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Keywords = resistive pulse sensor

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30 pages, 10389 KiB  
Review
Recent Advancements in Optical Fiber Sensors for Non-Invasive Arterial Pulse Waveform Monitoring Applications: A Review
by Jing Wen Chew, Soon Xin Gan, Jingxian Cui, Wen Di Chan, Sai T. Chu and Hwa-Yaw Tam
Photonics 2025, 12(7), 662; https://doi.org/10.3390/photonics12070662 - 30 Jun 2025
Viewed by 397
Abstract
The awareness of the importance of monitoring human vital signs has increased recently due to the outbreak of the COVID-19 pandemic. Non-invasive heart rate monitoring devices, in particular, have become some of the most popular tools for health monitoring. However, heart rate data [...] Read more.
The awareness of the importance of monitoring human vital signs has increased recently due to the outbreak of the COVID-19 pandemic. Non-invasive heart rate monitoring devices, in particular, have become some of the most popular tools for health monitoring. However, heart rate data alone are not enough to reflect the health of one’s cardiovascular function or arterial health. This growing interest has spurred research into developing high-fidelity non-invasive pulse waveform sensors. These sensors can provide valuable information such as data on blood pressure, arterial stiffness, and vascular aging from the pulse waveform. Among these sensors, optical fiber sensors (OFSs) stand out due to their remarkable properties, including resistance to electromagnetic interference, capability in monitoring multiple vital signals simultaneously, and biocompatibility. This paper reviews the latest advancements in using OFSs to measure human vital signs, with a focus on pulse waveform analysis. The various working mechanisms of OFSs and their performances in measuring the pulse waveform are discussed. In addition, we also address the challenges faced by OFSs in pulse waveform monitoring and explore the opportunities for future development. This technology shows great potential for both clinical and personal non-invasive pulse waveform monitoring applications. Full article
(This article belongs to the Special Issue Novel Advances in Optical Fiber Gratings)
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19 pages, 6101 KiB  
Article
Modern Capabilities of Semi-Airborne UAV-TEM Technology on the Example of Studying the Geological Structure of the Uranium Paleovalley
by Ayur Bashkeev, Alexander Parshin, Ilya Trofimov, Sergey Bukhalov, Danila Prokhorov and Nikolay Grebenkin
Minerals 2025, 15(6), 630; https://doi.org/10.3390/min15060630 - 10 Jun 2025
Cited by 1 | Viewed by 367
Abstract
Unmanned systems provide significant prospects for improving the efficiency of electromagnetic geophysical exploration in mineral prospecting and geological mapping, as they can significantly increase the productivity of field surveys by accelerating the movement of the measuring system along the site, as well as [...] Read more.
Unmanned systems provide significant prospects for improving the efficiency of electromagnetic geophysical exploration in mineral prospecting and geological mapping, as they can significantly increase the productivity of field surveys by accelerating the movement of the measuring system along the site, as well as minimizing problems in cases where the pedestrian walkability of the site is a challenge. Lightweight and cheap UAV systems with a take-off weight in the low tens of kilograms are unable to carry a powerful current source; therefore, semi-airborne systems with a ground transmitter (an ungrounded loop or grounded at the ends of the line) and a measuring system towed on a UAV are becoming more and more widespread. This paper presents the results for a new generation of semi-airborne technology SibGIS UAV-TEMs belonging to the “line-loop” type and capable of realizing the transient/time-domain (TEM) electromagnetics method used for studying a uranium object of the paleovalley type. Objects of this type are characterized by a low resistivity of the ore zone located in relatively high-resistivity host rocks and, from the position of the geoelectric structure, can be considered a good benchmark for assessing the capabilities of different electrical exploration technologies in general. The aeromobile part of the geophysical system created is implemented on the basis of a hexacopter carrying a measuring system with an inductive sensor, an analog of a 50 × 50 m loop, an 18-bit ADC with satellite synchronization, and a transmitter. The ground part consists of a galvanically grounded supply line and a current source with a transmitter creating multipolar pulses of quasi-DC current in the line. The survey is carried out with a terrain drape based on a satellite digital terrain model. The article presents the results obtained from the electromagnetic soundings in comparison with the reference (drilled) profile, convincingly proving the high efficiency of UAV-TEM. This approach to pre-processing UAV–electrospecting data is described with the aim of improving data quality by taking into account the movement and swaying of the measuring system’s sensor. On the basis of the real data obtained, the sensitivity of the created semi-airborne system was modeled by solving a direct problem in the class of 3D models, which allowed us to evaluate the effectiveness of the method in relation to other geological cases. Full article
