Search Results (321)

This study presents an experimental characterization and numerical assessment of Cu–Al–Be (CAB) shape memory alloys (SMAs) for potential applications in U-shaped flexural plate (UFP) seismic dampers. Six alloy compositions were evaluated through monotonic tensile tests, ASTM F2516 superelastic protocols, and increasing-amplitude cyclic loading to identify the material exhibiting stable superelastic behavior at room temperature. Among the tested materials, alloy CAB4.76-A showed the most favorable response, with high transformation stress, stable pseudoelastic behavior, and strain recovery exceeding 95% for strains up to 2.5%. A phenomenological finite element model based on the Auricchio constitutive formulation was calibrated using experimental data within the validated strain range (ε ≤ 0.025), showing good agreement in stiffness and stress prediction. The calibrated model was subsequently applied to simulate the response of a UFP device under orthogonal cyclic loading. The results indicate a strong dependence on loading orientation due to coupled bending–torsion effects, with the 90° direction exhibiting significantly higher strength and energy dissipation capacity. Comparison with analytical formulations originally developed for steel UFPs showed that these expressions provide approximate estimates when applied to SMA-based devices. The results suggest that Cu–Al–Be alloys are a promising alternative for UFP applications, while highlighting the importance of loading orientation and the need for future experimental validation at a device scale. Full article

Future lunar missions, like the International Lunar Research Station (ILRS), demand single-launch multi-point operations, urgently requiring reusable energy-absorbing structures. Integrating shape memory alloy (SMA) into honeycombs offers a promising solution; however, deformation exceeding the SMA’s recoverable limit induces structural residual deformation, altering the configuration and degrading subsequent energy absorption. To address this, we propose a semi-analytical, data-calibrated hybrid model predicting SMA honeycomb residual deformation. A four-stage linear constitutive model is established capturing superelasticity and martensitic yielding. Cell walls are idealized as equivalent beams. Using layered fiber integration and numerical interpolation, a nonlinear moment–curvature relationship is constructed, enabling rapid structural residual deflection evaluation from material residual strains. Finite element results confirm that initial residual deformation stabilizes the honeycomb into a reusable configuration, governing subsequent plateau stresses. Calibrated by uniaxial test data, the proposed model accurately predicts residual deformation ratios and reusable plateau stresses with errors within 8%. By bridging material-level strain with structural-level deformation, this approach circumvents computationally expensive full-scale simulations and costly experimental trials, providing a highly efficient tool for designing reusable SMA absorbers. Full article

Background/Objectives: Changes in the mechanical behavior of orthodontic archwires during clinical use are not fully understood, particularly when different bracket systems are employed. Self-ligating (SL) brackets have gained considerable popularity in orthodontic practice in recent years, largely due to claims of improved treatment efficiency and biomechanical performance. Nevertheless, current evidence has not consistently demonstrated statistically significant differences between conventional ligation (CL) brackets and SL systems. The aim of this study was to evaluate changes in the mechanical properties and degradation over time of nickel-titanium (NiTi) archwires after clinical use in orthodontic treatments performed with CL and SL brackets. Methods: A comparative study was conducted using archwires retrieved from orthodontic patients. Round 0.014-inch NiTi wires (GC Orthodontics America Inc., IL, USA) were analyzed. The archwires were used in 60 patients treated with either CL or SL appliances and evaluated at four time points: before clinical use (T0), and after 1 month (T1), 2 months (T2), and 3 months (T3) of intraoral service. Mechanical testing was performed according to ISO 15841:2014 + Amd. 1:2020 using a three-point bending test with a universal testing machine (Z005 Test Control II Universal Testing Machine, Zwick Roell, Kennesaw, GA, USA). The variables analyzed included the mean force delivered by the archwires at deflections of 3 mm (F3), 2 mm (F2), 1 mm (F1), and 0.5 mm (F0.5), as well as the slope of the superelastic plateau at 2 mm, 1 mm, and 0.5 mm. The static and dynamic friction coefficients, as well as the friction forces associated with the wires and the two types of brackets, were determined using a modified MTS-Bionix servo-hydraulic testing machine. The tests were conducted at 37 °C in a saline environment. Results: Both groups showed changes in the superelastic behavior of NiTi archwires. Alterations increased with longer intraoral exposure. In the SL group, significant modifications were already observed after one month of clinical use, with a reduction in the force delivered and a loss of superelastic characteristics. These changes remained relatively stable thereafter, with no statistically significant differences during the following months. In contrast, the CL group showed a progressive reduction in force delivery and superelasticity over time. This is due to the difference in friction between the wire and the CL bracket compared to the SL bracket, which results in greater force transfer for tooth movement. Conclusions: Overall, differences in the mechanical behavior of archwires between CL and SL systems were observed during the initial stages of clinical use. However, these differences diminished over time, and no significant differences were detected after three months. Considering the progressive degradation of mechanical properties, the reuse of archwires that have remained intraorally for more than three months may not be advisable. Full article

