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Keywords = cyclical fatigue test

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18 pages, 11273 KiB  
Article
The Effect of Different Tightening Torques of Implant Cone Morse Abutment Connection Under Dynamic Fatigue Loading: An In Vitro Study
by Felice Lorusso, Antonio Scarano, Sergio Rexhep Tari, Ishita Singhal, Funda Goker, Maria Costanza Soldini, Gianluca Martino Tartaglia and Massimo Del Fabbro
Biomimetics 2025, 10(8), 511; https://doi.org/10.3390/biomimetics10080511 - 4 Aug 2025
Viewed by 115
Abstract
Background: The implant–abutment joint is important for the long-term marginal tissue integrity in terms of biomimetic design that replicates the natural dentition under mastication forces. This study aimed to evaluate conical implant–abutment joints coupled at different tightening torque values through a mechanical fatigue [...] Read more.
Background: The implant–abutment joint is important for the long-term marginal tissue integrity in terms of biomimetic design that replicates the natural dentition under mastication forces. This study aimed to evaluate conical implant–abutment joints coupled at different tightening torque values through a mechanical fatigue test. Methods: Eighty conic implants (Ø: 3.8 mm L: 10 mm) with a 6° cone morse joint were embedded in resin blocks with an inclination of 30° ± 2°. The samples were divided into 8 groups (4 Test and 4 Control). The implant–abutment joints were coupled with different tightening torques: 25 Ncm (Group I), 30 Ncm (Group II), 35 Ncm (Group III) and 40 Ncm (Group IV). An in vitro cyclic loading test (1 × 104 loads) was performed for 4 Test groups, while 4 Control groups did not receive any forces. All the samples were assessed with Scanning Electron Microscopy to compare the microfractures and microgaps on flexion and extension points. Results: Microscopy observation results showed significant differences among torque groups. We found that 30 Ncm had the best stability with less microgap. Conclusions: Tightening torque plays an important role in the distortion of the cone morse joint under mechanical forces. However, further studies should be conducted to validate the results using different implant–abutment joints for comparison. Full article
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24 pages, 11098 KiB  
Article
Fracture Mechanisms of Electrothermally Fatigued 631 Stainless Steel Fine Wires for Probe Spring Applications
by Chien-Te Huang, Fei-Yi Hung and Kai-Chieh Chang
Appl. Sci. 2025, 15(15), 8572; https://doi.org/10.3390/app15158572 (registering DOI) - 1 Aug 2025
Viewed by 188
Abstract
This study systematically investigates 50 μm-diameter 631 stainless steel fine wires subjected to both sequential and simultaneous electrothermomechanical loading to simulate probe spring conditions in microelectronic test environments. Under cyclic current loading (~104 A/cm2), the 50 μm 631SS wire maintained [...] Read more.
This study systematically investigates 50 μm-diameter 631 stainless steel fine wires subjected to both sequential and simultaneous electrothermomechanical loading to simulate probe spring conditions in microelectronic test environments. Under cyclic current loading (~104 A/cm2), the 50 μm 631SS wire maintained electrical integrity up to 0.30 A for 15,000 cycles. Above 0.35 A, rapid oxide growth and abnormal grain coarsening resulted in surface embrittlement and mechanical degradation. Current-assisted tensile testing revealed a transition from recovery-dominated behavior at ≤0.20 A to significant thermal softening and ductility loss at ≥0.25 A, corresponding to a threshold temperature of approximately 200 °C. These results establish the endurance limit of 631 stainless steel wire under coupled thermal–mechanical–electrical stress and clarify the roles of Joule heating, oxidation, and microstructural evolution in electrical fatigue resistance. A degradation map is proposed to inform design margins and operational constraints for fatigue-tolerant, electrically stable interconnects in high-reliability probe spring applications. Full article
(This article belongs to the Special Issue Application of Fracture Mechanics in Structures)
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21 pages, 3663 KiB  
Article
A Study on the Road Performance of the Self-Healing Microcapsule for Asphalt Pavement
by Pei Li, Rongyi Ji, Chenlong Zhang, Jinghan Xu, Mulian Zheng and Xinghan Song
Materials 2025, 18(15), 3483; https://doi.org/10.3390/ma18153483 - 25 Jul 2025
Viewed by 343
Abstract
Asphalt pavement cracking is an important factor affecting its service life. Under certain conditions, the self-healing behavior of asphalt itself can repair pavement cracks. However, the self-healing ability of asphalt itself is limited. In order to strengthen the self-healing ability of asphalt, the [...] Read more.
