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Keywords = rough fracture

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17 pages, 2564 KB  
Article
Dynamic Analysis of the Rod-Traction System for Ship-Borne Aircraft Under High Sea States
by Guofang Nan, Chen Zhang, Bodong Zhang, Sirui Yang and Jinrui Hu
Aerospace 2026, 13(1), 107; https://doi.org/10.3390/aerospace13010107 - 22 Jan 2026
Viewed by 46
Abstract
The transfer of aircraft on deck relies on the traction system, which is easily affected by the offshore environment. Violent ship motion in the complex marine environment poses a great threat to the aircraft traction process, such as the tire sideslip, off-ground phenomena, [...] Read more.
The transfer of aircraft on deck relies on the traction system, which is easily affected by the offshore environment. Violent ship motion in the complex marine environment poses a great threat to the aircraft traction process, such as the tire sideslip, off-ground phenomena, the aircraft overturning, traction rod fatigue fracture, and so on. Therefore, it has merits in both academia and engineering practice to study the dynamic behaviors of the ship-borne aircraft towing system under high sea states. Considering the intricate coupling motions of the hull roll, pitch, and heave, the dynamic analysis of the towing system with rod are carried out based on the multibody dynamics theory. The influence of the sea state level and the traction speed on the dynamic characteristics of the towing system is investigated. The results indicate that noticeable tire sideslip occurs under sea state 3, with the peak lateral tire force increasing by approximately 250% compared with sea state 2. Under sea state 4, intermittent off-ground phenomena are observed, accompanied by a further increase of about 22% in lateral tire force. These findings provide quantitative insights into the dynamic characteristics and operational limits of rod-traction systems for ship-borne aircraft in rough marine environments. Full article
(This article belongs to the Section Aeronautics)
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16 pages, 5786 KB  
Article
Advancing Circular Composite Strategies by Vitrimer-Enabled Reuse of Unidirectional Laminates
by Jannick Fuchs, Nico Schuhmann, Jonathan Alms and Christian Hopmann
Polymers 2026, 18(2), 300; https://doi.org/10.3390/polym18020300 - 22 Jan 2026
Viewed by 77
Abstract
To efficiently reuse endless fibre-reinforced composites after their life cycle, the recovery of endless fibres including matrix material with subsequent reprocessing in their original state is desirable. Thanks to their covalent adaptive networks, vitrimers offer ideal properties for enabling new repair and circular [...] Read more.
To efficiently reuse endless fibre-reinforced composites after their life cycle, the recovery of endless fibres including matrix material with subsequent reprocessing in their original state is desirable. Thanks to their covalent adaptive networks, vitrimers offer ideal properties for enabling new repair and circular strategies for composites. In order to evaluate the detachability—meaning the separation of single laminate layers—and recycling potential for continuous fibre reinforcement, process routes and quality parameters must be established. In this study, the double cantilever beam test is used to test the adhesion based on the detachment of continuous fibre layers, and the interlaminare fracture toughness of mode I (GIC) is measured as a parameter for the required energy for detachment. It was shown that GIC increases above the vitrimer transition temperature and is higher than for reference specimens with an epoxy matrix. Surface roughness is measured to determine the mechanical and thermal degradation of the chemical network structure and additionally shows fibre cracking and defects in fibre–matrix interfaces. This allows the recycling process to be evaluated up to the production of a second generation, with the aim of identifying the recycling potential of the vitrimer matrix and implementing it for industrial processes. An efficient recycling strategy of the continuous fibre-reinforced vitrimers was thus demonstrated by hot pressing at 190 °C for 45 min, giving vitrimer samples a second life. Full article
(This article belongs to the Section Innovation of Polymer Science and Technology)
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21 pages, 13400 KB  
Article
Numerical Simulation Study on the Influence of Physical Heterogeneity on the Dissolution Rate of Carbonate Rock
by Yunchao Lei, Zihao Li and Yuxiang Lv
Minerals 2026, 16(1), 110; https://doi.org/10.3390/min16010110 - 21 Jan 2026
Viewed by 65
Abstract
Seepage–dissolution in carbonate rock fractures serves as the core driver governing the evolution of key engineering projects, including reservoir dam stability, CO2 geological sequestration, and unstable rock collapse mitigation strategies. While physical heterogeneity (e.g., fracture aperture, mineral distribution) is widely recognized as [...] Read more.
