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Search Results (1,083)

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Keywords = aluminum/steel

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16 pages, 8293 KiB  
Article
Thermodynamic Modeling of Microstructural Design of Lightweight Ferritic Steels
by Tamiru Hailu Kori, Adam Skowronek, Jarosław Opara, Ana Paula Domingos Cardoso and Adam Grajcar
Metals 2025, 15(8), 912; https://doi.org/10.3390/met15080912 (registering DOI) - 16 Aug 2025
Abstract
Ferritic lightweight steels are an emerging class of low-density steels (LDSs) with promising mechanical properties. The study aimed to develop two ferritic lightweight steels with different Mn concentrations. Al was incorporated to achieve the lightweighting effect due to its relatively low atomic mass [...] Read more.
Ferritic lightweight steels are an emerging class of low-density steels (LDSs) with promising mechanical properties. The study aimed to develop two ferritic lightweight steels with different Mn concentrations. Al was incorporated to achieve the lightweighting effect due to its relatively low atomic mass of substitutional solutions. The C concentration was kept at a minimum level to avoid the precipitation of carbides and the Mn addition was intended to increase solid solution strengthening. Thermodynamic calculations (Thermo-Calc) were employed to design the composition, analyze the phase constituents, and predict the phase transformation behavior. Microstructural investigation and hardness tests were conducted to experimentally verify the calculations. Both produced alloys exhibited a fully ferritic microstructure. Compared to industrially produced DP980 steel, a density reduction of about 7.2% and 8.3% was attained for the Fe-0.04C-5.5Al-1.6Mn-0.075Nb and Fe-0.04C-5.6Al-5.5Mn-0.08Nb steels, respectively. The steel with the higher Mn content showed increased hardness attributed to its solution strengthening effect. An increase in the hardness values was also measured with the progress in hot-rolling thickness reductions for both alloys. The alloying elements influenced the microstructural characteristics, phase transformation behavior, density, and hardness of the newly designed lightweight steels. Full article
(This article belongs to the Special Issue Thermodynamic Modeling of Phase Equilibrium in Metallic Materials)
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14 pages, 3371 KiB  
Article
Development of a Molding Mixture for the Production of Large-Sized Casting Molds
by Vitaly Kulikov, Aristotel Issagulov, Pavel Kovalev, Svetlana Kvon, Igor Matveev and Saniya Arinova
J. Compos. Sci. 2025, 9(8), 436; https://doi.org/10.3390/jcs9080436 - 13 Aug 2025
Viewed by 182
Abstract
This study presents the results of research on the use of Portland cement as a binder for producing semi-permanent molds intended for large-scale castings made from complex alloyed steels. Based on the conducted experiments, the optimal composition of a molding mixture based on [...] Read more.
This study presents the results of research on the use of Portland cement as a binder for producing semi-permanent molds intended for large-scale castings made from complex alloyed steels. Based on the conducted experiments, the optimal composition of a molding mixture based on Portland cement was determined to manufacture large molds with high operational performance. The technological properties of the mixtures were investigated, focusing on the flowability, sedimentation stability, and strength after curing. The recommended mixture composition is as follows: Portland cement—18.75%; sand—56.5%; quartz powder—25%; water—25%. To accelerate the hardening process, the use of curing accelerators is advised. The most effective additives are a 9% aluminum nitrate solution at 0.6–1.5% by weight or sodium aluminate at 3–4%. This composition ensures the required strength within a short curing time. A specific thermal treatment regime is also recommended to further stabilize the mold structure: heating to 450 °C at a rate of 75 °C per hour, holding for 2 h, followed by controlled cooling together with the furnace. Full article
(This article belongs to the Section Composites Applications)
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13 pages, 837 KiB  
Article
Comparison of Gait Characteristics for Horses Without Shoes, with Steel Shoes, and with Aluminum Shoes
by Katherine Gottleib, Lauren Trager-Burns, Amy Santonastaso, Sophie Bogers, Stephen Werre, Travis Burns and Christopher Byron
Animals 2025, 15(16), 2376; https://doi.org/10.3390/ani15162376 - 13 Aug 2025
Viewed by 173
Abstract
Differences in horseshoe materials may have effects on gait that could change perceived esthetic qualities. Objective information regarding effects of shoeing on gait characteristics of horses is scant. The aim of this study was to determine differences in gait characteristics for horses under [...] Read more.
