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Search Results (1,135)

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Keywords = ultrasonic characteristic

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14 pages, 5364 KiB  
Article
Study on the Microbial Inactivation and Quality Assurance of Ultrasonic-Assisted Slightly Acidic Electrolyzed Water for Mirror Carp (Cyprinus carpio L.) Fillets During Refrigerated Storage
by Qiang Zhong, Xiufang Xia and Fangfei Li
Foods 2025, 14(15), 2652; https://doi.org/10.3390/foods14152652 - 29 Jul 2025
Viewed by 224
Abstract
The advancement of non-thermal disinfection technologies represents a critical pathway for ensuring food safety, meeting environmental sustainability requirements, and meeting consumer preferences for clean-label products. This study systematically evaluated the combined preservation effect of ultrasonic-assisted slightly acidic electrolyzed water (US+SAEW) on mirror carp [...] Read more.
The advancement of non-thermal disinfection technologies represents a critical pathway for ensuring food safety, meeting environmental sustainability requirements, and meeting consumer preferences for clean-label products. This study systematically evaluated the combined preservation effect of ultrasonic-assisted slightly acidic electrolyzed water (US+SAEW) on mirror carp fillets during refrigeration. Results demonstrated that US+SAEW exhibited superior antimicrobial efficacy compared to individual US or SAEW, achieving reductions of 0.73, 0.74, and 0.79 log CFU/g in total viable counts (TVC), Aeromonas bacteria, and lactic acid bacteria counts compared to the control, respectively. Furthermore, the combined intervention significantly suppressed microbial proliferation throughout the refrigeration period while simultaneously delaying protein and lipid degradation/oxidation induced by spoilage bacteria, thereby inhibiting the formation of alkaline nitrogenous compounds. Consequently, lower levels of pH, total volatile basic nitrogen (TVB-N), protein carbonyl, and thiobarbituric acid reactive substances (TBARS) were observed in US+SAEW compared to the other treatments. Multimodal characterization through low-field nuclear magnetic resonance (LF-NMR), texture, and color analysis confirmed that US+SAEW effectively preserved quality characteristics, extending the shelf life of mirror carp fillets by four days. This study provides a novel non-thermal preservation strategy that combines microbial safety maintenance with quality retention, offering particular advantages for thermolabile food. Full article
(This article belongs to the Special Issue Innovative Muscle Foods Preservation and Packaging Technologies)
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20 pages, 3148 KiB  
Article
Dynamic Ultrasonic Jamming via Time–Frequency Mosaic for Anti-Eavesdropping Systems
by Zichuan Yu, Lu Tang, Kai Wang, Xusheng Tang and Hongyu Ge
Electronics 2025, 14(15), 2960; https://doi.org/10.3390/electronics14152960 - 24 Jul 2025
Viewed by 194
Abstract
To combat microphone eavesdropping on devices like smartphones, ultrasonic-based methods offer promise due to human inaudibility and microphone nonlinearity. However, existing systems suffer from low jamming efficiency, poor energy utilization, and weak robustness. Based on these problems, this paper proposes a novel ultrasonic-based [...] Read more.
To combat microphone eavesdropping on devices like smartphones, ultrasonic-based methods offer promise due to human inaudibility and microphone nonlinearity. However, existing systems suffer from low jamming efficiency, poor energy utilization, and weak robustness. Based on these problems, this paper proposes a novel ultrasonic-based jamming algorithm called the Time–Frequency Mosaic (TFM) technique, which can be used for anti-eavesdropping. The proposed TFM technique can generate short-time, frequency-coded jamming signals according to the voice frequency characteristics of different speakers, thereby achieving targeted and efficient jamming. A jamming prototype using the Time–Frequency Mosaic technique was developed and tested in various scenarios. The test results show that when the signal-to-noise ratio (SNR) is lower than 0 dB, the text Word Error Rate (WER) of the proposed method is basically over 60%; when the SNR is 0 dB, the WER of the algorithm in this paper is on average more than 20% higher than that of current jamming algorithms. In addition, when the jamming system maintains the same distance from the recording device, the algorithm in this paper has higher energy utilization efficiency compared with existing algorithms. Experiments prove that in most cases, the proposed algorithm has a better jamming effect, higher energy utilization efficiency, and stronger robustness. Full article
(This article belongs to the Topic Addressing Security Issues Related to Modern Software)
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19 pages, 4649 KiB  
Article
Cavitation Erosion Performance of the INCONEL 625 Superalloy Heat-Treated via Stress-Relief Annealing
by Robert Parmanche, Olimpiu Karancsi, Ion Mitelea, Ilare Bordeașu, Corneliu Marius Crăciunescu and Ion Dragoș Uțu
Appl. Sci. 2025, 15(15), 8193; https://doi.org/10.3390/app15158193 - 23 Jul 2025
Viewed by 170
Abstract
Cavitation-induced degradation of metallic materials presents a significant challenge for engineers and users of equipment operating with high-velocity fluids. For any metallic material, the mechanical strength and ductility characteristics are controlled by the mobility of dislocations and their interaction with other defects in [...] Read more.