Seepage–dissolution in carbonate rock fractures serves as the core driver governing the evolution of key engineering projects, including reservoir dam stability, CO2 geological sequestration, and unstable rock collapse mitigation strategies. While physical heterogeneity (e.g., fracture aperture, mineral distribution) is widely recognized as a critical factor regulating dissolution processes, the specific influence of mineral distribution heterogeneity on dissolution rates still lacks quantitative quantification. To address this gap, this study focuses on limestone fractures and employs multi-component reactive transport numerical simulations to model acidic fluid (pH = 5.0) seepage–dissolution under two Darcy flux conditions (37.8/378 m·yr−1). It investigates the controlling mechanisms of fracture roughness (λb = 0.036~0.308) and calcite contents (55%, 75%, 95%) on dissolution dynamics, and analyzes spatial variations in local Darcy velocity, reaction rate, and effective dissolution rate (Reff,i). Results demonstrate that mineral distribution heterogeneity directly induces pronounced spatial heterogeneity in dissolution behavior: diffusion dominates under low flux (simulation duration: 48.3 days), forming discrete reaction fronts (~15 mm) controlled by mineral clusters; advection prevails under high flux (simulation duration: 4.83 days), generating alternating dissolution–deposition zones (~7.5 mm) with Reff,i one order of magnitude greater than that under low flux. Notably, 55% calcite content yields the highest Reff,i (1.87 × 10−11 mol·m−2·s−1), 0.94 orders of magnitude greater than that at 95% calcite content. A strong linear correlation (R2 > 0.98) exists between the Damköhler number (DaI) and Reff,i at the same calcite content. Furthermore, the synergistic interaction between fracture aperture and mineral heterogeneity amplifies dissolution complexity, with high roughness (λb = 0.308) coupled with 55% calcite content achieving the highest Reff,i of 2.1 × 10−11 mol·m−2·s−1. This study provides critical theoretical insights and quantitative data support for fractured rock mass evolution prediction models, geological hazard prevention, and geological carbon sequestration optimization. Full article
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28 pages, 5991 KB  
Article
Particle Transport in Self-Affine Rough Rock Fractures: A CFD–DEM Analysis of Multiscale Flow–Particle Interactions
by Junce Xu, Kangsheng Xue, Hai Pu and Xingji He
Fractal Fract. 2026, 10(1), 66; https://doi.org/10.3390/fractalfract10010066 - 19 Jan 2026
Viewed by 160
Abstract
Understanding particle transport in rough-walled fractures is essential for predicting flow behavior, clogging, and permeability evolution in natural and engineered subsurface systems. This study develops a fully coupled CFD–DEM framework to investigate how self-affine fractal roughness, represented by the Joint Roughness Coefficient (JRC), [...] Read more.
Understanding particle transport in rough-walled fractures is essential for predicting flow behavior, clogging, and permeability evolution in natural and engineered subsurface systems. This study develops a fully coupled CFD–DEM framework to investigate how self-affine fractal roughness, represented by the Joint Roughness Coefficient (JRC), governs fluid–particle interactions across multiple scales. Nine fracture geometries with controlled roughness were generated using a fractal-based surface model, enabling systematic isolation of roughness effects. The results show that increasing JRC introduces a hierarchy of geometric perturbations that reorganize the flow field, amplify shear and velocity-gradient fluctuations, and enhance particle–wall interactions. Particle migration exhibits a nonlinear response to roughness due to the competing influences of disturbance amplification and the formation of preferential high-velocity pathways. Furthermore, roughness-controlled scaling relations are identified for mean particle velocity, residence time, and energy dissipation, revealing JRC as a fundamental parameter linking geometric complexity to transport efficiency. Based on these findings, a unified mechanistic framework is established that conceptualizes fractal roughness as a multiscale geometric forcing mechanism governing hydrodynamic heterogeneity, particle dynamics, and dissipative processes. This framework provides new physical insight into transport behavior in rough fractures and offers a scientific basis for improved prediction of clogging, proppant placement, and transmissivity evolution in subsurface engineering applications. Full article
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16 pages, 5668 KB  
Article
Effect of Selectively Etched Al-Rich and Si-Rich Microstructures on the Adhesion of Polyimide Coatings to SLM AlSi10Mg
by Jianzhu Li, Shuo Yang and Yujie Li
Materials 2026, 19(2), 385; https://doi.org/10.3390/ma19020385 - 18 Jan 2026
Viewed by 154
Abstract
Interfacial adhesion between selective laser-melted (SLM) AlSi10Mg and polyimide (PI) insulating coatings is often limited by mismatched physicochemical properties. To improve adhesion, Al-rich and Si-rich microstructured surfaces were fabricated on the XY plane (perpendicular to the build direction) and the Z plane (parallel [...] Read more.