(This article belongs to the Special Issue Geoelectricity and Electrical Methods in Mineral Exploration)
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16 pages, 3286 KiB  
Article
Tachometric Cup Anemometer with Wind Direction Indicator and Fibre-Optic Signal Transmission
by Paweł Ligęza, Paweł Jamróz and Katarzyna Socha
Sensors 2025, 25(11), 3281; https://doi.org/10.3390/s25113281 - 23 May 2025
Viewed by 506
Abstract
This article presents an innovative design of a tachometric anemometer for measuring wind velocity and direction, which does not contain electronic components and systems or power supply systems in the measurement area. This device can be used in extremely unfavourable environmental operating conditions, [...] Read more.
This article presents an innovative design of a tachometric anemometer for measuring wind velocity and direction, which does not contain electronic components and systems or power supply systems in the measurement area. This device can be used in extremely unfavourable environmental operating conditions, in locations exposed to direct atmospheric discharges, in conditions requiring restrictive and intrinsic safety, in special military applications, and in measurements in the presence of extreme electromagnetic fields. An innovative optical–mechanical transducer is used in the anemometer. This transducer generates a light pulse signal, the frequency of which is a function of the flow velocity, and the duty cycle is a function of the wind direction. This signal is transmitted via optical fibre from the sensor assembly to the measuring station, located outside the measurement area. The design of the device is simple, durable, and resistant to environmental conditions. Full article
(This article belongs to the Section Environmental Sensing)
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14 pages, 3714 KiB  
Article
Scindapsus Aureus Resistive Random-Access Memory with Synaptic Plasticity and Sound Localization Function
by Lu Wang, Jiachu Xie, Wantao Su, Zhenjie Du and Mingzhu Zhang
Nanomaterials 2025, 15(9), 659; https://doi.org/10.3390/nano15090659 - 26 Apr 2025
Viewed by 399
Abstract
This work presents a memristive device based on a composite of Scindapsus aureus (SA) and gold nanoparticles (Au NPs), which exhibits excellent resistive switching characteristics and supports multiple forms of synaptic plasticity such as paired-pulse facilitation (PPF), spike-rate-dependent plasticity (SRDP), and spike-timing-dependent plasticity [...] Read more.
This work presents a memristive device based on a composite of Scindapsus aureus (SA) and gold nanoparticles (Au NPs), which exhibits excellent resistive switching characteristics and supports multiple forms of synaptic plasticity such as paired-pulse facilitation (PPF), spike-rate-dependent plasticity (SRDP), and spike-timing-dependent plasticity (STDP). The device demonstrates reliable retention, reproducibility, and switching stability. The SA:Au NP composite originates from a natural plant source and possesses green, biodegradable, and biocompatible features, highlighting its potential as a sustainable bio-memristive material for neuromorphic systems. Furthermore, the device exhibits sensitivity to the time interval between paired input pulses, simulating the neural response to interaural time differences (ITDs) in the auditory system. Although not a conventional acoustic sensor, its Δt-responsiveness based on synaptic behavior reveals promising potential in neuromorphic auditory perception and perceptual computing applications. This study provides a foundational synaptic unit for future artificial hearing systems capable of spatial sound localization. Full article
(This article belongs to the Section Nanoelectronics, Nanosensors and Devices)
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14 pages, 9159 KiB  
Article
Copper Nanoclusters Anchored on Crumpled N-Doped MXene for Ultra-Sensitive Electrochemical Sensing
by Hanxue Yang, Chao Rong, Shundong Ge, Tao Wang, Bowei Zhang and Fu-Zhen Xuan
Sensors 2025, 25(8), 2508; https://doi.org/10.3390/s25082508 - 16 Apr 2025
Viewed by 482
Abstract
Simultaneous detection of dopamine (DA) and uric acid (UA) is essential for diagnosing neurological and metabolic diseases but hindered by overlapping electrochemical signals. We present an ultrasensitive electrochemical sensor using copper nanoclusters anchored on nitrogen-doped crumpled Ti3C2Tx MXene [...] Read more.
