Search Results (672)

Auxetic materials and structures exhibit high energy absorption, vibration damping, and fracture toughness at the macroscopic level. Lightweight designs and perforated structures in buckling-restrained braces (BRBs) have garnered significant attention. However, existing auxetic cellular configurations remain relatively simplistic, with particularly limited options capable of synergizing with BRBs to achieve combined energy dissipation and seismic mitigation performance. This study introduces a novel composite auxetic cellular unit with a honeycomb structure of negative Poisson’s ratio and corresponding design method. The cellular unit is combined with a BRB to develop a new composite auxetic perforated BRB (NPR-BRB). Experimental and numerical simulation methods are used to investigate the effects of two core plate materials (Q235B and LY160), the reentrant angle, and the cross-sectional weakening rate of the composite honeycombs on the NPR-BRB’s performance under cyclic loading. In this study, four BRB specimens were fabricated, and the experimental results reveal that the fracture surface morphology (cup- and shell-shaped) depends on the deformation mechanism. One of the NPR-BRBs demonstrates stable hysteretic behavior, with an equivalent viscous damping ratio of 0.469 and a cumulative plastic strain of 219.7. Numerical simulations indicate that the LY160 BRB exhibits higher deformation capacity and energy dissipation, reducing stress concentration. The concavity angle has a negligible influence on performance. An increase in the cross-sectional weakening rate is correlated with a reduction in bearing capacity, hysteresis loop area, and compression–tension asymmetry, and an increase followed by a decrease in equivalent viscous damping ratio and cumulative plastic strain. The novel hybrid auxetic cellular units may enhance the energy dissipation performance of BRBs. Full article

This study describes the processing of microneedle (MN) arrays with three different heights of arrowhead (600 µm (A1), 800 µm (A2), and 1000 µm (A3)), pyramid (600 µm (P1), 800 µm (P2), and 1000 µm (P3)), and turret (600 µm (T1), 800 µm (T2), and 1000 µm (T3)) designs using a digital light processing (DLP)-based 3D printing method. The 3D-printed MNs were examined for their morphological characteristics and mechanical performance. Scanning electron microscopy (SEM) imaging confirmed that all of the MNs were fabricated without fracture or bending. Each design exhibited distinct structural characteristics: arrowhead MNs displayed a well-defined morphology with sharp tips, pyramid MNs showed slight layering, and turret MNs, characterized by a wider base and sharp tips, had a smoother surface compared to the other designs. Mechanical tests revealed that the arrowhead MNs carried less load and were more prone to bending, while the pyramid and turret designs provided higher mechanical stability and penetration capacity. The pyramid design (P3) showed the highest mechanical strength, while turret MNs offered a more stable performance despite lower penetration capacity. These findings highlight the critical role of geometric design in optimizing MN performance for effective transdermal drug delivery. Full article

Grinding semiconductor wafers with high hardness, such as SiC, remains a significant challenge due to the need to maximize material removal rates while minimizing subsurface damage. In the back-grinding process, two key parameters—the elastic modulus (Eb) of the grinding wheel bond and the fracture toughness (K_IC) of the wafer—play a critical role in governing the behavior of diamond and the extent of wafer damage. This study systematically investigated the effect of Eb and K_IC on diamond protrusion height (h_p), surface roughness (Ra), grinding forces, and the morphology of generated debris. The study encompassed four wafer types—Si, GaP, sapphire, and ground SiC—using five Back-Grinding Wheels (BGWs), with Eb ranging from 95.24 to 131.38 GPa. A log–linear empirical relationship linking ℎₚ to Eb and K_IC was derived and experimentally verified, demonstrating high predictive accuracy across all wafer–wheel combinations. Surface roughness (Ra) was measured in the range of 0.486 − 1.118𝜇m, debris size ranged from 1.41 to 14.74𝜇m, and the material removal rate, expressed as a thickness rate, varied from 555 to 1546𝜇m/h (equivalent to 75−209 mm³/min using an effective processed area of 81.07 cm²). For SiC, increasing the bond modulus from 95.24 to 131.38 GPa raised the average h_p from 9.0 to 1.2 um; the removal rate peaked at 122.07 GPa, where subsurface damage (SSD) was minimized, defining a practical grindability window. These findings offer practical guidance for selecting grinding wheel bond compositions and configuring process parameters. In particular, applying a higher Eb is recommended for harder wafers to ensure sufficient diamond protrusion, while an appropriate dressing must be employed to prevent adverse effects from excessive stiffness. By balancing removal rate, surface quality, and subsurface damage constraints, the results support industrial process development. Furthermore, the protrusion model proposed in this study serves as a valuable framework for optimizing bond design and grinding conditions for both current and next-generation semiconductor wafers. Full article