Differences in horseshoe materials may have effects on gait that could change perceived esthetic qualities. Objective information regarding effects of shoeing on gait characteristics of horses is scant. The aim of this study was to determine differences in gait characteristics for horses under various experimental shoeing conditions (barefoot, aluminum shoes, steel shoes) on two surfaces (asphalt and soft footing) using body- and hoof-mounted sensors. We hypothesized that shoeing would affect hoof arc height during early (arc height a) and late (arc height b) swing phases but would not affect other gait variables. Twelve healthy, adult, client-owned horses were evaluated at a trot on asphalt and soft footing under the three experimental shoeing conditions. No significant (p < 0.05) effects of shoeing were detected for gait symmetry (Q score), mediolateral hoof deviation, stride length, or midstance, breakover, swing, and landing stride phase times. Hoof arc height a was significantly (p < 0.001) lower for aluminum versus steel shoes for right and left forelimbs on asphalt and soft footing. Hoof arc height b was significantly higher for aluminum versus steel shoes on soft footing for left (p < 0.001) and right (p = 0.02) forelimbs. Findings indicate that shoe weights affect early and late swing phase hoof heights differently. Further investigation is warranted to determine whether measured hoof arc height changes affect subjective esthetics of gait. Full article
(This article belongs to the Section Equids)
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33 pages, 13337 KiB  
Article
Machinability of Basalt and Glass Fiber Hybrid Composites in Dry Drilling Using TiN/TiAlN-Coated Drill Bits
by Mehmet İskender Özsoy, Satılmış Ürgün, Sinan Fidan, Eser Yarar, Erman Güleç and Mustafa Özgür Bora
Polymers 2025, 17(16), 2172; https://doi.org/10.3390/polym17162172 - 8 Aug 2025
Viewed by 318
Abstract
Drilling-induced damage in fiber-reinforced polymer composite materials was measured excavating four laminates, basalt (B14), glass (G14) and their two sandwich type hybrids (B4G6B4, G4B6G4), with 6 mm [...] Read more.
Drilling-induced damage in fiber-reinforced polymer composite materials was measured excavating four laminates, basalt (B14), glass (G14) and their two sandwich type hybrids (B4G6B4, G4B6G4), with 6 mm twist drills at 1520 revolutions per minute and 0.10 mm rev−1 under dry running with an uncoated high-speed steel (HSS-R), grind-coated high-speed steel (HSS-G) or physical vapor deposition-coated (high-speed steel coated with Titanium Nitride (TiN) and Titanium Aluminum Nitride (TiAlN)) drill bits. The hybrid sheets were deliberately incorporated to clarify how alternating basalt–glass architectures redistribute interlaminar stresses during drilling, while the hard, low-friction TiN and TiAlN ceramic coatings enhance cutting performance by forming a heat-resistant tribological barrier that lowers tool–workpiece adhesion, reduces interface temperature, and thereby suppresses thrust-induced delamination. Replacement of an uncoated, grind-coated, high-speed-steel drill (HSS-G) with the latter coats lowered the mechanical and thermal loads substantially: mean thrust fell from 79–94 N to 24–30 N, and peak workpiece temperatures from 112 °C to 74 °C. Accordingly, entry/exit oversize fell from 2.5–4.7% to under 0.6% and, from the surface, the SEM image displayed clean fiber severance rather than pull-out and matrix smear. By analysis of variance (ANOVA), 92.7% of the variance of thrust and 86.6% of that of temperature could be accounted for by the drill-bit factor, thus confirming that the coatings overwhelm the laminate structure and hybrid stacking simply redistribute, but cannot overcome, the former influence. Regression models and an artificial neural network optimized via meta-heuristic optimization foretold thrust, temperature and delamination with an R2 value of 0.94 or higher, providing an instant-screening device with which to explore industrial application. The work reveals TiAlN- and TiN-coated drills as financially competitive alternatives with which to achieve ±1% dimensional accuracy and minimum subsurface damage during multi-material composite machining. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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25 pages, 2697 KiB  
Article
Thermal Performance Comparison of Working Fluids for Geothermal Snow Melting with Gravitational Heat Pipe
by Wenwen Cui, Yutong Chai, Soheil Asgarpour and Shunde Yin
Fluids 2025, 10(8), 209; https://doi.org/10.3390/fluids10080209 - 8 Aug 2025
Viewed by 269
Abstract
Snow and ice accumulation on transportation infrastructure presents significant safety and maintenance challenges in cold regions, while conventional removal methods are both energy-intensive and environmentally detrimental. This study proposes a passive Heat Pipe–Coupled Geothermal Snow Melting System (HP-GSMS) that harnesses shallow geothermal energy [...] Read more.