Cavitation-induced degradation of metallic materials presents a significant challenge for engineers and users of equipment operating with high-velocity fluids. For any metallic material, the mechanical strength and ductility characteristics are controlled by the mobility of dislocations and their interaction with other defects in the crystal lattice (such as dissolved foreign atoms, grain boundaries, phase separation surfaces, etc.). The increase in mechanical properties, and consequently the resistance to cavitation erosion, is possible through the application of heat treatments and cold plastic deformation processes. These factors induce a series of hardening mechanisms that create structural barriers limiting the mobility of dislocations. Cavitation tests involve exposing a specimen to repeated short-duration erosion cycles, followed by mass loss measurements and surface morphology examinations using optical microscopy and scanning electron microscopy (SEM). The results obtained allow for a detailed study of the actual wear processes affecting the tested material and provide a solid foundation for understanding the degradation mechanism. The tested material is the Ni-based alloy INCONEL 625, subjected to stress-relief annealing heat treatment. Experiments were conducted using an ultrasonic vibratory device operating at a frequency of 20 kHz and an amplitude of 50 µm. Microstructural analyses showed that slip bands formed due to shock wave impacts serve as preferential sites for fatigue failure of the material. Material removal occurs along these slip bands, and microjets result in pits with sizes of several micrometers. Full article
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17 pages, 3444 KiB  
Article
Multiphysics-Coupled Simulation of Ultrasound-Assisted Tailing Slurry Sedimentation
by Liang Peng and Congcong Zhao
Materials 2025, 18(15), 3430; https://doi.org/10.3390/ma18153430 - 22 Jul 2025
Viewed by 177
Abstract
This study establishes a multiphysics coupling model of acoustics, mechanics, and electrostatics through COMSOL, systematically explores the sound field distribution and stress–strain characteristics of tailing particles in sand silos under different frequencies of ultrasonic radiation, and proposes an optimization scheme for the sound [...] Read more.
This study establishes a multiphysics coupling model of acoustics, mechanics, and electrostatics through COMSOL, systematically explores the sound field distribution and stress–strain characteristics of tailing particles in sand silos under different frequencies of ultrasonic radiation, and proposes an optimization scheme for the sound field. The simulation results show that under 28 kHz ultrasonic radiation, the amplitude of sound pressure in the sand silo (173 Pa) is much lower than that at 40 kHz (1220 Pa), which can avoid damaging the original settlement mode of the tail mortar. At the same time, the periodic fluctuation amplitude of its longitudinal sound pressure is significantly greater than 25 kHz, which can promote settlement by enhancing particle tensile and compressive stress, achieving the best comprehensive effect. The staggered placement scheme of the transducer eliminates upward disturbance in the flow field by changing the longitudinal opposing sound field to oblique propagation, reduces energy dissipation, and increases the highest sound pressure level in the compartment to 130 dB. The sound pressure distribution density is significantly improved, further enhancing the settling effect. This study clarifies the correlation mechanism between ultrasound parameters and tailings’ settling efficiency, providing a theoretical basis for parameter optimization of ultrasound-assisted tailing treatment technology. Its results have important application value in the optimization of tailings settling in metal mine tailing filling. Full article
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27 pages, 4366 KiB  
Article
Fuzzy Logic-Based Optimization for Pseudocereal Processing: A Case Study on Buckwheat
by Mariana-Liliana Păcală, Anca Șipoș, Otto Ketney and Alexandrina Sîrbu
Processes 2025, 13(7), 2309; https://doi.org/10.3390/pr13072309 - 20 Jul 2025
Viewed by 471
Abstract
In response to the increasing consumer interest in the health benefits of plant-based foods, in this study, fuzzy logic modeling (FLM) was used to optimize the lactic fermentation process of several buckwheat (Fagopyrum esculentum)-based substrates (B-bSs), which were bio-prospected [...] Read more.
