Search Results (1,507)

Acoustic tweezers, as advanced micro/nano manipulation tools, play a pivotal role in biomedical engineering, microfluidics, and precision manufacturing. However, piezoelectric-based acoustic tweezers face performance limitations due to multi-physical coupling effects during microfabrication. This study proposes a novel approach using injection molding with embedded electronics (IMEs) technology to fabricate piezoelectric micro-ultrasonic transducers with micron-scale precision, addressing the critical issue of acoustic node displacement caused by thermal–mechanical coupling in injection molding—a problem that impairs wave transmission efficiency and operational stability. To optimize the IME process parameters, a hybrid multi-objective optimization framework integrating NSGA-II and MOPSO is developed, aiming to simultaneously minimize acoustic node displacement, volumetric shrinkage, and residual stress distribution. Key process variables—packing pressure (80–120 MPa), melt temperature (230–280 °C), and packing time (15–30 s)—are analyzed via finite element modeling (FEM) and validated through in situ tie bar elongation measurements. The results show a 27.3% reduction in node displacement amplitude and a 19.6% improvement in wave transmission uniformity compared to conventional methods. This methodology enhances acoustic tweezers’ operational stability and provides a generalizable framework for multi-physics optimization in MEMS manufacturing, laying a foundation for next-generation applications in single-cell manipulation, lab-on-a-chip systems, and nanomaterial assembly. Full article

As global demand for rare earth elements (REEs) increases, maintaining the production and supply chain is critical. Technologies capable of being used in the field and in situ in the subsurface for rapid REE detection and quantification facilitates the efficient mining of known resources and exploration of new and unconventional resources. Laser-induced breakdown spectroscopy (LIBS) is a promising technique for rapid elemental analysis both in the laboratory and in the field. Multiple articles have been published evaluating LIBS for detection and quantification of REEs; however, REEs in their natural deposits have not been adequately studied. In this work, detection and quantification of two REEs, La and Nd, have been studied in both synthetic and natural mineral matrices at concentrations relevant to REE extraction. Measurements were performed on REE-containing rock and coal samples (natural and synthetic) utilizing different LIBS instruments and techniques, specifically a commercial benchtop instrument, a custom benchtop instrument (single- and double-pulse modes), and a custom LIBS probe currently being developed for in situ, subsurface, borehole wall detection and quantification of REEs. Plasma expansion, emission intensity, detection limits, and double-pulse signal enhancement were studied. The limits of detection (LOD) were found to be 10/14 ppm for La and 15/25 ppm for Nd in simulated coal/rock matrices in single-pulse mode. Signal enhancement of 3.5 to 6-fold was obtained with double-pulse mode as compared to single-pulse operation. Full article

Taxco de Alarcón (Mexico) has been affected by mining activities and the presence of potentially toxic elements (PTEs). In this study, water samples from the Acamixtla, Taxco, and San Juan rivers were analyzed using Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) to determine PTE concentrations. Statistical analyses included principal component analysis, Pearson’s correlation, the Pollution Index, and a Health Risk Assessment. Additionally, solid samples from the San Juan River with leachate from the “La Guadalupana” Mine (RSJMG S2.3) were characterized using Fourier Transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscopy (SEM). Identified PTEs included As, Cr, Ni, Zn, Fe, Mn, Cu, Cd, Pb, Se, and Li. Principal component analysis explained 94.8% of the data variance, and Pearson’s correlation revealed significant associations (p < 0.05) among Fe, As, Cu, Cd, Pb, and Zn. The RSJMG S2.3 site exhibited the highest Pollution Index value (8491.56) and the highest health exposure risks. Lower contamination levels at other sites may be attributed to the complexation of PTEs with ferrihydrite, which was identified in the RSJMG S2.3 site through microscopy and infrared analyses. These findings suggest that the in situ formation of ferrihydrite may enhance the adsorption of PTEs, thereby mitigating environmental contamination and potential health risks. Full article

Aerated accumulation bioreactors represent a promising alternative for the aerobic bioremediation of solid contaminated substrates. However, achieving homogeneous mixing and effective air distribution remains a key design challenge in solid-phase systems. This study presents the design and construction of a novel pilot-scale aerated bioreactor equipped with an angled-paddle agitation system, specifically developed to improve solid mixing and aeration. To evaluate the geometric configuration, a series of simulations were performed using the Discrete Element Method (DEM), with particle dynamics analyzed through the Lacey Mixing Index ($LMI$). Four paddle angles (0°, 15°, 45°, and 55°) were compared, with the 45° configuration achieving optimal performance, reaching $LMI$ values above 0.95 in less than 15 s and maintaining high homogeneity at a filling volume of 70%. These results confirm that the paddle angle significantly influences mixing efficiency in granular media. While this work focuses on engineering design and DEM-based validation, future studies will include experimental trials to evaluate biodegradation kinetics. The proposed design offers a scalable and adaptable solution for ex situ bioremediation applications. This work reinforces the value of integrating DEM simulations early in the bioreactor development process and opens pathways for further optimization and implementation in real-world environmental remediation scenarios. Full article