Snow and ice accumulation on transportation infrastructure presents significant safety and maintenance challenges in cold regions, while conventional removal methods are both energy-intensive and environmentally detrimental. This study proposes a passive Heat Pipe–Coupled Geothermal Snow Melting System (HP-GSMS) that harnesses shallow geothermal energy to maintain snow-free surfaces without external energy input. Using Fluent-based CFD simulations, the system’s thermal performance was evaluated under various working fluids (ammonia, carbon dioxide, water) and pipe materials (stainless steel, aluminum). A one-dimensional thermal resistance model validated the CFD results under ammonia–stainless steel conditions, predicting a heat flux of 358.6 W/m2 compared to 361.0 W/m2 from the simulation, with a deviation of only 0.66%, confirming model accuracy. Ammonia demonstrated superior phase-change efficiency, with the aluminum–ammonia configuration yielding the highest heat flux (up to 677 W/m2), surpassing typical snow-melting thresholds. Aluminum pipes enhanced radial heat conduction without compromising phase stability, while water exhibited poor phase-change performance and CO2 showed moderate but stable behavior. Additionally, a dynamic three-node RC thermal network was employed to assess transient performance under realistic diurnal temperature variations, revealing surface heat fluxes ranging from 230 to 460 W/m2, with a daily average of approximately 340 W/m2. These findings demonstrate the HP-GSMS’s practical viability in cold climates and underscore the importance of selecting low-boiling-point fluids and high-conductivity materials for scalable, energy-efficient, and low-carbon snow-melting applications in urban infrastructure. Full article
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14 pages, 2146 KiB  
Article
Method for Determining the Contact and Bulk Resistance of Aluminum Alloys in the Initial State for Resistance Spot Welding
by Andreas Fezer, Stefan Weihe and Martin Werz
J. Manuf. Mater. Process. 2025, 9(8), 266; https://doi.org/10.3390/jmmp9080266 - 7 Aug 2025
Viewed by 262
Abstract
In resistance spot welding (RSW), the total electrical resistance (dynamic resistance) as the sum of bulk and contact resistance is a key variable. Both of these respective resistances influence the welding result, but the exact ratio to the total resistance of a real [...] Read more.
In resistance spot welding (RSW), the total electrical resistance (dynamic resistance) as the sum of bulk and contact resistance is a key variable. Both of these respective resistances influence the welding result, but the exact ratio to the total resistance of a real existing sheet is not known. Due to the high scatter in the RSW of aluminum alloys compared to steel, it is of interest to be able to explicitly determine the individual resistance components in order to gain a better understanding of the relationship between the initial state and the lower reproducibility of aluminum welding in the future. So far, only the total resistance and the bulk resistance could be determined experimentally. Due to the different sample shapes, it was not possible to consistently determine the contact resistance from the measurements. In order to realize this, a method was developed that contains the following innovations with the aid of simulation: determination of the absolute bulk resistance at room temperature (RT), determination of the absolute contact resistance at RT and determination of the ratio of bulk and contact resistance. This method makes it possible to compare the resistances of the bulk material and the surface in the initial state quantitatively. This now allows the comparison of batches regarding the surface resistance, especially for welding processes. For the aluminum sheets (EN AW-5182-O, EN AW-6014-T4) investigated, the method showed that the contact resistance dominates and the bulk resistance is less than 20%. These data can also be used to make predictions about the weldability of the alloy using artificial intelligence (AI). If experimental data are available, the method can also be applied to higher temperatures. Full article
(This article belongs to the Special Issue Recent Advances in Welding and Joining Metallic Materials)
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12 pages, 4963 KiB  
Article
Effect of Bias Voltage and Cr/Al Content on the Mechanical and Scratch Resistance Properties of CrAlN Coatings Deposited by DC Magnetron Sputtering
by Shahnawaz Alam, Zuhair M. Gasem, Nestor K. Ankah and Akbar Niaz
J. Manuf. Mater. Process. 2025, 9(8), 264; https://doi.org/10.3390/jmmp9080264 - 6 Aug 2025
Viewed by 240
Abstract
Chromium–aluminum nitride (CrAlN) coatings were deposited on polished H13 tool steel substrates using direct current (DC) magnetron sputtering. The Cr/Al composition in the target was varied by inserting either four or eight chromium (Cr) plugs into cavities machined into an aluminum (Al) plate [...] Read more.
