental Studies
by Krzysztof Dutkowski, Marcin Kruzel and Marcin Walczak
Energies 2025, 18(15), 4134; https://doi.org/10.3390/en18154134 - 4 Aug 2025
Abstract
The gyroid minimal surface is one type of triply periodic minimal surface (TPMS). TPMS is a minimal surface replicated in the three main directions of the Cartesian coordinate system. The minimal surface is a surface stretched between two objects, known as the smallest [...] Read more.
The gyroid minimal surface is one type of triply periodic minimal surface (TPMS). TPMS is a minimal surface replicated in the three main directions of the Cartesian coordinate system. The minimal surface is a surface stretched between two objects, known as the smallest possible area (e.g., a soap bubble with a saddle shape stretched between two parallel circles). The complicated shape of the TPMS makes its production possible only by additive methods (3D printing). This article presents the results of experimental studies on heat transfer and flow resistance in a heat exchanger made of stainless steel. The heat exchange surface, a TPMS gyroid, separates two working media: hot and cold water. The water flow rate was varied in the range from 8 kg/h to 25 kg/h (Re = 246–1171). The water temperature at the inlet to the exchanger was maintained at a constant level of 8.8 ± 0.3 °C and 49.5 ± 0.5 °C for cold and hot water, respectively. The effect of water flow rate on the change in its temperature, the heat output of the exchanger, the average heat transfer coefficient, pressure drop, and overall resistance factor was presented. Full article
(This article belongs to the Section J1: Heat and Mass Transfer)
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21 pages, 5750 KiB  
Article
Numerical Simulations of Coupled Vapor, Water, and Heat Flow in Unsaturated Deformable Soils During Freezing and Thawing
by Sara Soltanpour and Adolfo Foriero
Geotechnics 2025, 5(3), 51; https://doi.org/10.3390/geotechnics5030051 - 4 Aug 2025
Abstract
Freezing and thawing cycles significantly affect the mechanical and hydraulic behavior of soils, posing detrimental challenges for infrastructures in cold climates. This study develops and validates a coupled Thermal–Hydraulic–Mechanical (THM) model using COMSOL Multiphysics (Version 6.3) to demonstrate the complexities of vapor and [...] Read more.
Freezing and thawing cycles significantly affect the mechanical and hydraulic behavior of soils, posing detrimental challenges for infrastructures in cold climates. This study develops and validates a coupled Thermal–Hydraulic–Mechanical (THM) model using COMSOL Multiphysics (Version 6.3) to demonstrate the complexities of vapor and water flux, heat transport, frost heave, and vertical stress build-up in unsaturated soils. The analysis focuses on fine sand, sandy clay, and silty clay by examining their varying susceptibilities to frost action. Silty clay generated the highest amount of frost heave and steepest vertical stress gradients due to its high-water retention and strong capillary forces. Fine sand, on the other hand, produced a minimal amount of frost heave and a polarized vertical stress distribution. The study also revealed that vapor flux is more noticeable in freezing fine sand, while silty clay produces the greatest water flux between the frozen and unfrozen zones. The study also assesses the impact of soil properties including the saturated hydraulic conductivity, the particle thermal conductivity, and particle heat capacity on the frost-induced phenomena. Findings show that reducing the saturated hydraulic conductivity has a greater impact on mitigating frost heave than other variations in thermal properties. Silty clay is most affected by these changes, particularly near the soil surface, while fine sand shows less noticeable responses. Full article
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16 pages, 1313 KiB  
Article
Mycorrhizas Promote Total Flavonoid Levels in Trifoliate Orange by Accelerating the Flavonoid Biosynthetic Pathway to Reduce Oxidative Damage Under Drought
by Lei Liu and Hong-Na Mu
Horticulturae 2025, 11(8), 910; https://doi.org/10.3390/horticulturae11080910 (registering DOI) - 4 Aug 2025
Abstract
Flavonoids serve as crucial plant antioxidants in drought tolerance, yet their antioxidant regulatory mechanisms within mycorrhizal plants remain unclear. In this study, using a two-factor design, trifoliate orange (Poncirus trifoliata (L.) Raf.) seedlings in the four-to-five-leaf stage were either inoculated with Funneliformis [...] Read more.
Flavonoids serve as crucial plant antioxidants in drought tolerance, yet their antioxidant regulatory mechanisms within mycorrhizal plants remain unclear. In this study, using a two-factor design, trifoliate orange (Poncirus trifoliata (L.) Raf.) seedlings in the four-to-five-leaf stage were either inoculated with Funneliformis mosseae or not, and subjected to well-watered (70–75% of field maximum water-holding capacity) or drought stress (50–55% field maximum water-holding capacity) conditions for 10 weeks. Plant growth performance, photosynthetic physiology, leaf flavonoid content and their antioxidant capacity, reactive oxygen species levels, and activities and gene expression of key flavonoid biosynthesis enzymes were analyzed. Although drought stress significantly reduced root colonization and soil hyphal length, inoculation with F. mosseae consistently enhanced the biomass of leaves, stems, and roots, as well as root surface area and diameter, irrespective of soil moisture. Despite drought suppressing photosynthesis in mycorrhizal plants, F. mosseae substantially improved photosynthetic capacity (measured via gas exchange) and optimized photochemical efficiency (assessed by chlorophyll fluorescence) while reducing non-photochemical quenching (heat dissipation). Inoculation with F. mosseae elevated the total flavonoid content in leaves by 46.67% (well-watered) and 14.04% (drought), accompanied by significantly enhanced activities of key synthases such as phenylalanine ammonia-lyase (PAL), chalcone synthase (CHS), chalcone isomerase (CHI), 4-coumarate:coA ligase (4CL), and cinnamate 4-hydroxylase (C4H), with increases ranging from 16.90 to 117.42% under drought. Quantitative real-time PCR revealed that both mycorrhization and drought upregulated the expression of PtPAL1, PtCHI, and Pt4CL genes, with soil moisture critically modulating mycorrhizal regulatory effects. In vitro assays showed that flavonoid extracts scavenged radicals at rates of 30.07–41.60% in hydroxyl radical (•OH), 71.89–78.06% in superoxide radical anion (O2•−), and 49.97–74.75% in 2,2-diphenyl-1-picrylhydrazyl (DPPH). Mycorrhizal symbiosis enhanced the antioxidant capacity of flavonoids, resulting in higher scavenging rates of •OH (19.07%), O2•− (5.00%), and DPPH (31.81%) under drought. Inoculated plants displayed reduced hydrogen peroxide (19.77%), O2•− (23.90%), and malondialdehyde (17.36%) levels. This study concludes that mycorrhizae promote the level of total flavonoids in trifoliate orange by accelerating the flavonoid biosynthesis pathway, hence reducing oxidative damage under drought. Full article
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