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Search Results (1,113)

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38 pages, 5046 KiB  
Review
Photonics on a Budget: Low-Cost Polymer Sensors for a Smarter World
by Muhammad A. Butt
Micromachines 2025, 16(7), 813; https://doi.org/10.3390/mi16070813 - 15 Jul 2025
Viewed by 191
Abstract
Polymer-based photonic sensors are emerging as cost-effective, scalable alternatives to conventional silicon and glass photonic platforms, offering unique advantages in flexibility, functionality, and manufacturability. This review provides a comprehensive assessment of recent advances in polymer photonic sensing technologies, focusing on material systems, fabrication [...] Read more.
Polymer-based photonic sensors are emerging as cost-effective, scalable alternatives to conventional silicon and glass photonic platforms, offering unique advantages in flexibility, functionality, and manufacturability. This review provides a comprehensive assessment of recent advances in polymer photonic sensing technologies, focusing on material systems, fabrication techniques, device architectures, and application domains. Key polymer materials, including PMMA, SU-8, polyimides, COC, and PDMS, are evaluated for their optical properties, processability, and suitability for integration into sensing platforms. High-throughput fabrication methods such as nanoimprint lithography, soft lithography, roll-to-roll processing, and additive manufacturing are examined for their role in enabling large-area, low-cost device production. Various photonic structures, including planar waveguides, Bragg gratings, photonic crystal slabs, microresonators, and interferometric configurations, are discussed concerning their sensing mechanisms and performance metrics. Practical applications are highlighted in environmental monitoring, biomedical diagnostics, and structural health monitoring. Challenges such as environmental stability, integration with electronic systems, and reproducibility in mass production are critically analyzed. This review also explores future opportunities in hybrid material systems, printable photonics, and wearable sensor arrays. Collectively, these developments position polymer photonic sensors as promising platforms for widespread deployment in smart, connected sensing environments. Full article
(This article belongs to the Section A:Physics)
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13 pages, 665 KiB  
Review
Emerging Technologies for Injury Identification in Sports Settings: A Systematic Review
by Luke Canavan Dignam, Lisa Ryan, Michael McCann and Ed Daly
Appl. Sci. 2025, 15(14), 7874; https://doi.org/10.3390/app15147874 - 14 Jul 2025
Viewed by 164
Abstract
Sport injury recognition is rapidly evolving with the integration of new emerging technologies. This systematic review aims to identify and evaluate technologies capable of detecting injuries during sports participation. A comprehensive search of PUBMED, Sport Discus, Web of Science, and ScienceDirect was conducted [...] Read more.
Sport injury recognition is rapidly evolving with the integration of new emerging technologies. This systematic review aims to identify and evaluate technologies capable of detecting injuries during sports participation. A comprehensive search of PUBMED, Sport Discus, Web of Science, and ScienceDirect was conducted following the PRISMA 2020 guidelines. The review was registered on PROSPERO (CRD42024608964). Inclusion criteria focused on prospective studies involving athletes of all ages, evaluating tools which are utilised to identify injuries in sports settings. The review included research between 2014 and 2024; retrospective, conceptual, and fatigue-focused studies were excluded. Risk of bias was assessed using the Critical Appraisal Skills Program (CASP) tool. Of 4283 records screened, 70 full-text articles were assessed, with 21 studies meeting the final inclusion criteria. The technologies were grouped into advanced imaging (Magnetic Resonance Imaging (MRI), Diffusion Tensor Imaging (DFI), and Quantitative Susceptibility Mapping (QSM), with biomarkers (i.e., Neurofilament Light (NfL), Tau protein, Glial Fibrillary Acidic Protein (GFAP), Salivary MicroRNAs, and Immunoglobulin A (IgA), and sideline assessments (i.e., the King–Devick test, KD-Eye Tracking, modified Balance Error Scoring System (mBESS), DETECT, ImPACT structured video analysis, and Instrumented Mouth Guards (iMGs)), which demonstrated feasibility for immediate sideline identification of injury. Future research should improve methodological rigour through larger, diverse samples and controlled designs, with real-world testing environments. Following this guidance, the application of emerging technologies may assist medical staff, coaches, and national governing bodies in identifying injuries in a sports setting, providing real-time assessment. Full article
(This article belongs to the Special Issue Sports Injuries: Prevention and Rehabilitation)
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11 pages, 1841 KiB  
Article
Construction of Silane-Modified Diatomite-Magnetic Nanocomposite Superhydrophobic Coatings Using Multi-Scale Composite Principle
by Dan Li, Mei Wu, Rongjun Xia, Jiwen Hu and Fangzhi Huang
Coatings 2025, 15(7), 786; https://doi.org/10.3390/coatings15070786 - 3 Jul 2025
Viewed by 339
Abstract
To address the challenges of cotton cellulose materials being susceptible to environmental humidity and pollutant erosion, a strategy for constructing superhydrophobic functional coatings with biomimetic micro–nano composite structures was proposed. Through surface silanization modification, diatomite (DEM) and Fe3O4 nanoparticles were [...] Read more.