Asphalt pavement cracking is an important factor affecting its service life. Under certain conditions, the self-healing behavior of asphalt itself can repair pavement cracks. However, the self-healing ability of asphalt itself is limited. In order to strengthen the self-healing ability of asphalt, the microcapsule wrapped with a repair agent is pre-mixed into the asphalt mixture. When the crack occurs and spreads to the surface of the microcapsule, the microcapsule ruptures and the healing agent flows out to realize the self-healing of the crack. Current microcapsules are mostly prepared with healing agents and bio-oil as core materials, and their high-temperature resistance to rutting is poor. While the epoxy resin contains a three-membered cyclic ether, it can undergo ring-opening polymerization to bond and repair the asphalt matrix. In addition, research on microcapsules mainly focuses on the self-healing properties of microcapsule-modified asphalt. In fact, before adding microcapsules to asphalt to improve its self-healing performance, it is necessary to ensure that the asphalt has a good road performance. On this basis, the self-healing performance of asphalt is improved, thereby extending the service life of asphalt pavement. Therefore, two-component epoxy self-healing microcapsules (E-mic and G-mic) were first prepared in this paper. Then, a temperature scanning test, rheological test of bending beams, and linear amplitude scanning test were, respectively, conducted for the microcapsule/asphalt to evaluate its road performance, including the high-temperature performance, low-temperature crack resistance, and fatigue performance. Finally, the self-healing performance of microcapsules/asphalt was tested. The results showed that the self-developed epoxy self-healing microcapsules were well encapsulated and presented as spherical micron-sized particles. The average particle size of the E-mic was approximately 23.582 μm, while the average particle size of the G-mic was approximately 22.440 μm, exhibiting a good normal distribution. In addition, they can remain intact and unbroken under high-temperature conditions. The results of road performance tests indicated that the microcapsule/asphalt mixture exhibits an excellent high-temperature resistance to permanent deformation, low-temperature crack resistance, and fatigue resistance. The self-healing test demonstrated that the microcapsule/asphalt exhibited an excellent self-healing performance. When the microcapsule content was 4%, the self-healing rate reached its optimal level of 67.8%, which was 149.2% higher than that of the base asphalt. Full article
(This article belongs to the Special Issue Innovative Approaches in Asphalt Binder Modification and Performance)
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14 pages, 4639 KiB  
Article
CNTs/CNPs/PVA–Borax Conductive Self-Healing Hydrogel for Wearable Sensors
by Chengcheng Peng, Ziyan Shu, Xinjiang Zhang and Cailiu Yin
Gels 2025, 11(8), 572; https://doi.org/10.3390/gels11080572 - 23 Jul 2025
Viewed by 316
Abstract
The development of multifunctional conductive hydrogels with rapid self-healing capabilities and powerful sensing functions is crucial for advancing wearable electronics. This study designed and prepared a polyvinyl alcohol (PVA)–borax hydrogel incorporating carbon nanotubes (CNTs) and biomass carbon nanospheres (CNPs) as dual-carbon fillers. This [...] Read more.
The development of multifunctional conductive hydrogels with rapid self-healing capabilities and powerful sensing functions is crucial for advancing wearable electronics. This study designed and prepared a polyvinyl alcohol (PVA)–borax hydrogel incorporating carbon nanotubes (CNTs) and biomass carbon nanospheres (CNPs) as dual-carbon fillers. This hydrogel exhibits excellent conductivity, mechanical flexibility, and self-recovery properties. Serving as a highly sensitive piezoresistive sensor, it efficiently converts mechanical stimuli into reliable electrical signals. Sensing tests demonstrate that the CNT/CNP/PVA–borax hydrogel sensor possesses an extremely fast response time (88 ms) and rapid recovery time (88 ms), enabling the detection of subtle and rapid human motions. Furthermore, the hydrogel sensor also exhibits outstanding cyclic stability, maintaining stable signal output throughout continuous loading–unloading cycles exceeding 3200 repetitions. The hydrogel sensor’s characteristics, including rapid self-healing, fast-sensing response/recovery, and high fatigue resistance, make the CNT/CNP/PVA–borax conductive hydrogel an ideal choice for multifunctional wearable sensors. It successfully monitored various human motions. This study provides a promising strategy for high-performance self-healing sensing devices, suitable for next-generation wearable health monitoring and human–machine interaction systems. Full article
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12 pages, 395 KiB  
Article
Effects of Translucency-Enhancing Coloring Liquids on the Mechanical Properties of 3Y- and 4Y-TZP Zirconia Ceramics
by Andreas Pfeffer, Sebastian Hahnel, Angelika Rauch and Martin Rosentritt
Ceramics 2025, 8(3), 92; https://doi.org/10.3390/ceramics8030092 - 22 Jul 2025
Viewed by 276
Abstract
The aim of translucency-enhancing liquids (TEL) is to locally influence the phase composition of zirconia in order to increase its translucency. This study aimed to determine the influence of TEL on 3Y- and 4Y-TZP zirconia concerning roughness, hardness, wear, flexural strength, dynamic stability [...] Read more.
