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11 pages, 1564 KB  
Article
Surface Treatment and Analysis of 3D-Printed Plastic Molds for Prototype and Small-Series Injection Molding
by Karel Raz, Zdenek Chval, Frantisek Hula and Angelos Markopoulos
Polymers 2025, 17(22), 2977; https://doi.org/10.3390/polym17222977 - 8 Nov 2025
Viewed by 910
Abstract
Additive manufacturing (AM) has emerged as a promising technology for producing low-cost, customized tooling, particularly for prototyping and small-series injection molding. However, the inherent surface roughness and anisotropic properties of 3D-printed parts pose significant challenges for their direct use as functional mold inserts. [...] Read more.
Additive manufacturing (AM) has emerged as a promising technology for producing low-cost, customized tooling, particularly for prototyping and small-series injection molding. However, the inherent surface roughness and anisotropic properties of 3D-printed parts pose significant challenges for their direct use as functional mold inserts. This study investigates the effectiveness of various post-processing techniques on 3D-printed plastic inserts made from polyamide 12 (PA12) and glass bead-filled PA12 (PA12GB). The primary objective was to evaluate the impact of these surface treatments on the functional properties and service life of the mold inserts. A comprehensive analysis was conducted, including a detailed characterization of roughness using a confocal microscope, cross-sectional analysis to determine layer thickness, and tribological tests employing the ball-on-disc method to assess wear resistance. The study employed a modular injection mold and tested a range of surface finishing processes, including PostProcess Suspended Rotational Force (SRF) technology, metal decomposition coatings from HVM Plasma, and various methods from DyeMansion (Powershot S and Powerfuse). Results show a significant reduction in surface roughness across all methods. Notably, the vapor-based Powefuse treatment from DyeMansion achieved a surface roughness (Ra) of 1.2797 μm, which is below the typical Ra value of 1.6 μm for conventional metal molds, thereby making it suitable for high-quality molding applications. The tribological analysis provided critical insights into the durability and wear resistance of the treated surfaces, supporting their potential for extended use. This research validates the potential of specific post-processing methods to transform AM parts into functional tooling, enabling cost-effective and rapid prototyping in the plastics industry. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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19 pages, 4481 KB  
Article
Multi-Parameter Synchronous Identification Method for Dual Metal Rubber Clamps Considering Directional Differences in Mechanical Properties
by Kunpeng Xu, Ruize Wang and Bo Wang
Appl. Sci. 2025, 15(20), 11239; https://doi.org/10.3390/app152011239 - 20 Oct 2025
Viewed by 431
Abstract
Due to structural characteristics and connection dimensions, the dynamic characteristics of dual metal rubber clamps (DMRCs) show significant differences in bolt connection direction and opening direction. Accurately identifying the dynamic parameters of DMRC in different directions is of great significance for analyzing the [...] Read more.
Due to structural characteristics and connection dimensions, the dynamic characteristics of dual metal rubber clamps (DMRCs) show significant differences in bolt connection direction and opening direction. Accurately identifying the dynamic parameters of DMRC in different directions is of great significance for analyzing the dynamic characteristics and vibration control of aero-engine piping systems. This paper takes a DMRC-double straight pipe structure as the research object and establishes a dynamic model of this structure based on the finite element method as the mechanical parameter identification model of DMRCs. A refined simulation mechanism is adopted in the model to reflect the dynamic characteristics of the DMRC. The DMRC is simplified into four concentrated mass blocks and four spring-damping groups to simulate its mass, stiffness, and damping effects. Each spring-damping group consists of a linear spring, a rotational spring, and a damper. The four groups of springs are further divided into two directional groups to simulate the stiffness and damping effects in the opening direction and bolt connection direction, respectively. Four concentrated mass blocks are applied to the four nodes of the pipe to simulate the mass effect of DMRCs. Based on the dynamic model of the pipeline structure mentioned above, the synchronous identification algorithms and procedures for multiple mechanical parameters of DMRCs are proposed, aiming to minimize the deviation of natural characteristic indicators (natural frequency and peak of frequency response function) obtained through testing and model simulation. This method can synchronously identify linear stiffness, rotational stiffness, and damping in different directions. Finally, the effectiveness of the identification method is verified through experiments. Full article
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20 pages, 6754 KB  
Article
Study on the Wear Behavior Mechanism of SUS304 Stainless Steel During the Homogenization Process of LFP/NCM Slurry
by Xiangli Wen, Mingkun Bi, Lvzhou Li and Jianning Ding
Materials 2025, 18(19), 4457; https://doi.org/10.3390/ma18194457 - 24 Sep 2025
Viewed by 631
Abstract
During the homogenization process of lithium battery slurry, the slurry shearing process causes the surface of the homogenization equipment to wear and generate metal containing debris, which poses a risk of inducing battery self-discharge and even explosion. Therefore, inhibiting wear of homogenizing equipment [...] Read more.