Ischemic stroke is a major cause of death and disability and thus requires specialized treatment. The present work describes the design and control-oriented simulation of a smart steerable microcatheter tip based on Nitinol superelastic alloy for thrombectomy. The proposed framework allows for predictive and safe catheter navigation by combining experimental material characterization, electromechanical modeling, and control design. Experimental validations of key material properties, such as hemocompatibility, corrosion resistance, and full superelastic behavior, were incorporated into an environment created in MATLAB/Simulink. The bending curvature of a safe blood vessel was exactly followed by means of delay-guaranteed bandwidth-limited dynamical feedforward and feedback regulation. Simulation-based results validate steering and dynamic response, as well as safe interaction with blood vessel walls. Ultimately, from the work described in this paper, we hope to present a proposal for an entire framework for relating biomaterial properties with control performance that could stimulate safer and more efficient robot-assisted procedures in combating thromboembolic diseases. Full article

Cyclic superelasticity in laser powder bed fusion (LPBF)-fabricated NiTi alloys is strongly influenced by the scale of structural regulation. While conventional post-processing strategies are typically interpreted from a microstructural perspective, the distinct roles of bulk and surface regulation in governing cyclic functional response remain unclear. In this study, heat treatment and laser shock peening (LSP) are employed as representative bulk and surface regulation routes, respectively, to systematically investigate their effects on phase transformation and cyclic superelasticity. The results reveal that heat treatment and LSP operate through fundamentally different regulation modes. Heat treatment acts as a bulk regulation route, reconstructing the overall microstructure, promoting precipitation (NiTi₂ and Ni₄Ti₃), and modifying transformation pathways, which enhances recovery ratio but reduces recoverable strain. In contrast, LSP acts as a surface/subsurface regulation route, inducing gradient grain refinement and near-surface hardening while maintaining a B2-dominated matrix. As a result, the LSP-treated sample exhibits superior cyclic stability, with a stable recoverable strain of 9.93% and a superelastic strain of 5.10% after 10 cycles. These findings demonstrate that cyclic superelasticity is governed not only by phase constitution but also critically by the scale of structural regulation. This work provides a practical framework for selecting post-processing strategies to optimize functional performance in LPBF NiTi alloys. Full article

Flexible honeycomb skins offer a promising route for achieving continuous shape adaptation in morphing aircraft. In practical service, however, the skin must simultaneously accommodate large in-plane deformation while maintaining sufficient out-of-plane load-bearing capacity, which poses a fundamental design challenge. To address this trade-off, this study investigates an SMA-based U-shaped honeycomb under combined tensile deformation and aerodynamic pressure. A parametric finite element model incorporating SMA superelasticity is established, and an automated Abaqus–modeFRONTIER framework is developed for multi-objective optimization under dual loading conditions. The curvature radius, parallel-segment length, and middle-beam length are selected as design variables. The optimization objectives are defined as minimizing the maximum local strain under a prescribed tensile displacement and reducing the Z-direction displacement under aerodynamic loading as an indicator of out-of-plane bending resistance. The resulting Pareto front reveals the trade-off between flexibility and load-bearing capacity, and the sensitivities of the key geometric parameters are analyzed. Compared with the initial design, a representative optimized solution reduces the maximum local strain by 58.5% and the Z-direction displacement by 61.3%. These results provide a numerical basis for the design of SMA-based flexible skins for morphing aircraft. Full article

