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Keywords = recycled cold mix

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16 pages, 5489 KB  
Article
Valorization of Expanded Polystyrene by Embedding of High GFRP Loading Through Cold-Mixing Solvent-Assisted Process
by Federico Olivieri, Stefano Scognamiglio, Roberto Avolio, Rachele Castaldo, Mariacristina Cocca, Gennaro Gentile, Silvia Olivotto and Maria Emanuela Errico
Polymers 2026, 18(13), 1567; https://doi.org/10.3390/polym18131567 (registering DOI) - 24 Jun 2026
Abstract
The increasing accumulation of glass-fiber-reinforced polymer (GFRP) waste poses significant environmental challenges, calling for effective and scalable recycling strategies. In this work, a solvent-assisted cold mixing process was employed to incorporate very high amounts of GFRP (up to 75 wt%) into recycled expanded [...] Read more.
The increasing accumulation of glass-fiber-reinforced polymer (GFRP) waste poses significant environmental challenges, calling for effective and scalable recycling strategies. In this work, a solvent-assisted cold mixing process was employed to incorporate very high amounts of GFRP (up to 75 wt%) into recycled expanded polystyrene (ePS). The composites were deeply characterized, with particular attention to the role of particle size distribution and filler content. The results demonstrated that GFRP granulometry played a key role in determining composite performance. Intermediate particle sizes (0.25 mm) provided the best balance between dispersion, interfacial interaction, and mechanical properties, whereas excessively fine fractions introduced defects and reduced impact resistance (from 0.7 to 2.0 kJ/m2 going from dust to 0.25 mm at 75 wt%). Notably, the solvent-assisted approach has been widely recognized as an effective strategy to ensure homogeneous dispersion even at high filler contents, allowing subsequent melt processing without re-agglomeration. Recycled composites retained most of their chemical and mechanical properties after reprocessing, with only moderate performance losses mainly related to fiber fragmentation. Overall, this study demonstrates an effective and sustainable route for the simultaneous valorization of ePS and GFRP waste, enabling the production of highly loaded composites with preserved functionality and improved resource efficiency. Full article
(This article belongs to the Special Issue Functional Polymer Composites: Synthesis and Application)
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21 pages, 15578 KB  
Article
Microscopic Characterization and Efficiency Coefficient Evaluation of Modified Recycled Concrete Micropowder in Cementitious Materials
by Qiuyi Li, Pengfei Zhang, Mingxu Chen, Liang Wang, Gongbing Yue, Jinghua Yan, Chenyang Xu and Yuanxin Guo
Materials 2026, 19(11), 2391; https://doi.org/10.3390/ma19112391 - 3 Jun 2026
Viewed by 253
Abstract
To advance the development of sustainable buildings, this study investigates recycled cement-based materials. The core component of this material is concrete-based recycled micropowder (CRM), which is shaped and reinforced from recycled construction waste. It is then activated through high-temperature calcination to produce modified [...] Read more.
To advance the development of sustainable buildings, this study investigates recycled cement-based materials. The core component of this material is concrete-based recycled micropowder (CRM), which is shaped and reinforced from recycled construction waste. It is then activated through high-temperature calcination to produce modified recycled micropowder (MRM), and the resulting changes in its properties are analyzed. X-ray diffraction, Brunauer–Emmett–Teller surface area, and hydration heat tests reveal that cementitious materials incorporating MRM800 contain more C-S-H and other hydration products, exhibit lower porosity, and demonstrate stronger hydration reactions. The results show that 800 °C is the optimal calcination temperature for CRM activation. For recycled silica-based mortar (RSM), the introduction of an efficiency coefficient (Kλ) allows for a quantitative, scientific, and intuitive evaluation of the contributions of three admixtures, aiding in the optimization of the mix ratio. RSM with MRM showed improved performance, with compressive strength ranging from 24.3 to 42.3 MPa. A 20% MRM addition effectively enhanced the mechanical properties of the mortar, while the mixture with 10% MRM and a 1:3 cement-to-sand ratio exhibited only 8.23% strength loss and 0.78% mass loss after 50 freeze–thaw cycles. MRM can improve the compactness of the cement matrix and thus optimize its freeze–thaw resistance, providing an eco-friendly technical solution for the engineering application of recycled mortar in cold regions. Full article
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28 pages, 2998 KB  
Article
Optimization Design and Fatigue Performance of Foamed Asphalt Cold Recycled Mixtures
by Xianxin Zhu, Bin Li, Chen Zhao, Xiaoling Zou, Guoqiang Sun and Yanqiu Bi
Buildings 2026, 16(11), 2199; https://doi.org/10.3390/buildings16112199 - 29 May 2026
Viewed by 216
Abstract
Foamed asphalt cold recycling technology is one of the key engineering approaches to address the accumulation of large quantities of reclaimed asphalt pavement (RAP) in road maintenance and rehabilitation. However, a systematic design methodology that simultaneously accounts for long-term fatigue resistance and toughness [...] Read more.