The industrial production of high-speed steel via continuous casting has been impeded by considerable technical obstacles, due to its high carbon content and fast cooling speed, which predispose it to severe segregation and poor high-temperature plasticity; thus, industrial continuous casting of high-speed steel is virtually nonexistent. In 2022, a curved continuous casting process was successfully applied in the production of M2 high-speed steel; in our previous study, it was found that the carbides were finer and better distributed in the billets by curved continuous casting than those in the billets by ingot casting. The change in carbides in the billets is significant in subsequent processes for M2 high-speed steel produced by curved continuous casting. Therefore, it is necessary to investigate the high-temperature tensile properties of M2 high-speed steel produced by curved continuous casting. In this paper, high-temperature tensile tests were conducted using a GLEEBLE-3500 simulator (DSI, located in New York State, USA) at different temperatures and holding times with a certain strain rate to obtain the tensile strength and reduction of area, and then the morphology of carbides near the fracture surface was observed. The results showed that the tensile strength and reduction of area increased with the increase in temperature at 850 °C to 950 °C, and there existed a temperature range between 950 °C and 1120 °C with good thermoplasticity and a reduction of area from 45% to 50%. In addition, a sharp drop in thermoplasticity below 5% occurred at 1180 °C, which is due to the significant growth of carbides. The zero-strength temperature and plastic temperature were 1220 °C and 1200 °C, respectively. In addition, with the increase in holding time at 1150 °C, the reduction of area increased from 34% to 54%, and the tensile strength decreased from 92 MPa to 70 MPa and then increased to 82 MPa. The best solution for carbides in M2 high-speed steel produced by curved continuous casting occurred when the range of the P_HJ value was about 28.0 to 30.5. With the increase in P_HJ value, the shape of carbides gradually changed from fibrous to short rod-like and blocky during high-temperature diffusion. Full article

Fiber tow-gaps and overlaps formed during the Automated Fiber Placement (AFP) process pose a significant challenge by introducing non-uniform composite morphologies, often characterized by resin-rich regions and fiber waviness. These defects occur as deposited fibers sink into the gap regions during consolidation, with gap geometry determined during path planning. Such morphological inconsistencies can compromise structural reliability by initiating premature failure, particularly through localized out-of-plane waviness and resin accumulation. This study investigates the integration of high melting temperature thermoplastic veils, specifically polyetherimide (PEI), into fiber tow-gaps as a method to prevent ply sinking and reduce fiber waviness on both internal and external surfaces of the laminate. The PEI veils also serve to reinforce resin-rich regions by forming an interpenetrated network of high fracture toughness material within the brittle epoxy matrix. Tensile tests conducted on cross-ply laminates containing staggered gaps demonstrated that the inclusion of PEI veils modified the failure mode. The results suggest that the selective placement of thermoplastic veils within tow-gaps during AFP offers a viable strategy to mitigate manufacturing-induced non-uniform morphologies. Full article

Deicing salt effectively melts ice and snow to maintain traffic flow in seasonal freezing zones, but its erosion effect compromises the water stability and structural integrity of asphalt pavements. To comprehensively explore the impacts of salt erosion on the interfacial behaviors of rubber asphalt–aggregate systems, this study developed a multiscale characterization method integrating a macroscopic mechanical test, microscopic tests, and molecular dynamics (MD) simulations. Firstly, laboratory-controlled salt–freeze–thaw cycles were employed to simulate field conditions, followed by quantitative evaluation of interfacial bonding properties through pull-out tests. Subsequently, the atomic force microscopy (AFM) and Fourier transform infrared spectrometer (FTIR) tests were conducted to characterize the microscopic morphology evolution and chemical functional group transformations, respectively. Moreover, by combining the diffusion coefficients of water molecules, salt solution ions, and asphalt components, the mechanism of interfacial salt erosion was elucidated. The results demonstrate that increasing NaCl concentration and freeze–thaw cycles progressively reduces interfacial pull-out strength and fracture energy, with NaCl-induced damage becoming limited after twelve salt–freeze–thaw cycles. In detail, with exposure to 15 freeze–thaw cycles in 6% NaCl solution, the pull-out strength and fracture energy of the rubber asphalt–limestone aggregate decrease by 50.47% and 51.57%, respectively. At this stage, rubber asphalt exhibits 65.42% and 52.34% increases in carbonyl and sulfoxide indexes, respectively, contrasted by 49.24% and 42.5% decreases in aromatic and aliphatic indexes. Long-term exposure to salt–freeze–thaw conditions promotes phase homogenization, ultimately reducing surface roughness and causing rubber asphalt to resemble matrix asphalt morphologically. At the rubber asphalt–NaCl solution–aggregate interface, the diffusion of Na⁺ is faster than that of Cl⁻. Meanwhile, compared with other asphalt components, saturates exhibit notably enhanced mobility under salt erosion conditions. The synergistic effects of accelerated aging, salt crystallization pressure, and enhanced ionic diffusion jointly induce the deterioration of interfacial bonding, which accounts for the decrease in macroscopic pull-out strength. This multiscale investigation advances understanding of salt-induced deterioration while providing practical insights for developing durable asphalt mixtures in cold regions. Full article

