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Search Results (249)

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Keywords = continuous fiber-reinforced polymer

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22 pages, 4283 KiB  
Article
Characterization of Envira Fibers Endemic to the Amazon Rainforest and Their Potential for Reinforcement in Polymer Composites
by Miriane Alexandrino Pinheiro, Leoncio Soares Galvao Neto, Alisson Clay Rios da Silva, Sérgio Neves Monteiro, Felipe Perisse Duarte Lopes, Marcos Allan Leite dos Reis and Verônica Scarpini Candido
Polymers 2025, 17(17), 2284; https://doi.org/10.3390/polym17172284 (registering DOI) - 23 Aug 2025
Abstract
Natural lignocellulosic fibers (NLFs) replacing synthetic fibers have been used as reinforcement in polymer matrix composites. In this work, a lesser-known NLF endemic to the Amazon region, the envira fiber (Bocageopsis multiflora), was analyzed for its basic physical, thermochemical, morphological, and [...] Read more.
Natural lignocellulosic fibers (NLFs) replacing synthetic fibers have been used as reinforcement in polymer matrix composites. In this work, a lesser-known NLF endemic to the Amazon region, the envira fiber (Bocageopsis multiflora), was analyzed for its basic physical, thermochemical, morphological, and mechanical characteristics. In addition, epoxy matrix composites with 10, 20, 30, and 40 vol% of continuous and aligned envira fibers were evaluated by Fourier transform infrared spectroscopy (FTIR) and tensile tests. The results were statistically compared by ANOVA and Tukey’s test. The density found for the envira fiber was 0.23 g/cm3. The crystallinity index and microfibrilar angle obtained were 69.5% and 7.07°, respectively. Fiber thermal stability was found up to around 210 °C. FTIR confirmed the presence of functional groups characteristic of NLFs. Morphological analysis by SEM revealed that the envira fiber displayed fine bundles of fibrils and a rough surface along its length. The average strength value of the envira fiber was found to be 62 MPa. FTIR analysis of the composites confirmed the presence of the main constituents of the epoxy resin and NLFs. The tensile strength results indicated that the envira fiber addition increased the strength of the composites up to 40 vol%. The analysis of the fracture region revealed brittle aspects. These results indicate that envira fibers present potential reinforcement for polymer matrix composites and can be used in engineering applications, favored by their lightness and cost-effectiveness. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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22 pages, 3203 KiB  
Article
Axial Compression Behavior of Square RC Columns Confined by Rectangular BFRP and Hybrid Ties
by Amr M. A. Moussa, Arafa M. A. Ibrahim, Ahmed Elsayed, Zhishen Wu and Ahmed Monier
Infrastructures 2025, 10(8), 206; https://doi.org/10.3390/infrastructures10080206 - 8 Aug 2025
Viewed by 292
Abstract
This study investigates the axial compression behavior of square reinforced concrete (RC) columns confined by a novel type of rectangular closed basalt fiber-reinforced polymer (BFRP) tie fabricated using a continuous filament winding method, and hybrid steel–BFRP configurations. The proposed ties were developed to [...] Read more.
This study investigates the axial compression behavior of square reinforced concrete (RC) columns confined by a novel type of rectangular closed basalt fiber-reinforced polymer (BFRP) tie fabricated using a continuous filament winding method, and hybrid steel–BFRP configurations. The proposed ties were developed to overcome common limitations of conventional FRP stirrups, such as reduced tensile strength at bent regions and premature rupture. A total of five RC column specimens were tested under monotonic axial loading: one reference specimen with conventional steel ties, two specimens with BFRP ties spaced at 45 mm and 90 mm, and two hybrid specimens combining steel and BFRP ties. Experimental results showed that the steel-confined column achieved the highest peak axial load of 1793.2 kN and an ultimate strain value of 1.12. The specimen with closely spaced BFRP ties (45 mm) reached 94.7% of the peak load of the steel-confined specimen and exhibited over 137% higher axial strain capacity. The hybrid specimen with two interleaved BFRP ties achieved the highest confinement effectiveness ratio of 1.306. The findings demonstrate that the proposed BFRP ties offer a structurally viable and corrosion-resistant alternative to steel ties, particularly when used in hybrid systems. This research contributes to the development of durable, high-performance confinement strategies for RC columns in seismic and aggressive environmental conditions. Full article
(This article belongs to the Section Infrastructures and Structural Engineering)
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22 pages, 4383 KiB  
Article
High-Yield Precursor-Derived Si-O Ceramics: Processing and Performance
by Xia Zhang, Bo Xiao, Yongzhao Hou and Guangwu Wen
Materials 2025, 18(15), 3666; https://doi.org/10.3390/ma18153666 - 4 Aug 2025
Viewed by 273
Abstract
The precursor-derived ceramic route is recognized as an advanced and efficient technique for fabricating ceramic matrix composites, particularly suitable for the development and microstructural tailoring of continuous fiber-reinforced ceramic matrix composites. In this work, octamethylcyclotetrasiloxane and tetravinylcyclotetrasiloxane were employed as monomers to synthesize [...] Read more.
