Search Results (385)

Background: Oil-in-water nanoemulsions (NEs) represent versatile platforms for the delivery of hydrophobic compounds and find a wide range of applications in different fields such as food, cosmetics, agriculture, pharmaceutics, and oil and gas industries. Various methodologies can be applied for the preparation of NEs as low-energy and high-energy methods. Among them, high-energy ultrasonication (HEU) is a popular technique in research laboratories or small manufacturing facilities. However, a clear gap remains in understanding how, and to what extent, experimental parameters and the chemical and physical characteristics of the components affect the formation and properties of NEs through HEU. Methods: In this work, a comprehensive screening of factors (oil viscosity and density, surfactant type, processing parameters, and formulation composition) affecting NEs formation and quality was performed and an artificial neural network (ANN) was applied to determine the relative relevance of each parameter. Results: Oil viscosity revealed to be the primary factor affecting droplet size (Z_avg) and polydispersity index (PDI), with high-viscosity oils leading to poor emulsification into nanosized droplets. Higher processing temperatures improved NE formation by reducing viscosity during sonication. Ultrasound amplitude and pulse mode influenced NE characteristics, particularly under challenging conditions. Surfactant type and oil content had, instead, minor effects on the NEs’ features. ANN modelling accurately predicted NEs’ properties and identified critical viscosity limits for successful nanosized emulsification (Z_avg < 300 nm and PDI < 0.4). Conclusions: These findings provide a predictive basis for rational NE design under HEU, serving as a guide for researchers working in different fields. Full article

Laser-induced acoustic communication is a highly adaptable cross-medium technique that combines the advantages of optical transmission through air and acoustic transmission underwater. However, poor signal stability at high repetition frequencies currently hinders its widespread application. To address this, this paper proposes an innovative scanning focal-point method to enhance stability. Traditional methods such as beam scanning, focus control, and distributed interaction are primarily aimed at enhancing sound pressure in a specific direction, achieving near-field/far-field focusing, or improving the signal-to-noise ratio through coherent synthesis of ultrasonic intensity. In contrast, the method proposed in this paper is intended to avoid the interference of droplets and vapor generated by single-point breakdown under high repetition frequencies, which would otherwise degrade the laser-acoustic conversion efficiency. It is therefore an active defense strategy specifically targeting the stability of laser-induced acoustic communication. First, optical simulation software was used to analyze the effects of surface ripples and bubbles on focal spot displacement and size. Next, a single-pulse experimental system was developed to measure the range and duration of surface depressions caused by optical breakdown. Finally, a scanning focal-point system was constructed for comparative experiments, with results recorded via hydrophones and high-speed cameras. The maximum laser-induced acoustic signal generated by the scanning focal-point method is 7.4 times that produced by single-point breakdown. The experimental results demonstrate that the scanning focal-point method can effectively avoid the influence of water surface disturbance and steam on the optoacoustic conversion efficiency and significantly improve the amplitude and stability of the laser-induced acoustic signal. Full article

The increasing generation of waste toner from printers and photocopiers presents significant environmental and disposal challenges. This study investigates the feasibility of utilizing waste toner as a modifier in asphalt binder to enhance performance and sustainability. Bitumen with a penetration grade of 60/70 was modified with waste toner at varying contents (0–30%). The modified binders were evaluated using penetration, ductility, and softening-point tests to assess their physical behavior. Results indicate that increasing toner content reduces penetration and ductility while improving the softening point, indicating enhanced temperature resistance. Furthermore, asphalt mixtures were evaluated using both destructive (Marshall stability) and non-destructive testing (ultrasonic pulse velocity) methods to provide a comprehensive performance assessment. In addition, an artificial neural network (ANN) model was developed to predict and evaluate the performance of toner-modified mixtures. The findings demonstrate that waste toner can be effectively used as a sustainable modifier in asphalt mixtures, thereby improving material performance and reducing environmental impact. Full article