Interfacial adhesion between selective laser-melted (SLM) AlSi10Mg and polyimide (PI) insulating coatings is often limited by mismatched physicochemical properties. To improve adhesion, Al-rich and Si-rich microstructured surfaces were fabricated on the XY plane (perpendicular to the build direction) and the Z plane (parallel to the build direction) by acidic and alkaline etching, exploiting the characteristic microstructure of SLM AlSi10Mg. Surface topography, chemical composition, and wettability were characterized, and interfacial mechanical performance was evaluated by shear and pull-off tests. The microstructures increased surface roughness and improved wettability. The shear strength rose from 2.6 ± 1.5 MPa for the polished surface to 43.2 ± 8.6 MPa. The polished surface showed a pull-off strength of 2.2 ± 0.25 MPa. In pull-off tests, failure mainly occurred within the dolly/adhesive/PI system, indicating that the interfacial tensile strength exceeded the strength of the adhesive system; the maximum measured pull-off strength was 29.0 ± 1.3 MPa. Fractography predominantly showed cohesive failure in PI on Al-rich microstructures. Si-rich microstructures exhibited mixed failure, including fracture of the Si skeleton and tearing of PI, together with interfacial microcracks. Full article
(This article belongs to the Special Issue Friction, Wear and Surface Engineering of Materials)
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13 pages, 1385 KB  
Article
Mechanical Properties of Additively Manufactured Composite Resin vs. Subtractively Manufactured Hybrid Ceramic Implant-Supported Permanent Crowns Before and After Thermal Aging
by Nilufer Ipek Sahin and Emre Tokar
Micromachines 2026, 17(1), 116; https://doi.org/10.3390/mi17010116 - 16 Jan 2026
Viewed by 152
Abstract
This study aims to compare the surface roughness and fracture resistance of implant-supported permanent crowns additively manufactured using composite resins (Crowntec, VarseoSmile) versus subtractively manufactured polymer-infiltrated hybrid ceramic (VITA Enamic) at various wall thicknesses using an experimental setup as close to clinical as [...] Read more.
This study aims to compare the surface roughness and fracture resistance of implant-supported permanent crowns additively manufactured using composite resins (Crowntec, VarseoSmile) versus subtractively manufactured polymer-infiltrated hybrid ceramic (VITA Enamic) at various wall thicknesses using an experimental setup as close to clinical as possible. 180 crowns were fabricated in three thicknesses (1.0, 1.5, and 2.0 mm) and cemented onto titanium abutments. Experimental groups underwent thermal aging (10,000 cycles) to simulate one year of clinical service. Surface roughness was measured via profilometry, and fracture resistance was assessed using a universal testing machine. Composite resin crowns exhibited lower surface roughness and lower fracture resistance than subtractively manufactured crowns. No significant difference in fracture resistance was found between materials at 1.0 mm (p > 0.05). However, at 1.5 and 2.0 mm, hybrid ceramic network crowns showed significantly higher resistance (p < 0.01). It was concluded that, within the limitations of this 1-year simulated study, both material-method combinations met the biological threshold for surface roughness. Regarding fracture resistance, composite resins and hybrid ceramics satisfied clinical requirements for molar bite forces only at thicknesses of 1.5 mm and above. 1.0 mm thickness may pose a risk under high occlusal loads. Full article
(This article belongs to the Section D3: 3D Printing and Additive Manufacturing)
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15 pages, 5772 KB  
Article
Study on Formation Mechanism of Edge Cracks and Targeted Improvement in Hot-Rolled Sheets of Grain-Oriented Electrical Steel
by Weidong Zeng, Hui Tang, Xiaoyong Tang, Jiaming Wang, Zhongyu Piao and Fangqin Dai
Metals 2026, 16(1), 96; https://doi.org/10.3390/met16010096 - 15 Jan 2026
Viewed by 202
Abstract
Edge cracks in hot-rolled sheets of industrial grain-oriented electrical steel significantly affect the yield rate and pose substantial challenges to cold rolling fabrication. Eliminating such structural defects through hot rolling requires a thorough understanding of their formation mechanism. This study investigates the formation [...] Read more.