To address the challenges of cotton cellulose materials being susceptible to environmental humidity and pollutant erosion, a strategy for constructing superhydrophobic functional coatings with biomimetic micro–nano composite structures was proposed. Through surface silanization modification, diatomite (DEM) and Fe3O4 nanoparticles were functionalized with octyltriethoxysilane (OTS) to prepare superhydrophobic diatomite flakes (ODEM) and OFe3O4 nanoparticles. Following the multi-scale composite principle, ODEM and OFe3O4 nanoparticles were blended and crosslinked via the hydroxyl-initiated ring-opening polymerization of epoxy resin (EP), resulting in an EP/ODEM@OFe3O4 composite coating with hierarchical roughness. Microstructural characterization revealed that the micrometer-scale porous structure of ODEM and the nanoscale protrusions of OFe3O4 form a hierarchical micro–nano topography. The special topography combined with the low surface energy property leads to a contact angle of 158°. Additionally, the narrow bandgap semiconductor characteristic of OFe3O4 induces the localized surface plasmon resonance effect. This enables the coating to attain 80% light absorption across the 350–2500 nm spectrum, and rapidly heat to 45.8 °C within 60 s under 0.5 sun, thereby demonstrating excellent deicing performance. This work provides a theoretical foundation for developing environmentally tolerant superhydrophobic photothermal coatings, which exhibit significant application potential in the field of anti-icing and anti-fouling. Full article
(This article belongs to the Section Corrosion, Wear and Erosion)
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8 pages, 10733 KiB  
Article
Integrated NV Center-Based Temperature Sensor for Internal Thermal Monitoring in Optical Waveguides
by Yifan Zhao, Shihan Ding, Shuo Wang, Yiming Hu, Hongliang Liu, Zhen Shang and Yongjian Gu
Sensors 2025, 25(13), 4123; https://doi.org/10.3390/s25134123 - 2 Jul 2025
Viewed by 304
Abstract
Color centers in solids, such as nitrogen-vacancy (NV) centers in diamonds, have gained significant attention in recent years due to their exceptional properties for quantum sensing. In this work, we demonstrate an NV center-based temperature sensor integrated into an optical waveguide to enable [...] Read more.
Color centers in solids, such as nitrogen-vacancy (NV) centers in diamonds, have gained significant attention in recent years due to their exceptional properties for quantum sensing. In this work, we demonstrate an NV center-based temperature sensor integrated into an optical waveguide to enable internal temperature sensing. A surface-cladding optical waveguide was fabricated in a diamond wafer containing NV centers using femtosecond laser direct writing. By analyzing the resonant peaks of optically detected magnetic resonance (ODMR) spectra, we established a precise correlation between temperature changes induced by the pump laser and shifts in the ODMR peak positions. This approach enabled temperature monitoring with a sensitivity of 1.1 mK/Hz. These results highlight the significant potential of color centers in solids for non-contact, micro-scale temperature monitoring. Full article
(This article belongs to the Section Optical Sensors)
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16 pages, 533 KiB  
Review
Right Ventricular Dynamics in Tricuspid Regurgitation: Insights into Reverse Remodeling and Outcome Prediction Post Transcatheter Valve Intervention
by Philipp M. Doldi, Manuela Thienel and Kevin Willy
Int. J. Mol. Sci. 2025, 26(13), 6322; https://doi.org/10.3390/ijms26136322 - 30 Jun 2025
Viewed by 340
Abstract
Tricuspid regurgitation (TR) represents a significant, often silently progressing, valvular heart disease with historically suboptimal management due to perceived high surgical risks. Transcatheter tricuspid valve interventions (TTVI) offer a promising, less invasive therapeutic avenue. Central to the success of TTVI is Right Ventricular [...] Read more.
