Search Results (109)

Dissolved gas analysis (DGA) is an essential technique for the fault diagnosis and condition monitoring of oil-immersed power transformers. Among various characteristic gases, acetylene (C₂H₂) is a key indicator of high-energy discharge and arc faults. In this work, a high-sensitivity dissolved acetylene detection system is developed based on clamp-type quartz-enhanced photoacoustic spectroscopy (QEPAS). A specially designed clamp-type quartz tuning fork (Clamp-type QTF) is employed as the acoustic transducer to improve acoustic coupling efficiency and optical alignment tolerance. Compared with conventional standard quartz tuning forks, the clamp-type structure exhibits enlarged acoustic interaction volume, lower damping loss, and higher signal collection capability. A near-infrared distributed feedback (DFB) laser operating at 1531.6 nm is used as the excitation source. The dissolved gas is extracted from transformer oil using a headspace degassing module and introduced into the QEPAS cell for real-time measurement. Experimental results showed that the developed system achieves a 1σ-based SNR-estimated detection limit of 17 ppb at a 50 s integration time, derived from the continuous measurement of 0.75 ppm C₂H₂, with excellent linearity in the concentration range from 100 ppm to 500 ppm. The measured concentration of dissolved acetylene in transformer oil is in good agreement with gas chromatography (GC), validating the effectiveness and practical applicability of the proposed system. Full article

We report a deep learning-assisted quartz-enhanced photoacoustic spectroscopy (QEPAS) sensor for trace water vapor detection in air. A 1392 nm butterfly-packaged DFB laser is wavelength-modulated at f₀/2, and the QEPAS signal is retrieved by second-harmonic (2f) lock-in demodulation using a commercial quartz tuning fork gas cell. After optimizing the modulation depth to 400 mV, a 1D U-Net denoising network trained with pseudo-clean supervision is applied to the measured 2f traces, yielding an SNR improvement of 2.05× (3.11 dB). Allan deviation analysis indicates a minimum detection limit (MDL) of ~2.21 ppm at an optimum averaging time of ~619 s, corresponding to an ~2.1× improvement compared with the raw output. These results demonstrate that neural-network-based post-processing can improve QEPAS water vapor sensing performance without modifying the optical hardware. Full article

In the paper, a heterodyne quartz-enhanced photoacoustic spectroscopy (H-QEPAS)-based integrated methane (CH₄) sensor prototype is reported. The CH₄ absorption line located at 1650.96 nm was selected as the target spectral line. The design features an integrated, 3D-printed gas chamber for reduced size and weight. To realize the coordinated operation of each hardware component, a control program was designed based on LabVIEW platform, enabling the adjustment of various hardware parameters. The piezoelectric signal generated by the quartz tuning fork (QTF) was amplified via a trans-impedance amplifier (TIA), acquired by a data acquisition card (DAQ), and then transmitted to a virtual lock-in amplifier (LIA) on the PC terminal for processing. The dimensions of the integrated CH₄ sensor prototype are 33 cm in length, 27 cm in width, and 15 cm in height. The final test results demonstrate that the sensor prototype exhibits an excellent concentration linear response, with a detection limit of 26.72 ppm and a short detection time of approximately 4 s. Full article

A compact and high-sensitivity carbon monoxide (CO) detection system based on multi-pass cell enhanced light-induced thermoelastic spectroscopy (MPC-LITES) was developed for real-time monitoring. A 2.3 μm distributed feedback (DFB) diode laser targeting the CO absorption line at 4300.699 cm⁻¹ was employed, offering strong line intensity and minimal interference from H₂O, CO₂, NO₂, and SO₂. The optimal modulation depth of 0.76 cm⁻¹ produced the maximum second harmonic (2f) signal. Experimental results demonstrated excellent linearity (R² = 0.998) and a minimum detection limit of 230 ppb at 1 s, further reduced to 47 ppb at 367 s by Allan deviation analysis. Application tests were carried out for real-time monitoring of cigarette smoke in a 20 m² indoor environment. Under closed conditions, the CO concentration rapidly increased to approximately 165 ppm, while in ventilated conditions, it peaked at 45 ppm and decayed quickly due to air exchange. The results confirm that the proposed MPC-LITES sensor enables accurate, real-time detection of transient CO variations, demonstrating strong potential for indoor air quality evaluation, environmental safety, and public health protection. Full article

