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Keywords = tensile behavior

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22 pages, 3199 KB  
Article
Slip Behavior and Bidirectional Mechanical Model of Angle Steel Bolted Connections Under Axial Load
by Yongping Li, Dongming Yang, Junling Wu, Weiguo Wu, Ruiyuan Han, Yuan Xiang and Zhisong Xu
Buildings 2026, 16(9), 1709; https://doi.org/10.3390/buildings16091709 (registering DOI) - 26 Apr 2026
Abstract
Transmission towers are typically composed of angle steel members connected by ordinary bolts to form spatial truss systems, in which joint slip under axial loading can significantly influence structural performance. In subsidence areas, corrective lifting of tilted towers may cause internal force redistribution, [...] Read more.
Transmission towers are typically composed of angle steel members connected by ordinary bolts to form spatial truss systems, in which joint slip under axial loading can significantly influence structural performance. In subsidence areas, corrective lifting of tilted towers may cause internal force redistribution, transforming some compression members into tension members and resulting in joints subjected to both compressive and tensile forces. To investigate the slip deformation behavior of angle steel bolted connections under bidirectional axial loading, a series of experiments was conducted on specimens with different angle sizes and bolt numbers, complemented by finite element analysis. The results show that the load–slip relationship exhibits distinct staged characteristics, which can be divided into an initial linear stage, a slip stage, and a hole-bearing stage. The initial slip displacement is generally less than 1 mm, while the slip load and ultimate capacity increase significantly with bolt number, with the ultimate capacity under tension increasing by up to approximately 160% as the number of bolts increases from one to three. Although the slip evolution under compression and tension is generally similar, pronounced differences appear near the ultimate state, indicating a clear directional asymmetry. Based on these findings, a three-stage piecewise mechanical model is established, and a simplified bidirectional slip model is proposed by introducing asymmetric ultimate displacement and capacity parameters. Finite element simulations reproduce the failure modes and load–slip responses with good agreement, confirming the validity of the proposed model. The findings provide a useful reference for the design and performance evaluation of angle steel bolted connections in transmission tower structures. Full article
(This article belongs to the Section Building Structures)
16 pages, 14748 KB  
Article
Long-Term Functional Stability of Organic and Inorganic Modified Luminescent Lyocell Fibers for Security Applications
by Aleksandra Erdman, Jadwiga Gabor, Natalia Brzezińska, Maciej Pyza, Magdalena Popczyk, Piotr Kulpiński and Andrzej S. Swinarew
Materials 2026, 19(9), 1767; https://doi.org/10.3390/ma19091767 (registering DOI) - 26 Apr 2026
Abstract
Luminescent cellulose-based fibers are promising materials for anti-counterfeiting applications because they can provide covert and spectrally distinguishable optical signatures compatible with paper- and textile-based authentication systems. In this study, Lyocell fibers modified with selected inorganic and organic luminescent compounds were subjected to accelerated [...] Read more.
Luminescent cellulose-based fibers are promising materials for anti-counterfeiting applications because they can provide covert and spectrally distinguishable optical signatures compatible with paper- and textile-based authentication systems. In this study, Lyocell fibers modified with selected inorganic and organic luminescent compounds were subjected to accelerated xenon-lamp aging in order to evaluate their functional durability under simulated environmental exposure. The effects of aging on the mechanical properties and luminescent behavior of the fibers were investigated. The results showed that accelerated aging led to a reduction in tensile strength and elongation at break for all fiber variants, although the extent of these changes depended on the type of modifier. Spectroscopic analysis indicated that, despite changes in emission intensity, the characteristic luminescent responses of the modified fibers remained detectable after aging. These findings suggest that luminescent Lyocell fibers can retain their practical identification potential under the applied test conditions and may be considered promising candidates for use as covert security elements. The observed stability is attributed to the immobilization of luminophores within the cellulose matrix and the intrinsic photostability of the applied luminescent systems. At the same time, the study highlights the need for further investigations into the structural and photophysical stability of such systems under long-term environmental exposure. Full article
(This article belongs to the Section Advanced Composites)
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17 pages, 8023 KB  
Article
Effect of H1150M Heat Treatment on Functional Properties of 15-5 PH Stainless Steel Produced by Additive Manufacturing
by Maxim Bassis, Amnon Shirizly and Eli Aghion
Metals 2026, 16(5), 464; https://doi.org/10.3390/met16050464 (registering DOI) - 24 Apr 2026
Abstract
Additive manufacturing (AM) using powder bed fusion (PBF) has been the predominant printing method used over the last decade. The capability of this approach to produce complex parts with high precision has attracted the attention of major industries as a potential tool for [...] Read more.