During the homogenization process of lithium battery slurry, the slurry shearing process causes the surface of the homogenization equipment to wear and generate metal containing debris, which poses a risk of inducing battery self-discharge and even explosion. Therefore, inhibiting wear of homogenizing equipment is imperative, and systematic investigation into the wear behavior and underlying mechanisms of SUS304 stainless steel during homogenization is urgently required. In this study, lithium iron phosphate (LFP) and lithium nickel cobalt manganese oxide (NCM) cathode slurries were used as research objects. Changes in surface parameters, microstructure, and elemental composition of the wear region on SUS304 stainless steel under different working conditions were characterized. The results indicate that in the SUS304-lithium-ion battery slurry system, the potential wear mechanism of SUS304 gradually evolves with changes in load and rotational speed, following the order: adhesive wear (low speed, low load) → abrasive wear (medium speed, high load) → fatigue wear (high speed). Under high-load and high-rotational-speed conditions, oxidative corrosion wear on the ball–disc contact surface is particularly pronounced. Additionally, wear of SUS304 is more severe in the LFP slurry system compared to the NCM system. Macroscopic experiments also revealed that the speed effect is a core factor influencing the wear of SUS304, and the increase in its wear rate is more than twice that caused by the load effect. This study helps to clarify the wear behavior and wear mechanism evolution of homogenization equipment during the lithium battery homogenization process, providing data support and optimization direction for subsequent material screening and surface strengthening treatment of homogenization equipment components. Full article
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31 pages, 34013 KB  
Article
Vision-Based 6D Pose Analytics Solution for High-Precision Industrial Robot Pick-and-Place Applications
by Balamurugan Balasubramanian and Kamil Cetin
Sensors 2025, 25(15), 4824; https://doi.org/10.3390/s25154824 - 6 Aug 2025
Cited by 1 | Viewed by 2048
Abstract
High-precision 6D pose estimation for pick-and-place operations remains a critical problem for industrial robot arms in manufacturing. This study introduces an analytics-based solution for 6D pose estimation designed for a real-world industrial application: it enables the Staubli TX2-60L (manufactured by Stäubli International AG, [...] Read more.
High-precision 6D pose estimation for pick-and-place operations remains a critical problem for industrial robot arms in manufacturing. This study introduces an analytics-based solution for 6D pose estimation designed for a real-world industrial application: it enables the Staubli TX2-60L (manufactured by Stäubli International AG, Horgen, Switzerland) robot arm to pick up metal plates from various locations and place them into a precisely defined slot on a brake pad production line. The system uses a fixed eye-to-hand Intel RealSense D435 RGB-D camera (manufactured by Intel Corporation, Santa Clara, California, USA) to capture color and depth data. A robust software infrastructure developed in LabVIEW (ver.2019) integrated with the NI Vision (ver.2019) library processes the images through a series of steps, including particle filtering, equalization, and pattern matching, to determine the X-Y positions and Z-axis rotation of the object. The Z-position of the object is calculated from the camera’s intensity data, while the remaining X-Y rotation angles are determined using the angle-of-inclination analytics method. It is experimentally verified that the proposed analytical solution outperforms the hybrid-based method (YOLO-v8 combined with PnP/RANSAC algorithms). Experimental results across four distinct picking scenarios demonstrate the proposed solution’s superior accuracy, with position errors under 2 mm, orientation errors below 1°, and a perfect success rate in pick-and-place tasks. Full article
(This article belongs to the Section Sensors and Robotics)
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12 pages, 778 KB  
Article
Comparison of All-Suture Anchors and Metal Anchors in Arthroscopic Rotator Cuff Repair: Short-Term Clinical Outcomes and Anchor Pullout Risk
by Tolga Keçeci, Yusuf Polat, Abdullah Alper Şahin, Murat Alparslan, Serkan Sipahioğlu and Alper Çıraklı
J. Clin. Med. 2025, 14(8), 2619; https://doi.org/10.3390/jcm14082619 - 11 Apr 2025
Cited by 3 | Viewed by 2421
Abstract
Objectives: Metal anchors (MA), commonly used in the early stages of rotator cuff surgical treatment development, are associated with a high risk of complications, especially in osteoporotic bone. As an alternative to rigid anchors, all-suture anchors (ASA) have been introduced for the medial [...] Read more.