Chloride and sulfate ion attacks are among the leading causes of deterioration in reinforced concrete structures, leading to the corrosion of steel reinforcement, expansion, cracking, and premature structural failure. Early detection of these ion-induced deteriorations is essential not only for maintaining safety but also for supporting sustainability objectives by extending service life, reducing material consumption, and minimizing carbon-intensive repairs. This review synthesizes current advances in non-destructive testing (NDT) techniques used to identify and quantify the impacts of chloride and sulfate ions in reinforced concrete. The mechanisms of ion ingress and their associated degradation processes are examined together with the operating principles, strengths, and limitations of key NDT methods, including electrical resistivity, acoustic emission, infrared thermography, ground penetrating radar, and ultrasonic pulse velocity. By enabling timely maintenance decisions and reducing unnecessary demolition or intrusive testing, these NDT methods contribute directly to sustainable infrastructure management. Through comparative analysis and real-world case studies, the paper highlights the most effective NDT applications for deterioration scenarios and outlines emerging innovations that enhance accuracy, data interpretation, and long-term monitoring capabilities. The findings demonstrate how advancements in NDT support the development and preservation of durable and sustainable concrete structures. Full article

This study explores non-destructive techniques for characterizing the mechanical properties of materials pertinent to cultural heritage, emphasizing the preservation of sample integrity. A modified acoustic resonance method (MARM), utilizing a two-microphone configuration, is introduced for the simultaneous, fully non-contact determination of dynamic elastic modulus and damping (loss factor). The method is validated through comparison with the impulse excitation technique (IET) and ultrasonic pulse velocity testing (UT). The approach is applied to two material categories exhibiting contrasting porosities: dense natural stone and highly porous unfired clay. Results demonstrate strong concordance among all methods for stone, confirming the reliability of non-destructive techniques for homogeneous materials. Conversely, unfired clay displays greater variability attributable to its heterogeneous and porous nature, alongside increased damping. This investigation reveals that conventional modulus–strength correlations are not directly applicable to unfired clay. To address this, a simplified strength estimation model incorporating the estimated elastic modulus and porosity is proposed. The model achieves improved alignment with experimental data and delineates applicability boundaries for porous materials. The presented framework facilitates consistent, non-destructive evaluation of mechanical properties, with notable implications for the assessment and preservation of cultural heritage materials. Full article

The accuracy of transit-time ultrasonic flow measurement depends strongly on stable time-of-flight (TOF) extraction. However, threshold-based TOF methods are susceptible to emission transients, structural ringing, and repeated threshold crossings, which may cause false triggering and timing fluctuations. This paper proposes a time-of-flight extraction method based on time-sequenced pulses for ultrasonic flow measurement using an FPGA-based time-to-digital converter (TDC). The method equalizes signal input paths, combines peripheral path switching with FPGA gating to achieve windowed valid-edge extraction, and exploits the temporal correspondence among consecutive excitation pulses to construct multiple TOF observations from matched pulse pairs, thereby improving extraction stability and timing efficiency. A complete FPGA-TDC ultrasonic flow measurement platform based on a Zynq UltraScale+ device was developed, and TDC linearity, timing precision, and flow calibration experiments were conducted. After code-density calibration, the four channels achieved RMS values of about 20 ps, and within a flow range of 0.7–3.6 m³/h, the relative error with respect to the reference flowmeter remained within ±0.6%, with repeatability errors below 0.3%. The platform operated stably under the present experimental conditions. These results demonstrate improved TOF extraction stability and overall flow measurement performance without complex full-waveform processing. Full article

Mechanical locks have not been fully replaced by electrical locks and are still being researched and improved, along with advanced electronic methods of attack. Moreover, reading pin lengths by detecting their natural frequencies (lock decoding) to forge copies of a legitimate key can be done quickly using active or passive ultrasonic detectors. One possible method of defence against them is manufacturing lock pins using functionally graded materials (FGMs). A pin’s natural frequency (in the range 100 kHz–1 MHz) and hence its ultrasonic pulse transit/reflection time can be correlated to its length if it is made of a homogeneous material. The idea is to design pins made of functionally graded alloys to achieve equal natural frequencies, but also desired positions of standing wave nodes regardless of pin length. To calculate the composition of the FGM alloy, we must first develop mathematical models of a pin’s vibrations. Two simple and fast mathematical models are first derived from the finite-element model (FEM) of a pin. These models are used in an optimization procedure based on the Nelder–Mead simplex method to calculate optimal profiles of Young’s modulus and density along a pin’s longitudinal axis. A successful optimization procedure for 10 key pin lengths is performed to make a pin-tumbler lock resistant to ultrasonic attacks. Full article