Additive manufacturing (AM) using powder bed fusion (PBF) has been the predominant printing method used over the last decade. The capability of this approach to produce complex parts with high precision has attracted the attention of major industries as a potential tool for replacing traditional manufacturing technologies. 15-5 PH stainless steel is one of the alloys being studied as a candidate for PBF processes. Its superior strength and corrosion resistance have made it a highly attractive option in numerous industries, including the automotive, nuclear, and petrochemical industries. To enhance the properties of 15-5 PH stainless-steel AM parts following printing, one can use a thermal treatment such as age hardening. However, very little research exists regarding the functional properties of AM parts made from this alloy after heat treatment. This study aims to evaluate the effect of H1150M age hardening heat treatment following printing on the properties of 15-5 PH steel, particularly regarding its mechanical properties and environmental behavior. The microstructure was studied using both optical and electron microscopy, along with X-ray diffraction (XRD) analysis. The mechanical properties were examined by tensile testing and fracture toughness assessment. Corrosion behavior was analyzed in terms of potentiodynamic polarization and using impedance spectroscopy. The results obtained have shown that over-aging caused by H1150M heat treatment has a detrimental effect on the mechanical and environmental behavior of the tested alloy. This was primarily attributed to the formation of an austenitic phase within the inherent martensitic matrix, the generation of brittle phases (mainly carbonitrides of Cr and Nb) and a reduction in grain size. Full article
(This article belongs to the Section Additive Manufacturing)
24 pages, 5012 KB  
Article
Operando Mechanochemical Evolution of Cylindrical 18650 NMC Lithium-Ion Cell Under Progressive High-Rate and Deep-Discharge Conditions Using Fiber Bragg Grating Sensing
by Aung Ko Ko, Zungsun Choi and Jaeyoung Lee
Batteries 2026, 12(5), 151; https://doi.org/10.3390/batteries12050151 - 24 Apr 2026
Abstract
Operando mechanical behavior of lithium-ion batteries under aggressive conditions remains insufficiently quantified, especially under combined high-rate and deep-discharge operation. This study investigated strain evolution in a commercial 18650 NMC lithium-ion cell using surface-mounted fiber Bragg grating sensors across 20 sequential conditions combining five [...] Read more.