Chromium–aluminum nitride (CrAlN) coatings were deposited on polished H13 tool steel substrates using direct current (DC) magnetron sputtering. The Cr/Al composition in the target was varied by inserting either four or eight chromium (Cr) plugs into cavities machined into an aluminum (Al) plate target. Nitrogen was introduced as a reactive gas to facilitate the formation of the nitride phase. Coatings were deposited at substrate bias voltages of −30 V, −50 V, and −60 V to study the combined effects of composition and ion energy on coating properties. Compositional analysis of coatings deposited at a −50 V bias revealed Cr/Al ratios of approximately 0.8 and 1.7 for the 4- and 8-plug configurations, respectively. This increase in the Cr/Al ratio led to a 2.6-fold improvement in coating hardness. Coatings produced using the eight-Cr-plug target exhibited a nearly linear increase in hardness with increasing substrate bias voltage. Cross-sectional scanning electron microscopy revealed a uniform bilayer structure consisting of an approximately 0.5 µm metal interlayer beneath a 2–3 µm CrAlN coating. Surface morphology analysis indicated the presence of coarse microdroplets in coatings with the lower Cr/Al ratio. These microdroplets were significantly suppressed in coatings with higher Cr/Al content, especially at increased bias voltages. This suppression is likely due to enhanced ion bombardment associated with the increased Cr content, attributed to Cr’s relatively higher atomic mass compared to Al. Coatings with lower hardness exhibited greater scratch resistance, likely due to the influence of residual compressive stresses. The findings highlight the critical role of both Cr/Al content and substrate bias in tailoring the tribo-mechanical performance of PVD CrAlN coatings for wear-resistant applications. Full article
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16 pages, 7134 KiB  
Article
The Impact of an Object’s Surface Material and Preparatory Actions on the Accuracy of Optical Coordinate Measurement
by Danuta Owczarek, Ksenia Ostrowska, Jerzy Sładek, Adam Gąska, Wiktor Harmatys, Krzysztof Tomczyk, Danijela Ignjatović and Marek Sieja
Materials 2025, 18(15), 3693; https://doi.org/10.3390/ma18153693 - 6 Aug 2025
Viewed by 359
Abstract
Optical coordinate measurement is a universal technique that aligns with the rapid development of industrial technologies and new materials. Nevertheless, can this technique be consistently effective when applied to the precise measurement of all types of materials? As shown in this article, an [...] Read more.
Optical coordinate measurement is a universal technique that aligns with the rapid development of industrial technologies and new materials. Nevertheless, can this technique be consistently effective when applied to the precise measurement of all types of materials? As shown in this article, an analysis of optical measurement systems reveals that some materials cause difficulties during the scanning process. This article details the matting process, resulting, as demonstrated, in lower measurement uncertainty values compared to the pre-matting state, and identifies materials for which applying a matting spray significantly improves the measurement quality. The authors propose a classification of materials into easy-to-scan and hard-to-scan groups, along with specific procedures to improve measurements, especially for the latter. Tests were conducted in an accredited Laboratory of Coordinate Metrology using an articulated arm with a laser probe. Measured objects included spheres made of ceramic, tungsten carbide (including a matte finish), aluminum oxide, titanium nitride-coated steel, and photopolymer resin, with reference diameters established by a high-precision Leitz PMM 12106 coordinate measuring machine. Diameters were determined from point clouds obtained via optical measurements using the best-fit method, both before and after matting. Color measurements using a spectrocolorimeter supplemented this study to assess the effect of matting on surface color. The results revealed correlations between the material type and measurement accuracy. Full article
(This article belongs to the Section Optical and Photonic Materials)
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17 pages, 6882 KiB  
Article
Development and Evaluation of a Solar Milk Pasteurizer for the Savanna Ecological Zones of West Africa
by Iddrisu Ibrahim, Paul Tengey, Kelci Mikayla Lawrence, Joseph Atia Ayariga, Fortune Akabanda, Grace Yawa Aduve, Junhuan Xu, Robertson K. Boakai, Olufemi S. Ajayi and James Owusu-Kwarteng
Solar 2025, 5(3), 38; https://doi.org/10.3390/solar5030038 - 4 Aug 2025
Viewed by 316
Abstract
In many developing African countries, milk safety is often managed through traditional methods such as fermentation or boiling over firewood. While these approaches reduce some microbial risks, they present critical limitations. Firewood dependency contributes to deforestation, depletion of agricultural residues, and loss of [...] Read more.