The precursor-derived ceramic route is recognized as an advanced and efficient technique for fabricating ceramic matrix composites, particularly suitable for the development and microstructural tailoring of continuous fiber-reinforced ceramic matrix composites. In this work, octamethylcyclotetrasiloxane and tetravinylcyclotetrasiloxane were employed as monomers to synthesize a branched siloxane via ring-opening polymerization. A subsequent hydrosilylation reaction led to the formation of polyvinylsiloxane with a three-dimensional crosslinked structure. The precursor exhibited excellent fluidity, adjustable viscosity, and superior thermosetting characteristics, enabling efficient impregnation and densification of reinforcements through the polymer infiltration and pyrolysis process. Upon pyrolysis, the polyvinylsiloxane gradually converted from an organic polymer to an amorphous inorganic ceramic phase, yielding silicon oxycarbide ceramics with a high ceramic yield of 81.3%. Elemental analysis indicated that the resulting ceramic mainly comprised silicon and oxygen, with a low carbon content. Furthermore, the material demonstrated a stable dielectric constant (~2.5) and low dielectric loss (<0.01), which are beneficial for enhanced thermal stability and dielectric performance. These findings offer a promising precursor system and process reference for the low-cost production of high-performance, multifunctional ceramic matrix composites with strong potential for engineering applications. Full article
(This article belongs to the Special Issue Processing and Microstructure Design of Advanced Ceramics)
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20 pages, 4467 KiB  
Review
Structuring the Future of Cultured Meat: Hybrid Gel-Based Scaffolds for Edibility and Functionality
by Sun Mi Zo, Ankur Sood, So Yeon Won, Soon Mo Choi and Sung Soo Han
Gels 2025, 11(8), 610; https://doi.org/10.3390/gels11080610 - 3 Aug 2025
Viewed by 499
Abstract
Cultured meat is emerging as a sustainable alternative to conventional animal agriculture, with scaffolds playing a central role in supporting cellular attachment, growth, and tissue maturation. This review focuses on the development of gel-based hybrid biomaterials that meet the dual requirements of biocompatibility [...] Read more.