Edge cracks in hot-rolled sheets of industrial grain-oriented electrical steel significantly affect the yield rate and pose substantial challenges to cold rolling fabrication. Eliminating such structural defects through hot rolling requires a thorough understanding of their formation mechanism. This study investigates the formation mechanism of edge cracks in hot-rolled sheets, which are characterized by coarse strip-like grains with typical thicknesses ranging from 20 μm to 100 μm. Coarse, strip-shaped grains have low fracture stress, which is the cause of edge cracks. They originate from abnormally developed columnar grains in continuous casting slabs after reheating, which is unavoidable in industrial large-scale production. Inadequate fragmentation and insufficient recrystallization during rough rolling result in residual coarse grains of intermediate slabs, and their preferential deformation and outward protrusion lead to the formation of grooves. In the subsequent finishing rolling process, deformed coarse grains near the grooves undergo further elongation, developing into distinct strip-like structures. Based on the above mechanistic understanding, the edge microstructure under various rolling parameters was investigated, and targeted improvement measures for edge cracks were proposed. It is concluded that the edge quality can be significantly enhanced through increasing the total width reduction, additional rough rolling passes, and the implementation of edge heating during rough rolling. Quantitative analysis demonstrates that increasing the rolling passes from D to E significantly reduces the fraction of band structure from 64% to 48% and the average width of elongated grains from 43.5 μm to 38.4 μm. Full article
(This article belongs to the Section Metal Casting, Forming and Heat Treatment)
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17 pages, 2160 KB  
Article
Effect of Sandblasting, Tribochemical Silica Coating, CO2 Laser, and Plasma-Enhanced Chemical Vapor Deposition on Surface Characteristics and Shear Bond Strength of 3Y-TZP Zirconia
by Mohammed A. Alrabiah and Fahad Alkhudhairy
Crystals 2026, 16(1), 59; https://doi.org/10.3390/cryst16010059 - 14 Jan 2026
Viewed by 133
Abstract
To evaluate the influence of different surface conditioning protocols—sandblasting (SB), tribochemical silica coating (TBC), CO2 laser irradiation, and plasma-enhanced chemical vapor deposition (PECVD-Si coating for 49 min) on surface roughness (Ra), surface morphology, and composite-to-zirconia shear bond strength (SBS). Eighty 3Y-TZP plates [...] Read more.