Objectives: Metal anchors (MA), commonly used in the early stages of rotator cuff surgical treatment development, are associated with a high risk of complications, especially in osteoporotic bone. As an alternative to rigid anchors, all-suture anchors (ASA) have been introduced for the medial row, offering promising clinical outcomes and favorable biomechanical studies. We aimed to compare the clinical outcomes of MAs and ASAs in either single-row or in medial-row suture bridge techniques in arthroscopic rotator cuff repair. Our hypothesis was that in cases where ASA was used for at least 12 months of follow-up, more favorable results would be obtained as compared to rigid anchors, and intraoperative complications such as anchor pullout would be encountered less. Methods: In this retrospective cohort analysis, we reviewed patients who underwent arthroscopic rotator cuff repair between January 2020 and December 2022. Surgeries were performed by two senior surgeons in a single tertiary center. Patients who had undergone revision surgery, had a history of previous shoulder surgeries, had massive rotator cuff tears, and partial-thickness tears; or had concomitant subscapularis tears were excluded. Preoperative and postoperative scores, including Constant–Murley (CM), Disabilities of the Arm, Shoulder, and Hand (DASH), and visual analog scale (VAS), were compared. The minimum follow-up period was 12 months. Clinical assessment of shoulder range of motion included forward flexion, abduction, internal rotation, and external rotation. Intraoperative anchor-related complications were compared. All patients underwent the same surgical technique and postoperative rehabilitation protocol. Results: A total of 142 patients (89 females, 53 males; mean age: 57.4 years) were included in the study, with 67 patients in the ASA group and 75 in the MA group. The sex distribution and mean age were similar between groups. The ASA group had 15 traumatic tears, while the MA group had 13 (p < 0.05). The mean follow-up period was 21.6 months (range 12–40 months). Preoperative CM scores were statistically better in the ASA group, but this difference was not clinically relevant (p < 0.046). The mean CM score was 75.64, the mean DASH score was 8.57, and the mean VAS was 1.38 at the postoperative period in the MA group. The mean CM score was 78.40, the mean DASH score was 9.75, and VAS was 1.59 at the postoperative period in the ASA group. Seven cases experienced anchor pullout in the MA group, and thread breakage occurred in one patient of each group (p = 0.014). The mean age of the patients with anchor pullout was significantly higher (p = 0.002). This finding was not hypothesized in the initial study design but emerged during post-hoc analysis and highlights the importance of considering bone quality in elderly patients. Conclusions: The clinical outcomes of rotator cuff repairs using all-suture anchors or metal anchors are comparable. However, ASA use may offer an advantage in elderly patients by reducing the risk of anchor pullout. Further studies assessing tendon integrity and bone quality and incorporating long-term follow-up periods are recommended to support and validate the present findings. Full article
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32 pages, 5388 KB  
Article
The Effect of Long-Term Soil System Use and Diversified Fertilization on the Sustainability of the Soil Fertility—Organic Matter and Selected Trace Elements
by Agnieszka Andrzejewska and Maria Biber
Sustainability 2025, 17(7), 2907; https://doi.org/10.3390/su17072907 - 25 Mar 2025
Cited by 1 | Viewed by 2220
Abstract
It has been assumed that the long-term impact of a diversified soil use system (SUS) and the continuous application of manure and/or mineral fertilizers (NPK) affects the sustainability of soil fertility components. This influence is manifested through the content and distribution of nutrients, [...] Read more.