Operando mechanical behavior of lithium-ion batteries under aggressive conditions remains insufficiently quantified, especially under combined high-rate and deep-discharge operation. This study investigated strain evolution in a commercial 18650 NMC lithium-ion cell using surface-mounted fiber Bragg grating sensors across 20 sequential conditions combining five discharge rates (1–4.5 C) and four cutoff voltages (2.5–1.0 V). All tests were performed on a single cell using identical 0.5 C constant-current constant-voltage charging, followed by a 2 h rest period and controlled discharge, to systematically evaluate mechanochemical evolution with increasing electrochemical severity. Maximum tensile strain during charging ranged from 45 to 59 µε and showed limited sensitivity to discharge severity. In contrast, discharge behavior exhibited clear rate- and cutoff-dependent transitions from tensile to compressive deformation; the most severe condition (4.5 C, 1.0 V cutoff) produced a peak compressive strain of about −27 µε and the most negative residual strain after relaxation. Although temperature increased monotonically with C-rate, strain evolution was nonlinear and non-monotonic, indicating that electrochemically induced stress dominated over thermal expansion alone. These findings reveal progressive amplification of irreversible deformation under severe discharge and demonstrate the value of fiber Bragg grating sensing for operando assessment of electrochemical–mechanical coupling in cylindrical lithium-ion cells. Full article
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14 pages, 17178 KB  
Article
Investigation on the Microstructure and Mechanical Properties of 304 Stainless Steel Joints by Underwater Local Dry Laser Welding
by Xiaodong Zhang, Fangjie Cheng, Yingchao Feng, Jinping Liu, Zhuyuan Li, Yehua Wu, Ke Han and Qianxing Yin
Materials 2026, 19(9), 1723; https://doi.org/10.3390/ma19091723 - 23 Apr 2026
Viewed by 189
Abstract
In order to verify the feasibility of in situ repair of underwater local dry laser welding (ULDLW) on nuclear power reactor components, this work investigates the microstructure and mechanical properties of 304L austenitic stainless steel repaired by ULDLW using ER308L filler metal. Comprehensive [...] Read more.
In order to verify the feasibility of in situ repair of underwater local dry laser welding (ULDLW) on nuclear power reactor components, this work investigates the microstructure and mechanical properties of 304L austenitic stainless steel repaired by ULDLW using ER308L filler metal. Comprehensive comparison would be made between the ULDLW and conventional in-air laser welding to evaluate their applicability. The results demonstrate that the rapid cooling rate inherent to the underwater environment significantly influences solidification behavior and microstructural evolution. The weld metal (WM) solidifies in the ferritic–austenitic (FA) mode, with an increased proportion of lathy δ-ferrite at the expense of skeletal morphology compared to the in-air welds. Electron backscatter diffraction (EBSD) analysis reveals the substantial grain refinement in underwater welds, with average grain sizes of 39.4 μm versus 47.3 μm for in-air weld bead, accompanied by a higher fraction of low-angle grain boundaries (LAGBs). These microstructural modifications yield superior mechanical properties: underwater weld bead exhibits ultimate tensile strength (UTS) of 685.6 MPa, elongation of 57.5%, and impact toughness of 22.6 J, significantly exceeding the corresponding values for in-air welds (663.9 MPa, 51.8%, and 18.6 J, respectively). Fractographic analysis confirms ductile fracture mechanisms in both conditions. The enhanced performance is attributed to grain refinement strengthening via the Hall–Petch relationship and the increased LAGBs fraction, which impedes dislocation motion and crack propagation. Full article
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19 pages, 1328 KB  
Article
Evaluation of the Potential of a Fast-Curing Polymer Bioadhesive Hydrogel for Corneal Defect Repair
by Zohreh Arabpour, Soheil Sojdeh, Amirhosein Panjipour, Zahra Bibak Bejandi, Amal Yaghmour, Miranda Castillo, Anwar N. Khandaker, Mohammad Soleimani and Ali R. Djalilian
Gels 2026, 12(5), 357; https://doi.org/10.3390/gels12050357 - 23 Apr 2026
Viewed by 87
Abstract
Corneal defects are a major cause of vision loss and require rapid, biocompatible, and effective sealing methods to restore ocular integrity and prevent infection. Current clinical adhesives, such as cyanoacrylate and fibrin glue, are limited by problems such as poor biocompatibility and inadequate [...] Read more.