Remarkable advances in Quartz-Enhanced Photoacoustic Spectroscopy (QEPAS) made it one of the most effective gas-sensing techniques in terms of sensitivity and selectivity. Consequently, its range of possible applications is continuously expanding, but in some cases is still limited by the cost and/or size of the equipment needed to im-plement a complete QEPAS sensor. In particular, bulky and expensive lab instruments are often used to realize the electronic building blocks required by this technique, which prevents, for instance, integration of the system on board a drone. This work addresses this issue by presenting the development of compact electronic modules for a QEPAS sensor. A very low-noise, fully differential preamplifier for the quartz tuning fork, with digital output and programmable gain, has been designed and realized. A compact FPGA board hosts both an accurate function generation module, which synthesizes the signals needed to modulate the laser source, and an innovative lock-in amplifier based on the CORDIC algorithm. QEPAS sensors based on the designed electronics have been used for the detection of H₂O and CO₂ in ambient air, proving the full functionality of all the blocks. These results highlight the potential of compact electronics to promote portable and cost-effective QEPAS applications. Full article

This study designed and validated a dual-component beat-frequency quartz-enhanced photoacoustic spectroscopy (BF-QEPAS) gas detection system utilizing time-division multiplexing (TDM). By applying TDM to drive distributed feedback lasers, the system achieved the simultaneous detection of acetylene and methane. Its key innovation lies in exploiting the transient response of the quartz tuning fork (QTF) to acquire gas concentrations while concurrently capturing the QTF resonant frequency and quality factor in real-time. Owing to the short beat period and rapid system response, this approach significantly reduces time-delay constraints in time-division measurements, eliminating the need for periodic calibration inherent in conventional methods and preventing detection interruptions. The experimental results demonstrate minimum detection limits of 5.69 ppm for methane and 0.60 ppm for acetylene. Both gases exhibited excellent linear responses over the concentration range of 200 ppm to 4000 ppm, with the R² value for methane being 0.996 and for acetylene being 0.997. The system presents a viable solution for the real-time, calibration-free monitoring of dissolved gases in transformer oil. Full article

To enable the highly sensitive detection of acetylene (C₂H₂) dissolved in transformer oil, a high-power quartz-enhanced photoacoustic spectroscopy (QEPAS) sensing system is proposed. A standard 32.7 kHz quartz tuning fork (QTF) was employed as an acoustic transducer, coupled with an optimized acoustic resonator to enhance the acoustic signal. The laser power was boosted to 150 mW using a C-band erbium-doped fiber amplifier (EDFA), achieving a detection limit of 469 ppb for C₂H₂ with an integration time of 1 s. The headspace degassing method was utilized to extract dissolved gases from the transformer oil, and the equilibrium process for the release of dissolved C₂H₂ was successfully monitored using the developed high-power QEPAS system. This approach provides reliable technical support for the real-time monitoring of the operational safety of power transformers. Full article

This work demonstrates an ultra-compact optical gas-sensing system, consisting of a pigtailed laser diode emitting at 1392.5 nm for water vapor (H₂O) detection, a silicon nitride (Si₃N₄) optical waveguide to guide the laser light, and a custom-designed, low-frequency, and T-shaped Quartz Tuning Fork (QTF) as the sensitive element. The system employs both Quartz-Enhanced Photoacoustic Spectroscopy (QEPAS) and Light-Induced Thermoelastic Spectroscopy (LITES) techniques for trace gas sensing. A 3.8 mm-wide, S-shaped waveguide path was designed to prevent scattered laser light from directly illuminating the QTF. Both QEPAS and LITES demonstrated comparably low signal-to-noise ratios (SNRs), ranging from 1.6 to 3.2 for a 1.6% indoor H₂O concentration, primarily owing to the reduced optical power (~300 μW) delivered to the QTF excitation point. These results demonstrate the feasibility of integrating photonic devices and piezoelectric components into portable gas-sensing systems for challenging environments. Full article