Foamed asphalt cold recycling technology is one of the key engineering approaches to address the accumulation of large quantities of reclaimed asphalt pavement (RAP) in road maintenance and rehabilitation. However, a systematic design methodology that simultaneously accounts for long-term fatigue resistance and toughness has not yet reached a unified consensus or widespread application. Existing studies have investigated the effects of fine aggregate gradation or cement content on individual performance aspects of mixtures, but studies incorporating both factors into a unified experimental framework for parallel comparison of multiple performance indicators remain limited. To this end, this study designed three mineral aggregate gradations with significantly different fine aggregate contents and systematically evaluated the effects of gradation composition, foamed asphalt content, and cement dosage on the mechanical properties, moisture stability, high-temperature stability, and fatigue performance of the mixtures. Indirect tensile fatigue tests under a stress-controlled mode were conducted to determine the fatigue life of different gradations at four stress ratio levels. The results indicate that sufficient fine aggregate content, particularly particles smaller than 0.075 mm, is a key factor in enhancing mixture compactness, indirect tensile strength, and resistance to moisture damage. The effect of cement on fatigue performance exhibits stress-level dependency: at low stress ratios, the addition of cement improves fatigue life, whereas at high stress ratios, the increased brittleness of the material reduces fatigue resistance, which is consistent with findings reported in previous studies. Furthermore, this study provides comparative experimental data for different fine aggregate gradations. The optimal gradation scheme demonstrated superior overall performance across all evaluated indicators, verifying the feasibility of achieving a balance between strength and toughness through gradation optimization. Compared with conventional design methods guided by a single strength index, this study offers a more comprehensive basis for mix design optimization of foamed asphalt cold recycled mixtures and provides engineering references for their application in long-life pavement maintenance. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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24 pages, 2959 KB  
Article
Multi-Parameter Collaborative Optimization of Foamed Asphalt Cold Recycling Mixture Properties
by Wei Qiu, Bin Li, Ziyi Song, Xiaoling Zou, Mingjun Hu and Yanqiu Bi
Materials 2026, 19(10), 2123; https://doi.org/10.3390/ma19102123 - 18 May 2026
Viewed by 377
Abstract
This study examined the foaming characteristics of asphalt and their effects on the performance of cold recycled mixtures. The expansion ratio and half-life were used to evaluate effects of asphalt type, foaming temperature, and water content. The influence of asphalt content, gradation, cement [...] Read more.
This study examined the foaming characteristics of asphalt and their effects on the performance of cold recycled mixtures. The expansion ratio and half-life were used to evaluate effects of asphalt type, foaming temperature, and water content. The influence of asphalt content, gradation, cement content, curing time, and mixing water on mechanical properties and water stability was analyzed. The results indicate that asphalt type is the key factor affecting foaming performance. CNOOA asphalt showed optimal foaming at 160 °C with 2% water, achieving an expansion ratio of 27 and a half-life over 30 s. Optimal asphalt contents for gradations A and B are 3.5% and 2.5%, respectively. A 1.5% cement content provides the best performance balance. Dry and wet indirect tensile strengths increased by 91.18% and 205.56% after 3-day curing. The optimal mixing water ranges are 60–90% and 70–80% of optimum moisture content for gradations A and B. Curing time has the most significant influence on performance, followed by cement and asphalt content. This study provides a theoretical basis for optimizing foamed asphalt cold recycling. Full article
(This article belongs to the Section Construction and Building Materials)
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23 pages, 1046 KB  
Article
A Multi-Criteria Decision-Support Framework for Sustainable Asphalt Mixtures: Integrating Mechanical Performance and Environmental Impacts Through Structural Normalisation
by Caroline F. N. Moura, Hugo M. R. D. Silva and Joel R. M. Oliveira
Sustainability 2026, 18(10), 5070; https://doi.org/10.3390/su18105070 - 18 May 2026
Viewed by 176
Abstract
Sustainability assessment of road pavements requires the combined consideration of environmental and mechanical performance, since conventional mass-based Life Cycle Assessment (LCA) may lead to misleading conclusions. This study proposes a multi-criteria decision-support framework that integrates LCA results with key mechanical indicators through structural [...] Read more.