Corneal defects are a major cause of vision loss and require rapid, biocompatible, and effective sealing methods to restore ocular integrity and prevent infection. Current clinical adhesives, such as cyanoacrylate and fibrin glue, are limited by problems such as poor biocompatibility and inadequate stability. This study presents the design and evaluation of a fast-curable polymer bioadhesive hydrogel, a corneal glue formulated for efficient sealing of corneal defects. Hydrogels were synthesized from natural and synthetic polymers, including polyvinyl alcohol (PVA), sodium alginate (SA), and carboxymethyl cellulose (CMC), optimized for rapid gelation (~45 s), robust adhesion (~15 kPa), and mechanical strength (tensile strength ~0.35 MPa and storage modulus G′ indicating strong elastic behavior). Physicochemical and rheological properties, including swelling behavior and optical transparency (>90% transmittance across 400–700 nm), were characterized, including gelation time, swelling behavior, and mechanical strength. In vitro biocompatibility was assessed using human corneal epithelial cells to evaluate cytotoxicity and cell adhesion. Ex vivo studies on human cadaveric corneas with full-thickness defects measured adhesive strength and sealing efficacy through burst pressure (~38 mmHg) and leakage tests, with comparisons to commercial fibrin and cyanoacrylate adhesives. The optimized corneal glue exhibited fast curing, robust adhesion, high water retention with minimal swelling, favorable viscoelastic properties, and excellent cytocompatibility effectively sealing corneal defects in ex vivo models. These results highlight its potential as a promising fast-curable bioadhesive for corneal wound repair and ocular surface restoration. Full article
(This article belongs to the Special Issue Biofunctional Hydrogels for Biofabrication in Tissue Engineering)
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21 pages, 4018 KB  
Review
Industrial Artificial and Natural Fibers’ Cutting Mechanism—A Review
by Shanshan Hu, Mengmeng Ma, Zhiliang Wu, Yuyuan Huang, Qingrui Jiang and Chengji Yang
Micromachines 2026, 17(5), 513; https://doi.org/10.3390/mi17050513 (registering DOI) - 23 Apr 2026
Viewed by 171
Abstract
Industrial synthetic and natural fibers play an indispensable role in modern manufacturing, aerospace, automotive, and textile engineering. However, the enhanced mechanical performance of advanced industrial fibers has introduced significant challenges in cutting processes, since brittle, high-tensile, and viscoelastic fibers exhibit totally different fracture [...] Read more.
Industrial synthetic and natural fibers play an indispensable role in modern manufacturing, aerospace, automotive, and textile engineering. However, the enhanced mechanical performance of advanced industrial fibers has introduced significant challenges in cutting processes, since brittle, high-tensile, and viscoelastic fibers exhibit totally different fracture behaviors from conventional solid materials. At present, the complex motion coupling mechanisms between fibers and cutting tools under free-form conditions are insufficient; there is no unified framework for understanding the mechanisms of fiber cutting; it is difficult to effectively link the microscopic fracture physics of different fiber types with their macroscopic cutting properties. Furthermore, research into the dynamic interaction between the cutting tool and the fiber, cross-scale cutting characteristics, and tool wear mechanisms has not been sufficiently systematic, and non-contact cutting methods have not yet been the subject of systematic study. Through a systematic review, this review identified three primary categories of difficult-to-cut industrial fibers and summarized the distinctions in their fundamental material properties. The static, kinematic, and dynamic characteristics of fiber cutting under both free and fixed forms were discussed. The fracture mechanisms of fibers under diverse loading scenarios were also systematically revealed. Furthermore, this review summarizes the effects of cutting tool wear characteristics, geometric parameters, and material types on cutting performance. Finally, non-contact methods for cutting fiber were listed. Based on the above analysis, three critical directions for future research were proposed to bridge the existing knowledge gaps in the literature. This review of the interdisciplinary interactions among mechanics, materials science, and textile engineering provides a theoretical foundation and research directions for achieving high efficiency and a long tool life during cutting industrial fibers. Full article
(This article belongs to the Special Issue Advanced Manufacturing Technology and Systems, 4th Edition)
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18 pages, 1855 KB  
Article
Mechanisms of Microstructural and Defect Evolution in Laser Powder Bed Fusion-Fabricated In625 Induced by Heat Treatment
by Qing Chen, Yi Liu, Xuxing Duan, Xianjun Zhang, Gening He, Yu Sun and Changyuan Li
Materials 2026, 19(9), 1713; https://doi.org/10.3390/ma19091713 - 23 Apr 2026
Viewed by 84
Abstract
Heat treatment is essential for In625 fabricated by laser powder bed fusion (L-PBF), as it significantly influences microstructural evolution, defect behavior, and mechanical performance. In this study, the effects of different solution heat treatments on L-PBF-fabricated In625 were systematically investigated. Industrial computed tomography [...] Read more.