In response to the increasing consumer interest in the health benefits of plant-based foods, in this study, fuzzy logic modeling (FLM) was used to optimize the lactic fermentation process of several buckwheat (Fagopyrum esculentum)-based substrates (B-bSs), which were bio-prospected for the development of pseudocereal-based fermented foodstuffs. The experimental methodology involved obtaining B-bSs, either green or roasted, under various milling conditions and subjecting them to two different types of thermal treatment. This experimental design allowed us to obtain a set of experimental data, based on which a fuzzy system was developed and calibrated. The main physicochemical characteristics (pH, total titratable acidity, dynamic viscosity, and color) and sensory attributes (appearance, color, aroma, taste, texture or mouthfeel, and overall acceptability) of B-bSs were evaluated. The fuzzy logic approach proved useful for monitoring the evolution of lactic fermentation and for the rapid and accurate identification of situations that require technological interventions, acting as a reliable tool for the ongoing optimization of fermentation processes. Our study’s results showed that the optimal technological variants identified using FLM corresponded to green buckwheat milled with a 0.12 mm gap disk and a hammer mill and subjected to ultrasonic water bath treatment. The hedonic descriptive sensory evaluation also validated this conclusion. Full article
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23 pages, 6645 KiB  
Article
Encapsulation Process and Dynamic Characterization of SiC Half-Bridge Power Module: Electro-Thermal Co-Design and Experimental Validation
by Kaida Cai, Jing Xiao, Xingwei Su, Qiuhui Tang and Huayuan Deng
Micromachines 2025, 16(7), 824; https://doi.org/10.3390/mi16070824 - 19 Jul 2025
Viewed by 432
Abstract
Silicon carbide (SiC) half-bridge power modules are widely utilized in new energy power generation, electric vehicles, and industrial power supplies. To address the research gap in collaborative validation between electro-thermal coupling models and process reliability, this paper proposes a closed-loop methodology of “design-simulation-process-validation”. [...] Read more.
Silicon carbide (SiC) half-bridge power modules are widely utilized in new energy power generation, electric vehicles, and industrial power supplies. To address the research gap in collaborative validation between electro-thermal coupling models and process reliability, this paper proposes a closed-loop methodology of “design-simulation-process-validation”. This approach integrates in-depth electro-thermal simulation (LTspice XVII/COMSOL Multiphysics 6.3) with micro/nano-packaging processes (sintering/bonding). Firstly, a multifunctional double-pulse test board was designed for the dynamic characterization of SiC devices. LTspice simulations revealed the switching characteristics under an 800 V operating condition. Subsequently, a thermal simulation model was constructed in COMSOL to quantify the module junction temperature gradient (25 °C → 80 °C). Key process parameters affecting reliability were then quantified, including conductive adhesive sintering (S820-F680, 39.3 W/m·K), high-temperature baking at 175 °C, and aluminum wire bonding (15 mil wire diameter and 500 mW ultrasonic power/500 g bonding force). Finally, a double-pulse dynamic test platform was established to capture switching transient characteristics. Experimental results demonstrated the following: (1) The packaged module successfully passed the 800 V high-voltage validation. Measured drain current (4.62 A) exhibited an error of <0.65% compared to the simulated value (4.65 A). (2) The simulated junction temperature (80 °C) was significantly below the safety threshold (175 °C). (3) Microscopic