Search Results (168)

Carbon fiber-reinforced thermoplastic composites (CFRTPs) have attracted increasing attention in aerospace, transportation, marine engineering, and other advanced manufacturing fields owing to their high specific mechanical properties, impact resistance, weldability, reprocessibility, and potential recyclability. However, the high melt viscosity of thermoplastic matrices, the permeability limitations associated with different reinforcement architectures, and the chemical inertness of carbon fiber surfaces continue to restrict resin impregnation, interfacial bonding, defect control, and forming stability. This review systematically summarizes recent advances in CFRTP manufacturing from the perspective of material-derived processing challenges and interface engineering. First, representative thermoplastic matrix systems and reinforcement architectures are discussed, with emphasis on their effects on processability, crystallization behavior, resin flow, and load transfer. Subsequently, six major forming processes, including hot stamping, injection molding, pultrusion, filament winding, automated fiber placement, and additive manufacturing, are critically compared in terms of processing principles, typical defects, technical limitations, and application boundaries. Particular attention is given to process-induced quality issues such as voids, wrinkling, springback, fiber breakage, warpage, insufficient consolidation, and weak interlayer bonding. Finally, interface engineering strategies, including chemical surface modification, interfacial structural design, and functional interlayer design, are reviewed as practical routes to improve wetting, shorten impregnation pathways, and enhance fiber–matrix load transfer in high-viscosity thermoplastic systems. This review highlights that CFRTP manufacturing should be understood as a coupled materials–processing–interface problem rather than a single forming operation. Future development is discussed with emphasis on reproducible manufacturing, processability-oriented materials, scalable interface engineering, predictive modeling, and standardized structural validation. Full article

High-power 355 nm ultraviolet (UV) lasers, leveraging their short wavelength, high photon energy, and high absorption across a broad range of materials, have become indispensable light sources for precision manufacturing, semiconductor processing, and laser direct imaging (LDI). In this paper, we demonstrate a high-power 355 nm UV laser system based on a narrow-linewidth polarization-maintaining (PM) Yb-doped fiber laser and cascaded frequency conversion. A single-frequency semiconductor laser is employed as the seed source, with its spectral linewidth broadened to 0.32 nm (full width at half maximum, FWHM) via phase modulation to suppress stimulated Brillouin scattering (SBS). Through a PM master oscillator power amplifier (MOPA) architecture, a maximum average output power of 899 W at 1064 nm is achieved with a beam quality factor of M² = 1.12 (M²_x = 1.11, M²_y = 1.13). By employing lithium triborate (LiB₃O₅, LBO) crystals for extracavity cascaded second-harmonic generation (SHG) and sum-frequency generation (SFG), a maximum green output power of 613.7 W at 532 nm is obtained, corresponding to a SHG conversion efficiency of 68.2%, and a maximum UV output power of 227.1 W at 355 nm is achieved, with a total conversion efficiency of 25.2%. At the maximum output power, the UV beam quality factors are M² = 1.16 (M²_x = 1.24 and M²_y = 1.09), and the power fluctuation is better than ±1.5% root-mean-square (RMS) over 8 h of continuous operation. These results indicate that the cascaded frequency conversion approach based on narrow-linewidth PM fiber lasers possesses the capability for further scaling to higher-power single-path high-brightness UV output and can provide high-brightness UV sources for applications such as flexible printed circuit (FPC) laser cutting, flat-panel display laser direct imaging, and semiconductor wafer scribing. Full article

Relaxor ferroelectric single crystals, such as Pb(In₁/₂Nb₂/₃)O₃–Pb(Mg₁/₂Nb₂/₃)O₃–PbTiO₃, possess extraordinary electro-optic (EO) coefficients, offering immense potential for next-generation integrated modulators. However, the application of PIN-PMN-PT in fiber-optic gyroscopes (FOGs) is hindered by the challenge of fabricating high-quality optical waveguides with strict mode selectivity, as conventional diffusion typically excites multi-mode propagation. Here, the fabrication of high-quality, mode-selective waveguides is achieved in rhombohedral PIN-PMN-PT via a nickel in-diffusion technique. The resulting graded-index structures exhibit a Gaussian profile with a maximum refractive index change (∆n) of 1.53% while preserving the single crystal structure. Under specific processing conditions, we achieve precise mode selectivity, enabling exclusive transverse electric (TE) mode transmission. This mode selectivity fulfills the requirements for single-mode Y-branch geometries, establishing a robust platform for ultra-compact, low driving voltage modulators and advancing the miniaturization of inertial navigation and integrated photonic systems. Full article