It has been assumed that the long-term impact of a diversified soil use system (SUS) and the continuous application of manure and/or mineral fertilizers (NPK) affects the sustainability of soil fertility components. This influence is manifested through the content and distribution of nutrients, as well as some bioavailable heavy metals in the soil. This hypothesis was verified in 2022 in a long-term field experiment that started in 1957. It consisted of a seven-course crop rotation: potato–spring barley–winter triticale–alfalfa–alfalfa–winter wheat–winter rye and monocultures of these crops plus black fallow. The studies were carried out on three separate fields: black fallow (BF), winter wheat grown in monoculture (WW-MO), and crop rotation (WW-CR). Each of these experimental objects consists of five fertilizer variants (FVs) fertilized in the same way every year: absolute control (AC)—variant without fertilizers for 75 years; farmyard manure—FM; mineral fertilizers—NPK; mixed variant—NPK + FM; mineral fertilizers plus annually applied lime—NPK + L. The second factor was the soil layer: 0.0–0.3 m, 0.3–0.6 m, or 0.6–0.9 m. The obtained results clearly indicate that long-term fertilization with NPK + FM, especially in rotation with legumes, strengthens the eluviation/illuviation processes, decreasing the sustainability of soil fertility. Liming is a factor stabilizing the content and distribution of silt and clay particles in the soil. The key factor determining the content and distribution of micronutrients and heavy metals in the soil was the content of organic carbon (Corg). Its content decreased in the following order: WW-CR (13.2 ± 5.8) ≥ WW-MO (12.3 ± 6.9) > BF (6.6 ± 2.8 g·kg−1). The large variability resulted from a distribution trend with soil depth, which increased as follows: MO ≥ CR > BF. FVs with FM had the highest Corg content. NPK, regardless of the long-term soil use system (SUS), had the lowest content. Among the elements studied, the key one impacting the content of both micronutrients and heavy metals was iron (Fe). The Fe content decreased in the order BL (100%) > WW-MO (90.5%) > WW-CR (85%). The opposite tendency was found for the remaining elements, the content of which was consistent with the content of Corg, which was the highest in CR. The strongest impact of Fe, modified by the SUS, was found for Zn, Pb, and Cd. Despite the differences observed between SUSs, fertilization variants, and soil layers, the content of Fe and Mn was in the medium class, while Zn and Cu were in the high class of availability. The content of Ni was the highest for NPK + FM in WW-CR. The content of Pb was weakly affected by the long-term SUS but showed a strong tendency for accumulation in the topsoil layer. The content of Cd was the highest in BF, where it exceeded the threshold of 0.27 mg·kg−1. The long-term diversified SUS, as the main factor determining the sustainability of soil fertility, makes it possible to indicate the directions of humus accumulation and its distribution in the soil. It turned out to be a key factor, but in cooperation with Fe, it determined the content of micronutrients and bioavailable heavy metals in the soil. Full article
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23 pages, 6226 KB  
Article
Optimizing FSP Parameters for AA5083/SiC Composites: A Comparative Analysis of Taguchi and Regression
by Oritonda Muribwathoho, Velaphi Msomi and Sipokazi Mabuwa
Metals 2025, 15(3), 280; https://doi.org/10.3390/met15030280 - 5 Mar 2025
Viewed by 1144
Abstract
The fabrication of AA5083/SiC composites by the friction stir processing (FSP) method is the main objective of this study. The study looks at how the mechanical properties of the composites are affected by three important process parameters: traversal speed, rotational speed, and tilt [...] Read more.