The aim of translucency-enhancing liquids (TEL) is to locally influence the phase composition of zirconia in order to increase its translucency. This study aimed to determine the influence of TEL on 3Y- and 4Y-TZP zirconia concerning roughness, hardness, wear, flexural strength, dynamic stability and fracture force of fixed dental prostheses after thermal cycling and mechanical loading. Two zirconia materials (4Y-TZP; 3Y-TZP-LA, n = 8 per material and test) were investigated with and without prior application of TEL. Two-body wear tests were performed in a pneumatic pin-on-block design (50 N, 120,000 cycles, 1.6 Hz) with steatite balls (r = 1.5 mm) as antagonists. Mean and maximum vertical loss as well as roughness (Ra, Rz) were measured with a 3D laser-scanning microscope (KJ 3D, Keyence, J). Antagonist wear was determined as percent area of the projected antagonist area. Martens hardness (HM; ISO 14577-1) and biaxial flexural strength (BFS; ISO 6872) were investigated. The flexural fatigue limit BFSdyn was determined under cyclic loading in a staircase approach with a piston-on-three-ball-test. Thermal cycling and mechanical loading (TCML: 2 × 3000 × 5 °C/55 °C, 2 min/cycle, H2O dist., 1.2 × 106 force á 50 N) was performed on four-unit fixed dental prostheses (FDPs) (n = 8 per group) and the fracture force after TCML was determined. Statistics: ANOVA, Bonferroni test, Kaplan–Meier survival, Pearson correlation; α = 0.05. TEL application significantly influences roughness, hardness, biaxial flexural strength, dynamic performance, as well as fracture force after TCML in 3Y-TZP. For 4Y-TZP, a distinct influence of TEL was only identified for BFS. The application of TEL on 3Y- or 4Y-TZP did not affect wear. TEL application has a strong effect on the mechanical properties of 3Y-TZP and minor effects on 4Y-TZP. All effects of the TEL application are of a magnitude that is unlikely to restrict clinical application. Full article
(This article belongs to the Special Issue Advances in Ceramics, 3rd Edition)
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17 pages, 2470 KiB  
Article
Correlation Between Packing Voids and Fatigue Performance in Sludge Gasification Slag-Cement-Stabilized Macadam
by Yunfei Tan, Xiaoqi Wang, Hao Zheng, Yingxu Liu, Juntao Ma and Shunbo Zhao
Sustainability 2025, 17(14), 6587; https://doi.org/10.3390/su17146587 - 18 Jul 2025
Viewed by 356
Abstract
The fatigue resistance of cement-stabilized macadam (CSM) plays a vital role in ensuring the long-term durability of pavement structures. However, limited cementitious material (CM) content often leads to high packing voids, which significantly compromise fatigue performance. Existing studies have rarely explored the coupled [...] Read more.