In many developing African countries, milk safety is often managed through traditional methods such as fermentation or boiling over firewood. While these approaches reduce some microbial risks, they present critical limitations. Firewood dependency contributes to deforestation, depletion of agricultural residues, and loss of soil fertility, which, in turn, compromise environmental health and food security. Solar pasteurization provides a reliable and sustainable method for thermally inactivating pathogenic microorganisms in milk and other perishable foods at sub-boiling temperatures, preserving its nutritional quality. This study aimed to evaluate the thermal and microbial performance of a low-cost solar milk pasteurization system, hypothesized to effectively reduce microbial contaminants and retain milk quality under natural sunlight. The system was constructed using locally available materials and tailored to the climatic conditions of the Savanna ecological zone in West Africa. A flat-plate glass solar collector was integrated with a 0.15 cm thick stainless steel cylindrical milk vat, featuring a 2.2 cm hot water jacket and 0.5 cm thick aluminum foil insulation. The system was tested in Navrongo, Ghana, under ambient temperatures ranging from 30 °C to 43 °C. The pasteurizer successfully processed up to 8 L of milk per batch, achieving a maximum milk temperature of 74 °C by 14:00 GMT. Microbial analysis revealed a significant reduction in bacterial load, from 6.6 × 106 CFU/mL to 1.0 × 102 CFU/mL, with complete elimination of coliforms. These results confirmed the device’s effectiveness in achieving safe pasteurization levels. The findings demonstrate that this locally built solar pasteurization system is a viable and cost-effective solution for improving milk safety in arid, electricity-limited regions. Its potential scalability also opens avenues for rural entrepreneurship in solar-powered food and water treatment technologies. Full article
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20 pages, 9479 KiB  
Article
Clinch-Bonding Process for Ultra-High-Strength Steel and A5052 Aluminum Alloy Sheets
by Yohei Abe, Yu Tatara, Takahiro Hosokawa and Ryoto Yamauchi
Materials 2025, 18(15), 3556; https://doi.org/10.3390/ma18153556 - 29 Jul 2025
Viewed by 231
Abstract
Initially, the effects of sheet combinations for joining two sheets, including 780 MPa steel and A5052 aluminum alloy sheets, on the joined cross-sectional shapes of the sheets in a clinch-bonding process and the tension-shear load of joined sheets were investigated. The effect of [...] Read more.
Initially, the effects of sheet combinations for joining two sheets, including 780 MPa steel and A5052 aluminum alloy sheets, on the joined cross-sectional shapes of the sheets in a clinch-bonding process and the tension-shear load of joined sheets were investigated. The effect of an adhesive on the amounts of the interlock and the minimum thickness in the upper sheet was not large, whereas the effect of the sheet combination was observed. Subsequently, for joining the upper 980 MPa ultra-high-strength steel and lower aluminum alloy sheets in the clinch-bonding process, the effects of the die shape, punch velocity, and sheet holding force on the joinability were investigated. As a result, defect-free conditions were narrowly constrained. Finally, a method that involved controlling material flow using an adhesive with fine particles to increase friction between the sheets was introduced. The upper 980 MPa steel and lower aluminum alloy sheets were successfully joined using this approach. Full article
(This article belongs to the Section Metals and Alloys)
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18 pages, 6570 KiB  
Article
Deposition Process and Interface Performance of Aluminum–Steel Joints Prepared Using CMT Technology
by Jie Zhang, Hao Du, Xinyue Wang, Yinglong Zhang, Jipeng Zhao, Penglin Zhang, Jiankang Huang and Ding Fan
Metals 2025, 15(8), 844; https://doi.org/10.3390/met15080844 - 29 Jul 2025
Viewed by 329
Abstract
The anode assembly, as a key component in the electrolytic aluminum process, is composed of steel claws and aluminum guide rods. The connection quality between the steel claws and guide rods directly affects the current conduction efficiency, energy consumption, and operational stability of [...] Read more.