The fabrication of AA5083/SiC composites by the friction stir processing (FSP) method is the main objective of this study. The study looks at how the mechanical properties of the composites are affected by three important process parameters: traversal speed, rotational speed, and tilt angle. The Taguchi L9 design matrix was used to effectively investigate parameter effects, decreasing experimental trials and cutting expenses. Tensile testing measured tensile strength, whereas microhardness tests evaluated hardness. The findings showed that a maximum tensile strength of 243 MPa and a maximum microhardness of 94.80 HV were attained. The findings also showed that the optimal ultimate tensile strength (UTS) and percentage elongation (PE) were achieved at a tilt angle of 2°, a traverse speed of 30 mm per minute, and a rotating speed of 900 rev/min. On the other hand, a slightly greater traverse speed of 45 mm per minute was required to reach maximal microhardness (MH) with the same rotational speed and tilt angle. Analysis of variance (ANOVA) showed that rotational speed has a substantial impact on all mechanical properties, highlighting how important it is for particle dispersion and grain refining. This work is unique in that it systematically optimizes FSP parameters by using regression analysis and the Taguchi technique in addition to ANOVA. This allows for a better understanding of how these factors affect the mechanical properties of SiC-reinforced composites. The findings contribute to advancing the cost-effective fabrication of high-performance metal matrix composites for industrial applications requiring enhanced strength and durability. Full article
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17 pages, 2815 KB  
Article
Multi-Objective Optimisation of Welding Parameters for AZ91D/AA6082 Rotary Friction Welded Joints
by Radosław Winiczenko, Andrzej Skibicki and Paweł Skoczylas
Appl. Sci. 2025, 15(3), 1477; https://doi.org/10.3390/app15031477 - 31 Jan 2025
Viewed by 1558
Abstract
Recently, rotary friction welding has been used to join magnesium alloys. FRW uses friction heat to bond magnesium alloys with aluminium alloys. Combining these light alloys can provide many promising applications in the industry. The welding parameters such as friction and upsetting force, [...] Read more.
Recently, rotary friction welding has been used to join magnesium alloys. FRW uses friction heat to bond magnesium alloys with aluminium alloys. Combining these light alloys can provide many promising applications in the industry. The welding parameters such as friction and upsetting force, rotational speed, and welding time play a significant role in determining the joint strength. The paper presents a new approach to multi-objective optimisation of friction welding process parameters for AZ91D/AA6082 alloy joints. Multi-objective optimisation is based on artificial neural networks and genetic algorithms as non-conventional AI techniques. The methods were used to determine the following optimal welding process parameters: friction force, upsetting force and friction time for simultaneously maximised tensile strength and minimised metal loss (shortening) during welding. The ultimate tensile strength and metal loss of the friction welding joints were studied numerically and experimentally. Moreover, the influence of welding parameters on the ultimate tensile strength and shortening of friction joints was also studied. A genetic algorithm successfully found a set of welding parameters for which the joint strength increases from 24 to 81 MPA and the joint shortening decreases from 8.25 to 0.23 mm. The results show that a low friction force and upsetting force give a high value of tensile strength and the lowest shortening of the bimetal joints. Full article
(This article belongs to the Special Issue Advanced Welding Technology and Its Applications)
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13 pages, 2644 KB  
Article
Reverse Shoulder Arthroplasty Baseplate Stability Is Affected by Bone Density and the Type and Amount of Augmentation
by Daniel Ritter, Patric Raiss, Patrick J. Denard, Brian C. Werner, Manuel Kistler, Celina Lesnicar, Micheal van der Merwe, Peter E. Müller, Matthias Woiczinski, Coen A. Wijdicks and Samuel Bachmaier
Bioengineering 2025, 12(1), 42; https://doi.org/10.3390/bioengineering12010042 - 8 Jan 2025
Viewed by 3683
Abstract
Objective: This study evaluated the effects of bony increased offset (BIO) and metallic augments (MAs) on primary reverse shoulder arthroplasty (RSA) baseplate stability in cadaveric specimens with variable bone densities. Methods: Thirty cadaveric specimens were analyzed in an imaging and biomechanical investigation. Computed [...] Read more.
