Search Results (3,503)

The effect of dislocation pile-ups responsible for the generation or annihilation of dislocations during friction of Ag and Ni was considered. The steady-state friction was accompanied by the formation of twin bundles, intersecting twins, dislocations, adiabatic elongated shear bands, and intense dynamic recrystallization. The mechanisms of microstructural stability and friction instability were analyzed. The theoretical models of dislocation generation and annihilation in nanocrystalline FCC metals in the context of plastic deformation and failure development under friction were proposed. The transition to unstable friction was estimated. The damage of Ag was exhibited in the formation of pores, reducing the contact area and significantly increasing the shear stress. The brittle fracture of Ni represents a catastrophic failure associated with the formation of super-hard nickel oxide. Deformation resistance of the dislocation structures in the mesoscale and macroscale was compared. The coefficient of similitude (K) has been introduced in this work to compare plastic deformation at different scales. The model of the strength–ductility trade-off and microstructural instability is considered. The interaction between the migration of dislocation pile-ups and the driving forces applied to the grain boundaries was estimated. Nanostructure stabilization through the addition of a polycrystalline element (solute) to the crystal interiors in order to reduce the free energy of grain boundary interfaces was investigated. The thermodynamic driving force and kinetic energy barrier involved in strengthening, brittleness, or annealing under plastic deformation and phase formation in alloys and composite materials were examined. Full article

The reduced ductility caused by the brittle needle-like α′ martensite limits the application of TC4 alloys produced by selective laser melting (SLM). Appropriate heat treatment can improve the microstructures and properties of SLM-fabricated TC4 alloys. In this work, SLM-fabricated TC4 alloys underwent stress relief annealing at 600 °C and high-temperature annealing at 800 °C. The effects of heat treatment temperature on phase composition, microstructural morphology, grain orientation, and mechanical properties were investigated. Meanwhile, the microstructural evolution and fracture mechanisms during the heat treatment process were analyzed. The results indicate that after annealing at 600 °C, the needle-like α′ phase transforms into elongated α, and nano-β phase increases. When annealed at 800 °C, the α′ phase completely transforms into a more stable lath-shaped α phase and a short rod-shaped β phase, with the nano-β phase disappearing. The texture orientation gradually shifts from <0001> towards <01-10>, where slip systems are more active. Additionally, heat treatment promotes the transition of grain boundaries to high-angle grain boundaries, thereby alleviating stress concentration and enhancing solid-solution strengthening. After heat treatment, the ultimate tensile strength of the material slightly decreases, but the elongation significantly increases. As the annealing temperature increased, the elongation (EL) improved from 5.22% to 11.43%. Following high-temperature annealing at 800 °C, necking and larger dimples appear on the fracture surface, and the fracture mechanism shifts from a mixed brittle–ductile fracture to a ductile fracture. This work provides a theoretical basis for improving the microstructures and properties of SLM-fabricated TC4 alloys through heat treatment. Full article

To develop automotive steel with a higher strength–ductility balance, an 800 MPa grade Nb-Ti microalloyed dual-phase steel with high elongation was designed. Continuous annealing tests were conducted using a continuous annealing simulation testing machine. The effects of annealing temperature and aging temperature on the microstructure and mechanical properties were investigated through SEM, EBSD, TEM, and tensile testing. The results indicate that the microstructure of the steel primarily consists of ferrite, martensite, and a small amount of retained austenite. As the annealing temperature rises, the martensite content increases, and the retained austenite content first increases and then decreases. Therefore, the tensile strength and elongation initially increase and then decrease, while the yield strength gradually decreases. As the aging temperature rises, the martensite content decreases, while the tempering degree of martensite increases and the retained austenite content rises. Therefore, the tensile strength gradually decreases, and the yield strength and elongation gradually increase. The optimal comprehensive performance was achieved with an annealing temperature of 830 °C and an aging temperature of 330 °C, resulting in a tensile strength of 915 MPa, a yield strength of 470 MPa, and an elongation of 24.4%. This represents a 28.4% increase in elongation compared to conventional dual-phase steels of the same strength grade. The strength–ductility product reaches 22.3 GPa%. Full article