The anode assembly, as a key component in the electrolytic aluminum process, is composed of steel claws and aluminum guide rods. The connection quality between the steel claws and guide rods directly affects the current conduction efficiency, energy consumption, and operational stability of equipment. Achieving high-quality joining between the aluminum alloy and steel has become a key process in the preparation of the anode assembly. To join the guide rods and steel claws, this work uses Cold Metal Transfer (CMT) technology to clad aluminum on the steel surface and employs machine vision to detect surface forming defects in the cladding layer. The influence of different currents on the interfacial microstructure and mechanical properties of aluminum alloy cladding on the steel surface was investigated. The results show that increasing the cladding current leads to an increase in the width of the fusion line and grain size and the formation of layered Fe2Al5 intermetallic compounds (IMCs) at the interface. As the current increases from 90 A to 110 A, the thickness of the Al-Fe IMC layer increases from 1.46 μm to 2.06 μm. When the current reaches 110 A, the thickness of the interfacial brittle phase is the largest, at 2 ± 0.5 μm. The interfacial region where aluminum and steel are fused has the highest hardness, and the tensile strength first increases and then decreases with the current. The highest tensile strength is 120.45 MPa at 100 A. All the fracture surfaces exhibit a brittle fracture. Full article
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18 pages, 13429 KiB  
Article
Formation of Intermetallic Coatings on Titanium by Explosive Welding and Subsequent Heat Treatment of the Layered Metal Composite
by Artem Igorevich Bogdanov, Vitaliy Pavlovich Kulevich, Roman Evgenevich Novikov and Victor Georgievich Shmorgun
J. Compos. Sci. 2025, 9(7), 379; https://doi.org/10.3390/jcs9070379 - 21 Jul 2025
Viewed by 466
Abstract
An approach for the formation of intermetallic coatings on the titanium surface based on titanium aluminides is proposed. The approach involves producing a layered steel-aluminum-titanium metal composite via explosive welding, followed by heat treatment to form a diffusion zone at the steel–aluminum interface [...] Read more.
An approach for the formation of intermetallic coatings on the titanium surface based on titanium aluminides is proposed. The approach involves producing a layered steel-aluminum-titanium metal composite via explosive welding, followed by heat treatment to form a diffusion zone at the steel–aluminum interface with a thickness of more than 30 μm, sufficient for the spontaneous separation of the steel layer. As a result, an aluminum layer approximately 0.3 mm thick remains on the titanium surface. Subsequent heating at temperatures of 700–850 °C, below the allotropic transformation temperature of titanium, results in the transformation of the aluminum layer into titanium aluminides. The formation of the intermetallic coating structure occurs as a result of the upward transportation of TiAl3 fragments separated from the reaction zone by circulating melt flows. With increasing heat treatment time, these fragments become separated by the Al2O3 oxide phase. Full article
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12 pages, 4677 KiB  
Article
Lap Welding of Nickel-Plated Steel and Copper Sheets Using Coaxial Laser Beams
by Kuan-Wei Su, Yi-Hsuan Chen, Hung-Yang Chu and Ren-Kae Shiue
Materials 2025, 18(14), 3407; https://doi.org/10.3390/ma18143407 - 21 Jul 2025
Viewed by 302
Abstract
The laser heterogeneous lap welding of nickel-plated steel and Cu sheets has been investigated in this study. The YAG (Yttrium-Aluminum-Garnet) laser beam only penetrates the upper Ni-plated steel sheet and cannot weld the bottom Cu sheet due to the low absorption coefficient of [...] Read more.