Sustainability assessment of road pavements requires the combined consideration of environmental and mechanical performance, since conventional mass-based Life Cycle Assessment (LCA) may lead to misleading conclusions. This study proposes a multi-criteria decision-support framework that integrates LCA results with key mechanical indicators through structural normalisation, enabling the comparison of asphalt mixtures on an equivalent structural basis. Three sustainable asphalt mixtures were analysed, namely Hot Recycled Mix Asphalt (HRMA), Half-Warm Mix Asphalt (HWMA), and Cold Recycled Mixture (CRM), and compared with a reference Hot Mix Asphalt (HMA). Environmental impacts were quantified using a cradle-to-gate LCA, while mechanical performance was characterised through stiffness, fatigue resistance, rutting, and moisture susceptibility. These indicators were integrated into a Structural Contribution index and a Material Environmental Impact Ratio. The results show that, although CRM benefits from cold production and high recycling rates, its lower structural performance reduces its advantage when equivalent thickness is considered. HWMA emerges as the most favourable compromise within the adopted framework, combining lower environmental impacts with competitive structural performance, while HRMA offers the greatest structural contribution with competitive environmental performance. Sensitivity analysis confirms the robustness of the framework under realistic variations in weighting assumptions. The study demonstrates that incorporating structural performance into environmental assessment is essential to avoid misleading conclusions and to support more reliable decision-making in sustainable pavement design. Full article
(This article belongs to the Section Sustainable Materials)
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26 pages, 10706 KB  
Article
Design and Performance Evaluation of Cold-Recycled Asphalt Mixtures with Reclaimed Cement-Stabilized Bases
by Zhoucong Xu, Hui Wang, Liping Liu, Dongchang Zhang and Lijun Sun
Sustainability 2026, 18(9), 4391; https://doi.org/10.3390/su18094391 - 30 Apr 2026
Viewed by 506
Abstract
The sustainable utilization of multiple reclaimed pavement materials is a critical pathway toward green highway construction. This study investigates the performance and synergistic mechanisms of cold-recycled mixtures incorporating both Reclaimed Asphalt Pavement (RAP) and Reclaimed Cement-Stabilized Base (RCSB), using emulsified asphalt as the [...] Read more.