The fatigue resistance of cement-stabilized macadam (CSM) plays a vital role in ensuring the long-term durability of pavement structures. However, limited cementitious material (CM) content often leads to high packing voids, which significantly compromise fatigue performance. Existing studies have rarely explored the coupled mechanism between pore structure and fatigue behavior, especially in the context of solid-waste-based CMs. In this study, a cost-effective alkali-activated sludge gasification slag (ASS) was proposed as a sustainable CM substitute for ordinary Portland cement (OPC) in CSM. A dual evaluation approach combining cross-sectional image analysis and fatigue loading tests was employed to reveal the effect pathway of void structure optimization on fatigue resistance. The results showed that ASS exhibited excellent cementitious reactivity, forming highly polymerized C-A-S-H/C-S-H gels that contributed to a denser microstructure and superior mechanical performance. At a 6% binder dosage, the void ratio of ASS–CSM was reduced to 30%, 3% lower than that of OPC–CSM. The 28-day unconfined compressive strength and compressive resilient modulus reached 5.7 MPa and 1183 MPa, representing improvements of 35.7% and 4.1% compared to those of OPC. Under cyclic loading, the ASS system achieved higher energy absorption and more uniform stress distribution, effectively suppressing fatigue crack initiation and propagation. Moreover, the production cost and carbon emissions of ASS were 249.52 CNY/t and 174.51 kg CO2e/t—reductions of 10.9% and 76.2% relative to those of OPC, respectively. These findings demonstrate that ASS not only improves fatigue performance through pore structure refinement but also offers significant economic and environmental advantages, providing a theoretical foundation for the large-scale application of solid-waste-based binders in pavement engineering. Full article
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18 pages, 5060 KiB  
Article
Research on Fatigue Strength Evaluation Method of Welded Joints in Steel Box Girders with Open Longitudinal Ribs
by Bo Shen, Ming Liu, Yan Wang and Hanqing Zhuge
Crystals 2025, 15(7), 646; https://doi.org/10.3390/cryst15070646 - 15 Jul 2025
Viewed by 254
Abstract
Based on the engineering background of a new type of segmental-assembled steel temporary beam buttress, the fatigue strength evaluation method of the steel box girders with open longitudinal ribs was taken as the research objective. The fatigue stress calculation analysis and the full-scale [...] Read more.
Based on the engineering background of a new type of segmental-assembled steel temporary beam buttress, the fatigue strength evaluation method of the steel box girders with open longitudinal ribs was taken as the research objective. The fatigue stress calculation analysis and the full-scale fatigue loading test for the steel box girder local component were carried out. The accuracy of the finite-element model was verified by comparing it with the test results, and the rationality of the fatigue strength evaluation methods for welded joints was deeply explored. The results indicate that the maximum nominal stress occurs at the weld toe between the transverse diaphragm and the top plate at the edge of the loading area, which is the fatigue-vulnerable location for the steel box girder local components. The initial static-load stresses at each measuring point were in good agreement with the finite-element calculation results. However, the static-load stress at the measuring point in the fatigue-vulnerable position shows a certain decrease with the increase in the number of cyclic loads, while the stress at other measuring points remains basically unchanged. According to the finite-element model, the fatigue strengths obtained by the nominal stress method and the hot-spot stress method are 72.1 MPa and 93.8 MPa, respectively. It is reasonable to use the nominal stress S-N curve with a fatigue life of 2 million cycles at 70 MPa and the hot-spot stress S-N curve with a fatigue life of 2 million cycles at 90 MPa (FAT90) to evaluate the fatigue of the welded joints in steel box girders with open longitudinal ribs. According to the equivalent structural stress method, the fatigue strength corresponding to 2 million cycles is 94.1 MPa, which is slightly lower than the result corresponding to the main S-N curve but within the range of the standard deviation curve. The research results of this article can provide important guidance for the anti-fatigue design of welded joints in steel box girders with open longitudinal ribs. Full article
(This article belongs to the Section Crystalline Metals and Alloys)
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49 pages, 11671 KiB  
Review
Fatigue Failure Criteria of Asphalt Binders and Asphalt Mixtures: A Comprehensive Review
by Shizhan Xu, Zhigang Zhao, Honglei Wang, Chenguang Wan, Xiaofeng Wang, Zhenjun Wang and Xuanrui Zhang
Materials 2025, 18(14), 3267; https://doi.org/10.3390/ma18143267 - 10 Jul 2025
Viewed by 357
Abstract
This study presents a systematic review of fatigue analysis methodologies and failure criteria for asphalt binders and mixtures employed in various cyclic fatigue testing configurations. The investigation focuses on two principal predictive approaches: phenomenological models and mechanistic frameworks, which are commonly utilized to [...] Read more.