Frictional conditions at the workpiece–die interface are critical in metal forming, as significant plastic deformation generates heat that affects lubricant performance. Understanding lubricant behavior, especially its influence on friction under elevated temperatures, is essential for optimizing forming processes and meeting ecological demands. While the conventional ring compression test evaluates friction through inner diameter changes, it becomes unreliable when friction is transient. In this study, a warm ring compression test incorporating an in situ measurement system is proposed to evaluate the transient frictional behavior of lubricants under temperature rise due to plastic deformation. Results show that at T = 50 °C and 150 °C, the friction coefficient increases notably with the compression ratio, whereas at T = 100 °C, it remains relatively stable. This stability is likely due to the optimal performance of the chlorinated base lubricant at 100 °C, where boundary lubrication is most effective. At T = 50 °C, the additive activation is insufficient, and at T = 150 °C, thermal degradation may reduce its effectiveness. Finite element simulations using the transient friction coefficient reproduce the deformed ring cross-section with high accuracy, while those using constant friction values show less agreement. Full article

The worldwide air pollution situation reveals significant environmental challenges. In addition to being a major contributor to the deterioration of air quality, particulate matter (PM) is also an important factor affecting the performance of solar energy systems given its ability to decrease light transmission to solar panels. As part of our research, the present investigation involves monitoring concentrations of PM using a high-performance optical instrument, the in situ calibration protocol of which is described in detail. For the city of Rabat, observations revealed significant variations in concentrations between day and night, with peaks observed around 8 p.m. correlating with high relative humidity and low wind speeds, and the highest levels recorded in February with a monthly average value reaching 75 µm/m³. In addition, an experimental protocol was set up for an analysis of the elemental composition of particles in the same city using SEM/EDS, providing a better understanding of their morphology. To assess the impact of meteorological variables on PM concentrations in two distinct climatic environments, a database from the city of Marrakech for the year 2024 was utilized. Overall, the distribution of PM values during this period did not fluctuate significantly, with a monthly average value not exceeding 45 µm/m³. The random forest method identified the most influential variables on these concentrations, highlighting the strong influence of the type of environment. The findings provide crucial information for the modeling of solar installations’ soiling and for improving understanding of local air quality. Full article

The compressive capacity of helical anchors constitutes a pivotal performance parameter in geotechnical design. To precisely predict the compressive bearing behavior of helical anchors in aeolian sand, this study integrates in situ testing with finite element numerical analysis to systematically elucidate the non-linear evolution of its load-bearing mechanisms. The XGBoost algorithm enabled the rigorous quantification of the governing geometric features of compressive capacity, culminating in a computational framework for the bearing capacity factor (N_q) and lateral earth pressure coefficient (K_u). The research findings demonstrate the following: (1) Compressive capacity exhibits significant enhancement with increasing helix diameter yet displays limited sensitivity to helix number. (2) Load–displacement curves progress through three distinct phases—initial quasi-linear, intermediate non-linear, and terminal quasi-linear stages—under escalating pressure. (3) At embedment depths of H < 5D, tensile capacity diminishes by approximately 80% relative to compressive capacity, manifesting as characteristic shallow anchor failure patterns. (4) When H ≥ 5D, stress redistribution transitions from bowl-shaped to elliptical contours, with ≤10% divergence between uplift/compressive capacities, establishing 5D as the critical threshold defining shallow versus deep anchor behavior. (5) The helix spacing ratio (S/D) governs the failure mode transition, where cylindrical shear (CS) dominates at S/D ≤ 4, while individual bearing (IB) prevails at S/D > 4. (6) XGBoost feature importance analysis confirms internal friction angle, helix diameter, and embedment depth as the three parameters exerting the most pronounced influence on capacity. (7) The proposed computational models for N_q and K_u demonstrate exceptional concordance with numerical simulations (mean deviation = 1.03, variance = 0.012). These outcomes provide both theoretical foundations and practical methodologies for helical anchor engineering in aeolian sand environments. Full article