The sustainable utilization of multiple reclaimed pavement materials is a critical pathway toward green highway construction. This study investigates the performance and synergistic mechanisms of cold-recycled mixtures incorporating both Reclaimed Asphalt Pavement (RAP) and Reclaimed Cement-Stabilized Base (RCSB), using emulsified asphalt as the primary binder. A comprehensive experimental program was conducted to evaluate the effects of reclaimed material proportions, mixing sequences, and curing ages on the mechanical strength, moisture susceptibility, and high-temperature stability of the mixtures. Microscopic characterization via Scanning Electron Microscope (SEM) and Energy Dispersive Spectroscopy (EDS) were employed to elucidate the Interfacial Transition Zone (ITZ) evolution. Results indicate that an optimal RCSB incorporation range of 20–40% establishes a robust “stone-to-stone” rigid skeleton, significantly enhancing the splitting strength (up to 0.87 MPa) and durability (Splitting Strength Ratio, TSR > 91%). SEM observations confirm the formation of a dense interpenetrating network structure within this range, where cement hydration products and asphalt films achieve optimal chemo-physical bonding. Exceeding 40% RCSB leads to a moisture-starved state and a sharp decline in dynamic stability due to insufficient binder coating. Micro-morphological characterization reveals that the transition from macro-interfacial debonding to a robust cohesive failure mode is the fundamental driver for the performance peak at 20–40% RCSB. SEM observations confirm the formation of a dense interpenetrating network structure, where cement hydration products successfully anchor into the asphalt film. This optimized ITZ effectively eliminates the stress concentration and aggregate crushing seen in high-RAP mixtures, thereby ensuring superior mechanical integrity. Furthermore, a pre-wetting mixing sequence ensures a high-energy mineral surface that promotes the heterogeneous nucleation of cement. SEM results show that this prevents the competitive adsorption between cement and asphalt, transforming the ITZ from a friable, loose state into a densified crystalline adhesive matrix. Full article
(This article belongs to the Special Issue Asphalt Binder and Sustainable Pavement Design)
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16 pages, 833 KB  
Article
Study on the Optimization of Mix Proportions for Recycled Aggregate Concrete and Its Freeze–Thaw Resistance Performance
by Ping Zheng, Wei Deng, Wenyu Wei, Chao Pu, Zhiwei Yang, Bing Ma, Jialong Sheng and Peng Yin
Materials 2026, 19(9), 1683; https://doi.org/10.3390/ma19091683 - 22 Apr 2026
Viewed by 466
Abstract
The growing volume of construction and demolition waste has made discarded concrete a major source of urban solid waste, placing increasing pressure on land resources and the environment. Recycling waste concrete into recycled aggregate concrete (RAC) offers an effective solution for resource conservation [...] Read more.
The growing volume of construction and demolition waste has made discarded concrete a major source of urban solid waste, placing increasing pressure on land resources and the environment. Recycling waste concrete into recycled aggregate concrete (RAC) offers an effective solution for resource conservation and carbon reduction, aligning with the goals of sustainable development. However, due to the residual mortar, high porosity, and microcracks of recycled aggregates, RAC generally exhibits lower compactness, strength, and durability than conventional concrete, particularly under freeze–thaw conditions where degradation accelerates and service life decreases. To address these challenges, this study investigates the optimization of RAC mix design and its frost resistance performance for pavement base applications. An orthogonal experimental design was employed, with the water-to-binder ratio, recycled aggregate replacement ratio, and air-entraining agent dosage as key variables, while 7-day compressive strength, permeability coefficient, and rebound modulus served as evaluation indices. The influence and interaction of these factors were analyzed to determine an optimal mix meeting both mechanical and durability requirements. Rapid freeze–thaw cycling tests were then conducted to examine the variations in mass loss, relative dynamic modulus, and compressive strength retention, followed by exponential and damage variable modeling to characterize the degradation process. Results show that the water-to-binder ratio primarily governs strength, the replacement ratio affects stiffness and permeability, and the air-entraining agent significantly enhances frost resistance by improving pore structure. The optimized mix retained over 70% of its relative dynamic modulus after 300 freeze–thaw cycles, exhibiting superior durability. This work establishes a systematic framework for multi-factor optimization and durability evaluation of RAC, providing theoretical and practical guidance for its application in cold-region pavement bases. Full article
(This article belongs to the Special Issue Eco-Friendly and Low-Carbon Cement-Based Materials)
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33 pages, 1058 KB  
Review
Sustainable Asphalt Mixtures: A Review of Recycling and Low-Temperature Technologies for an Integrated Sustainability Assessment
by Caroline F. N. Moura, Hugo M. R. D. Silva and Joel R. M. Oliveira
Infrastructures 2026, 11(4), 139; https://doi.org/10.3390/infrastructures11040139 - 17 Apr 2026
Viewed by 1068
Abstract
Asphalt pavements are essential to modern transport infrastructure but remain highly dependent on virgin aggregates and petroleum-based binders, resulting in high energy demand and significant greenhouse gas emissions. In response, research has advanced recycled-material solutions and low-temperature asphalt technologies. However, sustainability is still [...] Read more.
