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Search Results (369)

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Keywords = carbon-fibre-reinforced composites

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21 pages, 4047 KB  
Article
Natural Frequency and Damping Characterisation of Aerospace Grade Composite Plates
by Rade Vignjevic, Nenad Djordjevic, Javier de Caceres Prieto, Nenad Filipovic, Milos Jovicic and Gordana Jovicic
Vibration 2025, 8(4), 72; https://doi.org/10.3390/vibration8040072 - 13 Nov 2025
Abstract
The natural frequencies and damping characterisation of a new aerospace grade composite material were investigated using a modified impulse method combined with the half power bandwidth method, which is applicable to the structures with a low damping. The composite material of interest was [...] Read more.
The natural frequencies and damping characterisation of a new aerospace grade composite material were investigated using a modified impulse method combined with the half power bandwidth method, which is applicable to the structures with a low damping. The composite material of interest was unidirectional carbon fibre reinforced plastic. The tests were carried out with three identical square 4.6 mm thick plates consisting of 24 plies. The composite plates were clamped along one edge in a SignalForce shaker, which applied a sinusoidal signal generated by the signal conditioner exiting the bending modes of the plates. Laser vibrometer measurements were taken at three points on the free end so that different vibrational modes could be obtained: one measurement was taken on the longitudinal symmetry plane with the other two 35 mm on either side of the symmetry plane. The acceleration of the clamp was also recorded and integrated twice to calculate its displacement, which was then subtracted from the free end displacement. Two material orientations were tested, and the first four natural frequencies were obtained in the test. Damping was determined by the half-power bandwidth method. A linear relationship between the loss factors and frequency was observed for the first two modes but not for the other two modes, which may be related to the coupling of the modes of the plate and the shaker. The experiment was also modelled by using the Finite Element Method (FEM) and implicit solver of LS Dyna, where the simulation results for the first two modes were within 15% of the experimental results. The novelty of this paper lies in the presentation of new experimental data for the natural frequencies and damping coefficients of a newly developed composite material intended for the vibration analysis of rotating components. Full article
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21 pages, 3170 KB  
Article
Understanding and Estimating the Electrical Resistance Between Surface Electrodes on a UD Carbon Fibre-Reinforced Composite Layer
by J. David Acosta, Meisam Jalalvand, Sheik Abdul Malik and Andrew Hamilton
J. Compos. Sci. 2025, 9(11), 615; https://doi.org/10.3390/jcs9110615 - 8 Nov 2025
Viewed by 206
Abstract
The potential for structural health monitoring (SHM) in fibre-reinforced polymers (FRPs) using electrical resistance measurements (ERMs) has gained increasing attention, particularly in carbon fibre-reinforced polymers (CFRPs). Most existing studies are limited to single-axis measurements on coupon-scale specimens, whereas industrial applications demand scalable solutions [...] Read more.
The potential for structural health monitoring (SHM) in fibre-reinforced polymers (FRPs) using electrical resistance measurements (ERMs) has gained increasing attention, particularly in carbon fibre-reinforced polymers (CFRPs). Most existing studies are limited to single-axis measurements on coupon-scale specimens, whereas industrial applications demand scalable solutions capable of monitoring large areas, with more complex sensing configurations. Structural health monitoring (SHM) of carbon fibre-reinforced polymers (CFRPs) using electrical resistance measurements offers a low-cost, scalable sensing approach. However, predicting surface resistance between arbitrarily placed electrodes on unidirectional (UD) CFRP laminates remains challenging due to anisotropic conductivity and geometric variability. This study introduces a practical analytical model based on two geometry-dependent parameters, effective width and effective distance, to estimate resistance between any two electrodes arbitrarily placed on UD CFRP laminates with 0° or 90° fibre orientations. Validation through finite element (FE) simulations and experimental testing demonstrates good matching, confirming the model’s accuracy across various configurations. Results show that the dominant electrical current path aligns with the fibre direction due to the material’s anisotropic conductivity, allowing simplification to a single-axis resistance model. The proposed model offers a reliable estimation of surface resistance and provides a valuable tool for electrode array configuration design in CFRP-based SHM. This work contributes to enabling low-cost and scalable electrical sensing solutions for the real-time monitoring of composite structures in aerospace, automotive, and other high-performance applications. Full article
(This article belongs to the Special Issue Carbon Fiber Composites, 4th Edition)
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22 pages, 2042 KB  
Article
Implementation of Composite Materials for Lightweighting of Industrial Vehicle Chassis
by Ivan Tomasi, Stefano Grandi, Giorgio Donzella and Luigi Solazzi
J. Compos. Sci. 2025, 9(11), 611; https://doi.org/10.3390/jcs9110611 - 5 Nov 2025
Viewed by 364
Abstract
This research study investigates the use of composite materials to reduce the weight of heavy industrial vehicle chassis. A new Carbon Fibre Reinforced Polymer (CFRP) crossmember was developed to replicate the mechanical performance of the traditional steel component while achieving substantial weight reduction. [...] Read more.