Study design: The advent of the Matrix Wave^TM System (Depuy-Synthes)—a bone-anchored Mandibulo-Maxillary Fixation (MMF) System—merits closer consideration because of its peculiarities. Objective: This study alludes to two preliminary stages in the evolution of the Matrix Wave^TM MMF System and details its technical and functional features. Results: The Matrix Wave^TM System (MWS) is characterized by a smoothed square-shaped Titanium rod profile with a flexible undulating geometry distinct from the flat plate framework in Erich arch bars. Single MWS segments are Omega-shaped and carry a tie-up cleat for interarch linkage to the opposite jaw. The ends at the throughs of each MWS segment are equipped with threaded screw holes to receive locking screws for attachment to underlying mandibular or maxillary bone. An MWS can be partitioned into segments of various length from single Omega-shaped elements over incremental chains of interconnected units up to a horseshoe-shaped bracing of the dental arches. The sinus wave design of each segment allows for stretch, compression and torque movements. So, the entire MWS device can conform to distinctive spatial anatomic relationships. Displaced fragments can be reduced by in-situ-bending of the screw-fixated MWS/Omega segments to obtain accurate realignment of the jaw fragments for the best possible occlusion. Conclusion: The Matrix Wave^TM MMF System is an easy-to-apply modular MMF system that can be assembled according to individual demands. Its versatility allows to address most facial fracture scenarios in adults. The option of “omnidirectional” in-situ-bending provides a distinctive feature not found in alternate MMF solutions. Full article

Additive manufacturing reshapes concrete construction, yet routine strength verification of printed elements still depends on destructive core sampling. This study evaluates whether standard 70 mm cubes—corrected by a single factor—can provide an equally reliable measure of in situ compressive strength. Five Portland-cement mixes, with and without ash-slag techno-mineral filler, were extruded into wall blocks on a laboratory 3D printer. For each mix, the compressive strengths of the cubes and ∅ 28 mm drilled cores were measured at 7, 14 and 28 days. The core strengths were consistently lower than the cube strengths, but their ratios remained remarkably stable: the transition coefficient clustered between 0.82 and 0.85 (mean 0.83). Ordinary least-squares regression of the pooled data produced the linear relation ${\widehat{R}}_{core}$ [MPa] = 0.97 ${\widehat{R}}_{cube}$ − 4.9, limiting the prediction error to less than 2 MPa (under 3% across the 40–300 MPa range) and outperforming more complex machine-learning models. Mixtures containing up to 30% ash-slag filler maintained structural-grade strength while reducing clinker demand, underscoring their sustainability potential. The results deliver a simple, evidence-based protocol for non-destructive strength assessment of 3D-printed concrete and provide quantitative groundwork for future standardisation of quality-control practices in additive construction. Full article

Adobe churches are representative of Andean architectural heritage, yet their structural vulnerability to seismic events remains a significant concern. This study evaluates the seismic performance of the 17th-century Church of Santo Tomás de Aquino in Rondocan, Peru, an adobe building that underwent conservation work in the late 1990s. The assessment combines in situ inspections and experimental testing with advanced nonlinear numerical modeling. A finite-element macro-model was developed and calibrated using sonic and ambient vibration tests to replicate the observed structural behavior. Nonlinear static (pushover) analyses were performed in the four principal directions to identify failure mechanisms and to evaluate seismic capacity using the Peruvian seismic code. Kinematic limit analyses were conducted to assess out-of-plane mechanisms using force- and displacement-based criteria. The results revealed critical vulnerabilities in the rear façade and lateral walls, particularly in terms of out-of-plane collapse, while the main façade exhibited a higher capacity but a brittle failure mode. This study illustrates the value of advanced numerical simulations, calibrated with field data, as effective tools for assessing seismic vulnerability in historic adobe buildings. The outcomes highlight the necessity of strengthening measures to balance life safety requirements with preservation goals. Full article

This study aims to rapidly in situ identify starch sausage samples with the improper addition of chicken bone paste. Chicken bones play important roles in building materials, biomass fuels, and as food additives after enzymatic hydrolysis, but no current research indicates that chicken bones can be directly added to food for consumption. Especially in starch sausages, the addition of chicken bone paste is highly controversial due to potential risks of esophageal laceration and religious concerns. This paper first uses laser-induced breakdown spectroscopy (LIBS) to investigate the elemental differences between starch sausages and chicken bone paste. By preparing mixtures of starch sausages and chicken bone paste at different ratios, the relationships between the spectral peak intensities of elements, such as Ca, Ba, and Sr, and the proportion of chicken bone paste were determined. Through processing methods such as normalization with reference spectral lines, selection of the signal of the second laser pulse at the same position, and electron temperature correction, the determination coefficients (R²) of each element’s spectral lines have significantly improved. Specifically, the R² values for Ca I, Ca II, Ba II, and Sr II have increased from 0.302, 0.694, 0.857, and 0.691 to 0.972, 0.952, 0.970, and 0.982, respectively. Finally, principal component analysis (PCA) was used to distinguish starch sausages, chicken bone paste, and their mixtures at different ratios, with further effective differentiation achieved through t-distributed stochastic neighbor embedding (t-SNE). The results show that LIBS technology can serve as an effective and rapid method for detecting elemental composition in food and distinguishing different food products, providing safety guarantees for food production and supervision. Full article