Vertical-External-Cavity Surface-Emitting Lasers (VECSELs) have gained significant attention over the past two decades due to their versatility in a wide range of photonic applications. This review focuses on VECSEL configurations for dual-wavelength emission, highlighting their use in high-resolution spectroscopy, terahertz (THz) generation, and advanced optical communication. We explore recent developments in VECSEL designs, including systems utilizing birefringent crystals for polarization-based frequency separation and configurations with dual-VECSEL chips or dual-gain regions within a single cavity. These two-wavelength VECSELs enable diverse operation modes, including narrow-linewidth, pulsed, multimode, and frequency-converted emission, with high-brightness output, excellent beam quality, and tunable wavelengths. Additionally, the review discusses advancements in dual-frequency VECSELs, with applications in LIDAR systems for environmental monitoring, highly stable optical clocks, and fiber sensors. We examine improvements in cavity design, semiconductor structures, and power stabilization, which have enhanced frequency stability and spectral purity, making VECSELs suitable for precision metrology and sensing applications. Full article

The 795 nm wavelength corresponds to the D1 transition of rubidium atoms and is widely used in atomic optical pumping, atomic clocks, magnetometers, and precision spectroscopy. For compact free-space collimation, beam shaping, and efficient fiber coupling, edge-emitting semiconductor lasers with reduced fast-axis (vertical) divergence are highly desirable, yet low-divergence designs at 795 nm remain limited. Here, we propose and demonstrate low-divergence photonic-crystal epitaxy (LD–PC) for 795 nm edge-emitting lasers. By engineering a periodic n-side photonic-crystal stack to place the fundamental vertical mode near the photonic band edge, the vertical mode is expanded while maintaining effective modal discrimination. Narrow-ridge Fabry–Pérot lasers based on GaAsP/AlGaAs single-quantum-well epitaxy were fabricated and characterized. The optimized LD–PC device (3 μm ridge width, 1 mm cavity length) delivers 227 mW at 200 mA with a threshold current of 23 mA, a slope efficiency of 1.28 W/A, and a peak wall-plug efficiency of 55% under continuous-wave operation at 25 °C. The measured far-field divergences (FWHMs) are 7.16° and 18.83° in the lateral and vertical directions, respectively, corresponding to a reduction in the vertical divergence from >40° in the reference structure to <20° with LD–PC. These results validate photonic-crystal epitaxy as an effective route toward compact, high-performance, low-divergence 795 nm semiconductor laser sources for rubidium-based atomic systems. Full article

We report on sub-50 fs pulse generation from a diode-pumped mode-locked laser based on an ytterbium-doped monoclinic potassium yttrium double tungstate crystal operating in the 1 μm spectral region. Pumping by a low-power, spatially single-mode, fiber-coupled laser diode at 976 nm, a maximum continuous-wave output power of 433 mW at 1066.1 nm was obtained. Using a quartz-based intracavity Lyot filter, an exceptionally broad continuous-wavelength tuning range of 98 nm was achieved. In the mode-locked regime, the diode-pumped Yb:KY(WO₄)₂ laser delivered soliton pulses as short as 46 fs at a central wavelength of 1069.2 nm by employing a SEmiconductor Saturable Absorber Mirror. To the best of our knowledge, these results represent the broadest continuous-wave tuning range and the shortest pulse duration ever reported for lasers based on ytterbium-doped monoclinic double tungstate crystals. Full article