examination using a Leica IVesta 3 microscope (55× magnification) confirmed the absence of voids at the sintering and bonding interfaces. (4) Frequency-dependent dynamic characterization revealed a 6 nH parasitic inductance via Ansys Q3D 2025 R1 simulation, with experimental validation at 8.3 nH through double-pulse testing. Thermal evaluations up to 200 kHz indicated 109 °C peak temperature (below 175 °C datasheet limit) and low switching losses. This work provides a critical process benchmark for the micro/nano-manufacturing of high-density SiC modules. Full article
(This article belongs to the Special Issue Recent Advances in Micro/Nanofabrication, 2nd Edition)
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22 pages, 4525 KiB  
Article
Comparison of Ultrasound-Microwave-Assisted and Hot Reflux Extractions of Polysaccharides from Alpinia officinarum Hance: Optimization, Characterization, and Antioxidant Activity
by Haibao Tang, Baogang Zhou, Mengge Sun, Yihan Wang, Ran Cheng, Tao Tan and Dongsheng Yang
Molecules 2025, 30(14), 3031; https://doi.org/10.3390/molecules30143031 - 19 Jul 2025
Viewed by 326
Abstract
Alpinia officinarum Hance exhibits various bioactivities, with polysaccharides being one of its key bioactive components. However, the relationship between the structural characteristics of these polysaccharides and their bioactivities remains unclear and underexplored. In this study, to optimize the extraction process, a Response Surface [...] Read more.
Alpinia officinarum Hance exhibits various bioactivities, with polysaccharides being one of its key bioactive components. However, the relationship between the structural characteristics of these polysaccharides and their bioactivities remains unclear and underexplored. In this study, to optimize the extraction process, a Response Surface Methodology-based design combined with single-factor experiments was applied to determine the optimal conditions for the ultrasonic-microwave-assisted extraction of polysaccharides from A. officinarum. The primary structural characteristics and antioxidant activities of two polysaccharide fractions, PAOR-1 extracted by ultrasonic-microwave-assisted extraction and PAOR-2 extracted by hot reflux extraction (HRE), were systematically compared. The optimal extraction conditions, including a liquid–solid ratio of 1:50, extraction time of 19 mins, and ultrasonic power of 410 W, yielded a maximum polysaccharide extraction rate of 18.28% ± 2.23%. The extracted polysaccharides were characterized as acidic polysaccharides with a three-dimensional structure. PAOR-1 and PAOR-2 have different monosaccharide compositions, surface morphologies, and thermal stabilities. The antioxidant activity in vitro studies suggest that PAOR-1 may have higher antioxidant activity than PAOR-2 due to its higher content of uronic acids, lower relative molecular mass, and a more closely packed spatial configuration. These findings provide a theoretical basis for the development and utilization of AOR. Full article
(This article belongs to the Collection Advances in Food Chemistry)
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17 pages, 5683 KiB  
Article
Synergistic Effect of Calcination Temperature and Silver Doping on Photocatalytic Performance of ZnO Material
by K. Kusdianto, Nurdiana Ratna Puri, Manabu Shimada, Suci Madhania and Sugeng Winardi
Materials 2025, 18(14), 3362; https://doi.org/10.3390/ma18143362 - 17 Jul 2025
Viewed by 220
Abstract
Ag-doped ZnO is a promising photocatalyst. However, the combined influence of the Ag doping concentration and furnace temperature has not been adequately explored, hindering the optimization of ZnO/Ag materials for practical applications. In this study, ZnO/Ag materials were synthesized via ultrasonic spray pyrolysis [...] Read more.