This study presents a systematic review of fatigue analysis methodologies and failure criteria for asphalt binders and mixtures employed in various cyclic fatigue testing configurations. The investigation focuses on two principal predictive approaches: phenomenological models and mechanistic frameworks, which are commonly utilized to forecast asphalt pavement fatigue life based on experimental data from different fatigue tests. A critical evaluation is conducted on the diverse failure criteria integrated within these analytical approaches, with particular emphasis on their respective merits and limitations. The current research findings reveal a notable absence of consensus regarding the precise definition of the fatigue failure criteria for asphalt materials. Furthermore, critical parameters including accuracy assessment, reliability verification, and sensitivity analysis of these failure criteria are identified as requiring enhanced research attention. This review recommends specific fatigue failure criteria classified according to fatigue testing methods and material types. This comprehensive analysis of fatigue failure mechanisms in asphalt composites aims to inform strategic refinements for future research trajectories and enhance durability-oriented pavement design practices. Full article
(This article belongs to the Section Construction and Building Materials)
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10 pages, 3895 KiB  
Article
Experimental Investigation on Heat Generation of Tread Rubber Materials Under Tensile-Compression Cyclic Conditions
by Pengtao Cao, Jian Wu, Tenglong She, Juqiao Su, Naichi Weng, Benlong Su and Youshan Wang
J. Compos. Sci. 2025, 9(7), 346; https://doi.org/10.3390/jcs9070346 - 3 Jul 2025
Viewed by 294
Abstract
Aiming at the heat generation behavior of rubber products such as tires under complex loads, the thermal behavior of tread rubber materials under tensile and compressive loads is investigated by using a torsional fatigue testing machine to comparatively analyze the temperature difference between [...] Read more.
Aiming at the heat generation behavior of rubber products such as tires under complex loads, the thermal behavior of tread rubber materials under tensile and compressive loads is investigated by using a torsional fatigue testing machine to comparatively analyze the temperature difference between the inside and outside of the rubber cylinders and the heating history under different torsion angles and rotational speeds. Results demonstrate that during the initial rotation phase under cyclic loading, the external surface temperature of the rubber material exceeds internal measurements. However, with the continuation of cyclic loading, the internal temperature progressively escalates beyond surface temperatures. Furthermore, the temperature rise exhibited significant correlations with both imposed torsional angles and operational rotational speeds. This study provides valuable insights into heat generation patterns of rubber materials under complex working conditions. Full article
(This article belongs to the Section Composites Manufacturing and Processing)
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15 pages, 3467 KiB  
Article
Carbon Nanotube Elastic Fabric Motion Tape Sensors for Low Back Movement Characterization
by Elijah Wyckoff, Sara P. Gombatto, Yasmin Velazquez, Job Godino, Kevin Patrick, Emilia Farcas and Kenneth J. Loh
Sensors 2025, 25(12), 3768; https://doi.org/10.3390/s25123768 - 17 Jun 2025
Viewed by 509
Abstract
Monitoring posture and movement accurately and efficiently is essential for both physical therapy and athletic training evaluation and interventions. Motion Tape (MT), a self-adhesive wearable skin-strain sensor made of piezoresistive graphene nanosheets (GNS), has demonstrated promise in capturing low back posture and movements. [...] Read more.
Monitoring posture and movement accurately and efficiently is essential for both physical therapy and athletic training evaluation and interventions. Motion Tape (MT), a self-adhesive wearable skin-strain sensor made of piezoresistive graphene nanosheets (GNS), has demonstrated promise in capturing low back posture and movements. However, to address some of its limitations, this work explores alternative materials by replacing GNS with multi-walled carbon nanotubes (MWCNT). This study aimed to characterize the electromechanical properties of MWCNT-based MT. Cyclic load tests for different peak tensile strains ranging from 1% to 10% were performed on MWCNT-MT made with an aqueous ink of 2% MWCNT. Additional tests to examine load rate sensitivity and fatigue were also conducted. After characterizing the properties of MWCNT-MT, a human subject study with 10 participants was designed to test its ability to capture different postures and movements. Sets of six sensors were made from each material (GNS and MWCNT) and applied in pairs at three levels along each side of the lumbar spine. To record movement of the lower back, all participants performed forward flexion, left and right bending, and left and right rotation movements. The results showed that MWCNT-MT exceeded GNS-MT with respect to consistency of signal stability even when strain limits were surpassed. In addition, both types of MT could assess lower back movements. Full article
(This article belongs to the Special Issue Sensing Technologies for Human Evaluation, Testing and Assessment)
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24 pages, 7600 KiB  
Article
Microstructure, Porosity, and Bending Fatigue Behaviour of PBF-LB/M SS316L for Biomedical Applications
by Conall Kirk, Weijie Xie, Shubhangi Das, Ben Ferguson, Chenliang Wu, Hau-Chung Man and Chi-Wai Chan
Metals 2025, 15(6), 650; https://doi.org/10.3390/met15060650 - 11 Jun 2025
Viewed by 1071
Abstract
Bending fatigue significantly affects the mechanical stability and lifespan of biomedical implants, such as bone plates and orthopaedic fixation devices, which undergo cyclic loading in the human body. This study examines the microstructure, porosity, and bending fatigue properties of PBF-LB/M SS316L. Samples were [...] Read more.