The conventional microstepping driving method suffers from significant periodic speed oscillations under ultra-low-speed conditions, which fail to meet the stringent demand for smooth operation of ultrasonic motors in semiconductor packaging. Most existing theories and simulations of ultrasonic motors adopt a macroscopic mechanical perspective; after extensive linearization and idealization, they can only provide preliminary mechanism analysis and fail to achieve precise quantitative computation. Moreover, they neglect critical factors such as the microstructure of contact surfaces, preload distribution, and vibration mode transmission, making it difficult to reflect the true characteristics of the motor—including strong nonlinearity, multiphysics coupling, and complex interface behavior—resulting in considerable discrepancies between theory and experiment. In this paper, a macro-micro multi-scale finite element model of a traveling-wave ultrasonic motor is established using ADINA and HyperMesh, fully accounting for the strong nonlinearity and multiphysics coupling effects. Based on the ultrasonic friction reduction theory and the beat traveling wave mechanism, the stator deformation, interface zoning characteristics, and torque output of the superimposed pulse driving method and the microstepping driving method are systematically compared. The simulated stator mode shapes are validated by laser scanning vibrometry experiments, and multiple speed tests ranging from 200 to 320 arcsec/s are conducted. Simulation results show that at a target speed of 900 arcsec/s, the superimposed pulse driving method reduces the speed fluctuation rate from 228% to 32%. Experimental results confirm that the speed fluctuation rate of the superimposed pulse driving method is consistently much lower than that of the microstepping driving method across the entire tested speed range. This study reveals the low-speed smooth operation mechanism of the superimposed pulse driving method, characterized by single-peak dominance and smooth alternation between the driving and braking zones, thereby fundamentally overcoming the inherent shortcomings of the traditional microstepping driving method. The proposed model can effectively replace costly direct interface measurements, providing a new method and reference for ultra-low-speed precision control of ultrasonic motors and for investigating the driving mechanisms of similar motors. Full article

Composite hydrogen storage vessels exhibit pronounced anisotropy, multilayered winding architectures, and strong ultrasonic attenuation, which severely degrade the focusing accuracy and defect visibility of the conventional isotropic total focusing method (TFM). To address these challenges, this study proposes an enhanced TFM framework for defect inspection in composite hydrogen storage vessels by integrating anisotropic delay correction, Gray-code coded excitation, and coherence-weighted reconstruction. First, an anisotropic propagation delay model is established using forward ray tracing to compensate for beam deviation and focusing mismatch induced by the anisotropic winding structure. Then, Gray-code excitation and pulse compression are introduced to improve signal energy and echo detectability under high-attenuation conditions. Finally, coherence-weighted imaging is applied to suppress incoherent background noise and structural artifacts, thereby enhancing defect contrast and image readability. The proposed method is validated on hydrogen storage vessel specimens containing artificial defects, with CT results used as references. Experimental results show that, compared with conventional isotropic TFM, the proposed collaborative approach significantly improves defect imaging quality for defects of different sizes and depths. The signal-to-noise ratio is increased from 7.2, 12.8, 14.8, and 7.4 dB for isotropic TFM to 32.5, 29.9, 52.6, and 42.7 dB, respectively, for the combined anisotropic, coded-excitation, and coherence-weighted TFM. In addition, the defect depth estimation remains stable and agrees well with the CT references, yielding approximately 9.0–9.6 mm for shallow defects and 18.7–19.3 mm for deeper defects. These results demonstrate that the proposed method can effectively improve defect detectability, image contrast, and depth characterization for embedded delamination-like artificial defects in composite hydrogen storage vessels, providing a promising ultrasonic imaging strategy for thick-walled anisotropic composite pressure structures. Full article