In this paper, the design of a novel deployable scissor-structural mechanism (SSM) for the morphing of a generic missile nose cone is presented. The aim of the study is to explore a geometric transformation specially designed for the missile’s flight envelope, ensuring optimal aerodynamic performance and decreasing the aerodynamic drag coefficient across different flight conditions, then to apply it. For the geometric transformation the proposed mechanism is composed of multiple scissor-like elements (SLEs), providing a reconfigurable structure capable of adjusting the nose cone shape dynamically. To achieve a continuous and smooth missile nose cone surface the study incorporates a superelastic alloy (SEA) skin, which can deform compatibly with the SLE movements. A computational routine provides the study with an optimum SSM configuration which makes the geometric transformation the best. The computational routine minimizes the structural error between deformed nose cone shape and target nose cone shape. Full article

While carbon fiber-reinforced polymer (CFRP) composites are widely utilized in aerospace applications due to their exceptional specific strength and stiffness, they are inevitably subjected to impact loads during service, which can easily induce internal damage such as delamination. To mitigate these issues, this study investigates the low-velocity impact behavior of an SMA-reinforced CFRP U-shaped structure, emphasizing the critical role of curing-induced residual stresses. A numerical model incorporating the thermal-mechanical manufacturing history was developed and validated against experimental data. Results indicate that while embedded superelastic SMA wires effectively suppress crack propagation and enhance energy absorption, neglecting residual stresses leads to a significant overestimation of structural rigidity and peak loads. Due to the coefficient of thermal expansion mismatch between the SMA wires and the resin matrix, the SMA-CFRP system exhibits higher sensitivity to initial internal stresses than pure CFRP. By accounting for the residual stress field, the relative error in predicted peak force and absorbed energy for the SMA-CFRP model was reduced from 9.3% to 3.5% and 18.9% to 7.8%, respectively. These findings demonstrate that residual stress lowers the failure threshold and is essential for capturing the synergistic effects of SMA phase transformation and matrix damage, providing a more accurate reconstruction of the structural energy balance. Full article

SMA bars, particularly those based on NiTi, exhibit superelastic and self-centering properties, providing damage-resistant, self-centering structural systems. However, their natural smoothness and low machinability pose a significant challenge to adequate mechanical anchorage. This paper experimentally measures the efficiency of two feasible wedge-type anchorage systems, wedge-and-barrel (WB) and spring anchor (SA), which are typically used in post-tensioning systems, and assesses their applicability for anchoring smooth-surfaced NiTi SMA bars. A total of 24 testing configurations were examined in this study. A complete monotonic tensile test regime was performed at steady loads with desired strain levels. The findings validate that both wedge-type anchorage systems were able to effectively anchor the SMA bars, although some performance differences were observed. The WB anchorage system showed increased stress capacity, improved load transfer efficiency, and less scatter across repeated tests, which can be attributed to its greater mechanical confinement and frictional interlock, exhibiting an increase of approximately 27% in stress capacity compared to the SA anchorage system. On the other hand, the SA system exhibited good anchorage performance. It showed a slightly lower stress response and greater variation at higher levels of deformation due to the spring’s compression mechanism. The results demonstrate the feasibility of using wedge-type anchorage systems to anchor SMA rebars for seismic applications and provide guidance for future anchorage design. Full article