This research study investigates the use of composite materials to reduce the weight of heavy industrial vehicle chassis. A new Carbon Fibre Reinforced Polymer (CFRP) crossmember was developed to replicate the mechanical performance of the traditional steel component while achieving substantial weight reduction. A multi-step approach was adopted: analytical and finite-element analyses were performed on single crossmembers to assess bending and torsional stiffness. The CFRP design achieved increases of 6.8% in torsional stiffness and 5.0% in bending stiffness, with a 68.1% weight reduction. After confirming stiffness equivalence, full chassis simulations were carried out to evaluate global performance. The steel model reproduced experimental results with a relative error of 1.13%, while the CFRP configuration enhanced overall torsional stiffness by 7.8%. Extending these results to all crossmembers, the initial cost increase of the CFRP solution could be recovered within about 2 years for the diesel scenario and 3.5 years for the electric one. Environmental benefits were also quantified, with annual CO2 reductions of 708.4 kg and 298.6 kg, and cost savings of up to 463.3 EUR/year and 299.8 EUR/year, respectively. Full article
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22 pages, 4598 KB  
Article
Machinability of Vitrified Semi-Finished Products: Chip Formation and Heat Development at the Cutting Edge
by Jannick Fuchs, Yehor Kozlovets, Jonathan Alms, Markus Meurer, Christian Hopmann, Thomas Bergs and Mustapha Abouridouane
Polymers 2025, 17(19), 2681; https://doi.org/10.3390/polym17192681 - 3 Oct 2025
Viewed by 434
Abstract
Fibre-reinforced composites are facing new challenges in the context particular in sustainability and recyclability. Vitrimers could be useful as new matrices to support the increase in sustainability. Due to their high strength, which is comparable to that of thermosets often used in composites, [...] Read more.
Fibre-reinforced composites are facing new challenges in the context particular in sustainability and recyclability. Vitrimers could be useful as new matrices to support the increase in sustainability. Due to their high strength, which is comparable to that of thermosets often used in composites, and their covalent adaptive networks, which make them reshapeable for scaled-up manufacturing and recycling purposes, they are very useful. Orthogonal cutting is used for precise reshaping and functional integration into carbon fibre reinforced plastics. Vitrimers could improve processing results at the cutting edge as well as surface quality thanks to their self-healing properties compared to brittle matrices, as well as enabling the recycling of formed chips and scrap. This study showcases the manufacturing of a carbon fibre-reinforced vitrimer using 4-aminophenyl disulfide as a hardener, with vacuum-assisted resin infusion. The temperature of chip formation and the cutting parameters are then shown for different fibre orientations, cutting widths and speeds. The observed cutting forces are lower (less than 140 N) and more irregular for fibre orientations 45°/135°, increasing with cutting depth, and fluctuating periodically during machining. Despite varying cutting speeds, the forces remain relatively constant in range between 85 N and 175 N for 0°/90° fibre orientation and 50 N and 120 N for 45°/135° fibre orientation, with no significant tool wear observed and lower-damage depth and overhanging fibres observed for 0°/90° fibre orientation. Damage observation of the cutting tool shows promising results, with lower abrasion observed compared to thermoset matrices. Microscopic images of the broached surface also show good quality, which could be improved by self-healing of the matrix at higher temperatures. Temperature measurements of chip formation using a high-speed camera show a high temperature gradient as cutting speeds increase, but the temperature only ever exceeds 180 °C at cutting speeds of 150 m/min, ensuring reprocessability since this is below the degradation temperature. Therefore, orthogonal cutting of vitrimers can impact sustainable composite processing. Full article
(This article belongs to the Section Polymer Networks and Gels)
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29 pages, 618 KB  
Review
End-of-Life Strategies for Wind Turbines: Blade Recycling, Second-Life Applications, and Circular Economy Integration
by Natalia Cieślewicz, Krzysztof Pilarski and Agnieszka A. Pilarska
Energies 2025, 18(19), 5182; https://doi.org/10.3390/en18195182 - 29 Sep 2025
Cited by 1 | Viewed by 1857
Abstract
Wind power is integral to the transformation of energy systems towards sustainability. However, the increasing number of wind turbines approaching the end of their service life presents significant challenges in terms of waste management and environmental sustainability. Rotor blades, typically composed of thermoset [...] Read more.