Simultaneous detection of dopamine (DA) and uric acid (UA) is essential for diagnosing neurological and metabolic diseases but hindered by overlapping electrochemical signals. We present an ultrasensitive electrochemical sensor using copper nanoclusters anchored on nitrogen-doped crumpled Ti3C2Tx MXene (Cu-N/Ti3C2Tx). The engineered 3D crumpled architecture prevents MXene restacking, exposes active sites, and enhances ion transport, while Cu nanoclusters boost electrocatalytic activity via accelerated electron transfer. Structural analyses confirm uniform Cu dispersion (3.0 wt%), Ti-N bonding, and strain-induced wrinkles, synergistically improving conductivity. The sensor achieves exceptional sensitivity (1958.3 and 1152.7 μA·mM−1·cm−2 for DA/UA), ultralow detection limits (0.058 and 0.099 μM for DA/UA), rapid response (<1.5 s), and interference resistance (e.g., ascorbic acid). Differential pulse voltammetry enables independent linear detection ranges (DA: 2–60 μM; UA: 5–100 μM) in biofluids, with 94.4% stability retention over 7 days. The designed sensor exhibits excellent capabilities for DA and UA detection. This work provides a novel design strategy for developing high-performance electrochemical sensors. Full article
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18 pages, 5446 KiB  
Article
Mitigating Electrochemical Effects in Resistive Frost-Detection Sensors
by Martim Lima Aguiar, Pedro Dinis Gaspar and Pedro Dinho Silva
Appl. Sci. 2025, 15(8), 4110; https://doi.org/10.3390/app15084110 - 8 Apr 2025
Viewed by 362
Abstract
Demand defrosting is a well-established strategy for improving defrost efficiency in refrigeration systems, and resistive frost-detection sensors provide a cost-effective means of enabling such control. However, copper electrode resistive sensors operating in water-based environments are susceptible to electrolysis, which degrades electrode integrity and [...] Read more.
Demand defrosting is a well-established strategy for improving defrost efficiency in refrigeration systems, and resistive frost-detection sensors provide a cost-effective means of enabling such control. However, copper electrode resistive sensors operating in water-based environments are susceptible to electrolysis, which degrades electrode integrity and compromises measurement reliability. This study investigates the impact of electrolysis on sensor performance and evaluates the effectiveness of an intermittent powering method in mitigating these effects. Two sensor excitation methods were experimentally tested: continuous voltage application and pulsed DC excitation with a 1.7% duty cycle. The results demonstrated that continuous excitation caused erratic measurements and electrode degradation due to ongoing electrochemical reactions. In contrast, the pulsed DC excitation method stopped observable electrolysis effects, leading to stable measurements and improved sensor longevity. These findings highlight pulsed DC excitation as a practical and effective solution for enhancing the accuracy and durability of resistive frost-detection sensors, making them more suitable for long-term use in commercial refrigeration system evaporators. Full article
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28 pages, 6590 KiB  
Article
Pulse Sensors Based on Laser-Induced Graphene Transferred to Biocompatible Polyurethane Networks: Fabrication, Transfer Methods, Characterization, and Application
by Vanja Vojnović, Marko Spasenović, Ivan Pešić, Teodora Vićentić, Milena Rašljić Rafajilović, Stefan D. Ilić and Marija V. Pergal
Chemosensors 2025, 13(4), 122; https://doi.org/10.3390/chemosensors13040122 - 2 Apr 2025
Viewed by 1207
Abstract
Flexible, wearable biomedical sensors based on laser-induced graphene (LIG) have garnered significant attention due to a straightforward fabrication process and exceptional electrical and mechanical properties. However, most relevant studies rely on commercial polyimide precursors, which suffer from inadequate biocompatibility and weak adhesion between [...] Read more.