Asphalt pavements are essential to modern transport infrastructure but remain highly dependent on virgin aggregates and petroleum-based binders, resulting in high energy demand and significant greenhouse gas emissions. In response, research has advanced recycled-material solutions and low-temperature asphalt technologies. However, sustainability is still often inferred from isolated environmental indicators, without consistent consideration of mechanical durability or economic feasibility throughout the life cycle. This review provides an integrated synthesis of sustainable asphalt mixtures by jointly examining recycling strategies, temperature-reduction processes (warm-mix, half-warm-mix, and cold-mix asphalt technologies), and their combined applications through an integrated performance–cost–environment perspective. The literature reveals substantial methodological fragmentation, with limited harmonisation of functional units, system boundaries, and allocation rules, which constrains cross-study comparability. Evidence indicates that reclaimed asphalt, recycled concrete aggregates, and steel slag can maintain or improve rutting resistance, stiffness, and moisture durability while enabling material cost savings of approximately 5–68%. Temperature-reduction technologies further achieve significant energy and GHG reductions in the production phase (20–70%), with integrated recycling–temperature-reduction systems showing the most consistent combined benefits. Overall, this review demonstrates that asphalt sustainability cannot be established through single-dimensional assessments but requires harmonised life-cycle frameworks that explicitly link environmental gains to mechanical performance, durability, and economic viability. Full article
(This article belongs to the Special Issue Sustainable Road Design and Traffic Management)
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21 pages, 3169 KB  
Article
Development of Cold-Recycled Asphalt Mixtures Incorporating Biomass-Derived Ashes and Reclaimed Asphalt Pavement
by Zainab Al Qraiti, Anmar Dulaimi, Marisa Sofia Fernandes Dinis de Almeida and Luís Filipe Almeida Bernardo
CivilEng 2026, 7(2), 25; https://doi.org/10.3390/civileng7020025 - 15 Apr 2026
Viewed by 555
Abstract
Comparing cold-recycled asphalt mixtures (CRAMs) to conventional hot-mix asphalt (HMA) shows that CRAMs offer several logistical, financial, and environmental advantages. However, such CRAMs, when using asphalt emulsion, still suffer from excessive water damage and poor early-age performance. The main aim of this study [...] Read more.
Comparing cold-recycled asphalt mixtures (CRAMs) to conventional hot-mix asphalt (HMA) shows that CRAMs offer several logistical, financial, and environmental advantages. However, such CRAMs, when using asphalt emulsion, still suffer from excessive water damage and poor early-age performance. The main aim of this study is to improve CRAMs by incorporating two biomass ashes and reclaimed asphalt pavement (RAP): palm leaf ash (PLA) and reed ash (RA) with different percentages of RAP. RAP was used in five percentage levels, 0%, 25%, 50%, 75%, and 100% by weight of mix, to develop the CRAMs. In addition, the improvement in CMA mechanical properties was assessed by incorporating PLA as filler replacement in five percentages, namely: 0%, 1.75%, 3.5%, 5.25%, and 7% by weight of aggregate. RA was used as an activator at 0.25%, 0.5, 1%, and 2% by weight of aggregate. The moisture susceptibility test, Indirect Tensile Strength Test (ITS), and Marshall test were used to assess the mechanical properties. The results obtained showed that the durability and mechanical properties of CMA are effectively enhanced with the addition of 1.5% PLA, 0.45% RA, and 5.5% Ordinary Portland Cement (OPC) as fillers. In addition, CRAMs with a higher percentage of RAP 75%, showed higher strength in terms of Marshall stability. These findings demonstrate that the studied CRAMs offer a reliable alternative for pavement applications, namely when sustainable and cost-effective materials are required. Full article
(This article belongs to the Section Construction and Material Engineering)
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14 pages, 3147 KB  
Article
Improving the Environmental Safety of Transport Equipment Using Biodiesel Produced from Waste Vegetable
by Sergey N. Krivtsov, Nina V. Nemchinova, Andrey A. Tyutrin, Daniil Iakovlev, Dmitry A. Tikhov-Tinnikov, Sergey P. Ozornin, Andrei V. Negovora and Filipp A. Vasilev
Appl. Sci. 2026, 16(7), 3487; https://doi.org/10.3390/app16073487 - 3 Apr 2026
Viewed by 714
Abstract
Issues related to the environmental safety of transport vehicles, the operation of which leads to environmental pollution, continue to be highly relevant. In this work, we consider the use of biofuel mixed with diesel fuel for internal combustion engines operating at low temperatures. [...] Read more.