The urgent global need for sustainable infrastructure drives the demand for high-value buildings and waste removal. This paper studies the feasibility of using recycled foam concrete aggregate (FCA) as a substitute for natural coarse aggregate (NCA) in concrete and studies its impact on rheology, mechanical degradation, shear resistance, and the full-range replacement ratio (0–100). The experimental results show that the monotonic change in the workability of fresh concrete determines the lubrication threshold at 60% replacement, which is driven by the volume proportion effect. Beyond this value, capillary suction dominates, and the viscosity rises rapidly. From a mechanical perspective, the porous structure of FCA is conducive to “internal curing” so that moisture is released from the drying interface, but it also becomes a source of defects that change the fault topology. Specifically, the critical transition of the shear failure mode shifts from the debonding of the interface to the crushing of the cross-particle aggregate. At this time, the shear capacity decreases substantially, experiencing a reduction of 71.8% when completely replaced. There is a strong correlation between ultrasonic pulse velocity (UPV), rebound number, and compressive strength, and a multivariate nonlinear regression model (R² > 0.85) with non-destructive strength prediction is ultimately obtained. Based on the balance between mechanical capacity and resource cyclability, an optimal alternative zone of 20% to 40% is proposed. This work not only provides a mechanism for multi-scale coupling between pore structure and structural properties but also provides a data-driven method for the safety assessment of lightweight recycled aggregate concrete (RAC). Full article

Ensuring the durability and safety of modern infrastructure critically depends on the quality and strength of concrete. The Ultrasonic Pulse Velocity (UPV) method is a widely used non-destructive testing technique for evaluating concrete properties; however, factors such as aggregate size distribution, compaction methods, and surface quality can significantly influence UPV results and their correlation with compressive strength. This study investigates the effects of different aggregate sizes and an innovative vibration-assisted compaction method—developed using piezoelectric (PZT) transducers—on the mechanical, ultrasonic, and surface properties of concrete. Four distinct aggregate size distributions were employed to produce sixteen concrete specimens with constant mix proportions. Unlike conventional low-frequency, high-power vibration practices, a high-frequency (40 kHz), low-power (120 W) vibration protocol was applied through PZT elements placed within the molds to enhance compaction and reduce entrapped air. Experimental results indicated that the heaviest specimen (7.13 kg) was the medium-aggregate sample compacted using tamping and rodding methods. The highest UPV value (4143 m/s) was obtained from the coarse-aggregate specimen subjected to three minutes of vibration. In contrast, the best compressive strength performance (22.73 MPa) was observed in the medium-aggregate specimen without any vibration treatment. The findings revealed that both aggregate size and advanced vibration techniques have significant effects on the mechanical properties, ultrasonic response, and surface quality of concrete. In addition, a proof-of-concept portable surface-finishing prototype consisting of a steel plate instrumented with multiple PZT transducers was developed, and preliminary trials qualitatively suggested improved surface leveling when applied in contact with the concrete surface. Surface roughness was quantified via image processing (Light Map 150 and Specular Map 150). The rough-area fraction decreased from ~29.8% in the untreated specimen to ~4.3% after ultrasonic application, indicating a marked improvement in surface leveling and overall surface quality. The results indicate that the applied PZT vibration protocol did not improve compressive strength; in several cases, particularly under prolonged excitation, a reduction in strength was observed. In contrast, a significant improvement in surface quality was achieved, with the rough-area fraction decreasing from approximately 29.8% to 4.3%. However, due to the limited number of specimens, the findings should be interpreted as preliminary. Overall, the method appears more promising as a surface enhancement technique rather than a direct alternative to conventional compaction methods. Full article

Cotton, a globally significant crop grown in over 100 countries, sustains a $40 billion market and provides employment for over 350 million people worldwide. However, plastic contamination remains a persistent challenge within the industry, degrading cotton fiber quality and disrupting ginning. Manual inspection and optical machine-vision systems struggle when plastic fragments are concealed by fibers or lack sufficient color contrast. To address these challenges, we developed an ultrasonic phased-array imaging system operating at 40 kHz under field-programmable gate array (FPGA) control. Transmitter elements emit pulsed ultrasound along radial paths, separate reflection receivers record echo amplitudes to form acoustic images, and a set of transmission receivers captures signal attenuation, which is overlaid onto the reflection-based image to highlight potential contaminants. In preliminary laboratory-based tests on both seed cotton and lint samples, the system successfully detected visually obscured plastic fragments as small as $2\mathrm{cm}\times 2\mathrm{cm}$ with an angular resolution limit of $\pm 3°$. Distinct reflection peaks and corresponding attenuation overlays were produced across the field of view, validating the system’s detection capabilities. These results demonstrate the feasibility of using ultrasonic imaging to reveal concealed plastics in cotton processing. Integrating this approach with existing optical methods could enhance contaminant-removal workflows and improve overall fiber quality and processing efficiency. Full article