This study explores the potential use of Polyethylene Terephthalate (PET) plastic bottles as void makers in short reinforced concrete columns under pure axial compression. Such a scheme promotes sustainability by decreasing the consumption of concrete and reducing the pollution that comes with the disposal of PET bottles. The experimental component of this study consisted of testing 16 reinforced concrete columns divided into two groups, based on the cross-section dimensions. One group contained eight columns of a length of 900 mm with a net cross-sectional area of about 40,000 mm², while the second group contained eight columns of a length of 1100 mm with a net cross-sectional area of about 62,500 mm². The diameter of the void within the small cross-section group was 100 mm and within the large cross-section group was 265 mm. The experimental program includes pairs of solid and corresponding void specimens with consideration of the size of the longitudinal steel reinforcement, lateral tie spacing, and concrete compressive strength. The tests are conducted using a universal test machine under displacement-controlled loading conditions with the help of strain gauges and Linear Variable differential transformers (LVDTs). The analysis of the test results showed that the columns that were embedded with a small void that occupied about 30% of the core area exhibited reductions of 9% in the ultimate capacity, 14% in initial stiffness, 20% in ductility, and 1% in residual strength. On the other hand, the columns that contained a large void occupying about 60% of the core area demonstrated reductions of 24% in the ultimate capacity, 34% in initial stiffness, and 26% in ductility, although the residual strength was slightly increased by 5%. The reason for the deficiency in the structural response in the latter case is because the void occupied a significant fraction of the concrete core. The theoretical part of this study showed that the ACI 318 code provisions can reasonably predict the uniaxial compressive strength of columns embedded with PET bottles if the void does not occupy more than 30% of the concrete core. This study confirmed that short columns embedded with relatively small voids made from PET bottles and subjected to pure axial compression create a balance between sustainability benefits and a structural performance tradeoff. Full article

To overcome brittle failure in conventional cold-formed steel–concrete (CFS-C) corner columns, this paper used fiber-reinforced concrete to replace ordinary concrete, investigating failure mechanisms and performance through systematic numerical simulations. A finite element model (FEM) was established and validated by experiments, and the errors for ultimate capacity were within 10%. A series of numerical models was established for parametric analyses focusing on the effects of the parameters of polypropylene fiber (PF), carbon fiber (CF), steel fiber (SF), and bamboo fiber (BF) with different volume dosages and the thickness of cold-formed steel (CFS) on the axial compression ultimate capacity and corresponding displacement of CFS composite corner columns. The results indicated that (1) PF effectiveness was dependent on steel thickness: thicker steel suppressed micro-defects, activated the toughening potential of PF, and increased the ultimate capacity of the columns by 24.8%. (2) CF had a critical dosage of 0.4%: at this dosage, CF increased the column’s ultimate capacity by 14.1% through stress redistribution, while when the dosage exceeded this value, fiber agglomeration caused a reduction in the column’s strength, with a maximum decrease of 16.2%. (3) SF effectiveness showed a linear increase: at a dosage of 1.6%, SF formed a synergistic three-dimensional bridging network and generated a confinement effect, increasing the column’s ultimate capacity by 36.5% and displacement by 92.2%. (4) BF mainly improved the ductility of columns: through crack bridging and pull-out energy dissipation, BF increased column displacement by 33.2%. (5) The modified Eurocode 4 formula could reduce the calculation error of ultimate capacity from 6.3% to within 1%. The findings guide optimal fiber selection and dosage in practice, promoting such columns’ use in seismic and load-bearing structures. Full article

Additive manufacturing (AM) via selective laser melting (SLM) is increasingly deployed in aerospace, biomedical, and tooling applications where complex geometries and high performance are required. Yet, process-induced anisotropy and microstructural heterogeneity can strongly affect mechanical and tribological behavior. This study systematically evaluates the combined effects of build orientation (0°, 45°, and 90° relative to the build plate) and post-build heat treatment (as-built, 600 °C, and 860 °C) on the phase constitution, microstructure, hardness, tensile response, and dry sliding wear of SLM-fabricated 316L stainless steel. X-ray diffraction indicated a fully austenitic (γ-fcc) structure without detectable secondary phases across all conditions. Orientation-dependent substructures were observed: ~1 µm equiaxed cellular features at 0°, finer 0.3–0.5 µm cells at 45°, and 1–2 µm elongated features at 90°. Microhardness varied with orientation; relative to 0°, 45° specimens were ~15 HV higher, whereas 90° specimens were ~10 HV lower. Heat treatment at 600 °C promoted refinement and recovery of the cellular network, most pronounced in the 45° orientation, while treatment at 860 °C largely erased melt pool boundary contrast, producing a more homogeneous particle-like microstructure. Tensile fractography revealed dimpled rupture in all cases; the 90° orientation showed finer dimples and lower hardness, consistent with a ductile failure mode under reduced constraint. Dry sliding wear tests identified adhesive wear, intensified by the build-up of transferred fragments, as the dominant mechanism in both as-built and 600 °C conditions. Changes to melt pool morphology after 860 °C heat treatment correlated with altered wear track widths, with the 0° condition showing a notable narrowing relative to the 600 °C state. These results highlight processing pathways for tailoring anisotropy, strength–ductility balance, and wear resistance in SLM 316L. Full article