Objective: This study evaluated the effects of bony increased offset (BIO) and metallic augments (MAs) on primary reverse shoulder arthroplasty (RSA) baseplate stability in cadaveric specimens with variable bone densities. Methods: Thirty cadaveric specimens were analyzed in an imaging and biomechanical investigation. Computed tomography (CT) scans allowed for preoperative RSA planning and bone density analysis. Three correction methods of the glenoid were used: (1) corrective reaming with a standard baseplate, which served as the reference group (n = 10); (2) MA-RSA (n = 10); and (3) angled BIO-RSA (n = 10). Each augment group consisted of 10° (n = 5) and 20° (n = 5) corrections. Biomechanical testing included cyclic loading in an articulating setup, with optical pre- and post-cyclic micromotion measurements in a rocking horse setup. Results: There were no differences in bone density between groups based on CT scans (p > 0.126). The BIO-RSA group had higher variability in micromotion compared to the MA-RSA and reference groups (p = 0.013), and increased total micromotion compared to the reference group (p = 0.039). Both augmentations using 20° corrections had increased variance in rotational stability compared to the reference group (p = 0.043). Micromotion correlated with the subchondral bone density in the BIO-RSA group (r = −0.63, p = 0.036), but not in the MA-RSA (p > 0.178) or reference (p > 0.117) groups. Conclusions: Time-zero baseplate implant fixation is more variable with BIO-RSA and correlates with bone density. Corrections of 20° with either augmentation approach increase variability in rotational micromotion. The preoperative quantification of bone density may be useful before utilizing 20° of correction, especially when adding a bone graft in BIO-RSAs. Full article
(This article belongs to the Special Issue Advances in Physical Therapy and Rehabilitation)
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15 pages, 14372 KB  
Article
Calibration of Dual-Polarised Antennas for Air-Coupled Ground Penetrating Radar Applications
by Samuel J. I. Forster, Anthony J. Peyton and Frank J. W. Podd
Remote Sens. 2024, 16(21), 4114; https://doi.org/10.3390/rs16214114 - 4 Nov 2024
Cited by 2 | Viewed by 2183
Abstract
Radar polarimetry is a technique that can be used to enhance target detection, identification and classification; however, the quality of these measurements can be significantly influenced by the characteristics of the radar antenna. For an accurate and reliable system, the calibration of the [...] Read more.
Radar polarimetry is a technique that can be used to enhance target detection, identification and classification; however, the quality of these measurements can be significantly influenced by the characteristics of the radar antenna. For an accurate and reliable system, the calibration of the antenna is vitally important to mitigate these effects. This study presents a methodology to calibrate Ultra-Wideband (UWB) dual-polarised antennas in the near-field using a thin elongated metallic cylinder as the calibration object. The calibration process involves measuring the scattering matrix of the metallic cylinder as it is rotated, in this case producing 100 distinct scattering matrices from which the calibration parameters are derived, facilitating a robust and stable solution. The calibration procedure was tested and validated using a Vector Network Analyser (VNA) and two quad-ridged antennas, which presented different performance levels. The calibration methodology demonstrated notable improvements, aligning the performance of both functioning and under-performing antennas to equivalent specifications. Mid-band validation measurements indicated minimal co-polar channel imbalance (<0.3 dB), low phase error (<0.8°) and improved cross-polar isolation (≈48 dB). Full article
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21 pages, 6832 KB  
Article
A SAW Wireless Passive Sensing System for Rotating Metal Parts
by Yue Zhou, Jing Ding, Bingji Wang, Feng Gao, Shurong Dong and Hao Jin
Sensors 2024, 24(20), 6703; https://doi.org/10.3390/s24206703 - 18 Oct 2024
Cited by 1 | Viewed by 1923
Abstract
Passive wireless surface acoustic wave (SAW) sensors are very useful for on-site monitoring of the working status of machines in complex environments, such as high-temperature rotating objects. For rotating parts, it is difficult to realize real-time and continuous monitoring because of the unstable [...] Read more.
Passive wireless surface acoustic wave (SAW) sensors are very useful for on-site monitoring of the working status of machines in complex environments, such as high-temperature rotating objects. For rotating parts, it is difficult to realize real-time and continuous monitoring because of the unstable sensing signal caused by the continuous change of the relative position of the rotating part to the sensor and shielding of the signal. In our SAW sensing system, we propose a loop antenna integrated with the rotating part to obtain a stable sensing signal owing to its omnidirectional radiation pattern. Methodologies for determining the antenna dimension, system operating frequency, and procedures for designing a SAW sensor tag are discussed in this paper. By fully utilizing the influence of metal rotor on antenna performance, the antenna needs no impedance matching elements while it provides sufficient gain, which equips the antenna with nearly zero temperature drift at a wide temperature-sensing range. Experimental verification results show that this sensing system can greatly improve the stability of the sensing signal significantly and can achieve a temperature sensing accuracy of ~1 °C at different rotational speeds, demonstrated by the feasibility of the loop antenna for monitoring the working status of rotating metal parts. Full article
(This article belongs to the Section Electronic Sensors)
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9 pages, 6452 KB  
Article
Influence of Continuous Rotation and Optimal Torque Reverse Kinematics on the Cyclic Fatigue Strength of Endodontic NiTi Clockwise Cutting Rotary Instruments
by Jorge N. R. Martins, Emmanuel J. N. L. Silva, Duarte Marques and Marco A. Versiani
Dent. J. 2024, 12(10), 317; https://doi.org/10.3390/dj12100317 - 30 Sep 2024
Cited by 4 | Viewed by 2297
Abstract
Objectives: The objective of the present study was to evaluate the cyclic fatigue strength of clockwise cutting rotary endodontic instruments when subjected to two different kinematics: continuous clockwise rotation and clockwise reciprocation movement under optimum torque reverse (OTR) motion. Methods: New ProTaper Next [...] Read more.