Flexible, wearable biomedical sensors based on laser-induced graphene (LIG) have garnered significant attention due to a straightforward fabrication process and exceptional electrical and mechanical properties. However, most relevant studies rely on commercial polyimide precursors, which suffer from inadequate biocompatibility and weak adhesion between the precursor material and the LIG layer. To address these challenges, we synthesized cross-linked polyurethanes (PUs) with good biocompatibility and used them as substrates for LIG-based wearable pulse sensors. During fabrication, we employed two methods of LIG transfer to achieve optimal transfer yield. We adjusted the thickness of PU films and tailored their mechanical and physicochemical properties by varying the soft segment content to achieve optimal sensor performance. Our findings demonstrate that the success of LIG transfer is strongly influenced by the structure and composition of the polymeric substrate. Tensile testing revealed that increasing the soft segment content in PU films significantly improved their tensile strength, elongation at break, and flexibility, with PU based on 50 wt.% soft segment content (PU-50) showing the best mechanical properties. LIG exhibited minimal sensitivity to humidity, while PU films maintained high transparency (>80% at 500 nm), and PU-50 was non-toxic, with less than 5% lactate dehydrogenase (LDH) release in endothelial cell cultures, confirming its biocompatibility. Adhesion tests demonstrated that LIG transferred onto PU-50 exhibited significantly stronger adhesion compared to other tested substrates, with only a 30% increase in electrical resistance after the Scotch tape test, ensuring stability for wearable sensors. The optimal substrate, a semicrystalline PU-50, yielded superior transfer efficiency. Among all tested sensors, the LIG/PU-50, featuring a 77 μm thick substrate with good mechanical properties and improved adhesion, exhibited the highest signal-to-noise ratio (SNR). This study showcases a skin-safe LIG/PU-based pulse sensor that has significant potential for applications as a wearable patch in medical and sports monitoring. Full article
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30 pages, 14392 KiB  
Article
High-Quality Perovskite Thin Films for NO2 Detection: Optimizing Pulsed Laser Deposition of Pure and Sr-Doped LaMO3 (M = Co, Fe)
by Lukasz Cieniek, Agnieszka Kopia, Kazimierz Kowalski and Tomasz Moskalewicz
Materials 2025, 18(5), 1175; https://doi.org/10.3390/ma18051175 - 6 Mar 2025
Cited by 2 | Viewed by 877
Abstract
This study investigates the structural and catalytic properties of pure and Sr-doped LaCoO3 and LaFeO3 thin films for potential use as resistive gas sensors. Thin films were deposited via pulsed laser deposition (PLD) and characterized using X-ray diffraction (XRD), X-ray photoelectron [...] Read more.