The research described in this article is a continuation of a series of studies on biocompatible materials, focused on finding the optimal alloy composition and heat treatment regimes. The use of materials with a low Young’s modulus ensures the long-term safety of the implant by reducing the stress shielding effect, which causes bone resorption. This work investigates the effect of alloying with niobium in the range of (8–10) at. % on the Ti-38Zr alloy, specifically its structure, mechanical properties, Young’s modulus, and superelasticity. In this study, plates of the Ti-38Zr-(8-10)Nb (at. %) alloy were investigated after quenching and subsequent annealing. In Ti-38Zr-(8-10)Nb alloys, quenching from 600 °C fixes the β-phase of Ti. In alloys with (8-9)Nb, this is a metastable β-phase, as evidenced by its superelastic behavior under cyclic tension. Annealing at 400 °C leads to a clear decomposition of the quenched high-temperature β-phase in Ti-38Zr-(8-9)Nb alloys into β- and α′-phases. Based on the mechanical test results, it can be inferred that the precipitation of the brittle ω-phase and the α′-phase occur concurrently, since annealing at 400 °C causes a pronounced embrittlement of the Ti-38Zr-(8–9)Nb alloys (with elongation dropping from ~15% to 0.7–2.5%, respectively) alongside a substantial increase in strength (from 500 MPa to 1010 MPa). For the Ti-38Zr-10Nb alloy, the ductility also declines but remains within acceptable limits (from ~14% to ~10%), while the strength rises from 520 MPa to 630 MPa. The Young’s modulus of the Ti-38Zr-(8-10)Nb alloy after quenching is ~80 GPa. After annealing, it increases to 95 GPa for alloys with (8-9)Nb, while for 10Nb it remains at approximately 80 GPa. Full article

This study investigates the pullout behaviour of hooked-end superelastic shape memory alloy (SMA) fibres embedded in concrete with the aim to develop an analytical model. Single fibre pullout experiments were performed to evaluate the mechanical response of SMA fibres with various hook geometries. A mathematical model based on the friction pulley method was then developed to predict the experimental pullout load versus displacement plots. The model integrates the tensile stress–strain response and the elastic–plastic constitutive behaviour of superelastic SMA materials, while also accounting for fibre slip and superelastic deformation during the pullout process. The pullout process is modelled through staged mechanisms including elastic response and debonding, progressive mechanical anchorage, and frictional pullout. The contribution of mechanical anchorage is governed by the elastic–superelastic strain distribution within the hook bends. The proposed model reasonably reproduces the overall load-slip response, peak pullout load, slip at peak load, and pullout energy for the three different fibre geometries extracted from normal strength and high-performance concrete matrix. The proposed mathematical model offers a transferable and predictive tool for assessing the pullout performance of hooked-end SMA fibres and supports their integration into design of SMA fibre-reinforced cementitious composites. Full article

Dual-phase layered microstructures containing alternating regions of soft and hard phases can produce alloys with a unique combination of strength and ductility. In this study, the molecular dynamics (MD) method was utilized to simulate nanoindentation of a Ni/NiTi/Ni nanostructured film (NSF). This film features a unique alternating FCC/B2/FCC microstructure, in which the B2-phase NiTi acts as a superelastic shape memory alloy (SMA). The results indicate that Ni/NiTi/Ni NSF significantly reduces its hardness due to the superelasticity of the B2 phase. The presence of the NiTi interlayer effectively blocks the propagation path of dislocations and stacking faults by transforming the local dislocations transferred from the upper layer into a large-scale coordinated phase transition, significantly reducing local deformation misalignment. As the thickness of the surface film λ increases, the dislocation slip plane propagating horizontally appears in the upper pure Ni layer. The thicker the surface film, the more horizontal slip planes are formed. This study provides new insights into the contact mechanical behavior of nanostructured films based on NiTi shape memory alloys from the perspective of atomic scale. Full article

NiTi Shape Memory Alloys (SMAs) display notable thermomechanical properties such as superelasticity and the elastocaloric effect, which makes them of interest for emerging solid-state cooling and thermal management applications. It is recognized that a considerable amount of work has been recently conducted to improve the understanding of the uniaxial tensile and compressive response of Ni-Ti SMAs; however, there has been limited work on the response to bending, which is an important operational mode in the practical designs of devices. This work consists of an experimental study of the thermomechanical response of Ni-Ti cantilever beams to cyclic bending. Nitinol samples (100 mm × 20 mm × 1 mm) were shape-set at 550 °C for 30 min and tested at 1800 rpm. The sample surface temperature change was monitored with infrared thermography data and analyzed with the Profile Mono Segment and Area Rectangle methods. The findings show that there was a measurable elastocaloric temperature change of approximately 4–5 °C, and temperature change increased by 21–25% as bending deflection increased from 31 mm to 33 mm. This was further shown to be nonlinear with the applied strain amplitude, reinforcing the strong coupling between mechanical and thermal response. The results demonstrate that Ni-Ti cantilever beams have significant potential for compact, sustainable solid-state cooling and energy storage applications, with thermal energy transfer strongly dependent on strain and energy transfer optimization. Full article