Quartz crystal out-of-plane vibration units are critical components of QMEMS devices. However, the fabrication of their 3D sidewall electrode structures presents significant challenges, particularly within ultrafine etched grooves. These challenges seriously limit further miniaturization, which is critical for portable and wearable electronic applications. In this paper, we propose a novel 3D self-masking fabrication strategy that enables the precise formation of sidewall electrodes by using the etched beam structure as a self-aligned pattern transfer medium. Based solely on photolithography and wet etching processes, this approach overcomes the limitations of the conventional shadow mask technique by improving alignment accuracy, process efficiency, and fabrication yields. In addition, a predictive mathematical model was developed to guide process optimization, enabling adaptive and reliable fabrication. Sidewall electrodes were successfully achieved in etched grooves as narrow as 45 μm, closely matching the theoretical predictions. To validate the approach, an ultra-miniaturized out-of-plane vibration unit with a beam spacing of just 150 μm—the narrowest reported to date—was fabricated, representing an 80% reduction compared to previously documented structures. The unit exhibited a repeatability error below 1.13%, confirming the precision and reliability of the proposed fabrication strategy. Full article

In this paper, an all-fiber light-induced thermoelastic spectroscopy (LITES) sensor based on hollow-core anti-resonant fiber (HC-ARF) and self-designed low-frequency quartz tuning fork (QTF) is reported for the first time. By utilizing HC-ARF as both the transmission medium and gas chamber, the laser tail fiber was spatially coupled with the HC-ARF, and the end of the HC-ARF was directly guided onto the QTF surface, resulting in an all-fiber structure. This design eliminated the need for lens combinations, thereby enhancing system stability and reducing cost and size. Additionally, a self-designed rectangular-tip QTF with a low resonant frequency of 8.69 kHz was employed to improve the sensor’s detection performance. Acetylene (C₂H₂), with an absorption line at 6534.37 cm⁻¹ (1.53 μm), was chosen as the target gas. Experimental results clearly demonstrated that the detection performance of the rectangular-tip QTF system was 2.9-fold higher than that of a standard commercial QTF system. Moreover, it exhibited an outstanding linear response to varying C₂H₂ concentrations, indicating its high sensitivity and reliability in detecting C₂H₂. The Allan deviation analysis was used to assess the system’s stability, and the results indicated that the system exhibits excellent long-term stability. Full article

A carbon dioxide (CO₂) sensor based on light-induced thermoelastic spectroscopy (LITES) using a 2 μm diode laser and a self-designed low-frequency trapezoidal-head QTF is reported for the first time in this invited paper. The self-designed trapezoidal-head QTF with a low resonant frequency of 9464.18 Hz and a high quality factor (Q) of 12,133.56 can significantly increase the accumulation time and signal level of the CO₂-LITES sensor. A continuous-wave (CW) distributed-feedback (DFB) diode laser is used as the light source, and the strongest absorption line of CO₂ located at 2004.01 nm is chosen. A comparison between the standard commercial QTF with the resonant frequency of 32.768 kHz and the self-designed trapezoidal-head QTF is performed. The experimental results show that the CO₂-LITES sensor with the self-designed trapezoidal-head QTF has an excellent linear response to CO₂ concentration, and its minimum detection limit (MDL) can reach 46.08 ppm (parts per million). When the average time is increased to 100 s based on the Allan variance analysis, the MDL of the sensor can be improved to 3.59 ppm. Compared with the 16.85 ppm of the CO₂-LITES sensor with the commercial QTF, the performance is improved by 4.7 times, demonstrating the superiority of the self-designed trapezoidal-head QTF. Full article