Cultured meat is emerging as a sustainable alternative to conventional animal agriculture, with scaffolds playing a central role in supporting cellular attachment, growth, and tissue maturation. This review focuses on the development of gel-based hybrid biomaterials that meet the dual requirements of biocompatibility and food safety. We explore recent advances in the use of naturally derived gel-forming polymers such as gelatin, chitosan, cellulose, alginate, and plant-based proteins as the structural backbone for edible scaffolds. Particular attention is given to the integration of food-grade functional additives into hydrogel-based scaffolds. These include nanocellulose, dietary fibers, modified starches, polyphenols, and enzymatic crosslinkers such as transglutaminase, which enhance mechanical stability, rheological properties, and cell-guidance capabilities. Rather than focusing on fabrication methods or individual case studies, this review emphasizes the material-centric design strategies for building scalable, printable, and digestible gel scaffolds suitable for cultured meat production. By systemically evaluating the role of each component in structural reinforcement and biological interaction, this work provides a comprehensive frame work for designing next-generation edible scaffold systems. Nonetheless, the field continues to face challenges, including structural optimization, regulatory validation, and scale-up, which are critical for future implementation. Ultimately, hybrid gel-based scaffolds are positioned as a foundational technology for advancing the functionality, manufacturability, and consumer readiness of cultured meat products, distinguishing this work from previous reviews. Unlike previous reviews that have focused primarily on fabrication techniques or tissue engineering applications, this review provides a uniquely food-centric perspective by systematically evaluating the compositional design of hybrid hydrogel-based scaffolds with edibility, scalability, and consumer acceptance in mind. Through a comparative analysis of food-safe additives and naturally derived biopolymers, this review establishes a framework that bridges biomaterials science and food engineering to advance the practical realization of cultured meat products. Full article
(This article belongs to the Special Issue Food Hydrocolloids and Hydrogels: Rheology and Texture Analysis)
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20 pages, 5397 KiB  
Article
Continuously Formed Fiber-Reinforced Thermoplastic Composite Rebar for Concrete Reinforcement
by Jacob C. Clark, William G. Davids, Roberto A. Lopez-Anido, Andrew P. Schanck and Cody A. Sheltra
J. Compos. Sci. 2025, 9(7), 378; https://doi.org/10.3390/jcs9070378 - 18 Jul 2025
Viewed by 772
Abstract
Despite the strength and ductility of steel reinforcing bars, their susceptibility to corrosion can limit the long-term durability of reinforced concrete structures. Fiber-reinforced polymer (FRP) reinforcing bars made with a thermosetting matrix offer corrosion resistance but cannot be field-bent, which limits flexibility during [...] Read more.
Despite the strength and ductility of steel reinforcing bars, their susceptibility to corrosion can limit the long-term durability of reinforced concrete structures. Fiber-reinforced polymer (FRP) reinforcing bars made with a thermosetting matrix offer corrosion resistance but cannot be field-bent, which limits flexibility during construction. FRP reinforcing bars made with fiber-reinforced thermoplastic polymers (FRTP) address this limitation; however, their high processing viscosity presents manufacturing challenges. In this study, the Continuous Forming Machine, a novel pultrusion device that uses pre-consolidated fiber-reinforced thermoplastic tapes as feedstock, is described and used to fabricate 12.7 mm nominal diameter thermoplastic composite rebars. Simple bend tests on FRTP rebar that rely on basic equipment are performed to verify its ability to be field-formed. The manual bending technique demonstrated here is practical and straightforward, although it does result in some fiber misalignment. Subsequently, surface deformations are introduced to the rebar to promote mechanical bonding with concrete, and tensile tests of the bars are conducted to determine their mechanical properties. Finally, flexural tests of simply-supported, 6 m long beams reinforced with FRTP rebar are performed to assess their strength and stiffness as well as the practicality of using FRTP rebar. The beam tests demonstrated the prototype FRTP rebar’s potential for reinforcing concrete beams, and the beam load–deformation response and capacity agree well with predictions developed using conventional structural analysis principles. Overall, the results of the research reported indicate that thermoplastic rebars manufactured via the Continuous Forming Machine are a promising alternative to both steel and conventional thermoset composite rebar. However, both the beam and tension test results indicate that improvements in material properties, especially elastic modulus, are necessary to meet the requirements of current FRP rebar specifications. Full article
(This article belongs to the Section Fiber Composites)
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20 pages, 917 KiB  
Article
Numerical Investigation of Buckling Behavior of MWCNT-Reinforced Composite Plates
by Jitendra Singh, Ajay Kumar, Barbara Sadowska-Buraczewska, Wojciech Andrzejuk and Danuta Barnat-Hunek
Materials 2025, 18(14), 3304; https://doi.org/10.3390/ma18143304 - 14 Jul 2025
Viewed by 298
Abstract
The current study demonstrates the buckling properties of composite laminates reinforced with MWCNT fillers using a novel higher-order shear and normal deformation theory (HSNDT), which considers the effect of thickness in its mathematical formulation. The hybrid HSNDT combines polynomial and hyperbolic functions that [...] Read more.