Issues related to the environmental safety of transport vehicles, the operation of which leads to environmental pollution, continue to be highly relevant. In this work, we consider the use of biofuel mixed with diesel fuel for internal combustion engines operating at low temperatures. This approach does not reduce the efficiency of transport, while also solving the issue of organic waste recycling. In this work, we address the possibility of reducing environmental pollution using carbon-neutral blended fuels based on esters of waste cooking oil (WCO), biobutanol, and diesel fuel for transport, tractor, and other equipment powered by a diesel internal combustion engine. In terms of the rate of biofuel implementation, Russia is still lagging behind the EU, China, and Japan, largely due to, inter alia, its climatic conditions with cold and long winters. The article also provides data on the possibility of using mixed biofuels under sub-zero temperatures. The process of forming a volumetric fuel supply through the common rail injector of the D4CB engine under changes in fuel pressure and drive pulse duration was also investigated, with the corresponding regression dependencies being presented. The losses of heat supplied into the cylinder when using a blend of diesel fuel and biodiesel (with 20 wt% butanol) in comparison with diesel fuel were analytically calculated. This made it possible to identify a function for adjusting fuel supply to compensate for power losses. The lubricity of fuel blends was assessed using the HFRR method. Full article
(This article belongs to the Section Ecology Science and Engineering)
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28 pages, 2602 KB  
Article
Comparative Life Cycle Assessment of Elastomeric Bitumen and Polymer Modified Bitumen Emulsion for Waterproofing Systems Based on Primary Data
by Jhony Raniery, Fábio de Oliveira Braga, Daiane Cecchin and Lucas Rosse Caldas
Sustainability 2026, 18(6), 2936; https://doi.org/10.3390/su18062936 - 17 Mar 2026
Viewed by 502
Abstract
Increasing attention to environmental performance in construction materials has intensified the need for robust Life Cycle Assessment (LCA) studies on bituminous waterproofing systems. This study addresses the lack of comparative LCAs based on primary data for hot-applied Elastomeric Modified Bitumen (EMB) and cold-applied [...] Read more.
Increasing attention to environmental performance in construction materials has intensified the need for robust Life Cycle Assessment (LCA) studies on bituminous waterproofing systems. This study addresses the lack of comparative LCAs based on primary data for hot-applied Elastomeric Modified Bitumen (EMB) and cold-applied Bitumen Emulsion (EMBE), two widely used materials with contrasting application methods and environmental profiles. While EMB has been moderately covered in the literature, this study contributes uniquely by providing one of the first LCAs based on primary data for EMBE, a formulation that is increasingly adopted in the construction sector but still underexplored in environmental assessments. The primary industrial data were combined with international LCI datasets (Ecoinvent) to model environmental impacts using SimaPro 9.4.0.3. Results show that EMBE demonstrates better climate performance (611 kg CO2 eq/t) but is more sensitive to specific additives, especially resins and plasticizers, which significantly increase Ozone Depletion Potential and photochemical ozone formation. The Environmental Product Declaration (EPD) survey analysis further highlights the influence of recycled content, cold mix technologies, and production energy sources on environmental performance. The findings indicate that the selection of waterproofing materials should consider not only technical performance but also the distribution of environmental impacts across the life cycle. Full article
(This article belongs to the Special Issue Life Cycle Assessment(LCA) of Sustainable Building Materials)
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18 pages, 1675 KB  
Article
Effect of a Recycling Agent on Binder and Mixture Performance of Cold Recycled Asphalt Mixes: A Dual-Scale Evaluation with Variability Assessment
by Sajjad Noura, Fahd Ben Salem and Alan Carter
Infrastructures 2026, 11(3), 97; https://doi.org/10.3390/infrastructures11030097 - 13 Mar 2026
Viewed by 490
Abstract
Cold recycled asphalt mixtures incorporate a high amount of reclaimed asphalt pavement (RAP), which offers more economic and environmental advantages than hot recycling techniques. Nevertheless, the presence of aged RAP binder frequently leads to reduced low-temperature performance and uncertainty in mechanical response. The [...] Read more.