Wind power is integral to the transformation of energy systems towards sustainability. However, the increasing number of wind turbines approaching the end of their service life presents significant challenges in terms of waste management and environmental sustainability. Rotor blades, typically composed of thermoset polymer composites reinforced with glass or carbon fibres, are particularly problematic due to their low recyclability and complex material structure. The aim of this article is to provide a system-level review of current end-of-life strategies for wind turbine components, with particular emphasis on blade recycling and decision-oriented comparison, and its integration into circular economy frameworks. The paper explores three main pathways: operational life extension through predictive maintenance and design optimisation; upcycling and second-life applications; and advanced recycling techniques, including mechanical, thermal, and chemical methods, and reports qualitative/quantitative indicators together with an indicative Technology Readiness Level (TRL). Recent innovations, such as solvolysis, microwave-assisted pyrolysis, and supercritical fluid treatment, offer promising recovery rates but face technological and economic as well as environmental compliance limitations. In parallel, the review considers deployment maturity and economics, including an indicative mapping of cost and deployment status to support decision-making. Simultaneously, reuse applications in the construction and infrastructure sectors—such as concrete additives or repurposed structural elements—demonstrate viable low-energy alternatives to full material recovery, although regulatory barriers remain. The study also highlights the importance of systemic approaches, including Extended Producer Responsibility (EPR), Digital Product Passports and EU-aligned policy/finance instruments, and cross-sectoral collaboration. These instruments are essential for enhancing material traceability and fostering industrial symbiosis. In conclusion, there is no universal solution for wind turbine blade recycling. Effective integration of circular principles will require tailored strategies, interdisciplinary research, and bankable policy support. Addressing these challenges is crucial for minimising the environmental footprint of the wind energy sector. Full article
(This article belongs to the Collection Feature Papers in Energy, Environment and Well-Being)
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25 pages, 5006 KB  
Article
Optimisation of Glass and Carbon Fibre-Reinforced Concrete with External Enzymatic Self-Healing: An Experimental and Environmental Impact Study
by Mohamed Rabie, Ali Bahadori-Jahromi and Ibrahim G. Shaaban
Buildings 2025, 15(19), 3455; https://doi.org/10.3390/buildings15193455 - 24 Sep 2025
Viewed by 855
Abstract
This study evaluates glass and carbon fibre-reinforced concrete in terms of performance, durability, environmental impact, and a novel enzymatic self-healing method. An experimental program was conducted on seven concrete mixes, including a plain control and mixes with varying dosages of glass and carbon [...] Read more.