Objectives: The objective of the present study was to evaluate the cyclic fatigue strength of clockwise cutting rotary endodontic instruments when subjected to two different kinematics: continuous clockwise rotation and clockwise reciprocation movement under optimum torque reverse (OTR) motion. Methods: New ProTaper Next X1 (n = 20) and X2 (n = 20) instruments were randomly divided into two subgroups (n = 10) based on kinematics (continuous rotation or OTR). The specimens were tested using a custom-made device with a non-tapered stainless-steel artificial canal measuring 19 mm in length, featuring a 6 mm radius and an 86-degree curvature. All instruments were tested with a lubricant at room temperature until a fracture occurred. The time to fracture and the length of the separated fragment were recorded. Subsequently, the fractured instruments were inspected under a scanning electron microscope for signs of cyclic fatigue failure, plastic deformation, and/or crack propagation. The subgroup comparisons for time to fracture and instrument length were performed using the independent samples t-test, with the level of statistical significance set at 0.05. Results: When using OTR movement, the ProTaper Next X1 increased the time to fracture from 52.9 to 125.8 s (p < 0.001), while the ProTaper Next X2 increased from 45.4 to 66.0 s (p < 0.001). No subgroup exhibited plastic deformations, but both showed dimpling marks indicative of cyclic fatigue as the primary mode of failure. Additionally, OTR movement resulted in more metal alloy microcracks. Conclusions: The use of OTR motion extended the lifespan of the tested instruments and resulted in a higher number of metal microcracks. This suggests that OTR motion helped to distribute the mechanical stress more evenly across the instrument, thereby relieving localized tension. As a result, it delayed the formation of a single catastrophic crack, enhancing the overall performance of the instruments during the experimental procedures. Full article
(This article belongs to the Special Issue Endodontics and Restorative Sciences: 2nd Edition)
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19 pages, 6895 KB  
Article
Evaluation Methods and Coupled Optimization at Macro- and Micro-Scales for Profiled Ring Rolling of Inconel718 Alloy
by Xinglin Zhu, Erting Dong, Xiaomin Qiao and Dong Liu
Materials 2024, 17(18), 4538; https://doi.org/10.3390/ma17184538 - 15 Sep 2024
Cited by 1 | Viewed by 1571
Abstract
The forming quality of profiled ring rolling not only encompasses macroscopic accuracy but also emphasizes the microstructure. Due to the multiple process parameters and complex metal flow during profiled ring rolling, the various forming defects are difficult to control and difficult to study [...] Read more.
The forming quality of profiled ring rolling not only encompasses macroscopic accuracy but also emphasizes the microstructure. Due to the multiple process parameters and complex metal flow during profiled ring rolling, the various forming defects are difficult to control and difficult to study theoretically. The objective of this study is to establish a comprehensive method for evaluating the forming quality of profiled rings, which considers both the macroscopic forming accuracy and the microstructure. Firstly, the synthetic size factor was defined, and the evolutionary relation between the section forming rate and the diameter growth rate of E-section ring rolling was analyzed in detail. The synthetic size factor can be used to describe the dimensional evolution and evaluate the forming accuracy of the profiled ring rolling process. Taking into full consideration the features of intermittent deformation in local areas, a microstructure evolution model of the Inconel718 alloy during E-section ring rolling, which can accurately predict the recrystallization volume fraction and average grain size of the final ring, was established. Then, combined with finite element simulation, the influence of the rotation speed of the driving roll on the macro-size evolution and microstructure was systematically analyzed. The results indicate that there is often a discrepancy between dimensional accuracy and microstructure uniformity in the optimization trend. For instance, the higher the rotation speed of the driving roll is, the more uniform the microstructure is, but the more difficult it is for the section profile to form. Finally, combined with response surface methodology (RSM), multi-parameter optimization was carried out with section forming accuracy and grain uniformity as the optimization objectives. By using the optimal parameters, an E-section ring with a complete profile and a uniform microstructure was obtained, with a maximum prediction error of the recrystallization volume fraction lower than 5%. The results show that the macroscopic and microscopic quality evaluation methods proposed in this study, as well as the optimization method combining RSM, can be effectively applied to the process optimization of profiled ring rolling. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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17 pages, 3296 KB  
Article
High-Precision Visual Servoing for the Neutron Diffractometer STRESS-SPEC at MLZ
by Martin Landesberger , Oguz Kedilioglu , Lijiu Wang , Weimin Gan , Joana Rebelo Kornmeier , Sebastian Reitelshöfer , Jörg Franke  and Michael Hofmann 
Sensors 2024, 24(9), 2703; https://doi.org/10.3390/s24092703 - 24 Apr 2024
Viewed by 1930
Abstract
With neutron diffraction, the local stress and texture of metallic components can be analyzed non-destructively. For both, highly accurate positioning of the sample is essential, requiring the measurement at the same sample location from different directions. Current sample-positioning systems in neutron diffraction instruments [...] Read more.