Inspired by natural gradient structures observed in biological systems such as lobster exoskeletons and bamboo, this study proposes a biomimetic strategy for developing advanced automotive materials that achieve an optimal balance between strength and ductility. Against this backdrop, the present work systematically reviews the design principles underlying natural gradient structures and examines the advantages and limitations of current additive manufacturing—specifically selective laser melting (AM-SLM)—as well as conventional forming and machining processes, in fabricating nature-inspired architectures. The research systematically explores hierarchical gradient designs which endow materials with superior mechanical properties, including enhanced strength, stiffness, and energy absorption capabilities. Two primary strengthening mechanisms—hetero-deformation-induced (HDI) hardening and precipitation hardening—were employed to overcome the conventional strength–ductility trade-off. Gradient-structured materials were fabricated using selective laser melting, and microstructural analyses demonstrated that controlled interface zones and tailored precipitation distribution critically influence property improvements. Based on these findings, an integrated material design strategy combining nature-inspired gradient architectures with post-processing treatments is presented, providing a versatile methodology to meet the specific performance requirements of automotive components. Overall, this work offers new insights for developing next-generation lightweight structural materials with exceptional ductility and damage tolerance and establishes a framework for translating bioinspired concepts into practical engineering solutions. Full article

Complex concentrated alloys (CCAs) have attracted significant attention due to their potential to develop materials with enhanced properties, such as increased hardness and strength. These properties are strongly influenced by the chemical composition and the processing method used. Body-centred cubic (BCC) structures are known to have high hardness but low fracture toughness, whereas face-centred cubic (FCC) structures typically exhibit lower hardness but higher toughness. In this study, Al-Cr-Cu-Fe-Mn-Ni CCAs with three distinct compositions were produced using pressureless sintering. One set of samples was prepared with equiatomic composition (composition E), whereas the compositions of the other two sets were defined based on thermodynamic calculations to obtain sintered samples predominantly formed by BCC (composition B) or FCC (composition F) phases. The samples were characterized using X-ray diffraction, scanning and transmission electron microscopy, energy-dispersive X-ray spectroscopy, electron backscatter diffraction, density measurements, hardness measurements, and uniaxial compression tests. For all compositions, good agreement was obtained between the phases predicted by thermodynamic calculations and those experimentally detected. In addition, significant differences in the mechanical properties were observed between samples with each composition. The samples with composition B exhibited the highest hardness, but almost no ductility. In contrast, samples with composition F showed the lowest yield strength and hardness, but the highest ductility. Samples with composition E had intermediate values between those of samples B and F. These differences were attributed to differences in the proportions and properties of the BCC and FCC phases in each composition and demonstrate that the mechanical properties of Al-Cr-Cu-Fe-Mn-Ni CCAs can be tailored using compositions defined based on thermodynamic calculations. Full article

This study investigates the microstructure evolution and mechanical properties of DSS2209 duplex stainless steel fabricated via cold metal transfer wire arc additive manufacturing (CMT-WAAM). The as-deposited thin-wall components exhibit significant microstructural heterogeneity along the build height due to thermal history variations. Optical microscopy, SEM-EDS, and EBSD analyses reveal distinct phase distributions: the bottom region features elongated blocky austenite with Widmanstätten austenite (WA) due to rapid substrate-induced cooling; the middle region shows equiaxed blocky austenite with reduced grain boundary austenite (GBA) and WA, attributed to interlayer thermal cycling promoting recrystallization and grain refinement (average austenite grain size: 4.16 μm); and the top region displays coarse blocky austenite from slower cooling. Secondary austenite (γ₂) forms in interlayer remelted zones with Cr depletion, impacting pitting resistance. Mechanical testing demonstrates anisotropy; horizontal specimens exhibit higher strength (UTS: 610 MPa, YS: 408 MPa) due to layer-uniform microstructures, while vertical specimens show greater ductility (elongation) facilitated by columnar grains aligned with the build direction. Hardness ranges uniformly between 225–239 HV. The study correlates process-induced thermal gradients (e.g., cooling rates, interlayer cycling) with microstructural features (recrystallization fraction, grain size, phase morphology) and performance, providing insights for optimizing WAAM of large-scale duplex stainless steel components like marine propellers. Full article

