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Open AccessArticle

Facile Fabrication of [email protected] Nanoparticles as Recyclable Nanocatalyst for Acylation of Amines in Water

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College of Petroleum Chemical Industry, Changzhou University, Changzhou 213164, China
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College of Biology and Environmental Engineering, Zhejiang Shuren University, Hangzhou 310015, China
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Authors to whom correspondence should be addressed.
Catalysts 2020, 10(2), 230; https://doi.org/10.3390/catal10020230
Received: 30 December 2019 / Revised: 13 February 2020 / Accepted: 13 February 2020 / Published: 14 February 2020
(This article belongs to the Section Nanostructured Catalysts)
In this report, novel [email protected] nanoparticles (GPT-Ni) were successfully prepared via click chemistry and were fully characterized by various spectroscopy measurements. The as-prepared catalysts could be used as a recyclable catalyst for the catalytic acylation of amines by employing N,N-dimethylacetamide (DMA), N,N-dimethylpropionamide (DMP), and N,N-dimethylformamide (DMF) as acylation reagents in water, providing the corresponding amides in good yields. The practicability of this methodology is highlighted by the good recyclability of the catalyst. A unique mechanism was proposed for the catalytic process. View Full-Text
Keywords: glycosylpyridyl-triazole; nickel nanoparticles; nanocatalyst; acylation of amines glycosylpyridyl-triazole; nickel nanoparticles; nanocatalyst; acylation of amines
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MDPI and ACS Style

Lin, Z.; Jin, J.; Qiao, J.; Tong, J.; Shen, C. Facile Fabrication of [email protected] Nanoparticles as Recyclable Nanocatalyst for Acylation of Amines in Water. Catalysts 2020, 10, 230.

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