NASICON-type Li_1+XFe_XTi_2-X(PO₄)₃ (x = 0.1, 0.3, 0.4) solid electrolytes for all-solid-state Li-ion batteries were synthesized using a sol–gel method. This study investigated the impact of substituting Fe³⁺ (0.645 Å), a trivalent cation, for Ti⁴⁺ (0.605 Å) on ionic conductivity. Li_1+XFe_XTi_2-X(PO₄)₃ samples, subjected to various sintering temperatures, were characterized using TG-DTA, XRD with Rietveld refinement, XPS, FE-SEM, and AC impedance to evaluate composition, crystal structure, fracture-surface morphology, densification, and ionic conductivity. XRD analysis confirmed the formation of single-crystalline NASICON-type Li_1+XFe_XTi_2-X(PO₄)₃ at all sintering temperatures. However, impurities in the secondary phase emerged owing to the high sintering temperature above 1000 °C and increased Fe content. Sintered density increased with the densification of Li_1+XFe_XTi_2-X(PO₄)₃, as evidenced by FE-SEM observations of sharper edges of larger quasi-cubic grains at elevated sintering temperatures. At 1000 °C, with Fe content exceeding 0.4, grain coarsening resulted in additional grain boundaries and internal cracks, thereby reducing the sintered density. Li_1.3Fe_0.3Ti_1.7(PO₄)₃ sintered at 900 °C exhibited the highest density among the other conditions and achieved the maximum total ionic conductivity of 1.51 × 10⁻⁴ S/cm at room temperature, with the lowest activation energy for Li-ion transport at 0.37 eV. In contrast, Li_1.4Fe_0.4Ti_1.6(PO₄)₃ sintered at 1000 °C demonstrated reduced ionic conductivity owing to increased complex impedance associated with secondary phases and grain crack formation. Full article

The aim of the present study is to investigate the mechanism behind corrosion destruction in laser-melted layers (LMLs) of AISI 321 austenitic stainless steel after electrochemical corrosion in Ringer’s solution. Surface morphology, microstructure, chemical composition, grain sizes, and orientation are studied using OM, SEM, EDS, and EBSD. It was confirmed that (1) the main mechanism behind corrosion destruction is identical between untreated and laser-melted steel, i.e., the selective destruction of the lower corrosion resistance phase (δ-ferrite) in the form of pits, and (2) the morphology and size of corrosion pits are different, as determined via δ-ferrite morphology, with narrow deep pits of uneven shape observed on the surface of wrought steel and rounded shallower pits seen in LML. The following mechanism is proposed with regard to corrosion destruction in LML: (1) the initial destruction of δ-ferrite; (2) the formation of an austenitic dendrite network; (3) the mechanical fracture of austenitic dendrites and pit formation; and (4) the growth of pits inside the grain. The following relationship between corrosion pit development and dendrite orientation in the LML is observed: (1) In the melted zone, with dendrite axes perpendicular to or inclined toward the surface, the corrosion pit grows within the grain. (2) At the melted zone/base metal (MZ/BM) boundary, with dendrite axes parallel to the surface, the corrosion pit develops in the heat-affected zone, along the MZ/BM boundary. Full article