The current study demonstrates the buckling properties of composite laminates reinforced with MWCNT fillers using a novel higher-order shear and normal deformation theory (HSNDT), which considers the effect of thickness in its mathematical formulation. The hybrid HSNDT combines polynomial and hyperbolic functions that ensure the parabolic shear stress profile and zero shear stress boundary condition at the upper and lower surface of the plate, hence removing the need for a shear correction factor. The plate is made up of carbon fiber bounded together with polymer resin matrix reinforced with MWCNT fibers. The mechanical properties are homogenized by a Halpin–Tsai scheme. The MATLAB R2019a code was developed in-house for a finite element model using C0 continuity nine-node Lagrangian isoparametric shape functions. The geometric nonlinear and linear stiffness matrices are derived using the principle of virtual work. The solution of the eigenvalue problem enables estimation of the critical buckling loads. A convergence study was carried out and model efficiency was corroborated with the existing literature. The model contains only seven degrees of freedom, which significantly reduces computation time, facilitating the comprehensive parametric studies for the buckling stability of the plate. Full article
(This article belongs to the Special Issue Mechanical Behavior of Advanced Composite Materials and Structures)
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58 pages, 38117 KiB  
Article
Multi-Disciplinary Investigations on the Best Flying Wing Configuration for Hybrid Unmanned Aerial Vehicles: A New Approach to Design
by Janani Priyadharshini Veeraperumal Senthil Nathan, Martin Navamani Chellapandian, Vijayanandh Raja, Parvathy Rajendran, It Ee Lee, Naveen Kumar Kulandaiyappan, Beena Stanislaus Arputharaj, Subhav Singh and Deekshant Varshney
Machines 2025, 13(7), 604; https://doi.org/10.3390/machines13070604 - 14 Jul 2025
Viewed by 507
Abstract
Flying wing Unmanned Aerial Vehicles (UAVs) are an interesting flight configuration, considering its benefits over aerodynamic, structural and added stealth aspects. The existing configurations are thoroughly studied from the literature survey and useful observations with respect to design and analysis are obtained. The [...] Read more.
Flying wing Unmanned Aerial Vehicles (UAVs) are an interesting flight configuration, considering its benefits over aerodynamic, structural and added stealth aspects. The existing configurations are thoroughly studied from the literature survey and useful observations with respect to design and analysis are obtained. The proposed design method includes distinct calculations of the UAV and modelling using 3D experience. The created innovative models are simulated with the help of computational fluid dynamics techniques in ANSYS Fluent to obtain the aerodynamic parameters such as forces, pressure and velocity. The optimization process continues to add more desired modifications to the model, to finalize the best design of flying wing frame for the chosen application and mission profile. In total, nine models are developed starting with the base model, then leading to the conventional, advanced and nature inspired configurations such as the falcon and dragonfly models, as it has an added advantage of producing high maneuverability and lift. Following this, fluid structure interaction analysis has been performed for the best performing configurations, resulting in the determination of variations in the structural behavior with the imposition of advanced composite materials, namely, boron, Kevlar, glass and carbon fiber-reinforced polymers. In addition to this, a hybrid material is designed by combining two composites that resulted in superior material performance when imposed. Control dynamic study is performed for the maneuvers planned as per mission profile, to ensure stability during flight. All the resulting parameters obtained are compared with one another to choose the best frame of the flying wing body, along with the optimum material to be utilized for future analysis and development. Full article
(This article belongs to the Special Issue Design and Application of Bionic Robots)
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30 pages, 5062 KiB  
Review
State-of-the-Art Review of Studies on the Flexural Behavior and Design of FRP-Reinforced Concrete Beams
by Hau Tran, Trung Nguyen-Thoi and Huu-Ba Dinh
Materials 2025, 18(14), 3295; https://doi.org/10.3390/ma18143295 - 12 Jul 2025
Viewed by 661
Abstract
Fiber-reinforced polymer (FRP) bars have great potential to replace steel bars in the design of reinforced concrete (RC) beams since they have numerous advantages such as high tensile strength and good corrosion resistance. Therefore, many studies including experiments and numerical simulations have focused [...] Read more.