Heat treatment is essential for In625 fabricated by laser powder bed fusion (L-PBF), as it significantly influences microstructural evolution, defect behavior, and mechanical performance. In this study, the effects of different solution heat treatments on L-PBF-fabricated In625 were systematically investigated. Industrial computed tomography was employed to characterize internal defects before and after heat treatment, while optical microscopy, EBSD, TEM, and EDS were used to analyze microstructural evolution. Room-temperature tensile tests evaluated mechanical properties. The results show that heat treatment at 1090 °C reduces porosity from 0.33% to 0.25%, whereas increasing the temperature to 1150 °C results in a further increase in porosity to 0.45%. This non-monotonic behavior is interpreted as the result of competing mechanisms, including partial closure of small pores at 1090 °C and pore coarsening/enlargement at higher temperatures, with the latter possibly involving the growth of sub-resolution pores into the CT-detectable range. Complete grain equiaxiality occurs after heat treatment at 1090 °C or higher, with average grain sizes below 100 μm, although grain coarsening becomes pronounced at higher temperatures. Samples heat-treated at 1150 °C exhibit reduced mechanical anisotropy, achieving tensile strength above 919 MPa and elongation up to 60%. These results clarify the mechanisms by which heat treatment governs microstructure–defect–property relationships in L-PBF In625, guiding its engineering application. Full article
(This article belongs to the Section Metals and Alloys)
23 pages, 36264 KB  
Article
A Mesoscopic Study on the Constraint Mechanism of Existing Pavement Rutting on the Mechanical Behavior of Sealcoat Based on Highways in China
by Zhanwei Zhao, Wenruo Fan, Hui Wang, You Zhou and Zhoucong Xu
Appl. Sci. 2026, 16(9), 4126; https://doi.org/10.3390/app16094126 - 23 Apr 2026
Viewed by 61
Abstract
Conventional maintenance models often neglect the impact of pre-existing rutting on sealcoat performance, particularly in high-temperature regions like Chongqing in China, where rut-related failures are common. Existing ruts impose geometric constraints that significantly alter stress redistribution within the new sealcoat layer, yet this [...] Read more.
Conventional maintenance models often neglect the impact of pre-existing rutting on sealcoat performance, particularly in high-temperature regions like Chongqing in China, where rut-related failures are common. Existing ruts impose geometric constraints that significantly alter stress redistribution within the new sealcoat layer, yet this constraint mechanism remains poorly understood due to limitations in laboratory observation. This study developed a mesoscopic AC16 + MS3 composite discrete element model to simulate the mechanical behavior of a sealcoat applied over a rutted pavement. To replicate real-world conditions, a constant pressure of 0.7 MPa, representing the standard tire ground pressure in JTG E20-2011, was applied at a temperature of 70 °C, reflecting extreme high-temperature stability limits. Virtual rutting tests and contact force chain analyses were conducted across varying existing pavement rut depths, including 0 mm, 3 mm, 6 mm, and 10 mm. The results indicate that existing ruts redirect stress transfer paths, causing vertical compressive force chains to densify within the rutted zone and tensile stress to concentrate at rut edges. Mastic-mastic contacts transmit over 65% of the load, identifying asphalt mortar as the primary load-transfer phase. Notably, a 10 mm existing rut depth induces a tensile vacuum zone at depths of 15–40 mm, disrupting the standard U-shaped stress distribution. These findings clarify how pre-existing geometries govern structural degradation, suggesting that maintenance in high-temperature regions must prioritize asphalt mortar performance to mitigate edge cracking and deformation. Full article
(This article belongs to the Special Issue New Trends in Road Materials and Pavement Design)
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21 pages, 2537 KB  
Article
Experimental–Numerical Framework for Evaluating the Mechanical Response of Cornus sanguinea L.-Reinforced Polypropylene Biocomposites
by Mustafa Öncül
Polymers 2026, 18(9), 1020; https://doi.org/10.3390/polym18091020 - 23 Apr 2026
Viewed by 176
Abstract
Polypropylene (PP) biocomposites reinforced with Cornus sanguinea L. (CS) pruning-waste particles were investigated using a combined experimental mechanics and finite element (FE) validation framework to support model-based design with an under-utilized lignocellulosic feedstock. Two particle-size fractions (<100 µm, LF1; 100–250 µm, LF2) were [...] Read more.