Tricuspid regurgitation (TR) represents a significant, often silently progressing, valvular heart disease with historically suboptimal management due to perceived high surgical risks. Transcatheter tricuspid valve interventions (TTVI) offer a promising, less invasive therapeutic avenue. Central to the success of TTVI is Right Ventricular Reverse Remodelling (RVRR), defined as an improvement in RV structure and function, which strongly correlates with enhanced patient survival. The right ventricle (RV) undergoes complex multi-scale biomechanical maladaptations, progressing from adaptive concentric to maladaptive eccentric hypertrophy, coupled with increased stiffness and fibrosis. Molecular drivers of this pathology include early failure of antioxidant defenses, metabolic shifts towards glycolysis, and dysregulation of microRNAs. Accurate RV function assessment necessitates advanced imaging modalities like 3D echocardiography, Cardiac Magnetic Resonance Imaging (CMR), and Computed Tomography (CT), along with strain analysis. Following TTVI, RVRR typically manifests as a biphasic reduction in RV volume overload, improved myocardial strain, and enhanced RV-pulmonary arterial coupling. Emerging molecular biomarkers alongside advanced imaging-derived biomechanical markers like CT-based 3D-TAPSE and RV longitudinal strain, are proving valuable. Artificial intelligence (AI) and machine learning (ML) are transforming prognostication by integrating diverse clinical, laboratory, and multi-modal imaging data, enabling unprecedented precision in risk stratification and optimizing TTVI strategies. Full article
(This article belongs to the Special Issue Biomechanics of Cardiovascular Remodeling)
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14 pages, 23403 KiB  
Article
Flexibly Reconfigurable Kerr Micro-Comb Based on Cascaded Si3N4 Micro-Ring Filters
by Jieyu Yang, Guang Chen, Lidan Lu, Jianzhen Ou, Chao Mei, Yingjie Xu, Wenbo Bo, Peng Wang, Xinyi Li and Lianqing Zhu
Photonics 2025, 12(7), 661; https://doi.org/10.3390/photonics12070661 - 30 Jun 2025
Viewed by 256
Abstract
In recent years, micro-combs, due to their compact structure and high efficiency, have proven to be a practical solution for optical sources. In this paper, an approach to flexibly modulating micro-combs is proposed, and a simulation platform based on Si3N4 [...] Read more.
In recent years, micro-combs, due to their compact structure and high efficiency, have proven to be a practical solution for optical sources. In this paper, an approach to flexibly modulating micro-combs is proposed, and a simulation platform based on Si3N4 micro-combs with highly integrated, tunable, and reconfigurable features is built. By means of the Lugiato–Lefever equation model, the dynamic evolution process of micro-combs is analyzed, and a micro-ring resonator is designed with a free spectral range of 7.24 nm, an effective mode area of 1.0829µm2, and coherent comb lines spanning over 125 THz. Cascaded silicon nitride micro-ring filters are utilized to obtain reconfigurable modulation effects for Kerr-frequency micro-combs. Due to the significance of flexibly controlled optical sources with high-repetition rates and multiple channels for system-on-chip, our proposal has potential in photonic integrated circuit systems, such as high-density photonic computing and large-capacity optical communications, in the future. Full article
(This article belongs to the Special Issue Photonic Integrated Circuits: Techniques, Insights and Devices)
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23 pages, 4126 KiB  
Article
Enhanced Hydrothermal Stability and Propylene Selectivity of Electron Beam Irradiation-Induced Hierarchical Fluid Catalytic Cracking Additives
by Nguyen Xuan Phuong Vo, Thuy Phuong Ngo, Van Tri Tran, Ngoc Thuy Luong, Phuc Nguyen Le and Van Chung Cao
Catalysts 2025, 15(7), 620; https://doi.org/10.3390/catal15070620 - 24 Jun 2025
Viewed by 1344
Abstract
A cheap, environmentally friendly, easily scalable post-treatment of Na-ZSM-5 (Si/Al molar ratio = 20 or 30) via electron-beam irradiation to produce hierarchical H-ZSM-5 as a propylene-increasing fluid catalytic cracking additive was performed. Higher specific surface areas and highly accessible porous systems were obtained [...] Read more.