To evaluate the influence of different surface conditioning protocols—sandblasting (SB), tribochemical silica coating (TBC), CO2 laser irradiation, and plasma-enhanced chemical vapor deposition (PECVD-Si coating for 49 min) on surface roughness (Ra), surface morphology, and composite-to-zirconia shear bond strength (SBS). Eighty 3Y-TZP plates were randomly allocated into four groups (n = 20) based on surface conditioning protocol: Group 1 (SB), Group 2 (CO2 laser), Group 3 (TBC), and Group 4 (PECVD-Si coating for 49 min). From each group, five specimens underwent Ra assessment using a contact profilometer, and five specimens were examined for surface morphology via scanning electron microscopy (SEM). The remaining ten specimens received resin composite buildup, followed by artificial aging. Subsequently, SBS testing was performed using a universal testing machine, and failure modes were evaluated under a stereomicroscope. Statistical analysis was conducted using one-way ANOVA with post hoc Tukey test and chi-square for fracture assessment(α = 0.05). Group 1 (SB) demonstrated the lowest Ra (0.844 ± 0.063 µm) and SBS (12.21 ± 4.6 MPa), whereas Group 4 (PECVD-Si coating for 49 min) exhibited the highest Ra (1.388 ± 0.098 µm) and SBS (30.48 ± 2.5 MPa). Intergroup comparison revealed no statistically significant differences between Groups 2 and 3 for both Ra and SBS values (p > 0.05). However, Groups 1 and 4 differed significantly in both parameters (p < 0.05). PECVD-based silica coating for 49 min demonstrated superior surface conditioning efficacy for 3Y-TZP, yielding significantly higher Ra and SBS values compared to sandblasting, tribochemical silica coating, and CO2 laser irradiation. Full article
(This article belongs to the Section Inorganic Crystalline Materials)
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21 pages, 3487 KB  
Article
Preparation and Performance Evaluation of Gelled Composite Plugging Agent Suitable for Fractured Formation
by Kecheng Liu, Kaihe Lv, Weiju Wang, Tao Ren, Jing He and Zhangkun Ren
Gels 2026, 12(1), 36; https://doi.org/10.3390/gels12010036 - 31 Dec 2025
Viewed by 180
Abstract
Lost circulation in fractured formations is a common yet challenging technical problem in drilling engineering. Conventional plugging methods often form sealing layers with poor stability and low pressure-bearing capacity. This study developed an efficient composite plugging agent composed of calcite particles (rigid particles), [...] Read more.
Lost circulation in fractured formations is a common yet challenging technical problem in drilling engineering. Conventional plugging methods often form sealing layers with poor stability and low pressure-bearing capacity. This study developed an efficient composite plugging agent composed of calcite particles (rigid particles), elastic gel particles, and polypropylene fibers. Utilizing a laboratory-scale fracture plugging evaluation apparatus and standard comparative experimental methods, the synergistic plugging effects of different composite systems were investigated. The results indicate that while single rigid particles can form a basic bridging structure, the pressure-bearing capacity of the resulting sealing layer is limited. Single elastic gel particles or fibrous materials struggle to effectively plug fractures of varying widths. Composite use of the plugging agents significantly enhanced the plugging performance, with the rigid/elastic/fiber ternary composite system demonstrating the best results. The optimal formulation (5% calcite particles + 3% elastic gel particles + 2% polypropylene fibers) achieved a plugging pressure-bearing capacity of 13 MPa for 2 mm-wide fractures, with a fluid loss of only 50 mL and temperature resistance up to 180 °C. Furthermore, the composite plugging agent exhibited good compatibility with the drilling fluid system and demonstrated excellent adaptability and plugging performance for fractures with different roughness levels, indicating promising potential for field application. Full article
(This article belongs to the Topic Polymer Gels for Oil Drilling and Enhanced Recovery)
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27 pages, 4782 KB  
Review
Recent Advances in Hybrid Non-Conventional Assisted Ultra-High-Precision Single-Point Diamond Turning
by Shahrokh Hatefi, Yimesker Yihun and Farouk Smith
Processes 2026, 14(1), 84; https://doi.org/10.3390/pr14010084 - 26 Dec 2025
Viewed by 713
Abstract
Ultra-precision single-point diamond turning (SPDT) remains the core process for fabricating optical-grade surfaces with nanometric roughness and sub-micrometer form accuracy. However, machining hard-to-cut or brittle materials such as high-entropy alloys, metals, ceramics, and semiconductors is limited by severe tool wear, high cutting forces, [...] Read more.