Over the past two decades, numerous studies have examined the etiological significance of DNA fragmentation in human sperm using methods such as the comet assay (CA), the sperm chromatin structure assay, the sperm chromatin dispersion assay, and the TUNEL assay. We developed single-cell pulsed-field gel electrophoresis techniques, including one-dimensional (1D-SCPFGE) and angle-modulated two-dimensional (2D-SCPFGE), to detect early signs of naturally occurring DNA fragmentation. Comparative studies using purified human sperm with and without DNA fragmentation revealed some technical limitations in the conventional methods. This technical review outlines the procedures to ensure the quantitative performance of SCPFGE: (1) The mass of naked DNA was prepared through simultaneous in-gel swelling and proteolysis, which are highly sensitive to chemical and physical factors. Notably, these processes are vulnerable to reactive oxygen species (ROS). We developed the anti-ROS SCPFGE system to prevent artifactual cleavages. (2) 1D-SCPFGE discharges long-chain fibers from the origin, separating fibrous and granular segments beyond the tips of the fibers. (3) During continuous electrophoresis after 150° rotation (2D-SCPFGE-0-150), long-chain fibers unexpectedly extended diagonally backward from the origin, with long fibrous segments pulled out from a bundle that extended during the first electrophoresis, indicating some fibrous segments were embedded within the long-chain fibers. Even when SCPFGE was employed, one-directional current led to false negatives. (4) 2D-SCPFGE with angle rotation is currently the most sensitive imaging method for single-nuclear DNA fibers. However, without knowing the size of DNA fragments, it remains a semi-quantitative analysis. (5) To prevent artifactual DNA cleavage caused by ice crystals, low-temperature liquid storage is recommended. (6) The in-gel proteolyzed naked DNA is suitable as a substrate for chemical and enzymatic DNA cleavage analyses. Full article

Entangled-photon sources are indispensable components in free-space quantum key distribution (QKD) systems. Here, we present a compact, lightweight, and robust airborne entangled-photon source (AEPS) based on a Sagnac loop structure with single-mode fiber coupling. To meet the drone requirements for miniaturization, lightweight design, and high robustness, we developed a highly integrated entangled-photon source using customized miniature optical components and an adhesive bonding technique. The total volume and weight are only 38 × 40 × 24 mm³ and 58 g, respectively. Entangled-photon pairs at 810 nm are generated via Type-II spontaneous parametric down-conversion (SPDC) in a periodically poled KTiOPO₄ (PPKTP) crystal. We achieve a quantum state fidelity of F = 0.986 ± 0.0017, a photon-pair generation rate of 3.03 × 10⁶ pairs/s/mW, and a CHSH Bell parameter of S = 2.764 ± 0.082. Owing to its excellent size, weight, performance, and stability, the proposed entangled-photon source is particularly well suited for drone-based free-space mobile quantum communication. Full article

Flax (Linum usitatissimum L.) is a crop widely cultivated for fiber and oil production. The screening method for flax breeding must effectively address the biochemical characteristics of flaxseeds. In this study, to characterize flax cultivars, we extracted oil, defatted kernel, hull, and mucilage from whole seeds for the ATR-FT-MIR and FT-Raman spectroscopic measurements. In addition, for ATR-FT-MIR analysis, oil samples were obtained by pressing the flaxseed directly onto the crystal surface. After removing any seed residues, a grease stain was used for the measurement, allowing for the acquisition of the oil spectrum from a single seed. This method also enabled the detection of free fatty acids, serving as evidence of seed damage. Both methods effectively estimated the degree of unsaturation as a cultivar marker. The vibrational spectra of defatted kernels showed strong protein features; polysaccharide bands dominated in hull and mucilage spectra. Discrimination of flax cultivars using principal component analysis of vibrational spectra in specific regions was the most promising for flaxseed oil and mucilage. Multivariate analysis of a set of selected variables sensitive to the flaxseed oil composition successfully distinguished all flax cultivars of this study. The strong correlation observed between ATR-FT-MIR and FT-Raman results confirmed that these methods are comparable for characterizing different grades of flaxseed oil. Full article