The paper industry is always looking for possible solutions for new fiber-based products, such as protective and cushioning materials. These materials must be carefully designed to provide effective cushioning while also being lightweight to reduce transportation costs. Additionally, they need to offer protection from environmental and mechanical damage, besides having good processability to ensure proper buffering. The widely used protective and cushioning materials, such as plastic foams and expanded or extruded polystyrene, create significant disposal challenges. Therefore, there is increasing demand for biodegradable and sustainable materials for cushioning applications. The focus of our research was to develop fiber-based foams and investigate the influence of different compositions (hardwood and softwood) of cellulose fibers on the basic (mass, thickness, density) and mechanical properties (three-point bend test, tensile properties). Foams made entirely from short eucalyptus fibers (100S) exhibited the highest density (28.0 ± 0.34 kg/m³) and lowest thickness (38.82 ± 4.21 mm), resulting in superior tensile strength and elastic modulus but lower strain at break. In contrast, foams composed of long spruce fibers (100L) had the lowest density (19.0 ± 0.27 kg/m³) and highest thickness (58.52 ± 1.50 mm), with lower strength and stiffness but much higher ductility and porosity (confirmed by ~30% higher air permeability compared to 100S). Blended formulations demonstrated intermediate behavior, with the 50S50L foam showing a favorable balance of strength, stiffness, and flexibility. Visual analysis confirmed heterogeneous fiber distribution with localized agglomerates and compaction at the bottom layer due to casting. To further interpret the complex relationships within the dataset and uncover patterns, Principal Component Analysis (PCA) was applied to all experimental results. The findings of the research contribute to the broader understanding of how different fiber types and blends impact the performance of sustainable cellulose-based foams, with potential implications for the development of biodegradable packaging and lightweight construction materials. Full article

High-entropy alloys (HEAs) have shown great promise for applications in extreme service environments due to their exceptional mechanical properties and thermal stability. However, traditional alloy design often struggles to balance multiple properties such as strength and ductility. Constructing heterogeneous microstructures has emerged as an effective strategy to overcome this challenge. With the rapid advancement of additive manufacturing (AM) technologies, their unique ability to fabricate complex, spatially controlled, and non-equilibrium microstructures offers unprecedented opportunities for tailoring heterostructures in HEAs with high precision. This review highlights recent progress in utilizing AM to engineer heterogeneous microstructures in high-performance HEAs. It systematically examines the multiscale heterogeneities induced by the thermal cycling effects inherent to AM techniques such as selective laser melting (SLM) and electron beam melting (EBM). The review further discusses the critical role of these heterostructures in enhancing the synergy between strength and ductility, as well as improving work-hardening behavior. AM enables the design-driven fabrication of tailored microstructures, signaling a shift from traditional “performance-driven” alloy design paradigms toward a new model centered on “microstructural control”. In summary, additive manufacturing provides an ideal platform for constructing heterogeneous HEAs and holds significant promise for advancing high-performance alloy systems. Its integration into alloy design represents both a valuable theoretical framework and a practical pathway for developing next-generation structural materials with multiple performance attributes. Full article

Metastable titanium alloys have been developed for biomedical use due to their lower elastic modulus, combined with high strength, good ductility, and excellent corrosion resistance. In this study, the electrochemical corrosion resistance of the alternative Ti-23.6Nb-5.1Mo-6.7Zr alloy was investigated. The alloy was initially homogenized at 1000 °C for 24 h and then tested under different processing conditions: 90% cold rolling; 90% cold rolling followed by annealing at 950 °C for 1 h and water quenching; and 90% cold rolling followed by aging at 300 °C, 400 °C, and 500 °C for 4 h each. Electrochemical behavior was assessed using anodic polarization, open circuit potential (OCP), and electrochemical impedance spectroscopy (EIS) tests in a synthetic solution (Ringer’s solution) to simulate body fluid. The obtained results demonstrate the stability of the passive film formed of the conventional and modified alloys, considering long-term use in the human body, regardless of the volumetric fraction and phase distribution across the various processing routes studied as β, α, α″ and ω. The electrochemical parameters, combined with Young’s modulus and hardness of the alternative alloys, enable the definition of a multicriteria selection method of the most suitable mechanical process routes to be used. The application focused on components of functional femoral stems. Full article