This study investigates the structural and catalytic properties of pure and Sr-doped LaCoO3 and LaFeO3 thin films for potential use as resistive gas sensors. Thin films were deposited via pulsed laser deposition (PLD) and characterized using X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), atomic force microscopy (AFM), nanoindentation, and scratch tests. XRD analysis confirmed the formation of the desired perovskite phases without secondary phases. XPS revealed the presence of La3+, Co3+/Co4+, Fe3+/Fe4+, and Sr2+ oxidation states. SEM and AFM imaging showed compact, nanostructured surfaces with varying morphologies (shape and size of surface irregularities) depending on the composition. Sr doping led to surface refinement and increased nanohardness and adhesion. Transmission electron microscopy (TEM) analysis confirmed the columnar growth of nanocrystalline films. Sr-doped LaCoO3 demonstrated enhanced sensitivity and stability in the presence of NO2 gas compared to pure LaCoO3, as evidenced by electrical resistivity measurements within 230 ÷ 440 °C. At the same time, it was found that Sr doping stabilizes the catalytic activity of LaFeO3 (in the range of 300 ÷ 350 °C), although its behavior in the presence of NO2 differs from that of LaCo(Sr)O3—especially in terms of response and recovery times. These findings highlight the potential of Sr-doped LaCoO3 and LaFeO3 thin films for NO2 sensing applications. Full article
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20 pages, 11640 KiB  
Article
The Influence of Sample Microfabrication and Annealing on the Mechanical Strain–Stress Behavior of Stainless Steels and Corrosion Resistant Aluminum Alloys in Micro-Tensile Tests
by Janko Auerswald, Joel Tenisch, Christoph Fallegger and Markus Seifert
Micromachines 2025, 16(3), 309; https://doi.org/10.3390/mi16030309 - 6 Mar 2025
Viewed by 785
Abstract
Miniaturized components for enhanced integrated functionality or thin sheets for lightweight applications often consist of face-centered cubic metals. They exhibit good strength, corrosion resistance, formability and recyclability. Microfabrication technologies, however, may introduce cold work or detrimental heat-induced lattice defects into the material, with [...] Read more.
Miniaturized components for enhanced integrated functionality or thin sheets for lightweight applications often consist of face-centered cubic metals. They exhibit good strength, corrosion resistance, formability and recyclability. Microfabrication technologies, however, may introduce cold work or detrimental heat-induced lattice defects into the material, with consequences for the mechanical properties. Austenitic stainless steels (1.4310, 1.4301) and aluminum alloys (EN AW-5005-H24, EN AW-6082-T6) were selected for this study. The influence of pulsed fiber laser cutting, microwaterjet cutting, and annealing on the strain–stress behavior was investigated. The micro-tensile test setup comprised a flex-structure force sensor, a laser extensometer, and a dedicated sample holder. Fiber laser cut 1.4310 samples exhibited early failure at low fracture strain in narrow shear band zones. The shear band zones were detectable on the sample surface, in the laser extensometer images, in the horizontal sections of the stress–strain curves, and in the microstructure. Inside the shear band zones, grains were strongly elongated and exhibited numerous parallel planar defects. Heat-induced chromium carbides, in combination with low stacking fault energy (SFE) and elevated carbon content, favored shear band zone formation in 1.4310. In contrast, microwaterjet cut high SFE materials EN AW-5005-H24 and EN AW-6082-T6, as well as low-carbon austenitic stainless steel 1.4301, exhibited uniform plastic deformation. Full article
(This article belongs to the Section D:Materials and Processing)
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17 pages, 3310 KiB  
Article
Fully Inkjet-Printed Flexible Graphene–Prussian Blue Platform for Electrochemical Biosensing
by Željka Boček, Marko Zubak and Petar Kassal
Biosensors 2025, 15(1), 28; https://doi.org/10.3390/bios15010028 - 8 Jan 2025
Cited by 2 | Viewed by 1543
Abstract
Prussian Blue (PB) is commonly incorporated into screen-printed enzymatic devices since it enables the determination of the enzymatically produced hydrogen peroxide at low potentials. Inkjet printing is gaining popularity in the development of electrochemical sensors as a substitute for screen printing. This work [...] Read more.