This study evaluates glass and carbon fibre-reinforced concrete in terms of performance, durability, environmental impact, and a novel enzymatic self-healing method. An experimental program was conducted on seven concrete mixes, including a plain control and mixes with varying dosages of glass and carbon fibres. Glass and carbon fibres were incorporated at identical dosages of 0.12%, 0.22%, and 0.43% fibre volume fraction (Vf) to enable direct comparison of their performance. The experimental investigation involved a comprehensive characterization of the concrete mixes. Fresh properties were evaluated via slump tests, while hardened properties were determined through compressive and split tensile strength testing. Durability was subsequently assessed by measuring the rate of water absorption, bulk density, and moisture content. Following this material characterization, a cradle-to-gate Life Cycle Assessment (LCA) was conducted to quantify the embodied carbon and energy. Finally, an evaluation of a novel Carbonic Anhydrase (CA)-based self-healing treatment on pre-cracked, optimised fibre-reinforced specimens was conducted. The findings highlight key performance trade-offs associated with fibre reinforcement. Although both fibre types reduced compressive strength, they markedly improved split tensile strength for glass fibres by up to 70% and carbon fibres by up to 35%. Durability responses diverged: glass fibres increased water absorption, while carbon fibres reduced water absorption at low doses, indicating reduced permeability. LCA showed a significant rise in environmental impact, particularly for carbon fibres, which increased embodied energy by up to 141%. The CA enzymatic solution enhanced crack closure in fibre-reinforced specimens, achieving up to 30% healing in carbon fibre composites. These findings suggest that fibre-reinforced enzymatic self-healing concrete offers potential for targeted high-durability applications but requires careful life-cycle optimisation. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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22 pages, 12946 KB  
Article
Tribological Characterization of Carbon Fibre Reinforced Polymer (CFRP) Sliding Against Ti and Al Alloy Counterbodies for Aerospace Applications
by Luís Vilhena, Sharjeel Ahmed Khan, André Garcia and Amílcar Ramalho
Materials 2025, 18(18), 4296; https://doi.org/10.3390/ma18184296 - 13 Sep 2025
Viewed by 594
Abstract
Carbon fibre reinforced polymer (CFRP) is a composite material known for its light weight and exceptional durability, composed of carbon fibres within a polymer matrix. Despite its high cost, CFRP is favoured for its outstanding strength-to-weight ratio and rigidity. It is widely used [...] Read more.
Carbon fibre reinforced polymer (CFRP) is a composite material known for its light weight and exceptional durability, composed of carbon fibres within a polymer matrix. Despite its high cost, CFRP is favoured for its outstanding strength-to-weight ratio and rigidity. It is widely used in the aerospace industry and ship superstructures, among others. These components often rub against different materials in various structural and mechanical assemblies. These interactions typically occur where metallic fasteners, bearings, hinges, and sliding components interface with CFRP parts causing, for example, fretting wear. The main novelty of the present study consists of a systematic comparison of titanium (Ti6Al4V) and aluminium (AA2024-T6) alloy spheres under identical test conditions, evaluating how each material interacts with different CFRP configurations. CFRP was tested against titanium and aluminium alloy spheres as counterbodies under reciprocating sliding conditions. Different contact conditions (applied loads) were used for tribotests. The wear volume and coefficient of friction were determined, as well as the wear mechanisms. Different analytical techniques were employed, such as profilometry, optical microscopy (OM), and scanning electron microscopy (SEM/EDS), to characterise the wear tracks. It was possible to determine the coefficient of friction as well as the wear rate on both CFRP specimens and their respective counterbodies. It was found that the coefficient of friction (CoF) depends on load, fibre orientation, and counterbody material, ranging from 0.14 to 0.29. The lowest wear rate coefficient was observed for CFRP sliding against titanium alloy in the layer configuration, at 1.48 × 10−13 mm3/N·m. In contrast, aluminium alloy counterbodies experienced significantly higher wear, with a maximum wear rate of 6.88 × 10−5 mm3/N·m. Wear volume increased with load across all conditions and was highest for the CFRP cross-section against aluminium alloy. Full article
(This article belongs to the Special Issue Carbon Fiber and Its Composites: State of the Art and Perspectives)
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5 pages, 666 KB  
Abstract
Full-Field Imaging for Evaluating Mode-II Fracture Toughness in CFRP Laminates
by Riccardo Cappello, Rafael Ruiz-Iglesias, Spyros Spyridonidis, Neha Chandarana and Janice M. Dulieu-Barton
Proceedings 2025, 129(1), 70; https://doi.org/10.3390/proceedings2025129070 - 12 Sep 2025
Viewed by 344
Abstract
To replicate delaminations at the coupon and substructural scales, simulated defects are often introduced into test specimens; therefore, understanding their behaviour within the laminate is essential. Full-field imaging is employed to investigate the effects of artificial defects in Carbon Fibre-Reinforced Polymer (CFRP) composites. [...] Read more.