Ag-doped ZnO is a promising photocatalyst. However, the combined influence of the Ag doping concentration and furnace temperature has not been adequately explored, hindering the optimization of ZnO/Ag materials for practical applications. In this study, ZnO/Ag materials were synthesized via ultrasonic spray pyrolysis by systematically varying both the furnace calcination temperature and the Ag doping concentration. The synthesized materials were analyzed through a range of spectroscopic methods to investigate their structural, morphological, and surface characteristics. Their photocatalytic activity was assessed by monitoring the degradation of methylene blue (MB) under ultraviolet light exposure. The findings indicate that the ZnO sample that was calcined at 400 °C exhibited the highest degradation efficiency among the undoped samples, which can be attributed to its submicron particle size, moderate crystallinity, and high surface hydroxylation. The sample with 5-wt% Ag doping achieved enhanced performance, demonstrating the best photocatalytic activity (65% MB degradation). This improvement was attributed to the synergistic effects of surface plasmon resonance and optimized interaction between the Ag nanoparticles and surface hydroxyl groups. Excessive Ag loading (10 wt%) led to reduced activity owing to potential agglomeration and recombination centers. These results highlight the critical role of both the thermal and chemical parameters in tailoring ZnO-based photocatalysts for wastewater treatment applications. Full article
(This article belongs to the Section Catalytic Materials)
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18 pages, 4389 KiB  
Article
Acoustic Wave Propagation Characteristics of Maize Seed and Surrounding Region with the Double Media of Seed–Soil
by Yadong Li, Caiyun Lu, Hongwen Li, Jin He, Zhinan Wang and Chengkun Zhai
Agriculture 2025, 15(14), 1540; https://doi.org/10.3390/agriculture15141540 - 17 Jul 2025
Viewed by 334
Abstract
When monitoring seed positions in soil using ultrasonic waves, the main challenge is obtaining acoustic wave characteristics at the seed locations. This study developed a three-dimensional ultrasonic model with the double media of seed–soil using the discrete element method to visualize signal variations [...] Read more.
When monitoring seed positions in soil using ultrasonic waves, the main challenge is obtaining acoustic wave characteristics at the seed locations. This study developed a three-dimensional ultrasonic model with the double media of seed–soil using the discrete element method to visualize signal variations and analyze propagation characteristics. The effects of the compression ratio (0/6/12%), excitation frequency (20/40/60 kHz), and amplitude (5/10/15 μm) on signal variation and attenuation were analyzed. The results show consistent trends: time/frequency domain signal intensity increased with a higher compression ratio and amplitude but decreased with frequency. Comparing ultrasonic signals at soil particles before and after the seed along the propagation path shows that the seed significantly absorbs and attenuates ultrasonic waves. Time domain intensity drops 93.99%, and first and residual wave frequency peaks decrease by 88.06% and 96.39%, respectively. Additionally, comparing ultrasonic propagation velocities in the double media of seed–soil and the single soil medium reveals that the velocity in the seed is significantly higher than that in the soil. At compression ratios of 0%, 6%, and 12%, the sound velocity in the seed is 990.47%, 562.72%, and 431.34% of that in the soil, respectively. These findings help distinguish seed presence and provide a basis for ultrasonic seed position monitoring after sowing. Full article
(This article belongs to the Topic Digital Agriculture, Smart Farming and Crop Monitoring)
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29 pages, 4633 KiB  
Article
Failure Detection of Laser Welding Seam for Electric Automotive Brake Joints Based on Image Feature Extraction
by Diqing Fan, Chenjiang Yu, Ling Sha, Haifeng Zhang and Xintian Liu
Machines 2025, 13(7), 616; https://doi.org/10.3390/machines13070616 - 17 Jul 2025
Viewed by 254
Abstract
As a key component in the hydraulic brake system of automobiles, the brake joint directly affects the braking performance and driving safety of the vehicle. Therefore, improving the quality of brake joints is crucial. During the processing, due to the complexity of the [...] Read more.