We report a dispersion-controlled Yb-doped fiber chirped pulse amplification (CPA) system incorporating a tunable chirped fiber Bragg grating (CFBG) stretcher and a single-grating transmission compressor for dynamic compensation of power-dependent nonlinear effect. During the pulse amplification, the CFBG introduces adjustable third-order dispersion (TOD). By tuning the initial TOD provided by CFBG from −0.1965 ps³ at 2.37 W to −0.1791 ps³ at 9.65 W, residual TOD is efficiently compensated with the power-dependent nonlinear effect. As a result, by optimizing the dispersion balance at each output power, nearly constant femtosecond pulses with a duration of 250 fs are obtained over the entire power range, confirming effective control of nonlinear and dispersive effects in the amplification. The high-quality 1030 nm pulses enable efficient second-harmonic generation (SHG) in a type-I BBO crystal, producing 3.56 W femtosecond output at around 515 nm with a pulse duration of 190 fs, close to the Fourier transform limit. These results demonstrate a robust approach to generating high-power and temporal coherent ultrafast pulses suitable for precision micromachining and two-photon polymerization. Full article

Distributed fiber-optic photoacoustic non-destructive testing (DFP-NDT) represents a paradigm shift from passive sensing to active probing, fundamentally transforming structural health monitoring through integrated fiber-based ultrasonic generation and detection capabilities. This review systematically examines DFP-NDT’s evolution by following the technology’s natural progression from fundamental principles to practical implementations. Unlike conventional approaches that require external excitation mechanisms, DFP-NDT leverages photoacoustic transducers as integrated active components where fiber-optical devices themselves generate and detect ultrasonic waves. Central to this technology are photoacoustic materials engineered to maximize conversion efficiency—from carbon nanotube-polymer composites achieving 2.74 × 10⁻² conversion efficiency to innovative MXene-based systems that combine high photothermal conversion with structural protection functionality. These materials operate within sophisticated microstructural frameworks—including tilted fiber Bragg gratings, collapsed photonic crystal fibers, and functionalized polymer coatings—that enable precise control over optical-to-thermal-to-acoustic energy conversion. Six primary distributed fiber-optic photoacoustic transducer array (DFOPTA) methodologies have been developed to transform single-point transducers into multiplexed systems, with low-frequency variants significantly extending penetration capability while maintaining high spatial resolution. Recent advances in imaging algorithms have particular emphasis on techniques specifically adapted for distributed photoacoustic data, including innovative computational frameworks that overcome traditional algorithmic limitations through sophisticated statistical modeling. Documented applications demonstrate DFP-NDT’s exceptional versatility across structural monitoring scenarios, achieving impressive performance metrics including 90 × 54 cm² coverage areas, sub-millimeter resolution, and robust operation under complex multimodal interference conditions. Despite these advances, key challenges remain in scaling multiplexing density, expanding operational robustness for extreme environments, and developing algorithms specifically optimized for simultaneous multi-source excitation. This review establishes a clear roadmap for future development where enhanced multiplexed architectures, domain-specific material innovations, and purpose-built computational frameworks will transition DFP-NDT from promising laboratory demonstrations to deployable industrial solutions for comprehensive structural integrity assessment. Full article

At present, phosphogypsum, as an industrial by-product, is a solid waste in phosphoric acid production, and its accumulation has caused serious environmental pollution. Furthermore, due to the insufficient insulation properties of traditional wall materials, the issue of a rising proportion of building energy consumption in total social energy consumption has become increasingly pressing. The study investigated vitrified beads as a light aggregate and phosphogypsum, mineral powder, and quicklime as an inorganic composite cementitious system to prepare the phosphogypsum-based lightweight thermal insulation material. The effect mechanism of the initial material ratio on the mechanical properties and micro-morphology of insulation materials was studied by macroscale mechanical property testing, X-ray diffraction, and scanning electron microscopy. Meanwhile, in order to meet the performance indexes specified in relevant standards, insulation materials were modified by adding sulfate aluminate cement, basalt fibers, and a waterproof agent to improve the strength, toughness, and water resistance. Based on the single-factor experimental design, the optimal dosage of various admixtures was obtained. The results indicated that the optimal properties of the sample were achieved when the binder–bead ratio was 1:4, the water–binder ratio was 1.6, the dosage of hydroxypropyl methylcellulose was 0.1%, and the solid content of waterborne acrylic emulsion was 24%. The optimal dosages of cement and fibers were 8% and 0.9%, respectively. The cement hydration products and gypsum crystals lapped through each other, filling the pores in the matrix and increasing the strength of the sample. In addition, the fibers could form a disordered network structure inside the matrix, disperse external force, weaken the stress concentration at the tip of internal cracks, and significantly improve the toughness of the modified sample. By incorporating 2.0% paraffin emulsion in the mortar and spraying 5 dilutions of sodium methyl silicate on the external surface, dense protective layers were formed both inside and outside the modified sample. The water absorption rate reduced from 30.27% to 23.30%, and the water resistance was increased to satisfy the specified requirement for the insulation material. Full article