Fiber-reinforced polymer (FRP) bars have great potential to replace steel bars in the design of reinforced concrete (RC) beams since they have numerous advantages such as high tensile strength and good corrosion resistance. Therefore, many studies including experiments and numerical simulations have focused on the behavior of FRP RC beams. In this paper, a comprehensive overview of previous studies is conducted to provide a thorough understanding about the behavior, the design, and the limitations of FRP RC beams. Particularly, experimental studies on FRP RC beams are collected and reviewed. In addition, the numerical analysis of FRP beams including the finite element (FE) analysis, the discrete element (DE) analysis, and artificial intelligence/machine learning (AI/ML) is summarized. Moreover, the international standards for the design of FRP RC beams are presented and evaluated. Through the review of previous studies, 93 tested specimens are collected. They can be a great source of reference for other studies. In addition, it has been found that the studies on the continuous beams and deep beams reinforced with FRP bars are still limited. In addition, more studies using DE analysis and AI/ML to analyze the response of FRP RC beams under loading conditions should be conducted. Full article
(This article belongs to the Section Construction and Building Materials)
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21 pages, 7773 KiB  
Article
Dynamic Properties and Vibration Control of Additively Manufactured Carbon and Glass Fiber Reinforced Polymer Composites Using MFC: A Numerical Study with Experimental Validation
by Ali Raza, Magdalena Mieloszyk, Rūta Rimašauskienė, Vytautas Jūrėnas, Nabeel Maqsood, Marius Rimašauskas and Tomas Kuncius
J. Manuf. Mater. Process. 2025, 9(7), 235; https://doi.org/10.3390/jmmp9070235 - 8 Jul 2025
Viewed by 530
Abstract
With the growing need for lightweight, durable, and high-performance structures, additively manufactured (AM) polymer composite structures have captured significant attention in the engineering community. These structures offer considerable advantages in various dynamic engineering sectors including automotive, aviation, and military. Thus, this investigation emphasizes [...] Read more.
With the growing need for lightweight, durable, and high-performance structures, additively manufactured (AM) polymer composite structures have captured significant attention in the engineering community. These structures offer considerable advantages in various dynamic engineering sectors including automotive, aviation, and military. Thus, this investigation emphasizes the numerical analysis of the dynamic properties and vibration control of AM polylactic acid (PLA) composite structures reinforced with continuous glass fibers (CGFR-PLA) and carbon fibers (CCFR-PLA), with 0°–0° and 0°–90° layer orientations. The findings of this numerical study are compared and validated against earlier published experimental results. Initially, the numerical models were created using the Abaqus CAE 2024, replicating the actual experimental models. The numerical bending modal frequency of each numerical model is determined, and the 0°–0° oriented models exhibited considerably higher values compared to the corresponding 0°–90° models. Significant differences were noted between the numerical and experimental values in the higher modes, mainly due to existence of voids and misalignment in the actual models that were not considered in numerical models. Following this, a numerical amplitude frequency response (AFR) analysis was conducted to observe vibration amplitude variations as a function of frequency. The AFR numerical results demonstrated consistent trends with the experimental results despite differences between the absolute values of both scenarios. Afterwards, vibration amplitude control analysis was performed under the influence of a macro fiber composite (MFC) actuator. The findings from both numerical and experimental cases revealed that vibration control was noticeably higher in 0°–0° oriented structures compared to 0°–90° structures. Experimental models demonstrated higher vibration control effectiveness than the corresponding numerical models. Although significant differences between the numerical and experimental vibration response values were observed in each composite structure, the numerical results exhibited consistent trends with the experiments. This discrepancy is attributed to the challenge of capturing all boundary conditions of the experimental scenario and incorporating them into the numerical simulation. Full article
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22 pages, 7385 KiB  
Article
Axial Performances of CFRP-PVC Confined RAC Columns: Experimental and Numerical Study
by Zidong Hu, Ruoyu Cao, Qiaoyun Wu, Cheng Zhao, Jie Li and Xuyong Chen
Buildings 2025, 15(12), 2089; https://doi.org/10.3390/buildings15122089 - 17 Jun 2025
Viewed by 335
Abstract
The use of recycled aggregate concrete (RAC) in construction mitigates environmental pollution by repurposing demolition waste, but its lower compressive strength compared to natural aggregate concrete (NAC) limits broader application. Although carbon fiber reinforced polymer (CFRP) composites and polyvinyl chloride (PVC) tubes have [...] Read more.