A cheap, environmentally friendly, easily scalable post-treatment of Na-ZSM-5 (Si/Al molar ratio = 20 or 30) via electron-beam irradiation to produce hierarchical H-ZSM-5 as a propylene-increasing fluid catalytic cracking additive was performed. Higher specific surface areas and highly accessible porous systems were obtained among the irradiated samples. A combination of 27Al, 1H magic angle spinning nuclear magnetic resonance and NH3-temperature-programmed desorption methods showed that upon irradiation, some of the framework’s tetrahedral Al atoms were removed as non-framework Al atoms via flexible coordination with Si-OH groups (either framework or non-framework defects), thus increasing the H-ZSM-5 acidity and stability during hydrothermal dealumination. The enhanced selectivity and stability toward propylene production over the irradiated H-ZSM-5 samples were attributed to the integration of the reserved population of medium acid sites into the highly accessible hierarchical network. N2 adsorption–desorption isotherm data showed that the Si-rich H-ZSM-5 samples possessed an obvious ink-bottle-shaped micro-mesopore network and a greater degree of disordered orientation of the straight pore systems toward the exterior surfaces. Micro-activity test data suggested that with an increasing Si/Al ratio, the H-ZSM-5 additives lost some extent of their cracking activity due to the constricted hierarchical pore network toward the exterior surface but gained more stability and selectivity for propylene due to the reserved medium acid sites. Full article
(This article belongs to the Section Industrial Catalysis)
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26 pages, 6795 KiB  
Article
Integrated Analysis of Pore and Fracture Networks in Deep Coal Seams: Implications for Enhanced Reservoir Stimulation
by Kaiqi Leng, Baoshan Guan, Chen Jiang and Weidong Liu
Energies 2025, 18(13), 3235; https://doi.org/10.3390/en18133235 - 20 Jun 2025
Viewed by 206
Abstract
This study systematically investigates the pore–fracture architecture of deep coal seams in the JiaTan (JT) block of the Ordos Basin using an integrated suite of advanced techniques, including nuclear magnetic resonance (NMR), high-pressure mercury intrusion, low-temperature nitrogen adsorption, low-pressure carbon dioxide adsorption, and [...] Read more.
This study systematically investigates the pore–fracture architecture of deep coal seams in the JiaTan (JT) block of the Ordos Basin using an integrated suite of advanced techniques, including nuclear magnetic resonance (NMR), high-pressure mercury intrusion, low-temperature nitrogen adsorption, low-pressure carbon dioxide adsorption, and micro-computed tomography (micro-CT). These complementary methods enable a quantitative assessment of pore structures spanning nano- to microscale dimensions. The results reveal a pore system overwhelmingly dominated by micropores—accounting for more than 98% of the total pore volume—which play a central role in coalbed methane (CBM) storage. Microfractures, although limited in volumetric proportion, markedly enhance permeability by forming critical flow pathways. Together, these features establish a dual-porosity system that governs methane transport and recovery in deep coal reservoirs. The multiscale characterization employed here proves essential for resolving reservoir heterogeneity and designing effective stimulation strategies. Notably, enhancing methane desorption in micropore-rich matrices and improving fracture connectivity are identified as key levers for optimizing deep CBM extraction. These insights offer a valuable foundation for the development of deep coalbed methane (DCBM) resources in the Ordos Basin and similar geological settings. Full article
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17 pages, 2351 KiB  
Article
The Value of Optical Coherence Tomography in Patients with Pituitary Adenoma and Its Association with Clinical Features: A Pilot Study
by Monika Duseikaite, Alvita Vilkeviciute, Igne Dumbliauskaite, Brigita Glebauskiene, Indre Zostautiene, Vita Rovite, Sheng-Nan Wu, Arimantas Tamasauskas and Rasa Liutkeviciene
J. Clin. Med. 2025, 14(12), 4318; https://doi.org/10.3390/jcm14124318 - 17 Jun 2025
Viewed by 642
Abstract
Background: The main mechanism of optic nerve damage in patients with pituitary adenoma (PA) is the pressure of optic chiasm. The retinal nerve fiber layer (RNFL), the ganglion cell layer (GCL)+, and GCL++ thickness measurement by optical coherence tomography (OCT), visual function [...] Read more.