This study compares the performance of a quartz tuning fork (QTF) with a highly sensitive ultrasound microphone in the context of acoustic measurements, applying the substitution calibration method. QTF sensors are increasingly used for high-precision tasks due to their sensitivity and stability, while microphones are still the standard in general acoustic measurements. The aim of this study is to evaluate both technologies across several key performance metrics, including linearity of response, sensitivity, noise characteristics, and acoustic detection limit. Which sensor is better suited to which acoustic and physical condition? The results show that QTFs perform exceptionally well in applications requiring high precision, especially in high-frequency and narrow-band measurements. The signal-to-noise-ratio (SNR) of the QTF at its resonance frequency is 14 dB higher than that of the microphone, whereas the detection limit and linearity are comparable. The findings suggest that QTF sensors are particularly advantageous for specialized applications like photoacoustic spectroscopy (PAS). Full article

Quartz-enhanced photoacoustic spectroscopy (QEPAS) has shown great promise for monitoring greenhouse gases and pollutants with a high measurement accuracy and limit of detection. A QEPAS sensor, which can achieve high photoacoustic signal gain without requiring the laser beam to pass through the two prongs of a quartz tuning fork (QTF), is reported. A custom QTF with a resonant frequency of 7.2 kHz and a quality factor of 8406 was employed as a sound detection element, and the parameters of the acoustic micro-resonator (AmR) in the off-beam QEPAS spectrophone were optimized. A signal-to-noise ratio (SNR) gain of 16 was achieved based on the optimal AmR dimensions compared to the bare custom QTF. Water vapor (H₂O) was detected utilizing the QEPAS sensor equipped with the off-beam spectrophone, achieving a minimum detection limit (MDL) of 4 ppm with a normalized noise equivalent absorption coefficient (NNEA) of 5.7 × 10⁻⁸ cm⁻¹·W·Hz^−1/2 at an integration time of 300 ms. Full article

A highly sensitive light-induced thermoelastic spectroscopy (LITES) sensor employing a charge amplifier (CA) is reported for the first time in this invited paper. CA has the merits of high input impedance and strong anti-interference ability. The usually used transimpedance amplifier (TA) and voltage amplifier (VA) were also studied under the same conditions for comparison. A standard commercial quartz tuning fork (QTF) with a resonant frequency of approximately 32.76 kHz was used as the photothermal signal transducer. Methane (CH₄) was used as the target gas in these sensors for performance verification. Compared to the TA-LITES sensor and VA-LITES sensor, the reported CA-LITES sensor shows improvements of 1.83 times and 5.28 times in the minimum detection limit (MDL), respectively. When compared to the LITES sensor without an amplifier (WA-LITES), the MDL has a 19.96-fold improvement. After further optimizing the gain of the CA, the MDL of the CA-LITES sensor was calculated as 2.42 ppm, which further improved the performance of the MDL by 30.3 times compared to the WA-LITES. Additionally, long-term stability is analyzed using Allan deviation analysis. When the average time of the sensor system is increased to 50 s, the MDL of the CA-LITES sensor system can be improved to 0.58 ppm. Full article

In this paper, a highly sensitive methane (CH₄) sensor based on light-induced thermoelastic spectroscopy (LITES) and a T-shaped quartz tuning fork (QTF) with hydrogen (H₂) and helium (He) enhancement techniques are reported for the first time. The low resonant frequency self-designed T-shaped QTF was exploited for improving the energy accumulation time. H₂ and He were utilized as surrounding gases for the T-shaped QTF to minimize energy loss, thereby enhancing the sensitivity of the LITES sensor. Additionally, a fiber-coupled multi-pass cell (FC-MPC) with a 40 m optical length was utilized to improve the optical absorption of CH₄. The frequency response of the T-shaped QTF with different concentrations of H₂ and He was investigated, and the Q factor in the H₂ and He environment increased significantly. Compared to operating QTF in a nitrogen (N₂) environment, the signal amplitude was enhanced by 2.9 times and 1.9 times in pure H₂ and He environments, respectively. This enhancement corresponded to a minimum detection limit (MDL) of 80.3 ppb and 113.6 ppb. Under different CH₄ concentrations, the T-shaped QTF-based H₂-enhanced CH₄-LITES sensor showed an excellent linear response. Furthermore, through Allan deviation analysis, the MDL of the T-shaped QTF-based H₂-enhanced CH₄-LITES can reach 38 ppb with an 800 s integration time. Full article