Bending fatigue significantly affects the mechanical stability and lifespan of biomedical implants, such as bone plates and orthopaedic fixation devices, which undergo cyclic loading in the human body. This study examines the microstructure, porosity, and bending fatigue properties of PBF-LB/M SS316L. Samples were analysed across three faces (top, front, and side) using optical microscopy (OM) and scanning electron microscopy (SEM) to observe microstructural features and porosity. Elemental composition was measured by energy-dispersive X-ray spectroscopy (EDX). Phase structures and grain orientations were characterised via X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). Four-point bending fatigue tests, conducted under two loading conditions, below and slightly above the yield point, demonstrated that defects inherent to the PBF-LB/M process, particularly micropores and unmelted powder particles, strongly influence fatigue crack initiation. Real-time monitoring of crack initiation and propagation on the external sample surface was performed using a high-speed digital microscope. These findings indicate the influence of microstructural defects on fatigue performance in PBF-LB/M SS316L, supporting the design and development of more reliable patient-specific biomedical implants. Full article
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26 pages, 4838 KiB  
Article
A Discrete-Element-Based Approach to Generate Random Parameters for Soil Fatigue Models
by Alessandro Tombari and Fedor Maksimov
J. Mar. Sci. Eng. 2025, 13(6), 1145; https://doi.org/10.3390/jmse13061145 - 9 Jun 2025
Viewed by 341
Abstract
The structural reliability of bottom-fixed offshore wind turbines is generally influenced by the dispersion of and variability in soil properties, which affect their ultimate capacity, serviceability, and both the short- and long-term fatigue. During an earthquake, the soil–pile system is subjected to intense [...] Read more.
The structural reliability of bottom-fixed offshore wind turbines is generally influenced by the dispersion of and variability in soil properties, which affect their ultimate capacity, serviceability, and both the short- and long-term fatigue. During an earthquake, the soil–pile system is subjected to intense cyclic loads that can lead to stiffness and strength degradation, typically captured through cyclic soil models. Calibration of soil parameter variability is fundamental for reliable structural assessments of wind turbine integrity. In this study, a method to generate randomness of the parameters affecting cyclic soil degradation models is proposed. Fatigue parameters are quantified through random cyclic undrained triaxial tests conducted using the Discrete Element Method. Deterministic simulations are first performed based on experimental results from the Liquefaction Experiments and Analysis Project for validation. Subsequently, variability in the initial particle size distribution functions is introduced to generate random soil samples, and triaxial simulations are repeated to quantify the dispersion of soil fatigue parameters. The proposed procedure is then applied through Monte Carlo simulations on the IEA 15-MW reference wind turbine, which is subjected to both short- and long-duration earthquakes. The results demonstrate the significant impact of soil degradation on the bending moment envelope, as well as the effect of soil uncertainty on tower fatigue, assessed using the damage equivalent load approach. Full article
(This article belongs to the Section Ocean Engineering)
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15 pages, 11857 KiB  
Article
Comparison of Cu Strengthened by Ionic Bonded Particles and Cu Strengthened by Metallic Bonded Particles
by Ke Han, Vince Toplosky, Rongmei Niu and Yan Xin
Materials 2025, 18(11), 2648; https://doi.org/10.3390/ma18112648 - 5 Jun 2025
Viewed by 379
Abstract
Cu matrix composites, because of their high mechanical strength, are often used as conductors in high-performance electrical applications. These composites are manufactured through thermomechanical processing, which introduces a high density of particles that act as obstacles to dislocation motion. Increasing the density of [...] Read more.