The use of recycled aggregate concrete (RAC) in construction mitigates environmental pollution by repurposing demolition waste, but its lower compressive strength compared to natural aggregate concrete (NAC) limits broader application. Although carbon fiber reinforced polymer (CFRP) composites and polyvinyl chloride (PVC) tubes have individually been shown to improve concrete strength and ductility, existing studies focus on fully wrapped CFRP jackets on NAC columns and do not systematically explore CFRP–PVC hybrid confinement using strips on RAC. To address this research gap, this study investigates the axial compressive behavior of CFRP–PVC–RAC columns by varying CFRP strip width (from 25 to 75 mm), strip spacing (from 31 to 77.5 mm), and the number of CFRP layers (one to nine) over a central PVC tube. Axial compression tests reveal that specimens with a central CFRP strip width equal to or greater than 75 mm achieve peak loads up to 1331 kN and that, after rupture of the central strip, the remaining strips continue to carry load, producing a more gradual stress–strain decline and enhanced ductility compared to fully wrapped controls (peak load 1219 kN). These results show that CFRP–PVC composites enhance the axial compressive strength and ductility of RAC columns. The confinement mechanism increases the ultimate axial strain and redistributes transverse stresses, delaying brittle failure and improving deformation capacity. When two or more CFRP layers are applied, strip width and spacing affect axial stress by no more than three percent. Increasing layers from one to four raises axial strength by approximately 23 percent, whereas adding layers beyond four yields diminishing returns, with less than a six percent increase. Finally, a multilayer lateral confined pressure formula is derived and validated against thirty-two specimens, exhibiting errors no greater than three percent and accurately predicting effective confinement. These findings offer practical guidance for optimizing strip dimensions and layering in CFRP–PVC reinforcement of RAC columns, achieving material savings without compromising performance. Full article
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32 pages, 2930 KiB  
Review
3D Printing Continuous Fiber Reinforced Polymers: A Review of Material Selection, Process, and Mechanics-Function Integration for Targeted Applications
by Haoyuan Zheng, Shaowei Zhu, Liming Chen, Lianchao Wang, Hanbo Zhang, Peixu Wang, Kefan Sun, Haorui Wang and Chengtao Liu
Polymers 2025, 17(12), 1601; https://doi.org/10.3390/polym17121601 - 9 Jun 2025
Viewed by 2851
Abstract
In recent years, the rapid development of three-dimensional (3D)-printed continuous fiber-reinforced polymer (CFRP) technology has provided novel strategies for customized manufacturing of high-performance composites. This review systematically summarizes research advancements in material systems, processing methods, mechanical performance regulation, and functional applications of this [...] Read more.
In recent years, the rapid development of three-dimensional (3D)-printed continuous fiber-reinforced polymer (CFRP) technology has provided novel strategies for customized manufacturing of high-performance composites. This review systematically summarizes research advancements in material systems, processing methods, mechanical performance regulation, and functional applications of this technology. Material-wise, the analysis focuses on the performance characteristics and application scenarios of carbon fibers, glass fibers, and natural fibers, alongside discussions on the processing behaviors of thermoplastic matrices such as polyetheretherketone (PEEK). At the process level, the advantages and limitations of fused deposition modeling (FDM) and photopolymerization techniques are compared, with emphasis on their impact on fiber–matrix interfaces. The review further examines the regulatory mechanisms of fiber orientation, volume fraction, and other parameters on mechanical properties, as well as implementation pathways for functional designs, such as electrical conductivity and self-sensing capabilities. Application case studies in aerospace lightweight structures and automotive energy-absorbing components are comprehensively analyzed. Current challenges are highlighted, and future directions proposed, including artificial intelligence (AI)-driven process optimization and multi-material hybrid manufacturing. This review aims to provide a comprehensive assessment of the current achievements in 3D printing CFRP technology and a forward-looking analysis of existing challenges, offering a systematic reference for accelerating the transformation of 3D printing CFRP technology from laboratory research to industrial-scale implementation. Full article
(This article belongs to the Special Issue Polymer-Based Composite Structures and Mechanical Metamaterials)
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12 pages, 4178 KiB  
Article
Evaluation of Conditions for Self-Healing of Additively Manufactured Polymer Composites with Continuous Carbon Fiber Reinforcement
by Marius Rimašauskas, Tomas Kuncius, Rūta Rimašauskienė and Tomas Simokaitis
J. Manuf. Mater. Process. 2025, 9(6), 179; https://doi.org/10.3390/jmmp9060179 - 28 May 2025
Cited by 2 | Viewed by 616
Abstract
Additive manufacturing (AM) is one of the most frequently used technologies to produce complex configuration products. Moreover, AM is very well known as a technology which is characterized by a low amount of generated waste and the potential to be called zero-waste technology. [...] Read more.