Nickel-titanium (NiTi) alloys are attractive for functional and biomedical applications due to their shape memory effect, superelasticity, and favorable corrosion resistance and biocompatibility. In this work, the influence of strut size on the compressive response of laser-based powder bed fusion (PBF-LB/M) fabricated NiTi ortho-octahedral porous scaffolds was systematically investigated using combined experiments and finite element simulations. Four scaffold designs with identical unit-cell size (2 mm) but different strut sizes (280, 320, 360, and 400 μm) were fabricated, and their forming quality and deformation behaviors were examined. The as-built scaffolds exhibited high geometric fidelity to the CAD models and stable manufacturability across the investigated parameter range. Quasi-static compression tests revealed a typical three-stage response (linear-elastic regime, plateau/collapse regime, and densification), with both elastic modulus and compressive strength increasing markedly with strut size. Specifically, the modulus increased from 1.17 to 4.28 GPa and the compressive strength increased from 155 to 564 MPa as the strut size increased from 280 to 400 μm. A pronounced oscillatory plateau was observed for the 280 μm scaffolds, indicating progressive layer-by-layer collapse, whereas larger struts promoted a shear-band-dominated failure mode characterized by an approximately 45° fracture zone. Explicit quasi-static simulations reproduced the experimentally observed collapse sequence and demonstrated that stress preferentially concentrates at nodal junctions, with load transfer dominated by struts aligned with the loading direction. The agreement between experiments and simulations confirms the predictive capability of the proposed modeling framework and provides mechanistic insights into geometry-controlled failure. These findings establish a structure-property-failure relationship for PBF-LB/M-fabricated NiTi octahedral scaffolds and offer practical guidance for tailoring stiffness, strength, and collapse mode through strut-size design. Full article

The complex coupling relationships among the thermal, mechanical, and electrical physical parameters of TiZrHf-based medium-entropy alloys represent a key factor restricting their practical applications under complex extreme environments. In this study, the thermo-mechanical-electrical coupling characteristics of TiZrHf and TiZrHfCu_0.8 medium-entropy alloys were systematically investigated using a self-developed experimental platform. The results demonstrate that TiZrHf and TiZrHfCu_0.8 alloys exhibit elastoplastic and superelastic-plastic compressive deformation behaviors, respectively, with both elastic modulus and ultimate strength decreasing monotonically with increasing temperature T. Electrical property measurements reveal that the electrical resistivities ρ of the two alloys range from 3 to 35 × 10⁻⁶ Ω·m. Notably, TiZrHfCu_0.8 possesses a lower resistivity that is independent of the test frequency f. Moreover, ρ increases with T but decreases with applied stress σ. At a frequency of 1 kHz, the real part of the relative dielectric constants ε_r of the alloys varies between −3.5 × 10⁸ and −0.5 × 10⁸ and increases with rising f, whereas the effects of T and σ on ε_r are opposite to those on ρ. Thermal property tests indicate that the thermal conductivities α of both alloys increase with T and eventually stabilize at 28.23 and 53.51 W·m⁻¹·K⁻¹, respectively, while the thermoelectric coefficients S are positively correlated with the heating rate, on the basis of comprehensive data analysis, multi-physical parameter (T, σ) dependent mathematical expressions for elastic modulus, strength, ρ, ε_r, α, and S were established, respectively. This work provides valuable insights into the material response mechanisms under complex service conditions, which are conducive to the optimization of alloy composition design and the promotion of their practical engineering applications. Full article