To replicate delaminations at the coupon and substructural scales, simulated defects are often introduced into test specimens; therefore, understanding their behaviour within the laminate is essential. Full-field imaging is employed to investigate the effects of artificial defects in Carbon Fibre-Reinforced Polymer (CFRP) composites. Centre Crack Ply (CCP) specimens are used to evaluate the Mode II fracture toughness of laminated composites from a simple tensile test. Two batches of specimens are manufactured using IM7/8552. Artificial defects are introduced using a steel film insert of 5 µm thickness. For the first type of samples, the inserts were coated with Frekote release agent, while for the second type, the steel inserts were incorporated into the laminate without coating. Additionally, a third batch of specimens with a [04, 90]s layup is manufactured. Thermoelastic Stress Analysis (TSA) and Digital Image Correlation (DIC) are employed to obtain full-field temperature and displacement data from the tested samples. The inclusion of 90-degree plies enhances thermal contrast exploiting, their anisotropic mechanical and thermal properties. First, the specimens are tested under monotonic loading to failure, with DIC used to capture strain distributions at damage initiation and failure. In addition, acoustic emission is employed to evaluate damage initiation. Load drops provide an indirect evaluation of fracture toughness. Results show that full-field imaging is capable of establishing how the release agent and the layup configuration influence damage initiation and propagation. The non-adiabatic thermoelastic response is shown to be effective in observing subsurface damage. Finally, a novel approach to evaluate fracture toughness from the temperature increase at the failure event is proposed. Full article
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13 pages, 4881 KB  
Article
Optimisation of Fibre-Reinforced Hybrid Composites Under Combined Loading
by Chensong Dong and Joseph Abel Philip Vaidyan
J. Compos. Sci. 2025, 9(9), 486; https://doi.org/10.3390/jcs9090486 - 8 Sep 2025
Cited by 1 | Viewed by 572
Abstract
Fibre-reinforced hybrid composites offer an effective balance between strength, weight, and cost by combining multiple fibre types within a single matrix. This study focuses on optimising the design of carbon/glass fibre-reinforced hybrid composites under combined bending and torsional loading using finite element analysis [...] Read more.
Fibre-reinforced hybrid composites offer an effective balance between strength, weight, and cost by combining multiple fibre types within a single matrix. This study focuses on optimising the design of carbon/glass fibre-reinforced hybrid composites under combined bending and torsional loading using finite element analysis (FEA) and response surface methodology. Twelve different layup configurations, including sandwich and non-sandwich hybrid designs, were analysed to identify the optimal ply angles and fibre volume fractions that maximise failure load while minimising material cost and density. The results reveal that sandwich-type layups, such as [C3G]S, [C2G2]S, and [CG3]S, demonstrate superior strength-to-weight performance, achieving failure loads exceeding 300 N. The study also confirms that optimal ply angles range from 12° to 30°, depending on the layup configuration, and that increasing the carbon fibre volume fraction generally enhances failure load, though an optimal balance with glass fibres must be maintained. The findings provide valuable design guidelines for engineers seeking to tailor hybrid composites for aerospace, automotive, and structural applications. Future work should focus on experimental validation and extending the analysis to additional loading conditions, such as impact and fatigue, to further improve the robustness of hybrid composite structures. Full article
(This article belongs to the Special Issue Recent Progress in Hybrid Composites)
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30 pages, 12838 KB  
Review
Recyclability of Composites in Commercial Aviation: Industrial Specificities, Readiness and Challenges
by Pedro Pinto, João Almeida, João Ferreira and Rui Miranda Guedes
J. Compos. Sci. 2025, 9(9), 471; https://doi.org/10.3390/jcs9090471 - 2 Sep 2025
Cited by 1 | Viewed by 2055
Abstract
The integration of composite materials into commercial aviation has transformed the industry by providing superior performance benefits, including enhanced fuel efficiency, reduced emissions, and improved structural integrity. With a significant shift towards aircraft featuring high contents of composite materials, the focus has also [...] Read more.