Thermally sprayed carbide cermet coatings, particularly those based on tungsten carbide (WC) and chromium carbide (Cr₃C₂) and produced with the high velocity oxygen fuel (HVOF) process, are used in tribological applications as environmentally friendly alternatives to electroplated hard chrome coatings. These functional coatings are especially prevalent in the automotive industry, offering excellent wear resistance. However, their mechanical and tribological performances are highly dependent on factors such as feedstock powders, spray parameters, and service conditions. This review aims to gain deeper insights into the above elements. It also outlines emerging advancements in HVOF technology—including in situ powder mixing, laser treatment, artificial intelligence integration, and the use of novel materials such as rare earth elements or transition metals—which can further enhance coating performance and broaden their applications to sectors such as the aerospace and hydro-machinery industries. Finally, this literature review focuses on process optimization and sustainability, including environmental and health impacts, critical material use, and operational limitations. It uses a life cycle assessment (LCA) as a tool for evaluating ecological performance and addresses current challenges such as exposure risks, process control constraints, and the push toward safer, more sustainable alternatives to traditional WC and Cr₃C₂ cermet coatings. Full article

Authenticity is a core principle in conservation guidelines and a key goal of heritage preservation, especially in Serbia, where many aging objects face ongoing deterioration. The subject of this study is the church within the Blagoveštenje Monastery complex in the Ovčar-Kablar gorge, built using stone from a local quarry at the beginning of the 17th century. The inclination of the structure, observed as progressively increasing over the centuries, raises important concerns regarding its stability. This research focuses on identifying the underlying causes of this phenomenon in order to support its long-term preservation. The methods used the study are long-term in situ observations including analysis, geodetic research, 3D laser imaging, geophysical, geological, archaeological research, evaluation of current condition, determination of structural failures and their cause and monitoring the structural behavior of elements. All methods were carried out in accordance with the definition of rehabilitation measures and the protection of masonry buildings. The main contribution of this study is identifying that the church’s inclination and deviation result from the northern foundation resting on weaker soil and a deeper rock mass compared to the southern side. The research approach and findings presented in this paper can serve as a guide for future endeavors aimed at identifying the causes of deformations and the restoration and structural rehabilitation of masonry buildings as cultural heritage. Full article

The elemental exchange fluxes at the sediment–water interface play a crucial role in Earth’s climate regulation, environmental change, and ecosystem dynamics. Accurate in situ measurements of these fluxes depend heavily on the performance of marine incubation devices, particularly their ability to achieve full mixing without causing sediment resuspension. This study presents a novel parameter calibration method for a marine in situ incubation device using a combination of computational fluid dynamics (CFD) simulations and laboratory experiments. The influence of the stirring paddle’s rotational speed on flow field distribution, complete mixing time, and sediment resus-pension was systematically analyzed. The CFD simulation results were validated against existing device data and actual experimental measurements. The deviation in complete mixing time between simulation and experiment was within −9.23% to 9.25% for 20 cm of sediment and −9.4% to 9.1% for 15 cm. The resuspension tests determined that optimal mixing without sediment disturbance occurs at rotational speeds of 25 r/min and 35 r/min for the two sediment depths, respectively. Further analysis showed that the stirring paddle effectively creates a uniform flow field within the chamber. This CFD-based calibration method provides a reliable approach to parameter tuning for various in situ devices by adjusting boundary conditions, offering a scientific foundation for device design and deployment, and introducing a new framework for future calibration efforts. Full article

In this study, graded cemented carbide layers were fabricated using Laser Powder-Directed Energy Deposition (LP-DED) to investigate the effects of laser input energy and WC content on crack formation, compositional distribution, and hardness. Two-layer structures were formed, with the first layer containing either 30.5 wt.% or 42.9 wt.% WC and the second layer containing 63.7 wt.% WC. Crack formation was evaluated in situ using acoustic emission (AE) sensors, and elemental composition and Vickers hardness were measured across the cross-section of the deposited layers. The results showed that crack formation increased with higher laser power and higher WC content in the first layer. Elemental analysis revealed that higher laser input led to greater Co enrichment and reduced W content near the surface. Additionally, the formation of brittle structures was observed under high-energy conditions, contributing to increased hardness but decreased toughness. These findings indicate that both WC content and laser energy strongly influence the microstructural evolution and mechanical properties of graded cemented carbide layers. Optimizing the balance between WC content and laser parameters is essential for improving the crack resistance and performance of cemented carbide layers in additive manufacturing applications. Full article