Polypropylene (PP) biocomposites reinforced with Cornus sanguinea L. (CS) pruning-waste particles were investigated using a combined experimental mechanics and finite element (FE) validation framework to support model-based design with an under-utilized lignocellulosic feedstock. Two particle-size fractions (<100 µm, LF1; 100–250 µm, LF2) were produced by grinding and sieving and incorporated into PP at 5–20 wt% via melt compounding and compression molding. Tensile and three-point bending properties were measured in accordance with ASTM D638 and ASTM D790. PP exhibited a tensile strength of 23.63 ± 0.51 MPa and a tensile modulus of 868 ± 21 MPa. Incorporation of LF1 particles increased tensile modulus monotonically, reaching 1020 ± 137 MPa at 20 wt%, while tensile strength decreased with filler content; by contrast, the 20 wt% LF2 formulation showed a pronounced strength reduction to 16.30 ± 0.25 MPa, indicating a disadvantageous size–loading interaction. In flexure, strength was comparatively insensitive to reinforcement (PP: 39.5 ± 0.34 MPa; reductions typically ≤7%), whereas flexural modulus increased to 2152 ± 27 MPa (LF1) and 2110 ± 34 MPa (LF2). FE models calibrated using true stress–true plastic strain data accurately reproduced tensile responses across the full strain range and flexural behavior within the pre-contact-dominated regime, demonstrating the suitability of PP/CS biocomposites for stiffness-driven applications. Full article
(This article belongs to the Special Issue Advanced Polymer Composites: Structure and Mechanical Properties)
31 pages, 2890 KB  
Article
Numerical and Experimental Assessment of Structural Performance and Axial Compression Capacity of Screw-Connected Built-Up Cold-Formed Steel Members
by Nefya Soysal and Zeynep Fırat Alemdar
Buildings 2026, 16(9), 1651; https://doi.org/10.3390/buildings16091651 - 22 Apr 2026
Viewed by 171
Abstract
Recently, cold-formed steel (CFS) structural systems have been increasingly used in building applications due to their lightweight characteristics, ease of fabrication, and efficient construction processes. Among these systems, built-up CFS columns are widely adopted to enhance load-carrying capacity; however, their axial compression behavior [...] Read more.
Recently, cold-formed steel (CFS) structural systems have been increasingly used in building applications due to their lightweight characteristics, ease of fabrication, and efficient construction processes. Among these systems, built-up CFS columns are widely adopted to enhance load-carrying capacity; however, their axial compression behavior and failure mechanisms have not yet been fully clarified. This study aims to investigate the axial compression performance of built-up cold-formed steel columns through a combined experimental and numerical approach. This study investigates the axial compression performance of built-up cold-formed steel columns using a combined experimental and numerical approach. Following the full-scale testing of five different configurations, finite element models were developed in ABAQUS using the obtained material properties. The experimental results were used to validate and calibrate the finite element models, which provided a detailed simulation of the nonlinear structural behavior of the columns. The experimental load–displacement responses were compared with the numerical results to evaluate the accuracy of the finite element models and to identify the axial load-carrying capacity and dominant failure modes of the built-up columns. Furthermore, the tensile pull-out behavior of 3.9 mm diameter self-drilling screws utilized in the built-up column connections was examined through expedient fastener tests to facilitate a more profound understanding of the load transfer mechanism. The results highlight the influence of built-up configuration and connection behavior on the axial compression performance of CFS columns, providing practical insights for improving the design and numerical modeling of screw-connected built-up cold-formed steel column systems. Full article
(This article belongs to the Section Building Structures)
19 pages, 6661 KB  
Article
Synergistic Effects of Fiber Inclination, Geometry, and Thermal Treatment on Fe-SMA Fiber Pull-Out Resistance in High-Performance Concrete
by Jan Białasik, Wojciech Podraza, Dominika Samulczyk and Alireza Tabrizikahou
Materials 2026, 19(8), 1668; https://doi.org/10.3390/ma19081668 - 21 Apr 2026
Viewed by 189
Abstract
Iron-based shape memory alloy (Fe-SMA) fibers can enhance cementitious composites through both crack bridging and thermally activated recovery stresses. Since fiber pull-out governs load transfer at the micro scale, understanding the combined effects of fiber geometry, inclination, and thermal treatment is essential. This [...] Read more.