Prussian Blue (PB) is commonly incorporated into screen-printed enzymatic devices since it enables the determination of the enzymatically produced hydrogen peroxide at low potentials. Inkjet printing is gaining popularity in the development of electrochemical sensors as a substitute for screen printing. This work presents a fully inkjet-printed graphene–Prussian Blue platform, which can be paired with oxidase enzymes to prepare a biosensor of choice. The graphene electrode was inkjet-printed on a flexible polyimide substrate and then thermally and photonically treated with intense pulsed light, followed by inkjet printing of a PB nanoparticle suspension. The optimization of post-printing treatment and electrode deposition conditions was performed to yield a platform with minimal sheet resistance and peak potential differences. A thorough study of PB deposition was conducted: the fully inkjet-printed system was compared against sensors with PB deposited chemically or by drop casting the PB suspension on different kinds of carbon electrodes (glassy carbon, commercial screen-printed, and in-house inkjet-printed electrodes). For hydrogen peroxide detection, the fully inkjet-printed platform exhibits excellent sensitivity, a wider linear range, better linearity, and greater stability towards higher concentrations of peroxide than the other tested electrodes. Finally, lactate oxidase was immobilized in a chitosan matrix, and the prepared biosensor exhibited analytical performance comparable to other lactate sensors found in the literature in a wide, physiologically relevant linear range for measuring lactate concentration in sweat. The development of mediator-modified electrodes with a single fabrication technology, as demonstrated here, paves the way for the scalable production of low-cost, wearable, and flexible biosensors. Full article
(This article belongs to the Special Issue Flexible Electronics for Biosensing)
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21 pages, 5252 KiB  
Article
A Multi-Layered Origami Tactile Sensory Ring for Wearable Biomechanical Monitoring
by Rajat Subhra Karmakar, Hsin-Fu Lin, Jhih-Fong Huang, Jui-I Chao, Ying-Chih Liao and Yen-Wen Lu
Biosensors 2025, 15(1), 8; https://doi.org/10.3390/bios15010008 - 27 Dec 2024
Cited by 1 | Viewed by 1559
Abstract
An origami-based tactile sensory ring utilizing multilayered conductive paper substrates presents an innovative approach to wearable health applications. By harnessing paper’s flexibility and employing origami folding, the sensors integrate structural stability and self-packaging without added encapsulation layers. Knot-shaped designs create loop-based systems that [...] Read more.
An origami-based tactile sensory ring utilizing multilayered conductive paper substrates presents an innovative approach to wearable health applications. By harnessing paper’s flexibility and employing origami folding, the sensors integrate structural stability and self-packaging without added encapsulation layers. Knot-shaped designs create loop-based systems that secure conductive paper strips and protect sensing layers. Demonstrating a sensitivity of 3.8 kPa−1 at subtle pressures (0–0.05 kPa), the sensors detect both minimal stimuli and high-pressure inputs. Electrical modeling of various origami configurations identifies designs with optimized performance with a pentagon knot offering higher sensitivity to support high-sensitivity needs. Meanwhile a square knot provides greater precision and quicker recovery, balancing sensitivity and stability for real-time feedback devices. The enhanced elastic modulus from folds remains within human skin’s elasticity range, ensuring comfort. Applications include grip strength monitoring and pulse rate detection from the thumb, capturing pulse transit time (PTT), an essential cardiovascular biomarker. This design shows the potential of origami-based tactile sensors in creating versatile, cost-effective wearable health monitoring systems. Full article
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22 pages, 10725 KiB  
Review
Hardware Testing Methodologies for Wide Bandgap High-Power Converters
by Zibo Chen, Zhicheng Guo, Chen Chen and Alex Q. Huang
Electronics 2024, 13(19), 3918; https://doi.org/10.3390/electronics13193918 - 3 Oct 2024
Cited by 3 | Viewed by 1989
Abstract
Wide bandgap (WBG) power semiconductor devices are increasingly replacing silicon IGBTs in high-power and high-voltage power electronics applications. However, there is a significant gap in the literature regarding efficient testing methodologies for high-power and high-voltage converters under constrained laboratory resources. This paper addresses [...] Read more.