The crushing of used drip irrigation tape is a crucial step in the recycling and reuse of drip irrigation tapes. Incomplete crushing and low efficiency are among the main factors restricting its reprocessing. Investigating the fracture characteristics and the mechanism of fracture during the crushing process is key to solving this problem. Therefore, this study constructs a stretching fracture platform to investigate the influence of stretching speed on the fracture characteristics and reveals the fracture mechanism by analyzing fracture morphology, force-displacement curves, fracture energy, and microstructure. The results show that as the speed increases, the limit strain decreased from 117.7% to 38.7%, and the fracture location always occurs at the junction between the necked and non-necked area, the fracture mode transitions from ductile fracture to brittle fracture, the deformation mode shifts from being dominated by elastoplastic deformation to being dominated by elastic deformation, and the mechanical response curve changes from five stages to three stages. When the stretching speed increases from 60 mm/s to 70 mm/s, a jump phenomenon is observed in macroscopic and microscopic. As the speed increases, the total energy absorbed by the drip irrigation tape decreases from 1.29 × 10⁻² J/mm³ to 0.39 × 10⁻² J/mm³. Brittle fracture primarily absorbs energy for the disintegration and fracture of lamellae in the spherulites at the fracture surface. Ductile fracture primarily absorbs energy for the extension of the fibrous structure, and the mechanical properties of the necked area are strengthened, which leads to the fracture location always occurring at the junction between the necked and non-necked area. Full article

A systematic study was conducted on the fatigue performance of Q500qENH weathering steel welded joints under low-temperature conditions of −40 °C in this paper. Low-temperature fatigue tests were conducted on V-groove butt joints and cross-shaped welded joints and S-N curves with a 95% reliability level were obtained. A comparative analysis with the Eurocode 3 reveals that low-temperature conditions lead to a regular increase in the design fatigue strength for both types of welded joints. Fracture surface morphology was examined using scanning electron microscopy, and combined with fracture characteristic analysis, the fatigue fracture mechanisms of welded joints under low-temperature conditions were elucidated. Based on linear elastic fracture mechanics theory, a numerical simulation approach was employed to investigate the fatigue crack propagation behavior of welded joints. The results indicate that introducing an elliptical surface initial crack with a semi-major axis length of 0.4 mm in the model effectively predicts the fatigue life and crack growth patterns of both joint types. A parametric analysis was conducted on key influencing factors, including the initial crack size, initial crack location, and initial crack angle. The results reveal that these factors exert varying degrees of influence on the fatigue life and crack propagation paths of welded joints. Among them, the position of the initial crack along the length direction of the fillet weld has the most significant impact on the fatigue life of cross-shaped welded joints. Full article

The fracture behavior of a locking pin used in the penultimate-stage blades of a 600 MW steam turbine in a thermal power plant was investigated through microstructural and microhardness characterization, fracture surface and energy-dispersive spectroscopy (EDS) analysis, as well as finite element load simulation. The microhardness values measured on the cross-section of the service pins ranged from 528 to 541 HV0.1, showing little difference from the unused pins. Scanning electron microscopy analysis revealed that approximately 70% of the fracture surfaces exhibited an intergranular “rock candy” morphology. The results indicate that pin failure was primarily caused by the combined effects of fretting wear and stress corrosion cracking (SCC). Specifically, vibration at the blade root, impeller, and pins due to start–stop cycles and load variations led to fretting wear, forming pits approximately 75 μm in size. Under the combined effects of weakly corrosive wet steam environments and shear stresses, SCC initiated at the high stress concentration points of these pits. Early crack propagation primarily followed original austenite grain boundaries, while later stages mainly extended along martensite plate boundaries. As cracks advanced, the cross-sectional area gradually decreased, causing the effective shear stress to increase until it exceeded the shear strength, ultimately leading to fracture. These findings not only provide a scientific basis for enhancing the reliability of steam turbine locking pins and extending their service life, but also contribute to a broader understanding of the failure mechanisms of key components operating under corrosive and fluctuating load environments. Full article

Recent studies have demonstrated that the utilisation of aluminium in electrical applications has increased substantially, particularly in the context of power cables. The substitution of copper with aluminium in cable fabrication is predominantly driven by economic considerations. When designing such cables, it is imperative to ascertain their functional properties, including their electrical conductivity and mechanical properties, and their operational properties, which include rheological, thermal, and material fatigue resistance. This is to ensure that the aluminium and copper cables are compatible. The primary challenge confronting researchers in this domain pertains to predicting and forecasting the failure of overhead cables during their operational lifecycle. One of the most significant and prevalent operational hazards is fatigue damage. This article presents the experimental results of fatigue tests on single Al and Cu wires in various states of mechanical reinforcement. The parameters of the Wöhler curve were determined, and a comparative analysis of the morphology of fatigue damage in single copper and aluminium wires was performed. It was found that copper wires are more fatigue-resistant than aluminium wires. In the case of high-cycle fatigue, this difference can amount to 10⁶ cycles. An analysis of fatigue fracture morphology showed that fractures have a developed surface and that plastic deformation makes a significant contribution in the case of low-cycle fatigue. In the case of high-cycle fatigue, many cracks were observed in the copper wires. No such cracks were observed in the aluminium wires. Full article