Iron-based shape memory alloy (Fe-SMA) fibers can enhance cementitious composites through both crack bridging and thermally activated recovery stresses. Since fiber pull-out governs load transfer at the micro scale, understanding the combined effects of fiber geometry, inclination, and thermal treatment is essential. This study experimentally investigated the pull-out behavior of hooked-end Fe-SMA fibers embedded in high-performance concrete (HPC). A total of 54 ASTM C307-type briquette specimens were tested using single-hook (3D) and double-hook (4D) fibers at inclination angles of 60°, 75°, and 90° under ambient, 100 °C, and 200 °C conditions. Additional flexural, compressive, and direct tensile tests were conducted on plain HPC exposed to the same thermal regime. At ambient temperature, 4D fibers showed 50–70% higher peak pull-out forces than 3D fibers. Heating to 100 °C further increased pull-out resistance by about 6–17%, and the 4D-60-100 configuration achieved the highest performance. In contrast, exposure to 200 °C reduced pull-out resistance by about 5–12% below ambient values. Overall, a 60° inclination generally provided a better response, while 90° produced the lowest. The results confirm that moderate thermal activation combined with double-hook geometry is the most effective strategy for maximizing Fe-SMA fiber–matrix load transfer in HPC. Full article
(This article belongs to the Section Construction and Building Materials)
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27 pages, 8866 KB  
Article
PLA/Collagen/Hydroxyapatite Ternary Biocomposites for Biodegradable Bone Screw Applications
by Ayşegül Uzuner-Demir, Rumeysa Yıldırım, Hürol Koçoğlu, Mihriban Aydoğan-Gemici, Zehra Betül Ahi, Fatih Arıcan, Olcay Mert, Güralp Özkoç and Mehmet Kodal
Polymers 2026, 18(8), 1005; https://doi.org/10.3390/polym18081005 - 21 Apr 2026
Viewed by 462
Abstract
Poly(lactic acid) (PLA)-based biocomposites incorporating collagen (COLL) and hydroxyapatite (HA) were produced via melt micro-compounding and subsequent injection molding. 1,4-phenylene diisocyanate (PDI) was employed as a compatibilizer, while poly(ethylene glycol) (PEG) was used as a plasticizer. The morphological, thermal, rheological, and mechanical properties, [...] Read more.