The affordability, ease of manufacturing, and assembly efficiency of cold-formed steel profiles have contributed to their widespread use in structural applications. However, the presence of holes in these profile webs is likely to reduce their mechanical resistance. This study explores the bending behavior of a built-up box section constructed using lipped and unlipped C-profiles, which are commonly utilized in the construction industry. The investigation focuses on the influence of self-drilling screw layout density and hole distribution within the section. A total of 30 different models were analyzed, considering three primary variables: the spacing of self-drilling screws, hole diameter, and the number of holes. The steel profiles were connected using self-drilling screws with spacing intervals of 100, 200, and 400 mm. Key parameters, such as moment capacity, effects on elastic zones, shear forces on screws, and ductility, were examined in relation to these variables. The findings indicate that reducing screw spacing and increasing the number of holes are crucial design factors for improving joint strength. However, while greater screw spacing enhances ductility, it leads to lower plastic deformation rates. Additionally, optimizing the number of holes in the section proved to be an effective strategy for improving ductility in the analyzed models. Mathematical evaluation confirmed that hole number and screw spacing significantly affect moment capacity and estimation stability, highlighting the need for their joint optimization in structural design. Full article

Metallic nanolaminates generally show ultra-high strength but low ductility due to their vulnerability to shear instability during deformation. Herein, we report the simultaneous enhancement in hardness (by 11.9%) and suppression of shear instability in a 10 nm Cu/Zr nanolaminate, achieved by introducing a nanoscale Cu₆₃Zr₃₇ amorphous interfacial layer (AIL) between the crystalline Cu and Zr layers via magnetron sputtering. The effect of AIL and its thickness (h) (h = 2, 5, and 10 nm) on the hardness and shear instability behavior was explored using nano- and micro-indentation tests. An abnormal increase in hardness occurs at h = 2 nm when h is decreased from 10 to 2 nm, deviating from the prediction of the rule of mixtures. This abnormal strengthening is attributed to thinner AIL, which induces an increased density of crystalline/amorphous interfaces, thereby generating a pronounced interface strengthening effect. The micro-indentation results show that shear banding was suppressed in the nanolaminate with AIL, as evidenced by fewer shear bands as compared to its homogeneous counterpart. This enhanced resistance to shear instability may originate from the crystalline/amorphous interface that provides more sites for dislocation nucleation, emission, and annihilation. Furthermore, two distinct shear banding modes were observed in the nanolaminate with AIL; i.e., a cutting-like shear banding emerged at h = 10 nm, whereas a kinking-like shear banding occurred at h = 2 nm. The potential mechanism of the AIL-thickness-dependent shear banding was analyzed based on the crack propagation model of the Griffith criterion. This study provides a comprehensive insight into the strengthening and tunable shear instability of super-nano metallic laminates by AIL. Full article

To evaluate the mechanical properties of connectors in timber–concrete composite (TCC) structures under low-cycle reversed loading, eighteen push-out specimens were designed and fabricated following the standard push-out test method. This study presents the first comparative analysis of the seismic performance between notch-bolted and ordinary bolted connections across three bolt diameters (12 mm, 16 mm, and 20 mm), addressing a gap in systematic experimental data for different connection types. Key performance indices under cyclic loading—including stiffness degradation, strength degradation, energy dissipation capacity, and ductility—were investigated. Furthermore, cumulative damage analysis elucidated the damage accumulation process, establishing a damage index (Dw) based on an energy method and proposing Dw = 0.6 as a critical early-warning threshold for failure. Practical recommendations for seismic design and engineering applications are provided. The results demonstrate that compared to ordinary bolted connections, notch-bolted connections achieve a 15–30% increase in ultimate bearing capacity and exhibit superior stiffness. Specimens with 16 mm bolts exhibited optimal ductility (ductility coefficient ξ = 3.6), while notch-bolted connections maintained stable ductility within the range of ξ = 2–3. Finally, a numerical model was developed using ANSYS finite element software. Validation against experimental results confirmed the model’s accuracy in simulating structural behavior. This research elucidates the cumulative damage mechanisms in TCC structures under cyclic loading, providing a theoretical basis for design optimization and valuable insights for promoting the seismic application of these composite systems. Full article