As a key component in the hydraulic brake system of automobiles, the brake joint directly affects the braking performance and driving safety of the vehicle. Therefore, improving the quality of brake joints is crucial. During the processing, due to the complexity of the welding material and welding process, the weld seam is prone to various defects such as cracks, pores, undercutting, and incomplete fusion, which can weaken the joint and even lead to product failure. Traditional weld seam detection methods include destructive testing and non-destructive testing; however, destructive testing has high costs and long cycles, and non-destructive testing, such as radiographic testing and ultrasonic testing, also have problems such as high consumable costs, slow detection speed, or high requirements for operator experience. In response to these challenges, this article proposes a defect detection and classification method for laser welding seams of automotive brake joints based on machine vision inspection technology. Laser-welded automotive brake joints are subjected to weld defect detection and classification, and image processing algorithms are optimized to improve the accuracy of detection and failure analysis by utilizing the high efficiency, low cost, flexibility, and automation advantages of machine vision technology. This article first analyzes the common types of weld defects in laser welding of automotive brake joints, including craters, holes, and nibbling, and explores the causes and characteristics of these defects. Then, an image processing algorithm suitable for laser welding of automotive brake joints was studied, including pre-processing steps such as image smoothing, image enhancement, threshold segmentation, and morphological processing, to extract feature parameters of weld defects. On this basis, a welding seam defect detection and classification system based on the cascade classifier and AdaBoost algorithm was designed, and efficient recognition and classification of welding seam defects were achieved by training the cascade classifier. The results show that the system can accurately identify and distinguish pits, holes, and undercutting defects in welds, with an average classification accuracy of over 90%. The detection and recognition rate of pit defects reaches 100%, and the detection accuracy of undercutting defects is 92.6%. And the overall missed detection rate is less than 3%, with both the missed detection rate and false detection rate for pit defects being 0%. The average detection time for each image is 0.24 s, meeting the real-time requirements of industrial automation. Compared with infrared and ultrasonic detection methods, the proposed machine-vision-based detection system has significant advantages in detection speed, surface defect recognition accuracy, and industrial adaptability. This provides an efficient and accurate solution for laser welding defect detection of automotive brake joints. Full article
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32 pages, 6074 KiB  
Review
High-Quality Manufacturing with Electrochemical Jet Machining (ECJM) for Processing Applications: A Comprehensive Review, Challenges, and Future Opportunities
by Yong Huang, Yi Hu, Xincai Liu, Xin Wang, Siqi Wu and Hanqing Shi
Micromachines 2025, 16(7), 794; https://doi.org/10.3390/mi16070794 - 7 Jul 2025
Viewed by 521
Abstract
The enduring manufacturing goals are increasingly shifting toward ultra-precision manufacturing and micro-nano fabrication, driven by the demand for sophisticated products. Unconventional machining processes such as electrochemical jet machining (ECJM), electrical discharge machining (EDM), electrochemical machining (ECM), abrasive water jet machining (AWJM), and laser [...] Read more.
The enduring manufacturing goals are increasingly shifting toward ultra-precision manufacturing and micro-nano fabrication, driven by the demand for sophisticated products. Unconventional machining processes such as electrochemical jet machining (ECJM), electrical discharge machining (EDM), electrochemical machining (ECM), abrasive water jet machining (AWJM), and laser beam machining (LBM) have been widely adopted as feasible alternatives to traditional methods, enabling the production of high-quality engineering components with specific characteristics. ECJM, a non-contact machining technology, employs electrodes on the nozzle and workpiece to establish an electrical circuit via the jet. As a prominent special machining technology, ECJM has demonstrated significant advantages, such as rapid, non-thermal, and stress-free machining capabilities, in past research. This review is dedicated to outline the research progress of ECJM, focusing on its fundamental concepts, material processing capabilities, technological advancements, and its variants (e.g., ultrasonic-, laser-, abrasive-, and magnetism-assisted ECJM) along with their applications. Special attention is given to the application of ECJM in the semiconductor and biomedical fields, where the demand for ultra-precision components is most pronounced. Furthermore, this review explores recent innovations in process optimization, significantly boosting machining efficiency and quality. This review not only provides a snapshot of the current status of ECJM technology, but also discusses the current challenges and possible future improvements of the technology. Full article
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16 pages, 4591 KiB  
Article
Influence of Process Parameters on the Ultrasonic Atomization Efficiency and Possibility of Testing Properties of Liquid Metals
by Rafał Szostak-Staropiętka, Wojciech Presz, Roksana Pawlic, Anna Dziubińska and Katarzyna Kołacz
Metrology 2025, 5(3), 39; https://doi.org/10.3390/metrology5030039 - 2 Jul 2025
Viewed by 245
Abstract
Over recent years, ultrasonic atomization, especially with regard to liquid metals, has become an object of increased interest, mainly from industry, for additive manufacturing, but also from investigators, for research purposes. A strong correlation between the average particle size, distribution of particle sizes, [...] Read more.