Background: The main mechanism of optic nerve damage in patients with pituitary adenoma (PA) is the pressure of optic chiasm. The retinal nerve fiber layer (RNFL), the ganglion cell layer (GCL)+, and GCL++ thickness measurement by optical coherence tomography (OCT), visual function evaluation, and magnetic resonance imaging (MRI) can be used to predict visual function recovery. In our study, we investigated the associations between visual acuity (VA), visual field (VF), RNFL, GCL changes, and the findings of MRI in patients with PA. Methods: This study was conducted in the Departments of Ophthalmology and Neurosurgery of the Lithuanian University of Health Sciences Hospital. A total of 25 patients diagnosed with PA were included in the study group, and 27 healthy subjects were included in the control group. The thickness of the RNFL and ganglion cell layer (GCL+, GCL++) and optic nerve disc diameter was analysed with OCT. Moreover, an MRI was performed for patients with PA. Results: The RNFL thickness around the optic disk measured preoperatively was reduced significantly in the temporal quadrant in PA patients compared with the control group (median (min; max); mean rank: 73.5 (52; 109); 58.39 vs. 69.5 (16; 168); 46.14; p = 0.038). We found that it was reduced significantly only in the inferior quadrant of the macro-PA group compared to the micro-PA group (median (min; max); mean rank: 99.5 (61; 115); 21.07 vs. 106.5 (90; 121); 32.15), p = 0.008, respectively). The RNFL thickness was reduced significantly only in the inferior quadrant of the non-active PA group compared to the active PA group (median (min; max); mean rank: 118.5 (49; 144); 17.42 vs. 130.5 (77; 156); 28.05), p = 0.028, respectively). RNFL thickness was reduced significantly only in the temporal quadrant in the PA with suprasellar extension group compared to the PA without suprasellar extension group (median (min; max); mean rank: 67.5 (16; 99); 21.66 vs. 72 (58; 168); 30.39), p = 0.036, respectively). Furthermore, GCL++ thickness was reduced significantly in total and in superior and inferior sectors of the PA with suprasellar extension group compared to the PA without suprasellar extension group (median (min; max); mean rank: 98.5 (57; 113); 21.8; 101 (61; 121); 21.48 and 102.5 (59; 116); 21.71 vs. 103.5 (95; 115); 30.2; 106.5 (90; 115); 30.61 and 104.5 (95; 113); 30.32), p = 0.043; p = 0.028 and p = 0.038, respectively). In the control group, significant positive correlations were found between optic disc area and the total RNFL thickness (r = 0.440, p < 0.001). In the PA group, significant correlations were observed between optic rim area and total RNFL thickness (r = 0.493, p < 0.001) and all quadrants, with the strongest in the nasal quadrant (r = 0.503, p < 0.001). A moderate to strong negative correlation was found between visual field (VF) defects and RNFL thickness, with the strongest correlation observed in the superior quadrant. Conclusions: OCT offers a detailed insight into the microscopic structural and functional changes throughout the entire visual pathway in patients with PA. Our findings demonstrate a significant negative correlation between RNFL thickness and visual field defects, highlighting the clinical relevance of OCT measurements in visual function assessment. Moreover, the results suggest that optic rim area may be a more reliable indicator of RNFL thickness variations than optic disc area in patients with PA. Full article
(This article belongs to the Section Clinical Neurology)
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10 pages, 2060 KiB  
Article
Passive Frequency Tunability in Moiré-Inspired Frequency Selective Surfaces Based on Full-Wave Simulation
by Jieun Hwang and Sungcheol Hong
Micromachines 2025, 16(6), 702; https://doi.org/10.3390/mi16060702 - 12 Jun 2025
Viewed by 671
Abstract
This paper presents a simulation-based investigation of passive frequency tunability in frequency-selective surfaces (FSSs) enabled by Moiré pattern interference. By overlapping two identical hexagonal FSS layers and introducing rotational misalignment between them, we demonstrate that the resulting Moiré patterns induce significant shifts in [...] Read more.