The integration of composite materials into commercial aviation has transformed the industry by providing superior performance benefits, including enhanced fuel efficiency, reduced emissions, and improved structural integrity. With a significant shift towards aircraft featuring high contents of composite materials, the focus has also turned to the challenges associated with the end-of-life management of these materials. Unlike metals, composites are notoriously difficult to recycle due to the strong bonding between fibres and resin, creating significant environmental and economic challenges. The methodology employed—consisting of an extensive literature review that prioritises a holistic approach—aims to provide an overview of the status of composite recyclability in aviation. With this, the report investigates the durability of composites under operational conditions, the associated environmental factors, and their impact on the recycling potential. The dismantling processes for decommissioned aircraft are analysed to identify strategies that preserve material integrity for effective recycling. Established recycling methods are critically evaluated alongside innovative approaches. The study highlights the limitations of current techniques in terms of costs, energy consumption, and material degradation while exploring emerging technologies that aim to overcome these barriers. It is concluded that currently available techniques do not possess the industrial maturity required to handle the amount of composite materials being employed in aviation. Moreover, there is a clear discontinuity between the developments in the usage of composites and their end-of-life recycling, which can cause serious environmental and economic challenges in future years. By combining information regarding composite usage and aircraft retirements, assessing the environmental and economic implications of composite recycling as well as available techniques, and proposing pathways for improvement, this research underscores the importance of adopting sustainable practices in aviation. The findings aim to contribute to the development of a circular economy within the aerospace sector, ensuring the long-term viability and environmental responsibility of future composite-intensive aircraft designs. This is performed by calling for a multi-stakeholder strategy to drive recycling readiness and facilitate the evolution towards a circular economy in aviation, leading to more sustainable design, production, and dismantlement of aircraft in the future. Full article
(This article belongs to the Section Composites Applications)
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18 pages, 4673 KB  
Article
Influence of Electrical Parameters in a Composite Wing Actuated by Shape Memory Alloys Wires: A Numerical–Experimental Study
by Miriam Battaglia, Valerio Acanfora and Aniello Riccio
J. Compos. Sci. 2025, 9(9), 460; https://doi.org/10.3390/jcs9090460 - 1 Sep 2025
Viewed by 1091
Abstract
This study investigates the influence of electrical actuation parameters on the performance of a morphing composite aerodynamic profile actuated by Shape Memory Alloy (SMA) wires. A fully coupled electro-thermo-mechanical finite element model has been developed to simulate the transient response of NiTi SMA, [...] Read more.
This study investigates the influence of electrical actuation parameters on the performance of a morphing composite aerodynamic profile actuated by Shape Memory Alloy (SMA) wires. A fully coupled electro-thermo-mechanical finite element model has been developed to simulate the transient response of NiTi SMA, capturing the nonlinear interplay between temperature evolution, phase transformation, and mechanical deformation under Joule heating. The model incorporates phase-dependent material properties, heat effects, and geometric constraints, enabling accurate prediction of actuation dynamics. To validate the model, a morphing spoiler prototype has been fabricated using high-performance additive manufacturing with a carbon fibre-reinforced polymer. The SMA wires have been pretensioned and electrically actuated at different current levels (3 A and 6 A), and the resulting deformation has been recorded through video analysis with embedded timers. Experimental measurements confirmed the model’s ability to predict both actuation time and displacement, with maximum deflections of 33 mm and 40 mm corresponding to different current inputs. This integrated approach demonstrates an efficient and compact solution for active aerodynamic surfaces without the need for mechanical linkages, enabling future developments in adaptive structures for automotive and aerospace applications. Full article
(This article belongs to the Special Issue Metal Composites, Volume II)
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26 pages, 6652 KB  
Article
Advancing the Capability of Additively Manufactured Continuous Fibre-Reinforced Polymers for Structural Applications: The Effect of Nitrogen-Purging and Post-Annealing on the Tensile Performance
by Zizhao Peng, Jiahui Li, Yvonne Durandet, Antonella Sola, Adrian Trinchi, Phuong Tran, Wei Gao, Xuemei Liu and Dong Ruan
Polymers 2025, 17(17), 2314; https://doi.org/10.3390/polym17172314 - 27 Aug 2025
Viewed by 972
Abstract
Additively manufactured continuous fibre-reinforced polymers (CFRPs) offer promising mechanical properties for engineering applications, including aerospace and automotive load-bearing structures. However, challenges such as weak interlayer bonding and low strength compared to traditional composites remain. This paper presents an experimental investigation into the effects [...] Read more.