Over recent years, ultrasonic atomization, especially with regard to liquid metals, has become an object of increased interest, mainly from industry, for additive manufacturing, but also from investigators, for research purposes. A strong correlation between the average particle size, distribution of particle sizes, and other process parameters like frequency and vibration amplitude was noted based on the analysis of available theoretical studies, simulations and experiments. The influence of parameters of the atomized fluid-like viscosity and surface tension on process parameters was also mentioned. The objective of this study is further research on the feasibility of using ultrasonic atomization to examine the properties of liquids, especially metals in liquid state. It attempts to close a gap in existing knowledge in searching for a new, possibly simple and cost-effective method to study the properties of liquid metals and further clarify the relationship between ultrasonic atomization parameters (amplitude, frequency, characteristics of metal being spilled on a vibrating surface) and obtained atomization results meant by average particle size and atomization time. Using numerical modeling (finite element method and computational fluid dynamics) as a methodology, combined with tests of using ultrasonic atomization as an instrument to determine properties of liquid metals, was considered as an introduction to a series of experiments. These tests were followed by real experiments that are also presented. At the first stage, numerical modeling was applied to a case of a specific liquid being spilled over a vibrating surface of different angles of inclination and specified, constant frequency and amplitude. The results of the simulation are in line with the current state of knowledge about ultrasonic atomization. Moreover, they can provide some more information on scalability, thus easing the comparison of the results of other experiments presented in the available literature. As a result, the relationship between fluid properties and the average size of atomized particles was demonstrated independently of the surface inclination angle. In the same way, the dependence of successful atomization on a sufficiently thin layer of a liquid was demonstrated. Thirdly, a correlation between the aforementioned layer thickness and the value of vibration amplitude has also been shown. Taking all the above into consideration, ultrasonic atomization can also be considered a research method and can be applied to study the properties of liquid metals. Further research, simulations and experimentation will be conducted to verify, develop and describe this method in full. Full article
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25 pages, 4783 KiB  
Article
Experimental Study on Carbonization and Strengthening Performance of Recycled Aggregate
by Mingqiang Lin, Xiang Li, Maozhi Wei and Qun Xie
Buildings 2025, 15(13), 2309; https://doi.org/10.3390/buildings15132309 - 1 Jul 2025
Viewed by 276
Abstract
In order to address a challenging issue in the recycling of construction debris, the impact of carbonization treatment on the characteristics of recycled aggregates (RCAs) was experimentally examined in this work. Both direct carbonization and carbonization following calcium hydroxide pretreatment were used in [...] Read more.
In order to address a challenging issue in the recycling of construction debris, the impact of carbonization treatment on the characteristics of recycled aggregates (RCAs) was experimentally examined in this work. Both direct carbonization and carbonization following calcium hydroxide pretreatment were used in the study to assess the impact of carbonization on the physical characteristics of recycled aggregates. According to the findings, carbonization raised the recycled aggregates’ apparent density while drastically lowering their porosity and water absorption (by as much as 20–30%). Although the recycled aggregate’s crushing index marginally increased with age, its overall physical qualities remained excellent. Pretreatment with calcium hydroxide can improve the physical characteristics of recycled aggregates, further optimize their pore structure, and efficiently encourage the carbonation process. Furthermore, recycled aggregate’s crushing index can be considerably decreased and its quality much enhanced by the ultrasonic cavitation treatment. According to the study, the carbonation-treated recycled aggregate’s microstructure was denser in the interfacial transition zone and had a stronger link with the cement paste, improving the recycled aggregate concrete’s overall performance. XRD, infrared spectral analysis, and SEM scanning were used to determine the increased calcium carbonate content in the recycled aggregate following carbonation treatment as well as its microstructure improvement process. The findings offer fresh concepts for achieving resource efficiency and environmental preservation through the use of recycled aggregates in concrete, as well as theoretical backing for their use. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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17 pages, 4371 KiB  
Article
Research on Nondestructive Testing Method Based on Magnetic Characteristics of Electron Beam Weld Defects
by Qiangqiang Cheng, Jijun Liu, Yisong Wang, Guisuo Xia and Chunquan Li
Sensors 2025, 25(13), 4094; https://doi.org/10.3390/s25134094 - 30 Jun 2025
Viewed by 255
Abstract
In view of the problems of poor safety, slow detection speed, and low accuracy of existing nondestructive testing (NDT) technologies, such as X-ray methods and ultrasonic detection in detecting electron beam weld defects in aluminum alloys, this study proposes a weak magnetic NDT [...] Read more.