This paper presents a simulation-based investigation of passive frequency tunability in frequency-selective surfaces (FSSs) enabled by Moiré pattern interference. By overlapping two identical hexagonal FSS layers and introducing rotational misalignment between them, we demonstrate that the resulting Moiré patterns induce significant shifts in the resonance frequency without any external bias or active components. Using full-wave simulations in HFSS, we show that rotating the second layer from 0° to 30° can shift the resonant frequency from 4.4 GHz down to 1.2 GHz. This tunable behavior emerges solely from geometrical manipulation, offering a low-complexity alternative to active tuning methods that rely on varactors or micro-electromechanical systems (MEMSs). We discuss the theoretical basis for this tuning mechanism based on effective periodicity modulation via rotational interference and highlight potential applications in passive reconfigurable filters and refractive index sensors. The proposed approach provides a promising route for implementing tunable electromagnetic structures without compromising simplicity, power efficiency, or integration compatibility. Full article
(This article belongs to the Special Issue Novel Electromagnetic and Acoustic Devices)
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12 pages, 1280 KiB  
Review
SIU-ICUD: Comprehensive Imaging in Prostate Cancer—A Focus on MRI and Micro-Ultrasound
by Cesare Saitta, Wayne G. Brisbane, Hannes Cash, Sangeet Ghai, Francesco Giganti, Adam Kinnaird, Daniel Margolis and Giovanni Lughezzani
Soc. Int. Urol. J. 2025, 6(3), 39; https://doi.org/10.3390/siuj6030039 - 7 Jun 2025
Viewed by 374
Abstract
Background/Objectives: The diagnostic approach to prostate cancer (PCa) has evolved from systematic biopsies to imaging-guided strategies that improve detection of clinically significant PCa (csPCa) while reducing overdiagnosis. Multiparametric magnetic resonance imaging (mpMRI) has emerged as the gold standard for pre-biopsy evaluation, while micro-ultrasound [...] Read more.
Background/Objectives: The diagnostic approach to prostate cancer (PCa) has evolved from systematic biopsies to imaging-guided strategies that improve detection of clinically significant PCa (csPCa) while reducing overdiagnosis. Multiparametric magnetic resonance imaging (mpMRI) has emerged as the gold standard for pre-biopsy evaluation, while micro-ultrasound (MicroUS) offers a promising alternative with real-time imaging capabilities. Methods: We examined the principles, image interpretation frameworks (Prostate Imaging Reporting and Data System (PI-RADS) and Prostate Risk Identification using Micro UltraSound (PRI-MUS)), and clinical applications of mpMRI and MicroUS, comparing their diagnostic accuracy in biopsy-naïve patients, repeat biopsy scenarios, active surveillance, and staging. Results: mpMRI improves csPCa detection, reduces unnecessary biopsies, and enhances risk stratification. Landmark studies such as PRECISION (Prostate Evaluation for Clinically Important Disease: Sampling Using Image Guidance or Not?) and PRIME (Prostate Imaging Using MRI±Contrast Enhancement) confirm its superiority over systematic biopsy. However, mpMRI remains resource-intensive, with limitations in accessibility and interpretation variability. Conversely, MicroUS, with its high-resolution real-time imaging, shows non-inferiority to mpMRI and potential advantages in magnetic resonance imaging (MRI)-ineligible patients. It improves lesion visualization and biopsy targeting, with ongoing trials such as OPTIMUM (Optimization of prostate biopsy—Micro-Ultrasound versus MRI) evaluating its standalone efficacy. Conclusions: mpMRI and MicroUS are complementary modalities in PCa diagnosis. While mpMRI remains the preferred imaging standard, MicroUS offers an alternative, particularly in patients with MRI contraindications. Combining these techniques could enhance diagnostic accuracy, reduce unnecessary interventions, and refine active surveillance strategies. Future research should focus on integrating both modalities into standardized diagnostic pathways for a more individualized approach. Full article
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23 pages, 5181 KiB  
Article
Fractal Characterization and NMR Analysis of Curing-Dependent Pore Structures in Cemented Tailings Waste RockBackfill
by Jianhui Qiu, Xin Xiong and Keping Zhou
Fractal Fract. 2025, 9(6), 367; https://doi.org/10.3390/fractalfract9060367 - 4 Jun 2025
Cited by 1 | Viewed by 501
Abstract
This study investigates the coupled effects of waste rock-to-tailings ratio (WTR) and curing temperature on the pore structure and mechanical performance of cemented tailings waste rock backfill (CTRB). Four WTRs (6:4, 7:3, 8:2, 9:1) and curing temperatures (20–50 °C) were tested. Low-field nuclear [...] Read more.