Ultra-precision single-point diamond turning (SPDT) remains the core process for fabricating optical-grade surfaces with nanometric roughness and sub-micrometer form accuracy. However, machining hard-to-cut or brittle materials such as high-entropy alloys, metals, ceramics, and semiconductors is limited by severe tool wear, high cutting forces, and brittle fracture. To overcome these challenges, a new generation of non-conventional assisted and hybrid SPDT platforms has emerged, integrating multiple physical fields, including mechanical, thermal, magnetic, chemical, or cryogenic methods, into the cutting zone. This review comprehensively summarizes recent advances in hybrid non-conventional assisted SPDT platforms that combine two or more assistive techniques such as ultrasonic vibration, laser heating, magnetic fields, plasma or gas shielding, ion implantation, and cryogenic cooling. The synergistic effects of these dual-field platforms markedly enhance machinability, suppress tool wear, and extend ductile-mode cutting windows, enabling direct ultra-precision machining of previously intractable materials. Recent key case studies are analyzed in terms of material response, surface integrity, tool life, and implementation complexity. Comparative analysis shows that hybrid SPDT can significantly reduce surface roughness, extend diamond tool life, and yield optical-quality finishes on hard-to-cut materials, including ferrous alloys, composites, and crystals. This review concludes by identifying major technical challenges and outlining future directions toward optimal hybrid SPDT platforms for next-generation ultra-precision manufacturing. Full article
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23 pages, 3622 KB  
Article
Influence of Dispersed Phase Reinforcement on Performance and Wear Mechanism of Ceramic Tools in Rough Milling of Inconel 718
by Paweł Piórkowski and Wojciech Borkowski
Appl. Sci. 2026, 16(1), 62; https://doi.org/10.3390/app16010062 - 20 Dec 2025
Viewed by 300
Abstract
Machining nickel-based superalloys, such as Inconel 718, poses a significant technological challenge due to their high-temperature strength and low thermal conductivity, leading to rapid tool wear. This paper presents a comprehensive comparative analysis of two roughing strategies: high-feed milling and plunge milling, utilizing [...] Read more.
Machining nickel-based superalloys, such as Inconel 718, poses a significant technological challenge due to their high-temperature strength and low thermal conductivity, leading to rapid tool wear. This paper presents a comprehensive comparative analysis of two roughing strategies: high-feed milling and plunge milling, utilizing a unique custom-designed milling head. The primary objective was to evaluate the impact of tool material reinforcement on the process by comparing SiC whisker-reinforced ceramic inserts (CW100) with non-reinforced inserts (CS300). The experiment involved measuring cutting force components, power consumption, and analyzing tool wear progression (VBB) and mechanisms. Results showed that the presence of the reinforcing phase is critical for reducing the axial force component (Fz), particularly in plunge milling, where CW100 inserts achieved a 30–35% force reduction and avoided the catastrophic failure observed in non-reinforced ceramics. Microscopic analysis confirmed that composite inserts undergo predictable abrasive wear, whereas CS300 inserts are prone to brittle fracture and spalling. Multi-criteria optimization using Grey Relational Analysis (GRA) identified high-feed milling with reinforced inserts as the most efficient strategy, while also positioning plunge milling with composites as a competitive, less energy-intensive alternative. Full article
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15 pages, 12323 KB  
Article
Research on Machining Characteristics of C/SiC Composite Material by EDM
by Peng Yu, Ziyang Yu, Lize Wang, Yongcheng Gao, Qiang Li and Yiquan Li
Micromachines 2025, 16(12), 1423; https://doi.org/10.3390/mi16121423 - 18 Dec 2025
Viewed by 339
Abstract
Carbon fiber reinforced silicon carbide (C/SiC) composite material exhibits exceptional properties, including high strength, high stiffness, low density, outstanding high-temperature performance, and corrosion resistance. Consequently, they are widely used in aerospace, defense, and automotive engineering. However, their anisotropic, high hardness, and brittle characteristics [...] Read more.