To evaluate the impact of different surface treatment regimens, Neodymium-doped yttrium orthovanadate (Nd: YVO4) laser, Toluidine blue (TB) activated Low-level laser therapy (LLLT), and Bioactive glass particles (BAGPs) on the surface roughness (Ra), surface morphology, and bond strength (BS) of Glass fiber posts (GFP) bonded to canal dentin. Forty single human rooted incisors with a closed apex were included. The endodontic treatment was performed, followed by post space preparation. Fifty-six GFP were sorted into four categories based on the conditioning method used (n = 14). Group 1: H₂O₂, Group 2: Nd: YVO4 laser, Group 3: TB-LLLT, and Group 4: BAGPs. Surface Ra and topographic changes were identified using a profilometer and Scanning Electron Microscopy (SEM). Post cementation was executed by utilizing self-adhesive resin cement. Analysis of BS and fracture pattern was performed using a universal testing machine and a stereomicroscope, respectively. Variance analysis with Tukey’s test was used to compare Ra and BS between the study groups at different root sections (p < 0.05). Group 2 (Nd: YVO4 laser) displayed the highest Ra scores (1051.54 ± 0.087 µm) and BS at all thirds. Whereas Group 3 TB-activated LLLT exhibited the lowest outcomes of Ra (539.39 ± 0.091) and BS at all three sections. Comparison among the investigated groups displayed that Group 1 (H₂O₂) and Group 2 Nd: YVO₄ exhibited comparable outcomes of Ra and BS (p ˃ 0.05). Nd: YVO₄ laser has the potential to roughen the surface of GFP, thereby enhancing its BS to resin cement Full article

Glass-ceramic optical components are extensively employed in advanced optical systems. The high-hardness and low-fracture toughness of glass-ceramics make it prone to cracks and subsurface damage during conventional cutting. The laser-assisted diamond cutting method can significantly improve the nano-cutting performance of glass-ceramics by locally heating and softening the material. However, its dynamic removal mechanisms remain unclear. The coupling mechanisms between the laser thermal field and the mechanical response of the material require further investigation. This study aims to reveal the dynamic removal mechanisms of glass-ceramics under laser-assisted nanoscale cutting conditions through numerical simulations and systematic experiments. It includes a systematic analysis of the effects of laser heating on chip morphology, temperature fields, stress fields, and cutting forces using a laser-assisted nano-cutting model. Additionally, through nanoscale taper cutting experiments, this study quantifies the enhancement effect of laser power on the critical depth of no observed surface cracks (NOSC). Finally, subsurface integrity results elucidate the mechanisms through which laser assistance inhibits crack propagation. The findings will provide theoretical support for optimizing laser-assisted cutting parameters and achieving high-quality machining of glass-ceramics. Full article

Al₂O₃-3% TiO₂-xAl (x = 0, 20, 40, 60 wt.%) composite coatings were prepared on Q235 substrate by plasma spraying technology, and the effects of pure Al phase addition on the microstructure and wear properties of the coatings were compared and analyzed. The results show that a unique splash-like structure was formed on the surface of the coating, and this structure became more obvious with the increase in Al content. Cross-sectional analysis shows that the introduction of pure Al phase reduces the large pores and cracks in the coating, forming a slender band structure. XRD analysis shows that the addition of pure Al phase leads to a decrease in the diffraction peak intensity of α-Al₂O₃, while the diffraction peak intensity of Al phase and γ-Al₂O₃ gradually increases, especially in the coating with 40% Al content; the diffraction peak of γ-Al₂O₃ increases significantly. XPS analysis further confirms that with the increase in Al content, a new pure Al peak appears in the Al element spectrum, and the peaks of α-Al₂O₃ and γ-Al₂O₃ fluctuate. In addition, the porosity of the coating decreases first and then increases and then decreases again with the increase in Al content. The porosity of the coating with 60% Al content is the lowest, at only 5.14%. Microhardness test results show that with the increase in Al content, the microhardness of the coating gradually decreases, and the fracture morphology changes from brittle fracture to irregular fracture, with the appearance of pull-out areas, indicating that the pure Al phase effectively improves the brittleness of the coating. However, the friction and wear test results show that the friction coefficient of the coating increases with the increase in Al content. The pure Al₂O₃ coating has high hardness and excellent wear resistance, while the coating with 60% Al content has the highest friction coefficient and the most severe wear. Moreover, adhesive wear phenomena appear on the coating surface with high Al content. Full article