Additively manufactured continuous fibre-reinforced polymers (CFRPs) offer promising mechanical properties for engineering applications, including aerospace and automotive load-bearing structures. However, challenges such as weak interlayer bonding and low strength compared to traditional composites remain. This paper presents an experimental investigation into the effects of nitrogen (N2) purging during printing and thermal annealing after printing on the tensile performance of additively manufactured CFRPs. Tensile tests were conducted on Onyx specimens produced by material extrusion and reinforced with continuous carbon fibre filaments (CFF), glass fibre filaments (GFF), or Kevlar fibre filaments (KFF). Results showed that N2-purging and post-annealing had different effects on the tensile properties of various CFRPs. Particularly, N2-purging, post-annealing, and their combination enhanced both the Young’s modulus and ultimate tensile strength (UTS) of KFF/Onyx specimens. For GFF/Onyx specimens, both treatments had a minor effect on the Young’s modulus but enhanced UTS. CFF/Onyx specimens exhibited improved Young’s modulus with N2-purging, while both treatments reduced UTS. The different response of the CFRPs was associated with diverse governing failure mechanisms, as proved by microstructural and fracture surface inspection. Additionally, differential scanning calorimetry (DSC) and X-ray diffraction (XRD) analyses also revealed the thermal behaviour and crystal structures that influence the mechanical properties of CFRPs. Full article
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20 pages, 4388 KB  
Article
Investigation of Cryogenic Mechanical Performance of Epoxy Resin and Carbon Fibre-Reinforced Polymer Composites for Cryo-Compressed Hydrogen Storage Onboard Gas Vessels
by Liangliang Qi, Keqing Wang, Zhoutian Ge, Zhuangzhuang Cao, Peiyu Hu, Yuhang He, Sohail Yasin and Jianfeng Shi
Polymers 2025, 17(17), 2296; https://doi.org/10.3390/polym17172296 - 25 Aug 2025
Cited by 1 | Viewed by 1185
Abstract
To address the brittle matrix failure frequently observed in filament-wound composite layers of onboard pressure vessels operating under cryogenic and high-pressure conditions, we studied a bisphenol-A epoxy resin (DGEBA) system modified with polyetheramine (T5000) and 3,4-Epoxycyclohexylmethyl 3′,4′-epoxycyclohexanecarboxylate (CY179). The curing and rheological behavior [...] Read more.
To address the brittle matrix failure frequently observed in filament-wound composite layers of onboard pressure vessels operating under cryogenic and high-pressure conditions, we studied a bisphenol-A epoxy resin (DGEBA) system modified with polyetheramine (T5000) and 3,4-Epoxycyclohexylmethyl 3′,4′-epoxycyclohexanecarboxylate (CY179). The curing and rheological behavior of the modified resin were first evaluated, revealing a favorable processing, with viscosity suitable for wet-filament winding. Subsequently, its coefficient of thermal expansion (CTE) and tensile properties were characterized over the 300 K–90 K range, demonstrating a linear increase in elastic modulus and tensile strength with decreasing temperature. Carbon fibre-reinforced polymer composites (CFRP) were then fabricated using this resin system, and both longitudinal and transverse tensile tests, along with microscopic fracture surface analyses, were conducted. The results showed that CFRP-0° specimens exhibited an initial increase followed by a decrease in elastic modulus with decreasing temperature, whereas CFRP-90° specimens demonstrated pronounced cryogenic strengthening, with tensile strength and modulus enhanced by 52.2% and 82.4%, respectively. The findings provide comprehensive properties for the studied resin system and its CFRP under room temperature (RT) to cryogenic conditions, offering a basis for the design and engineering of cryo-compressed hydrogen storage vessels. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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22 pages, 2499 KB  
Article
Low-Power Vibrothermography for Detecting Barely Visible Impact Damage in CFRP Laminates: A Comparative Imaging Study
by Zulham Hidayat, Muhammet Ebubekir Torbali, Nicolas P. Avdelidis and Henrique Fernandes
Appl. Sci. 2025, 15(15), 8514; https://doi.org/10.3390/app15158514 - 31 Jul 2025
Cited by 1 | Viewed by 649
Abstract
This study explores the application of low-power vibrothermography (LVT) for detecting barely visible impact damage (BVID) in carbon fibre-reinforced polymer (CFRP) laminates. Composite specimens with varying impact energies (2.5–20 J) were excited using a single piezoelectric transducer with a nominal centre frequency of [...] Read more.