Carbon fiber reinforced silicon carbide (C/SiC) composite material exhibits exceptional properties, including high strength, high stiffness, low density, outstanding high-temperature performance, and corrosion resistance. Consequently, they are widely used in aerospace, defense, and automotive engineering. However, their anisotropic, high hardness, and brittle characteristics make them a typical difficult-to-machine material. This paper focuses on achieving high-quality micro hole machining of C/SiC composite material via electrical discharge machining. It systematically investigates electrical discharge machining characteristics and innovatively develops a hollow internal flow helical electrode reaming process. Experimental results reveal four typical chip morphologies: spherical, columnar, blocky, and molten. The study uncovers a multi-mechanism cutting process: the EDM ablation of the composite involves material melting and explosive vaporization, the intact extraction and fracture of carbon fibers, and the brittle fracture and spalling of the SiC matrix. Discharge energy correlates closely with surface roughness: higher energy removes more SiC, resulting in greater roughness, while lower energy concentrates on m fibers, yielding higher vaporization rates. C fiber orientation significantly impacts removal rates: processing time is shortest at θ = 90°, longest at θ = 0°, and increases as θ decreases. Typical defects such as delamination were observed between alternating 0° and 90° fiber bundles or at hole entrances. Cracks were also detected at the SiC matrix–C fiber interface. The proposed hole-enlargement process enhances chip removal efficiency through its helical structure and internal flushing, reduces abnormal discharges, mitigates micro hole taper, and thereby improves forming quality. This study provides practical references for the EDM of C/SiC composite material. Full article
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16 pages, 3888 KB  
Review
Bone–Ti-Alloy Interaction in Hip Arthroplasty of Patients with Diabetes, Dyslipidaemia, and Kidney Dysfunction: Three Case Reports and Brief Review
by Cosmin Constantin Baciu, Ana Maria Iordache, Teodoru Soare, Nicolae Catalin Zoita, Cristiana Eugenia Ana Grigorescu and Mircea Bogdan Maciuceanu Zarnescu
Medicina 2025, 61(12), 2228; https://doi.org/10.3390/medicina61122228 - 17 Dec 2025
Viewed by 284
Abstract
Background and Objectives: Organ dysfunctions affect the quality of bone and body fluids. This case report seeks links between the underlying conditions of three patients undergoing hip arthroplasty (HA) with uncemented implants, the quality of their bones, and their Ti-6Al-4V orthopaedic implants, [...] Read more.
Background and Objectives: Organ dysfunctions affect the quality of bone and body fluids. This case report seeks links between the underlying conditions of three patients undergoing hip arthroplasty (HA) with uncemented implants, the quality of their bones, and their Ti-6Al-4V orthopaedic implants, on different time spans. Femoral stems are investigated. A brief review supports our findings. Materials and Methods: Cases: two women (F1 35+, F2 80+), and one man (M 65+), all having diabetes, dyslipidaemia, and kidney dysfunction. Samples: a segment of a broken 7-year-old stem, bone with a metallic layer, soft tissue, segments of one spare stem, and synthetic plasma enriched with glucose and urea according to the biochemistry tests of the respective patients. Vast studies show that cholesterol influences bone quality only. The stem pieces were ultrasonicated for 7 h at 37 °C in synthetic plasma. Scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), and profilometry investigated the Ti-alloy samples, electrochemistry analysed the post-sonication plasma, and histopathology examination was performed on the soft tissue remnants on the broken stem. Results: EDX show that all stem samples are Ti-6Al-4V with minute additions of other elements and hydroxyapatite (HAp) coating. SEM and profilometry analysis are consistent for the roughness in the outer layers of the stems. Electrochemistry on the bone fragment shows migration of vanadium during the 6 months since fracture to revision for M. Conclusions: Stems in altered synthetic plasma are affected by glucose and urea. Metal migration from the prostheses can occur through the chemical interactions between body fluids with abnormal biochemistry and the orthopaedic prostheses, favoured by cracks and concurring with wear following friction during usual movements. Cholesterol influences on the bone quality. Full article
(This article belongs to the Special Issue Clinical Research in Orthopaedics and Trauma Surgery)
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17 pages, 14709 KB  
Article
Unexpected Enhancement of High-Cycle Fatigue Property in Hot-Rolled DP600 Steel via Grain Size Tailoring
by Yu Song, Cheng Zhang, Yu-An Chen, Mingyue Yang, Chao Zhang, Bing Lu, Yuhe Huang, Jun Lu and Shuize Wang
Materials 2025, 18(24), 5658; https://doi.org/10.3390/ma18245658 - 17 Dec 2025
Viewed by 299
Abstract
This work systematically investigates the high-cycle fatigue (HCF) properties and fatigue crack growth (FCG) behavior of hot-rolled dual-phase (DP) steels with comparable tensile strength but distinctly different yield strength (458 MPa for the FG sample and 355 MPa for the CG sample), grain [...] Read more.