Reinforced cement concrete (RCC) water tanks are essential for water storage and distribution facilities in every region. The durability and structural integrity of RCC water tanks are crucial to maintaining an uninterrupted water supply to the surrounding areas. This study evaluates the structural integrity and functionality of a water tank in Karaikal, a coastal region in the Union Territory of Puducherry, India, subject to severe exposure conditions characterized by high humidity and temperature variability. An RCC water tank with a capacity of 10 lakh L in Thirunallar, Karaikal, is considered in this study. The methodology for the condition assessment includes visual inspection, non-destructive testing (NDT), and structural analysis in STAAD PRO software. NDT, including the Schmidt rebound hammer test and ultrasonic pulse velocity (UPV) test, was employed to evaluate the indicative compressive strength and in situ quality of an RCC water tank. The structure was modelled using structural drawings obtained from the Public Works Department, Karaikal. The NDT testing findings were incorporated into the model, and the structure was analyzed. Finally, the induced stress from the STAAD Pro model was compared with the in situ concrete compressive strength to assess the tank’s structural safety. The rebound hammer test results indicate that the in situ compressive strength of the tank’s beams and columns ranges from 12 MPa to 43 MPa, and the STAAD Pro analysis shows induced stresses ranging from 2.42 to 10.59 MPa. The comparison shows that the structure has higher safety margins. Hence, the deterioration observed during the visual inspection was not due to a deficiency in structural strength but rather to durability issues caused by environmental distress. Finally, suitable repair and rehabilitation methods were recommended to mitigate the deterioration based upon NDT measurements and the outputs of the structural analysis. Full article

Conventional admixture-based self-healing technologies are often limited by inadequate internal water supply and a scarcity of unhydrated gel particles. Therefore, this study proposes a new self-healing method that leverages the synergistic interplay between the chemical repair of sodium silicate and the physical clogging of superabsorbent polymers (SAPs) to overcome the aforementioned limitations. The healing efficiency of cement mortar was assessed through compressive strength recovery, capillary water absorption, and ultrasonic pulse velocity (UPV). Microstructural evolution and healing mechanisms were elucidated using scanning electron microscopy (SEM) and X-ray diffraction (XRD). Results indicate that at an optimal dosage (0.5 wt.% for both admixtures), the healing performance is significantly enhanced: the compressive strength recovery rate reaches 103.1%, the capillary water absorption coefficient decreases by 16.57 × 10⁻³, and the UPV recovery achieves 95.4%. Microstructural analysis reveals that sodium silicate facilitates the reaction between ${\mathrm{Ca}}^{2+}$ and ${\mathrm{S}\mathrm{i}\mathrm{O}}_3^{2-}$ ions, leading to the in situ precipitation of dense C-S-H gel at the crack interface, thereby enabling chemical repair. In contrast, SAP contributes to physical sealing via a swelling and release mechanism. Full article

The early detection and monitoring of stress-induced damage in concrete is a key goal for nondestructive evaluation and structural health monitoring of civil structures. Both linear and nonlinear ultrasonic testing methods have been developed for this purpose. The Ultrasonic Pulse Velocity (UPV) test is the standard linear technique and is reliable and easy to use, but it typically detects defects only after micro-cracks coalesce or grow beyond a threshold size. To enable earlier detection, features extracted from the nonlinear ultrasonic response—especially harmonics generation—have been proposed. However, these approaches often require complex measurement protocols, and their signal-to-noise ratio (SNR) can be limited. In this study, we leverage an exponential swept-sine pulse-compression (ESS–PuC) procedure to characterize both linear and nonlinear responses from a single measurement. We define and extract several features from both responses, and use them to monitor micro-crack initiation and growth in concrete specimens under gradually increasing compressive load. This enables a qualitative comparison of their characteristics and performance in detecting crack formation. Full article