Bloch-like surface waves (BLSWs) are electromagnetic waves generated at the interface between a dielectric medium and a photonic crystal. BLSWs have significant potential for sensing applications, since their electromagnetic fields are tightly confined near the interface, reaching comparable sensitivities to those of surface plasmon polariton (SPP)-based devices, but with higher figures of merit (FOM). This work explores a sensor based on BLSW at the interface formed by a TiO₂ thin film deposited on the flat surface of a laterally polished photonic crystal fiber (PCF). The performance of the sensor is studied when the TiO₂ film is partially removed, transforming the nanolayer into a nanostrip. The results of this study contribute to the optimization of the sensing performance of the proposed structure. Full article

This study aimed to develop an industrially scalable coating route for enhancing the oxidation resistance of carbon fiber fabrics, a critical requirement for next-generation aerospace and high-temperature composite structures. To achieve this goal, synthesis of hexagonal boron nitride (h-BN) layers was achieved via a single wet step in which the fabric was impregnated with an ammonia–borane/THF solution and subsequently nitrided for 2 h at 1000–1500 °C in flowing nitrogen. Thermogravimetric analysis coupled with X-ray diffraction revealed that amorphous BN formed below ≈1200 °C and crystallized completely into (002)-textured h-BN (with lattice parameters a ≈ 2.50 Å and c ≈ 6.7 Å) once the dwell temperature reached ≥1300 °C. Complementary XPS, FTIR and Raman spectroscopy confirmed a near-stoichiometric B:N ≈ 1:1 composition and the elimination of O–H/N–H residues as crystallinity improved. Low-magnification SEM (100×) confirmed the uniform and large-area coverage of the BN layer on the carbon fiber tows, while high-magnification SEM revealed a progressive densification of the coating from discrete nanospheres to a continuous nanosheet barrier on the fibers. Oxidation tests in flowing air shifted the onset of mass loss from 685 °C for uncoated fibers to 828 °C for the coating produced at 1400 °C; concurrently, the peak oxidation rate moved ≈200 °C higher and declined by ~40%. Treatment at 1500 °C conferred no additional benefit, indicating that 1400 °C provides the optimal balance between full crystallinity and limited grain coarsening. The resulting dense h-BN film, aided by an in situ self-healing B₂O₃ glaze above ~800 °C, delayed carbon fiber oxidation by ≈140 °C. Overall, the process offers a cost-effective, large-area alternative to vapor-phase deposition techniques, positioning BN-coated carbon fiber fabrics for robust service in extreme oxidative environments. Full article

In this study, the oxidation of industrial hemp staple fibers by the TEMPO/NaBr/NaClO system was explored by the real-time monitoring of the changes in reaction rate, selective oxidative conversion, and reaction time under different operating conditions such as TEMPO usage, NaBr usage, NaClO usage, reaction time, and reaction temperature. We propose a variable-speed competition mechanism between NaClO and TEMPO, which provides experimental support for the long-standing hypothesis that hypochlorite delays acid formation through modulation of the HOCl/OCl⁻ and HOBr/OBr⁻ equilibrium dynamics. The innovative use of combined analysis for several consecutive first-order reactions to investigate the rate-limiting reactions of TEMPO, TEMPO⁺, and TEMPOH over a range of concentrations revealed that the reaction that generates TEMPOH is the key rate-limiting reaction. We characterize the apparent oxidation kinetics of industrial hemp staple fiber in the TEMPO/NaBr/NaClO system using a pseudo-first-order kinetic model, revealing distinct apparent reaction rates across both primary and secondary bast fiber regions. This paper explained the difference in reaction rate between the two aspects of microfibril spatial structure and cellulose crystal structure. The single-factor analysis indicates that reaction time and temperature exert the most significant influence on the conversion rate of selective oxidation within this system. Full article