Cu matrix composites, because of their high mechanical strength, are often used as conductors in high-performance electrical applications. These composites are manufactured through thermomechanical processing, which introduces a high density of particles that act as obstacles to dislocation motion. Increasing the density of these particles enhances the mechanical strength of the conductors, which we tested under static loading. Under cyclic loading, especially pulsed electrical mechanical loading, conductors may soften, harden, or even fail. Failure is likely to occur whenever the applied stress exceeds the flow stress of the conductors. Understanding and predicting the performance of conductors under cyclic loading can help researchers estimate the lifespan of any apparatus made from these conductors. The performance of conductors depends on whether the strengthening particles are characterized by ionic interatomic bonding or metallic bonding. During fabrication, we observed both the accumulation of dislocations and the dissolution of particles (which added more solute atoms to the matrix). Because both dislocations and solute atoms tend to migrate at room temperature or higher, the complexity of microstructure changes increases in composites under cyclic loading. To minimize such complexity, we designed our test to determine fatigue properties at 77 K. We subjected the conductors to cyclic fatigue tests using a load-controlled mode (the mode most commonly used in applications). This work sheds light on the correlation between tensile properties and fatigue properties in our composite conductors. We found that the correlation varied, depending on whether the conductors had been strengthened by ionic bond or metallic bond particles. Full article
(This article belongs to the Special Issue Fatigue Crack Growth in Metallic Materials (Volume II))
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17 pages, 6934 KiB  
Article
Fatigue Life Anisotropy of API 5L X42 Pipeline Steel in Axial Force-Controlled Tests
by Manuel A. Beltrán-Zúñiga, Jorge L. González-Velázquez, Diego I. Rivas-López, Héctor J. Dorantes-Rosales, Carlos Ferreira-Palma, Felipe Hernández-Santiago and Fernando Larios-Flores
Materials 2025, 18(11), 2484; https://doi.org/10.3390/ma18112484 - 26 May 2025
Viewed by 372
Abstract
Fatigue endurance anisotropic behavior was evaluated for an API 5L X42 pipeline steel through axial force-controlled fatigue tests amongst Longitudinal, Diagonal, and Circumferential directions. This study shows that fatigue life anisotropy is mainly controlled by pearlite banding degree (Ai) and [...] Read more.
Fatigue endurance anisotropic behavior was evaluated for an API 5L X42 pipeline steel through axial force-controlled fatigue tests amongst Longitudinal, Diagonal, and Circumferential directions. This study shows that fatigue life anisotropy is mainly controlled by pearlite banding degree (Ai) and ferritic grain orientation (Ω12). Also, it is foreseen that the observed behavior can be related to the dislocation arrays generated by the cyclic loading in relation to microstructure orientation, and the interactions of the fatigue crack tip with the microstructure during the crack propagation stage. Full article
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15 pages, 6019 KiB  
Article
Effect of Service Temperature on the Mechanical and Fatigue Behaviour of Metal–Polymer Friction Stir Composite Joints
by Arménio N. Correia, Rodrigo J. Coelho, Daniel F. O. Braga, Mafalda Guedes, Ricardo Baptista and Virgínia Infante
Polymers 2025, 17(10), 1366; https://doi.org/10.3390/polym17101366 - 16 May 2025
Cited by 1 | Viewed by 466
Abstract
This study investigates the mechanical and fatigue behaviour of friction stir composite joints fabricated from an aluminum alloy (AA6082-T6) and a glass fibre-reinforced polymer (Noryl® GFN2) under different service temperature conditions. The joints were tested under both quasi-static and cyclic loading at [...] Read more.
This study investigates the mechanical and fatigue behaviour of friction stir composite joints fabricated from an aluminum alloy (AA6082-T6) and a glass fibre-reinforced polymer (Noryl® GFN2) under different service temperature conditions. The joints were tested under both quasi-static and cyclic loading at three different temperatures (23, 75, and 130 °C). Fracture surfaces were analyzed, and the probabilistic S–N curves were derived using Weibull distribution. Results indicated that increasing the service temperature caused a non-linear decrease in both the quasi-static and fatigue strength of the joints. Compared to room temperature, joints tested at 75 °C and 130 °C showed a 10% and 50% reduction in average tensile strength, respectively. The highest fatigue strength occurred at 23 °C, while the lowest was at 130 °C, in line with the quasi-static results. Fatigue stress-life plots displayed a semi-logarithmic nature, with lives ranging from 102 to 105 cycles for stress amplitudes between 7.7 and 22.2 MPa at 23 °C, 7.2 to 19.8 MPa at 75 °C, and 6.2 to 13.5 MPa at 130 °C. The joints’ failure occurred in the polymeric base material close to joints’ interface, highlighting the critical role of the polymer in limiting joints’ performance, as confirmed by thermal and scanning electron microscopy analyses. Full article
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