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2,9-Dimethyl-11-(3-pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphepine 11-oxide

Department of Industrial Chemistry “Toso Montanari”, Alma Mater Studiorum-University of Bologna, Viale del Risorgimento 4, 40136 Bologna, Italy
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Molbank 2020, 2020(1), M1109; https://doi.org/10.3390/M1109
Received: 15 November 2019 / Revised: 9 January 2020 / Accepted: 13 January 2020 / Published: 14 January 2020
2,9-Dimethyl-11-(3-pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphepine 11-oxide was synthesized (yield 50%) by a two-step procedure. The first step starts with a benzothiadiphosphole and bis-Grignard reagent, and the second step consists of adding the sodium salt of a derivative of cardanol. The structure of newly synthesized compound was elucidated based on 1H-NMR, 13C-NMR, 31P-NMR, IR, Electron Spray Ionization (ESI)–MS, Gas Chromatography-Mass Spectroscopy (GC–MS), and Electron Spray Ionization-High Resolution Mass Spectroscopy (ESI–HRMS).
Keywords: cardanol; benzothiadiphosphole; polydentate ligand cardanol; benzothiadiphosphole; polydentate ligand
MDPI and ACS Style

Micheletti, G.; Mazzacurati, M.; Telese, D.; Boga, C. 2,9-Dimethyl-11-(3-pentadecylphenoxy)dibenzo[c,f][1,2,5]dithiaphosphepine 11-oxide. Molbank 2020, 2020, M1109.

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