Wide bandgap (WBG) power semiconductor devices are increasingly replacing silicon IGBTs in high-power and high-voltage power electronics applications. However, there is a significant gap in the literature regarding efficient testing methodologies for high-power and high-voltage converters under constrained laboratory resources. This paper addresses this gap by presenting comprehensive, hardware-focused testing methodologies for high-power and high-voltage WBG power semiconductor-based converter bring-up before the control validation phase steps in. The proposed methods enable thorough evaluation and validation of converter hardware, including device switching characteristics, driving circuit functionality, thermal management performance, insulation integrity, and sustained operation at full power. We utilized the double pulse test (DPT) to characterize switching performance in a two-level phase leg configuration, extract circuit parasitics, and validate magnetic components. The DPT was further applied to optimize gate driving circuits, validate overcurrent protection mechanisms, and measure device on-resistance. Additionally, a multicycle test was introduced to rapidly assess steady-state converter performance and estimate efficiency. Recognizing the critical role of thermal management in high-power converters, our methodologies extend to the experimental extraction of key thermal parameters—such as junction-to-ambient thermal resistance and thermal capacitance—via a heat loss injection method. A correlation method between temperature sensor measurements and junction temperature is presented to enhance the accuracy of device temperature monitoring during tests. To ensure reliability and safety, dielectric withstand tests and partial discharge measurements were conducted at both component and converter levels under conventional 60 Hz sinusoidal and high-frequency PWM waveforms. Finally, we highlight the importance of testing converters under full voltage, current, and thermal conditions through power circulating tests with minimal power consumption, applicable to both non-isolated and isolated high-power converters. Practical examples are provided to demonstrate the effectiveness and applicability of these hardware testing methodologies. Full article
(This article belongs to the Special Issue Advances in Power Converter Design, Control and Applications)
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20 pages, 5259 KiB  
Article
Voltammetric Sensor Based on Titania Nanoparticles Synthesized with Aloe vera Extract for the Quantification of Dithiophosphates in Industrial and Environmental Samples
by Javier E. Vilasó-Cadre, Alondra Ramírez-Rodríguez, Juan Hidalgo, Iván A. Reyes-Domínguez, Roel Cruz, Mizraim U. Flores, Israel Rodríguez-Torres, Roberto Briones-Gallardo, Luis Hidalgo and Juan Jesús Piña Leyte-Vidal
Chemosensors 2024, 12(9), 195; https://doi.org/10.3390/chemosensors12090195 - 22 Sep 2024
Cited by 1 | Viewed by 1860
Abstract
In this work, TiO2 spherical nanoparticles with a mean diameter of 10.08 nm (SD = 4.54 nm) were synthesized using Aloe vera extract. Rutile, brookite, and anatase crystalline phases were identified. The surface morphology of a carbon paste electrode does not change [...] Read more.
In this work, TiO2 spherical nanoparticles with a mean diameter of 10.08 nm (SD = 4.54 nm) were synthesized using Aloe vera extract. Rutile, brookite, and anatase crystalline phases were identified. The surface morphology of a carbon paste electrode does not change in the presence of nanoparticles; however, the surface chemical composition does. The voltammetric response to dicresyl dithiophosphate was higher when the electrode was modified with TiO2 nanoparticles. After an electrochemical response study from pH 1.0 to 12.0, pH 7.0 was selected for the electroanalysis. The electroactive area of the modified sensor was 0.036 cm2, while it was 0.026 cm2 for the bare electrode. The oxidation process showed mixed adsorption-diffusion control. The charge transfer resistance of the modified sensor (530.1 Ω, SD = 4.08 Ω) was much lower than that of the bare electrode (4298 Ω, SD = 8.53 Ω). The linear quantitative range by square wave voltammetry was from 5 to 150 μmol/L, with a limit of detection of 1.89 μmol/L and a limit of quantification of 6.26 μmol/L under optimal pulse parameters of 50 Hz frequency, 1 mV step potential, and 25 mV pulse amplitude. The sensor response was repeatable and reproducible over 30 days. The results on real flotation and synthetically contaminated soil samples were statistically equivalent to those obtained by UV-vis spectrophotometry. A dithiocarbamate showed an interfering effect on the sensor response to dithiophosphate. Full article
(This article belongs to the Special Issue Advances in Electrochemical Sensing and Analysis)
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28 pages, 8377 KiB  
Review
Research Progress on Saccharide Molecule Detection Based on Nanopores
by Bohua Yin, Wanyi Xie, Shaoxi Fang, Shixuan He, Wenhao Ma, Liyuan Liang, Yajie Yin, Daming Zhou, Zuobin Wang and Deqiang Wang
Sensors 2024, 24(16), 5442; https://doi.org/10.3390/s24165442 - 22 Aug 2024
Cited by 2 | Viewed by 2012
Abstract
Saccharides, being one of the fundamental molecules of life, play essential roles in the physiological and pathological functions of cells. However, their intricate structures pose challenges for detection. Nanopore technology, with its high sensitivity and capability for single-molecule-level analysis, has revolutionized the identification [...] Read more.