This study explores the application of low-power vibrothermography (LVT) for detecting barely visible impact damage (BVID) in carbon fibre-reinforced polymer (CFRP) laminates. Composite specimens with varying impact energies (2.5–20 J) were excited using a single piezoelectric transducer with a nominal centre frequency of 28 kHz, operated at a fixed excitation frequency of 28 kHz. Thermal data were captured using an infrared camera. To enhance defect visibility and suppress background noise, the raw thermal sequences were processed using principal component analysis (PCA) and robust principal component analysis (RPCA). In LVT, RPCA and PCA provided comparable signal-to-noise ratios (SNR), with no consistent advantage for either method across all cases. In contrast, for pulsed thermography (PT) data, RPCA consistently resulted in higher SNR values, except for one sample. The LVT results were further validated by comparison with PT and phased array ultrasonic testing (PAUT) data to confirm the location and shape of detected damage. These findings demonstrate that LVT, when combined with PCA or RPCA, offers a reliable method for identifying BVID and can support safer, more efficient structural health monitoring of composite materials. Full article
(This article belongs to the Special Issue Application of Acoustics as a Structural Health Monitoring Technology)
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22 pages, 7286 KB  
Article
Enhancing Mechanical Properties of Three-Dimensional Cementitious Composites Through 3 mm Short Fibre Systems: Single and Hybrid Types
by Han Yao, Yujie Cao, Yangling Mei and Zhixuan Xiong
Buildings 2025, 15(14), 2519; https://doi.org/10.3390/buildings15142519 - 18 Jul 2025
Viewed by 1100
Abstract
Three-dimensionally printed cement-based composites emerge as a research hotspot in the fields of construction engineering in recent years. Current research primarily focuses on the reinforcement mechanisms of individually incorporated fibres, while a significant gap remains in the synergistic effects of hybrid fibre systems. [...] Read more.
Three-dimensionally printed cement-based composites emerge as a research hotspot in the fields of construction engineering in recent years. Current research primarily focuses on the reinforcement mechanisms of individually incorporated fibres, while a significant gap remains in the synergistic effects of hybrid fibre systems. This study investigates the effects of mono-doping (0.2 wt.% and 0.4 wt.% by the mass of the cement) and hybrid-doping (0.1 wt.% + 0.1 wt.% by the mass of the cement) with 3 mm polypropylene, basalt, and carbon fibres on the fresh-state properties and mechanical behaviours. Through quantitative characterisation of the flowability and mechanical performance of short-fibre-reinforced 3D-printed cementitious composites (SFR3DPC), coupled with comprehensive testing including digital image correlation, X-ray diffraction, and scanning electron microscopy, several key findings are obtained. The experimental results indicate that the addition of excess fibres reduces fluidity, which affects the mechanical performance and make the anisotropy of the composites more pronounced. While the single addition of 0.2 wt.% CF shows the most significant improvement in flexural and compressive strengths, the hybrid combination of 0.1 wt.% CF and 0.1 wt.% BF shows the greatest increase in interlayer bond strength by 26.7%. The complementary effect of the hybrid fibres contributes to the damage mode of the composites from brittle fracture to quasi-brittle behaviour at the physical level. These findings offer valuable insights into optimising the mechanical performance and improving defects of 3D-printed cementitious composites with short fibres. Full article
(This article belongs to the Special Issue Advanced Research on Cementitious Composites for Construction)
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