In view of the problems of poor safety, slow detection speed, and low accuracy of existing nondestructive testing (NDT) technologies, such as X-ray methods and ultrasonic detection in detecting electron beam weld defects in aluminum alloys, this study proposes a weak magnetic NDT method based on the geomagnetic field. Firstly, the finite element analysis method was used to establish a simulation model of aluminum alloy electron beam welding defects, and the distribution characteristics of the magnetic field around weld defects, such as cracks and pores, were obtained. Then, the magnetic anomaly signal at the crack weld was identified by combining the wavelet transform and the least squares method. Finally, experimental tests show that the proposed method can safely, quickly, and accurately detect the defects of aluminum alloy electron beam welds. Full article
(This article belongs to the Section Physical Sensors)
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23 pages, 4608 KiB  
Article
Step-by-Step Analysis of a Copper-Mediated Surface-Initiated Atom-Transfer Radical Polymerization Process for Polyacrylamide Brush Synthesis Through Infrared Spectroscopy and Contact Angle Measurements
by Leonardo A. Beneditt-Jimenez, Isidro Cruz-Cruz, Nicolás A. Ulloa-Castillo and Alan O. Sustaita-Narváez
Polymers 2025, 17(13), 1835; https://doi.org/10.3390/polym17131835 - 30 Jun 2025
Viewed by 431
Abstract
Polymer brushes (PBs) are transformative surface-modifying nanostructures, yet their synthesis via controlled methods like copper-mediated surface-initiated atom-transfer radical polymerization (Cu0-SI-ATRP) faces reproducibility challenges due to a lack of understanding of parameter interdependencies. This study systematically evaluates the Cu0-SI-ATRP process [...] Read more.
Polymer brushes (PBs) are transformative surface-modifying nanostructures, yet their synthesis via controlled methods like copper-mediated surface-initiated atom-transfer radical polymerization (Cu0-SI-ATRP) faces reproducibility challenges due to a lack of understanding of parameter interdependencies. This study systematically evaluates the Cu0-SI-ATRP process for polyacrylamide brushes (PAM-PBs), aiming to clarify key parameters that influence the synthesis process. This evaluation followed a step-by-step characterization that tracked molecular changes through infrared spectroscopy (IR) and surface development by contact angle (CA) through two different mixing methods: ultrasonic mixing and process simplification (Method A) and following literature-based parameters (Method B). Both methods, consisting of surface activation, 3-aminopropyltriethoxysilane (APTES) deposition, bromoisobutyryl bromide (BiBB) anchoring, and polymerization, were analyzed by varying parameters like concentration, temperature, and time. Results showed ultrasonication during surface activation enhanced siloxane (1139→1115 cm−1) and amine (1531 cm−1) group availability while reducing APTES concentration to 1 Vol% without drying sufficed for BiBB anchoring. BiBB exhibited insensitivity to concentration but benefited from premixing, evidenced by sharp C–Br (~1170 cm−1) and methyl (3000–2800 cm−1) bands. Additionally, it was observed that PAM-PBs improved with Method A, which had reduced variance in polymer fingerprint regions compared to Method B. Adding to the above, CA measurements gave complementary step-by-step information along the modifications of the surface, revealing distinct wettability behaviors between bulk PAM and synthesized PAM-PBs (from 51° to 37°). As such, this work identifies key parameter influence (e.g., mixing, BiBB concentration), simplifies steps (drying omission, lower APTES concentration), and demonstrates a step-by-step, systematic parameter decoupling that reduces variability. In essence, this detailed parameter analysis addresses the PAM-PBs synthesis process with better reproducibility than the previously reported synthesis method and achieves the identification of characteristic behaviors across the step-by-step process without the imperative need for higher-cost characterizations. Full article
(This article belongs to the Special Issue State-of-the-Art Polymer Science and Technology in Mexico)
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