Saccharides, being one of the fundamental molecules of life, play essential roles in the physiological and pathological functions of cells. However, their intricate structures pose challenges for detection. Nanopore technology, with its high sensitivity and capability for single-molecule-level analysis, has revolutionized the identification and structural analysis of saccharide molecules. This review focuses on recent advancements in nanopore technology for carbohydrate detection, presenting an array of methods that leverage the molecular complexity of saccharides. Biological nanopore techniques utilize specific protein binding or pore modifications to trigger typical resistive pulses, enabling the high-sensitivity detection of monosaccharides and oligosaccharides. In solid-state nanopore sensing, boronic acid modification and pH gating mechanisms are employed for the specific recognition and quantitative analysis of polysaccharides. The integration of artificial intelligence algorithms can further enhance the accuracy and reliability of analyses. Serving as a crucial tool in carbohydrate detection, we foresee significant potential in the application of nanopore technology for the detection of carbohydrate molecules in disease diagnosis, drug screening, and biosensing, fostering innovative progress in related research domains. Full article
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18 pages, 6965 KiB  
Article
Optimizing Piezoelectric Bimorphs for Energy Harvesting from Body Motion: Finger Movement in Computer Mouse Clicking
by Theetuch Chinachatchawarat, Theerawat Pattarapongsakorn, Patitta Ploypray, Thitima Jintanawan and Gridsada Phanomchoeng
Energies 2024, 17(16), 4121; https://doi.org/10.3390/en17164121 - 19 Aug 2024
Cited by 3 | Viewed by 1612
Abstract
Electrical devices are integral to daily life, but limited battery life remains a significant issue. A proposed solution is to convert dissipated energy from human motion into electricity using piezoelectric materials. This study investigates lead–zirconate–titanate (PZT) piezoelectric materials in bimorph configuration, conducts performance [...] Read more.
Electrical devices are integral to daily life, but limited battery life remains a significant issue. A proposed solution is to convert dissipated energy from human motion into electricity using piezoelectric materials. This study investigates lead–zirconate–titanate (PZT) piezoelectric materials in bimorph configuration, conducts performance tests to understand their characteristics and determine the optimal load resistance, and develops an energy-harvesting prototype. Performance tests adjusted input parameters and varied load resistance and input magnitude to optimize power gained from the PZT bimorph. A suitable human movement for the application of the bimorph is a mouse-clicking motion by fingers. A prototype was created by integrating the bimorph into a computer mouse to capture energy from clicks. The results showed that the deformation rate of the PZTs, input magnitude, and resistance load were key factors in optimization. The bimorph configuration produced 0.34 mW of power and 5.5 V at an optimum load of 5072 Ω, requiring less effort to generate electricity. For the computer mouse energy harvester case, it yielded a total average power of approximately 38.4 μW per click with a click frequency of 4 Hz. This power could be used to support IoT devices such as human sensors (e.g., CO2, temperature, and pulse sensors) and smart home sensors, enabling comprehensive health and environmental monitoring. In conclusion, input specifications, magnitude, and load resistance are essential for optimizing piezoelectric energy harvesters. Full article
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