Cold recycled asphalt mixtures incorporate a high amount of reclaimed asphalt pavement (RAP), which offers more economic and environmental advantages than hot recycling techniques. Nevertheless, the presence of aged RAP binder frequently leads to reduced low-temperature performance and uncertainty in mechanical response. The influence of slack wax on full-depth reclamation (FDR) mixtures with bitumen emulsion is assessed in this study using a dual-scale approach. The approach integrates both chemical and rheological binder-scale characterization with mixture-scale mechanical performance with variability assessment. At the binder scale, the binder beam rheometer (BBR), dynamic shear rheometer (DSR), and Fourier transform spectroscopy (FTIR) indicated that the addition of 10% recycling agent improved the low-temperature properties. The improvement at lower temperatures shifted the BBR temperature from −23 °C to −30 °C, which ultimately resulted in a less negative ΔTc, from −0.7 °C to −0.3 °C, and moderately improved high-temperature stiffness. Moreover, the FTIR analysis indicated a reduction in oxidation-related chemical markers, as evidenced by the reduced carbonyl and sulfoxide indices. At the mixture scale, complex modulus shows a systematic decrease in stiffness, particularly at lower temperatures of −25 °C and −15 °C, and a reduced phase angle, suggesting higher elastic dominance. The reduction is observed at all temperatures and frequencies. Rutting resistance of both formulations remains below 3% after 30,000 cycles. The complex modulus coefficient of variability was found to be 8–12%, comparable to that of hot mix asphalt. In conclusion, the findings suggest that the recycling agent provides a controlled restoration of viscoelastic properties in cold recycled mixtures without compromising structural integrity. This underscores the significance of multi-scale evaluation and variability assessment when characterizing high RAP recycling agents under the studied materials and dosage. Full article
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20 pages, 5943 KB  
Article
Characteristics of Waste Concrete Powder-Based Artificial Fine Aggregate and Its Application in Concrete
by Wei Xu, Liang Zhan, Yang Lei, Lei Xue, Yuguang Zhao, Jun Zhao and Qianyi Zhao
Materials 2026, 19(4), 690; https://doi.org/10.3390/ma19040690 - 11 Feb 2026
Viewed by 542
Abstract
Waste concrete powder (WCP), characterized by low reactivity and limited utilization potential, is rapidly accumulating due to the increasing volume of demolition and recycling activities, creating significant environmental and resource challenges. Meanwhile, the shortage of natural fine aggregate (NFA) has become increasingly severe. [...] Read more.
Waste concrete powder (WCP), characterized by low reactivity and limited utilization potential, is rapidly accumulating due to the increasing volume of demolition and recycling activities, creating significant environmental and resource challenges. Meanwhile, the shortage of natural fine aggregate (NFA) has become increasingly severe. To address these issues, this study develops a sustainable approach that utilizes WCP as the main raw material, together with fly ash (FA), ground granulated blast-furnace slag (GGBFS), ordinary Portland cement (OPC), and sulphoaluminate cement (SAC), to produce a WCP-based artificial fine aggregate (WAFA) through a cold-bonding process. The physical, mechanical, and microstructural properties of WAFA were systematically analyzed, and its concrete performance was evaluated by replacing NFA at 100% volume. The results show that WAFA exhibits a regular spherical morphology and, after grading adjustment, meets the Zone II sand requirements of GB/T 14684-2022. Increasing the cement content from 2% to 10% raises the 28-day single-particle compressive strength (SPCS) from 12.98 MPa to 23.08 MPa (a 77.8% increase), while enhancing WCP reactivity improves SPCS from 16.17 MPa to 22.80 MPa (a 29.1% increase). Higher cement content and WCP reactivity also promote the formation of C–S–H gel and ettringite (AFt), resulting in higher bulk density, reduced water absorption, and a denser microstructure. In concrete applications, WAFA substantially improves workability, with slump values exceeding those of NFA and recycled fine aggregate (RFA) concretes. Although WAFA concrete exhibits slightly lower compressive and splitting tensile strengths compared with NFA concrete, optimized mix design allows the achievement of target strength grades from C30 to C50, with the C50-W10-50 mixture showing the most favorable mechanical performance. In summary, WAFA shows potential for contributing to the high-value utilization of construction waste and the reduction in natural sand consumption. Full article
(This article belongs to the Section Construction and Building Materials)
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32 pages, 13039 KB  
Article
Freeze-Thaw Behavior and Damage Prediction of Mixed Recycled Coarse Aggregate Concrete
by Huaiqin Liu, Jiale Chen, Ping Zhang, Weina Li, Wei Su, Tian Su, Shangwei Gong and Bangxiang Li
Buildings 2026, 16(2), 368; https://doi.org/10.3390/buildings16020368 - 15 Jan 2026
Cited by 20 | Viewed by 1198
Abstract
To address the freeze-thaw (F-T) durability of concrete structures in severely cold plateau regions, this study investigates recycled coarse aggregate concrete (RCAC) by designing mixtures with varying replacement ratios of recycled brick aggregate (RBA). Rapid freeze-thaw cycling tests are conducted in combination with [...] Read more.