The laser heterogeneous lap welding of nickel-plated steel and Cu sheets has been investigated in this study. The YAG (Yttrium-Aluminum-Garnet) laser beam only penetrates the upper Ni-plated steel sheet and cannot weld the bottom Cu sheet due to the low absorption coefficient of the YAG laser beam. Incorporating a blue-light and fiber laser into the coaxial laser beam significantly improves the quality of the weld fusion zone. The fiber laser beam can penetrate the upper nickel-plated steel sheet, and the blue-light laser beam can melt the bottom copper sheet. Introducing the blue-light laser to the coaxial laser beams overcomes the low reflectivity of the bottom copper sheet. The fiber/blue-light coaxial laser continuous welding can achieve the best integrity and defect-free welding. It shows potential in the mass production of the next generation of lithium batteries. Full article
(This article belongs to the Special Issue Fusion Bonding/Welding of Metal and Non-Metallic Materials)
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19 pages, 1343 KiB  
Article
Two-Step Plasma Electrolytic Oxidation of Advanced High-Strength Steel in Aluminate and Silicate Solutions
by Roy Morgenstern, Thomas Mehner and Thomas Lampke
Coatings 2025, 15(7), 850; https://doi.org/10.3390/coatings15070850 - 19 Jul 2025
Viewed by 346
Abstract
This work aims to clarify whether the individual advantages of the two commonly used silicate- and aluminate-based electrolytes for the plasma electrolytic oxidation (PEO) of steel can be combined in a two-step process. The first PEO step was carried out in an aluminate–phosphate [...] Read more.
This work aims to clarify whether the individual advantages of the two commonly used silicate- and aluminate-based electrolytes for the plasma electrolytic oxidation (PEO) of steel can be combined in a two-step process. The first PEO step was carried out in an aluminate–phosphate electrolyte with pulsed voltage and anodic amplitudes between 150 V and 200 V. The second PEO step was carried out at an increased anodic voltage amplitude of 400 V in a silicate–phosphate electrolyte. As a reference, PEO was conducted in a single step in the same silicate–phosphate electrolyte at an increased anodic voltage amplitude of up to 400 V. The microstructural layer analysis was carried out using SEM and EDX analyses, Raman spectroscopy and XRD analysis. Heterogeneous layers containing iron oxide and iron phosphate form in the silicate–phosphate electrolyte at anodic voltage amplitudes up to 300 V by electrochemical reactions. Further increasing the anodic voltage amplitude up to 400 V results in heterogeneous layers, too. PEO in the aluminate–phosphate electrolyte at 150 V causes the formation of thin, amorphous layers mainly consisting of aluminum and iron oxides. At 200 V amplitude, a PEO layer with pronounced open porosity is formed, which primarily consists of the crystalline phases corundum and hercynite. During subsequent PEO in the silicate–phosphate electrolyte, the previously formed layers were replaced by a macroscopically homogeneous layer that is mostly nanocrystalline and may contain amorphous iron(-aluminum) phosphates and oxides as well as silicon oxide. It can be concluded that the two-step PEO process is suitable for the production of more homogeneous PEO layers. Full article
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15 pages, 4528 KiB  
Article
Changes in the Structure and Mechanical Properties of the SAV-1 Alloy and Structural Fe-Cr-Ni Steels After Long-Term Service as Core Materials in Nuclear Reactors
by Alexey Dikov, Sergey Kislitsin, Boris Ivanov, Ruslan Kiryanov and Egor Maksimkin
Materials 2025, 18(14), 3391; https://doi.org/10.3390/ma18143391 - 19 Jul 2025
Viewed by 303
Abstract
This article presents the results of studies of the degradation of the structure and mechanical properties of the core materials BN-350 fast neutron and research WWR-K reactors required to justify the service life extension of early-generation power and research reactors. Extending the service [...] Read more.
This article presents the results of studies of the degradation of the structure and mechanical properties of the core materials BN-350 fast neutron and research WWR-K reactors required to justify the service life extension of early-generation power and research reactors. Extending the service life of nuclear reactors is a modern problem, since most operating reactors are early-generation reactors that have exhausted their design lifespan. The possibility of extending the service life is largely determined by the condition of the structural materials of the nuclear facility, i.e., their residual resources must ensure safe operation of the reactor. For the SAV-1 alloy, the structural material of the WWR-K reactor, studies were conducted on witness samples which were in the active zone during its operation for 56 years. It was found that yield strength and tensile strength of the irradiated SAV-1 alloy decreased by 24–48%, and relative elongation decreased by ~2% compared to the unirradiated alloy. Inside the grains and along their boundaries, there were particles of secondary phases enriched with silicon, which is typical for aged aluminum alloys. For irradiated structural steels of power reactors, studied at 350–450 C, hardening and a damping nature of creep were revealed, caused by dispersion hardening and the Hall–Petch effect. Full article
(This article belongs to the Section Energy Materials)
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