This study investigates the coupled effects of waste rock-to-tailings ratio (WTR) and curing temperature on the pore structure and mechanical performance of cemented tailings waste rock backfill (CTRB). Four WTRs (6:4, 7:3, 8:2, 9:1) and curing temperatures (20–50 °C) were tested. Low-field nuclear magnetic resonance (NMR) was used to characterize pore size distributions and derive fractal dimensions (Da, Db, Dc) at micropore, mesopore, and macropore scales. Uniaxial compressive strength (UCS) and elastic modulus (E) were also measured. The results reveal that (1) the micropore structure complexity was found to be a key indicator of structural refinement, while excessive temperature led to pore coarsening and strength reduction. Da = 2.01 reaches its peak at WTR = 7:3 and curing temperature = 40 °C; (2) at this condition, the UCS and E achieved 20.5 MPa and 1260 MPa, increasing by 45% and 38% over the baseline (WTR = 6:4, 20 °C); (3) when the temperature exceeded 40 °C, Da dropped significantly (e.g., to 1.51 at 50 °C for WTR = 7:3), indicating thermal over-curing and micropore coarsening; (4) correlation analysis showed strong negative relationships between total pore volume and mechanical strength (R = −0.87 for δavs.UCS), and a positive correlation between Da and UCS (R = 0.43). (5) multivariate regression models incorporating pore volume fractions, T2 relaxation times, and fractal dimensions predicted UCS and E with R2 > 0.98; (6) the hierarchical sensitivity of fractal dimensions follows the order micro-, meso-, macropores. This study provides new insights into the microstructure–mechanical performance relationship in CTRB and offers a theoretical and practical basis for the design of high-performance backfill materials in deep mining environments. Full article
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14 pages, 1549 KiB  
Article
Equalizing the In-Ear Acoustic Response of Piezoelectric MEMS Loudspeakers Through Inverse Transducer Modeling
by Oliviero Massi, Riccardo Giampiccolo and Alberto Bernardini
Micromachines 2025, 16(6), 655; https://doi.org/10.3390/mi16060655 - 29 May 2025
Viewed by 1806
Abstract
Micro-Electro-Mechanical Systems (MEMS) loudspeakers are attracting growing interest as alternatives to conventional miniature transducers for in-ear audio applications. However, their practical deployment is often hindered by pronounced resonances in their frequency response, caused by the mechanical and acoustic characteristics of the device structure. [...] Read more.
Micro-Electro-Mechanical Systems (MEMS) loudspeakers are attracting growing interest as alternatives to conventional miniature transducers for in-ear audio applications. However, their practical deployment is often hindered by pronounced resonances in their frequency response, caused by the mechanical and acoustic characteristics of the device structure. To mitigate these limitations, we present a model-based digital signal equalization approach that leverages a circuit equivalent model of the considered MEMS loudspeaker. The method relies on constructing an inverse circuital model based on the nullor, which is implemented in the discrete-time domain using Wave Digital Filters (WDFs). This inverse system is employed to pre-process the input voltage signal, effectively compensating for the transducer frequency response. The experimental results demonstrate that the proposed method significantly flattens the Sound Pressure Level (SPL) over the 100 Hz-10 kHz frequency range, with a maximum deviation from the target flat frequency response of below 5 dB. Full article
(This article belongs to the Special Issue Exploration and Application of Piezoelectric Smart Structures)
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22 pages, 5676 KiB  
Article
Research on Rheological Behavior and Strength Characteristics of Cement-Based Grouting Materials
by Xuewei Liu, Hao Qu, Bin Liu, Yuan Zhou, Jinlan Li, Wei Deng and Weilong Tao
Buildings 2025, 15(11), 1796; https://doi.org/10.3390/buildings15111796 - 23 May 2025
Viewed by 356
Abstract
The mechanical properties of grouting materials and their cured grouts significantly impact the reinforcement effectiveness in deep coal mine roadways. This study employed shear rheology tests of slurry, structural tests, NMR (nuclear magnetic resonance), and uniaxial compression tests to comparatively analyze the mechanical [...] Read more.