Additive manufacturing (AM) is one of the most frequently used technologies to produce complex configuration products. Moreover, AM is very well known as a technology which is characterized by a low amount of generated waste and the potential to be called zero-waste technology. As is known, there are seven main groups of technologies described in the ISO/ASTM 52900 standard that allow the use of very different materials from polymers to metals, ceramics, and composites. However, the increased utilization of additively manufactured composites for different applications requires a deeper analysis of production processes and materials’ characteristics. Various AM technologies can be used to produce complex composite structures reinforced with short fibers; however, only material extrusion (MEX)-based technology is used for the production of composites reinforced with continuous fibers (CFs). At this time, five different methods exist to produce CF-reinforced composite structures. This study focuses on co-extrusion with the towpreg method. Because of the complexity and layer-by-layer nature of the process, defects can occur during production, such as poor interlayer adhesion, increased porosity, insufficient impregnation, and others. To eliminate or minimize defects’ influence on mechanical properties and structural integrity of additively manufactured structures, a hypothesis was proposed involving heat treatment. Carbon fiber’s conductive properties can be used to heal the composite structures, by heating them up through the application of electric current. In this research article, an experimental evaluation of conditions for additively manufactured composites with continuous carbon fiber reinforcement for self-healing processes is presented. Mechanical testing was conducted to check the influence of heat treatment on the flexural properties of the composite samples. Full article
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18 pages, 5271 KiB  
Article
Advancing High-Performance Composites in Additive Manufacturing (AM) Through Pre-Impregnation and Direct Ink Writing for Scalable 3D Printing
by Yuanrui Wang, Yuchen Ding, Kai Yu and Guoying Dong
J. Compos. Sci. 2025, 9(5), 218; https://doi.org/10.3390/jcs9050218 - 29 Apr 2025
Viewed by 1191
Abstract
Additive manufacturing (AM) has the potential to revolutionize the fabrication of continuous carbon fiber-reinforced polymer composites (CCFRPCs). Among AM techniques, direct ink writing (DIW) with ultraviolet (UV) curable resin shows promise for creating CCFRPCs with high manufacturing speed, high fiber volume fraction, and [...] Read more.
Additive manufacturing (AM) has the potential to revolutionize the fabrication of continuous carbon fiber-reinforced polymer composites (CCFRPCs). Among AM techniques, direct ink writing (DIW) with ultraviolet (UV) curable resin shows promise for creating CCFRPCs with high manufacturing speed, high fiber volume fraction, and low energy consumption. However, issues such as incomplete curing and weak interfacial bonding, particularly in dense fiber bundles, limit the mechanical performance. This study addressed these challenges using pre-impregnated systems (PISs), which is a process developed to impregnate dry fiber bundles with partially cured resin before being used for DIW printing, to enhance resin-fiber adhesion and fiber–fiber bonding within fiber bundles. By optimizing resin viscosity and curing conditions in the PIS process, samples treated by PIS achieved improved mechanical properties. Tensile and bending tests revealed significant performance gains over non-PIS treated samples, with tensile stiffness increasing by at least 39% and bending stiffness by 45% in 3K fiber bundles. Tensile samples with thicker fiber bundles (6K and 12K) exhibited similar improvements. On the other hand, while all samples exhibit enhanced mechanical properties under bending deformation, the improvement of flexural stiffness and strength with thicker fiber bundles is shown to be less significant than those with 3K fiber bundles. Overall, composites made with PIS-treated fibers can enhance mechanical performance compared with those made with non-PIS-treated fibers, offering the scaling capability of printing thicker fiber bundles to reduce processing time while maintaining improved properties. It emphasizes the importance of refining the pre-processing strategies of large continuous fiber bundles in the AM process to achieve optimal mechanical properties. Full article
(This article belongs to the Special Issue Additive Manufacturing of Advanced Composites, 2nd Edition)
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19 pages, 6866 KiB  
Article
Experimental Investigation on Mechanical Properties of Glass Fiber–Nanoclay–Epoxy Composites Under Water-Soaking: A Comparative Study Using RSM and ANN
by Manjunath Shettar, Ashwini Bhat, Nagaraj N. Katagi and Mandya Channegowda Gowrishankar
J. Compos. Sci. 2025, 9(4), 195; https://doi.org/10.3390/jcs9040195 - 21 Apr 2025
Cited by 1 | Viewed by 788
Abstract
Fiber-reinforced polymer composites are exposed to severe environmental conditions throughout their intended lifespan. It is essential to investigate how they age when exposed to cold and hot water to increase the durability of fiber-reinforced polymer composites. This work uses a hand lay-up process [...] Read more.