Poly(lactic acid) (PLA)-based biocomposites incorporating collagen (COLL) and hydroxyapatite (HA) were produced via melt micro-compounding and subsequent injection molding. 1,4-phenylene diisocyanate (PDI) was employed as a compatibilizer, while poly(ethylene glycol) (PEG) was used as a plasticizer. The morphological, thermal, rheological, and mechanical properties, as well as surface wettability, degradation behavior, and cytotoxicity, were comprehensively evaluated. SEM and DSC analyses revealed the phase distribution and thermal transitions, while rheological measurements showed that PEG reduced melt viscosity by increasing chain mobility. Mechanical performance was evaluated using tensile, impact, and DMA tests on standard specimens, indicating that HA primarily enhanced stiffness (elastic modulus), whereas PEG improved toughness, resulting in higher impact strength. Biodegradable bone screw prototypes were produced with the same formulations and subjected to torsion, enzymatic degradation, and MTT cytotoxicity tests. Degradation results indicated that biocomposites containing PEG, collagen, and HA exhibited accelerated mass loss. Overall, the 70/20/10 PLA/COLL/HA/PEG/PDI formulation was more suitable for soft (trabecular) bone tissue, while the 70/10/20 PLA/COLL/HA/PDI formulation showed advantages for hard (cortical) bone tissue applications. Full article
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12 pages, 1629 KB  
Article
Influence of Belt Construction on Strain Rate During Tensile Testing of Rubber–Textile Conveyor Belts
by Ľubomír Ambriško and Lucia Čabaníková
Appl. Sci. 2026, 16(8), 3983; https://doi.org/10.3390/app16083983 - 20 Apr 2026
Viewed by 217
Abstract
Rubber–textile conveyor belts with polyester–polyamide (EP) carcasses are widely used in bulk material handling, where their mechanical performance significantly affects their reliability, safety and service life. Due to the anisotropic structure of the textile reinforcement, the deformation of EP belts is strongly dependent [...] Read more.
Rubber–textile conveyor belts with polyester–polyamide (EP) carcasses are widely used in bulk material handling, where their mechanical performance significantly affects their reliability, safety and service life. Due to the anisotropic structure of the textile reinforcement, the deformation of EP belts is strongly dependent on the loading direction. This study investigates the deformation rate behavior of rubber–textile conveyor belts under uniaxial tensile loading, with an emphasis on the differences between the longitudinal (warp) and transverse (weft) directions. The experimental results show that the strain rate is controlled by different deformation mechanisms of the textile components, which leads to significantly different deformation kinetics under warp and weft loading. The findings provide new insights into the time-dependent tensile behavior of EP belts and support the optimization of the textile carcass design for better durability and sustainability under severe operating conditions. Full article
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21 pages, 9132 KB  
Article
PLA Biocomposites Reinforced with Cinnamon-Treated Flax Fibers
by Magdalena Stepczyńska, Alona Pawłowska and Rafał Malinowski
Materials 2026, 19(8), 1632; https://doi.org/10.3390/ma19081632 - 18 Apr 2026
Viewed by 242
Abstract
In this research, PLA biocomposites reinforced with 20 wt% flax fibers modified with 1, 5, 10, and 20% concentrations of trans-cinnamic acid (TC) were prepared. The materials were systematically characterized to evaluate their structural, thermal, viscoelastic, surface, and functional properties. Thermal stability and [...] Read more.
In this research, PLA biocomposites reinforced with 20 wt% flax fibers modified with 1, 5, 10, and 20% concentrations of trans-cinnamic acid (TC) were prepared. The materials were systematically characterized to evaluate their structural, thermal, viscoelastic, surface, and functional properties. Thermal stability and phase transitions were analyzed using thermogravimetric analysis (TG) and differential scanning calorimetry (DSC), while viscoelastic behavior and molecular relaxation processes were investigated by dynamic mechanical analysis (DMA). To elucidate failure mechanisms and interfacial quality, fracture surface morphology after tensile testing was observed using scanning electron microscopy (SEM). Surface wettability was determined through water contact angle measurements, and antibacterial activity against Escherichia coli and Staphylococcus aureus was evaluated to assess the functional potential of the developed biocomposites. The results demonstrated that moderate fiber modification improved interfacial adhesion and enhanced thermo-mechanical performance. The highest contact angles were observed for 5% and 10% TC concentrations, indicating increased surface hydrophobicity, while strong antibacterial activity (R ≥ 6) was achieved for 10% and 20% TC. The research confirms that trans-cinnamic acid concentration governs multiple structure–property relationships, enabling controlled tuning of mechanical reinforcement and antibacterial functionality. Full article
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