To address the freeze-thaw (F-T) durability of concrete structures in severely cold plateau regions, this study investigates recycled coarse aggregate concrete (RCAC) by designing mixtures with varying replacement ratios of recycled brick aggregate (RBA). Rapid freeze-thaw cycling tests are conducted in combination with macro- and microscale analytical techniques to systematically elucidate the frost resistance and damage mechanisms of mixed recycled coarse aggregate concrete. When the RBA content is 50%, the concrete demonstrates relatively better frost resistance within the mixed recycled aggregate system. This is evidenced by the lowest mass loss rate coupled with the highest retention ratios for both the relative dynamic elastic modulus (RDEM) and the compressive strength. Micro-analysis indicates that an appropriate amount of RBA can optimize the pore structure, exerting a “micro air-cushion” buffering effect. Blending RBA with recycled concrete aggregate (RCA) may create functional complementarity between pores and the skeleton, effectively delaying freeze–thaw damage. A GM (1,1) damage prediction model based on gray system theory is established, which demonstrates high accuracy (R2 > 0.92). This study provides a reliable theoretical basis and a predictive tool for the durability design and service life assessment of mixed recycled coarse aggregate concrete engineering in severely cold regions. Full article
(This article belongs to the Special Issue Low-Carbon Materials and Advanced Engineering Technologies)
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15 pages, 5732 KB  
Article
The Influence of Sand Ratio on the Freeze–Thaw Performance of Full Solid Waste Geopolymer Concrete
by Tong Qiu, Yuan Wen, Xinzhuo Yang, Jian Zhou, Xuan Gao and Xi Liu
Buildings 2026, 16(1), 76; https://doi.org/10.3390/buildings16010076 - 24 Dec 2025
Viewed by 428
Abstract
To clarify the effect of sand ratio on the freeze–thaw performance of full solid waste geopolymer concrete (FSWGC) and establish a constitutive model for its post-freeze–thaw mechanical behavior, FSWGC was prepared via alkali activation—using fly ash, slag, silica fume as cementitious materials, and [...] Read more.
To clarify the effect of sand ratio on the freeze–thaw performance of full solid waste geopolymer concrete (FSWGC) and establish a constitutive model for its post-freeze–thaw mechanical behavior, FSWGC was prepared via alkali activation—using fly ash, slag, silica fume as cementitious materials, and cold-bonded geopolymer lightweight aggregates (CBGLAs) and recycled sand as aggregates. With sand ratios (0.45, 0.55, 0.65) as the core variable, rapid freeze–thaw tests were conducted to measure mass loss, relative dynamic elastic modulus, mechanical properties, and axial compressive stress–strain characteristics of FSWGC. Results show that higher sand ratios significantly aggravate freeze–thaw damage: after 100 cycles, the 0.65 sand ratio specimen has a mass loss rate of 4.61% and a relative dynamic elastic modulus retaining only 34.4% of its initial value, with accelerated strength degradation. This is due to yjr weakened wrapping of recycled sand by cementitious materials, forming a weak interfacial transition zone. The modified Guo constitutive model for FSWGC, and the further established model considering freeze–thaw cycles, accurately describe the stress–strain curve of FSWGC before and after freeze–thaw. This study provides theoretical and experimental support for FSWGC mix optimization, durability design, and mechanical response calculation in cold regions. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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