The mechanical properties of grouting materials and their cured grouts significantly impact the reinforcement effectiveness in deep coal mine roadways. This study employed shear rheology tests of slurry, structural tests, NMR (nuclear magnetic resonance), and uniaxial compression tests to comparatively analyze the mechanical characteristics of a composite cement-based grouting material (HGC), ordinary Portland cement (OPC), and sulfated aluminum cement (SAC) slurry and their cured grouts. The HGC (High-performance Grouting Composite) slurry is formulated with 15.75% sulfated aluminum cement (SAC), 54.25% ordinary Portland cement (OPC), 10% fly ash, and 20% mineral powder, achieving a water/cement ratio of 0.26. The results indicate that HGC slurry more closely follows power-law flow characteristics, while OPC and SAC slurries fit better with the Bingham model. The structural recovery time for HGC slurry after high-strain disturbances is 52 s, significantly lower than the 312 s for OPC and 121 s for SAC, indicating that HGC can quickly produce hydration products that re-bond the flocculated structure. NMR T2 spectra show that HGC cured grouts have the lowest porosity, predominantly featuring inter-nanopores, whereas OPC and SAC have more super-nanopores. Uniaxial compression tests show that the uniaxial compressive strength of HGC, SAC, and OPC samples at various curing ages gradually decreases. Compared to traditional cementitious materials, HGC exhibits a rapid increase in uniaxial compressive strength within the first seven days, with an increase rate of approximately 77.97%. Finally, the relationship between micropore distribution and strength is analyzed, and the micro-mechanisms underlying the strength differences of different grouting materials are discussed. This study aids in developing a comparative analysis system of mechanical properties for deep surrounding rock grouting materials, providing a reference for selecting grouting materials for various engineering fractured rock masses. Full article
(This article belongs to the Special Issue Trends and Prospects in Cementitious Material)
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19 pages, 2112 KiB  
Article
Accurate Deep Potential Model of Temperature-Dependent Elastic Constants for Phosphorus-Doped Silicon
by Miao Gao, Xiaorui Bie, Yi Wang, Yuhang Li, Zhaoyang Zhai, Haoqi Lyu and Xudong Zou
Nanomaterials 2025, 15(10), 769; https://doi.org/10.3390/nano15100769 - 20 May 2025
Viewed by 2376
Abstract
Accurate predictions of elastic properties under varying doping concentrations and temperatures are critical for designing reliable silicon-based micro-/nano-electro-mechanical systems (MEMS/NEMS). Empirical potentials typically lack accuracy for elastic predictions, whereas density functional theory (DFT) calculations are precise but computationally expensive. In this study, we [...] Read more.
Accurate predictions of elastic properties under varying doping concentrations and temperatures are critical for designing reliable silicon-based micro-/nano-electro-mechanical systems (MEMS/NEMS). Empirical potentials typically lack accuracy for elastic predictions, whereas density functional theory (DFT) calculations are precise but computationally expensive. In this study, we developed a highly accurate and efficient machine learning-based Deep Potential (DP) model to predict the elastic constants of phosphorus-doped silicon (Si64−xPx, x = 0, 1, 2, 3, 4) within a temperature range of 0–500 K. The DP model was rigorously validated against benchmark DFT results. At 0 K, the elastic constants predicted by our DP model exhibited excellent agreement with experimental data, achieving a mean absolute percentage error (MAPE) of only 2.88%. We investigated the effects of doping on elastic constants in single-crystal silicon and determined their second-order temperature coefficients. The calculations demonstrated distinct doping-induced variations, showing pronounced decreases in C11 and C44 and a moderate increase in C12. Finite-element analyses using the fitted temperature coefficients indicated improved thermal stability of silicon resonators through phosphorus doping. Our study explores the integration of machine learning-based atomic-scale simulations with MEMS/NEMS design, providing practical guidance for optimal dopant selection to enhance silicon resonator thermal stability. Full article
(This article belongs to the Section Theory and Simulation of Nanostructures)
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