Fiber-reinforced polymer composites are exposed to severe environmental conditions throughout their intended lifespan. It is essential to investigate how they age when exposed to cold and hot water to increase the durability of fiber-reinforced polymer composites. This work uses a hand lay-up process to create composites with different weight percentages of glass fiber, nanoclay, and epoxy. ASTM guidelines are followed for performing tensile and flexural tests. The input parameters, varying wt.% of glass fiber and nanoclay, are continuous, and the aging condition is deemed a categorical factor. The mechanical properties are considered as response variables (output). The mechanical properties are optimized using Response Surface Methodology (RSM), while Artificial Neural Networks (ANNs) provide a reliable predictive model with high correlation coefficients. The findings demonstrate that ANNs outperform RSM in flexural strength prediction, whereas RSM offers greater accuracy for tensile strength modeling. SEM analysis of the fracture surfaces reveals the causes of specimen failure under tensile load, with distinct differences between dry, cold, and boiling water-soaked specimens. Full article
(This article belongs to the Section Composites Modelling and Characterization)
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20 pages, 6291 KiB  
Article
Enhancing the Strength of 3D-Printed Polymer Exoprosthetic Socket by Localized Non-Planar Continuous Carbon Fiber Reinforcement
by Daria Dolgikh, Evgeniy Lobov, Igor Bezukladnikov, Aleksandr Shalimov and Mikhail Tashkinov
Polymers 2025, 17(8), 1097; https://doi.org/10.3390/polym17081097 - 18 Apr 2025
Viewed by 665
Abstract
This study investigates strategies to enhance the structural integrity of 3D-printed orthopedic transtibial exoskeleton sockets by integrating non-planar reinforcement with structured prepreg rods composed of continuous carbon fibers, leveraging multi-axis additive manufacturing techniques. A prototype of a cylindrical polyamide 3D-printed exoskeleton socket is [...] Read more.
This study investigates strategies to enhance the structural integrity of 3D-printed orthopedic transtibial exoskeleton sockets by integrating non-planar reinforcement with structured prepreg rods composed of continuous carbon fibers, leveraging multi-axis additive manufacturing techniques. A prototype of a cylindrical polyamide 3D-printed exoskeleton socket is examined. Numerical modeling using progressive failure analysis, incorporating material property degradation models, successfully simulated damage accumulation in the studied 3D-printed structures. Numerical simulations revealed that crack formation initiates in the socket’s distal section, aligning with physical test observations. Targeted localized reinforcement with carbon rods effectively strengthened the high-load regions of the prosthetic devices. A method to improve product strength by optimization of the internal architecture of the embedded reinforcements in the local stress concentrator zones is proposed. The results demonstrate a reduction in stress concentrations within prostheses when using carbon fiber reinforcements. Multi-axis dual extrusion non-planar additive manufacturing techniques were used to produce the developed prototypes. Surface morphology was examined, and optimal process parameters were determined to enhance printing quality. The developed approach enables precise reinforcement of custom-shaped sockets with complex geometries. Full article
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