With neutron diffraction, the local stress and texture of metallic components can be analyzed non-destructively. For both, highly accurate positioning of the sample is essential, requiring the measurement at the same sample location from different directions. Current sample-positioning systems in neutron diffraction instruments combine XYZ tables and Eulerian cradles to enable the accurate six-degree-of-freedom (6DoF) handling of samples. However, these systems are not flexible enough. The choice of the rotation center and their range of motion are limited. Industrial six-axis robots have the necessary flexibility, but they lack the required absolute accuracy. This paper proposes a visual servoing system consisting of an industrial six-axis robot enhanced with a high-precision multi-camera tracking system. Its goal is to achieve an absolute positioning accuracy of better than 50μm. A digital twin integrates various data sources from the instrument and the sample in order to enable a fully automatic measurement procedure. This system is also highly relevant for other kinds of processes that require the accurate and flexible handling of objects and tools, e.g., robotic surgery or industrial printing on 3D surfaces. Full article
(This article belongs to the Section Sensors and Robotics)
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15 pages, 8604 KB  
Article
Experimental Investigation of Hydraulic Fracturing Fluid Based on Pseudo Gemini Surfactant with Polysaccharide Addition
by Mihail Silin, Lyubov Magadova, Kira Poteshkina, Polina Krisanova, Andrey Filatov and Denis Kryukov
Gels 2024, 10(1), 30; https://doi.org/10.3390/gels10010030 - 28 Dec 2023
Cited by 4 | Viewed by 2375
Abstract
In the last decade, hydrogels for hydraulic fracturing based on viscoelastic surfactants have been actively studied. Interest in these systems is justified by their unique qualities: good viscoelasticity and the ability to form stable suspensions of proppant or sand, destruction without the formation [...] Read more.
In the last decade, hydrogels for hydraulic fracturing based on viscoelastic surfactants have been actively studied. Interest in these systems is justified by their unique qualities: good viscoelasticity and the ability to form stable suspensions of proppant or sand, destruction without the formation of bridging agents, hydrophobization of the rock surface and metal of technological equipment, as well as oil-cleaning properties. These qualities are most often provided by a minimum set of components—a surfactant and an electrolyte. However, the absence of a polymer limits the use of these gels in formations where fluid leakoff is possible. In this article, a liquid was studied, based on a pseudo gemini surfactant (PGVES) with the addition of a water-soluble polysaccharide. The objects of study were selected based on the assumption of interactions between PGVES and the polymer; interactions which favorably influence the technological characteristics of the fracturing fluid. To confirm the hypothesis, rheological studies were carried out. These included rotational viscometry and oscillatory studies at various temperatures. The settling velocity of particles of various proppant fractions was studied and tests were carried out to assess fluid leakoff. The performed experiments show an improvement in the characteristics of the PGVES-based gel under the influence of the polysaccharide. In particular, the rheological properties increase significantly, the stability of proppant suspensions improves, and the fluid leakoff of systems decreases, all of which expands the possibility of using these fracturing fluids and makes this area of experimentation promising. Full article
(This article belongs to the Special Issue Polymer Gels for the Oil and Gas Industry)
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