This work systematically investigates the high-cycle fatigue (HCF) properties and fatigue crack growth (FCG) behavior of hot-rolled dual-phase (DP) steels with comparable tensile strength but distinctly different yield strength (458 MPa for the FG sample and 355 MPa for the CG sample), grain sizes and morphologies. Contrary to the conventional Hall–Petch relationship, the coarse-grained (CG) sample demonstrates superior fatigue performance. This enhancement is reflected in its higher fatigue strength, combined with an elevated FCG threshold and a reduced FCG rate in the Paris regime of FCG behavior. Fracture morphologies and FCG path analyses reveal that this enhanced fatigue resistance attributes to pronounced crack path tortuosity in the CG microstructure. The tortuous crack path enhances roughness-induced crack closure effects in the near-threshold regime while promoting more frequent crack deflection during stable propagation, collectively reducing the effective driving force for crack growth. The experimental evidence confirms that properly designed CG microstructures with appropriate phase distribution can provide superior fatigue resistance in hot-rolled DP steels. Full article
(This article belongs to the Section Metals and Alloys)
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16 pages, 21768 KB  
Article
Evaluation of Fracture Toughness and Surface Roughness of a Novel Experimental Short Fiber-Reinforced CAD/CAM Block Material (In Vitro Study)
by Zakaria Jamal Mohammad and Diyar Khalid Bakr
Coatings 2025, 15(12), 1485; https://doi.org/10.3390/coatings15121485 - 16 Dec 2025
Viewed by 366
Abstract
The existing scientific literature indicates that flowable short fiber-reinforced composites (SFRCs) can be used for direct restoration due to their favorable mechanical properties. However, there is a lack of data on the mechanical properties of SFRCs designed specifically for indirect CAD/CAM restorations. This [...] Read more.
The existing scientific literature indicates that flowable short fiber-reinforced composites (SFRCs) can be used for direct restoration due to their favorable mechanical properties. However, there is a lack of data on the mechanical properties of SFRCs designed specifically for indirect CAD/CAM restorations. This study aims to fabricate a novel experimental SFRC CAD/CAM block and evaluate its fracture toughness and polishability as an indirect restoration in comparison with different conventional resin-based CAD/CAM blocks with different compositions. Fourier-transform infrared spectroscopy (FTIR) was employed to analyze the chemical structure of the Experimental SFRC group, while the microstructure of specimens from each group was examined using scanning electron microscopy (SEM). Then, this study divided the specimens into three groups—Group 1 (Grandio blocks), Group 2 (Cerasmart 270), and Group 3 (Experimental SFRC)—with 30 specimens in each group. Each group was then subdivided into sub-groups for the fracture toughness test, which evaluated resistance to crack propagation, and the surface roughness test, which assessed surface topography. FTIR analysis showed that the experimental SFRC exhibited distinct spectral changes after polymerization, confirming successful chemical reactions and network formation. SEM analysis showed that the Experimental SFRC block had a polymeric matrix with randomly oriented, well-dispersed short fibers. Grandio blocs exhibited a dense nanohybrid structure with irregular fillers, while Cerasmart 270 displayed a more uniform microstructure with evenly dispersed nano-sized spherical fillers. The Experimental SFRC showed the highest fracture toughness (2.758 MPa·√m), surpassing the other groups (p < 0.05) and highlighting its superior resistance to crack propagation. Regarding surface roughness Ra, the novel Experimental SFRC group (0.182) presented a significant difference compared to other groups (p < 0.05) but within clinical acceptance, and they can be well polished for clinical use after milling. The Cerasmart 270 block showed the lowest surface roughness Ra (0.135) among the groups, which is attributed to its filler size, geometry, and composition, resulting in a smoother surface. The higher fracture toughness of the Experimental SFRC among the groups suggests superior resistance to crack propagation, attributed to the incorporation of short fibers that enhance energy absorption and reduce brittleness, thereby supporting its suitability for high-stress-bearing clinical applications. Full article
(This article belongs to the Special Issue Progress and Prospects in Dental Materials and Endodontic Sciences)
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