Search Results (170)

Peeling behavior of soft materials is important in a wide range of applications, e.g., electronics, healthcare, etc. When applied on soft substrates, soft adhesives demonstrate unique mechanical behaviors compared to adhesives applied on rigid substrates. Adhesive properties can be conveniently measured by “peel testing”. The focus of this work is characterization of commercial glues on fabric substrates using commonly used peel tests. We investigate energy dissipation on textile substrates. For practical applications, we aim to develop a systematic approach for selecting adhesives for soft, flexible substrates. Here, we developed a multi-criteria framework for evaluating adhesives using data from peel tests. The criteria used here consider the shape and stability of the T-peel trace. The results of the multi-criteria evaluation were compared to traditionally used peel strength and fracture energy. Although E6000 produced the highest peel force ($1.82\pm 0.27 \mathrm{N} \mathrm{m}{\mathrm{m}}^{-1}$) and the largest apparent fracture energy, ${\mathrm{G}}_{\mathrm{c}}$ ($8673\pm 1545 \mathrm{J} {\mathrm{m}}^{-2}$), it showed large force oscillation ($\mathrm{S}\mathrm{S}\mathrm{A}=4.05\pm 0.83 \mathrm{N}$). Fabri-Fuse was selected based on its low oscillation ($\mathrm{S}\mathrm{S}\mathrm{A}=0.69\pm 0.29 \mathrm{N}$), lowest $\mathrm{C}\mathrm{o}{\mathrm{V}}_{{\mathrm{F}}_{\mathrm{c}\mathrm{i}}}$(4.0%), high peel stability index (PSI), and high displacement at break. Functional evaluation showed that Fabri-Fuse increased strain-to-electrical-failure to $34.95\pm 2.43\mathrm{\%},$ higher than direct printing on fabric or printing on E6000 (highest peel strength). These results suggest that metrics that consider the shape of the peel trace and inter-sample repeatability provide a useful alternative for selecting adhesives other than highest peel strength. Full article

Engineered bamboo composites (EBCs) are increasingly considered as sustainable alternatives to tropical hardwoods in structural applications. In jacking systems, performance is primarily governed by compression perpendicular-to-grain (bearing), although improper use may introduce flexural demands. This study evaluates the bearing and flexural behavior of Dragonwood, a commercial parallel strand bamboo (PSB), in comparison to Ekki (Lophira alata) through 120 full-scale tests. Dragonwood exhibited higher mean bearing capacity than Ekki, with yield stresses exceeding those of Ekki by over 60%, indicating strong potential for bearing-dominated applications such as in jacking. However, face-bonded specimens showed sensitivity to glue-line orientation, resulting in flexural strength reductions of up to 42% and undesirable shear failures. Increasing adhesive content and pressing pressure in the manufacturing process did not eliminate this behavior. Single-lift specimens removed the glue-line and showed improved failure behavior in flexure, although with reduced strength. The results demonstrate that manufacturing strategy heavily influences PSB performance. While single-lift Dragonwood products show the most potential, further testing under bearing is required before its suitability for jacking applications can be fully established. Full article

Waste plastics have attracted widespread attention in asphalt modification because of their environmental and economic benefits. However, the incorporation of waste plastics may weaken asphalt–aggregate interfacial adhesion, thereby increasing the risk of moisture damage in asphalt pavements. Although liquid anti-stripping agents have been widely used in conventional asphalt systems, their effectiveness and performance evolution in waste plastic-modified asphalt (WPA) remain insufficiently understood. To address this gap, this study systematically investigated the effects of two liquid anti-stripping agents, AJ-1 and AMR-II, on the adhesion, rheological properties, and aging behavior of WPA. Specifically, asphalt–aggregate adhesion was evaluated using water-boiling and binder bond strength tests, rheological properties were characterized by dynamic shear rheometer and bending beam rheometer tests, and aging behavior was analyzed through rolling thin-film oven test, pressurized aging vessel, and Fourier transform infrared spectroscopy. The results show that waste plastics reduce the adhesion performance at the asphalt-aggregate interface, whereas anti-stripping agents compensate for this loss. Compared with AJ-1, AMR-II showed stronger adhesion enhancement, increasing the asphalt residual coating ratio by approximately 1.5%–3.5% and the pull-off tensile strength by 17.4%–28.1%, while the corresponding improvements for AJ-1 were approximately 1.3%–2.7% and 13.0%–25.0%, respectively. As the dosage of both anti-stripping agents increased, the penetration index decreased, the temperature susceptibility increased, the softening point generally decreased, and the ductility increased markedly. Temperature sweep results show that both AJ-1 and AMR-II reduce the high-temperature performance of WPA. According to the bending beam rheometer results, AMR-II also enhances the low-temperature performance of WPA. Aging test results indicate that both anti-stripping agents increase the aging sensitivity of WPA to some extent, but the adverse effect of AMR-II on aging resistance is smaller than that of AJ-1, and AMR-II better preserves the low-temperature ductility and adhesion performance after aging. Overall, this study provides a binder scale evaluation showing that 0.4% AMR-II may offer a more balanced strategy for improving the adhesion and service performance of WPA. Full article

Adhesives and sealants are critical yet still underrepresented components in packaging science. Existing reviews mainly address specific chemistries, sealing technologies, or application niches, whereas integrated analyses of adhesive and sealant families within a unified packaging-system framework remain limited. This review addresses this gap by proposing a three-dimensional classification framework—functional role, material chemistry and activation mechanism, and performance constraints—that connects functional roles, processing routes, regulatory constraints, and circularity requirements. The framework is applied across natural, synthetic, hot-melt, pressure-sensitive, and tie-layer adhesives, as well as conventional thermoplastic, barrier-oriented, and biodegradable sealant systems. Special attention is given to hybrid systems operating at the boundary between bonding and sealing, and to the performance–recyclability trade-offs that arise in multilayer architectures. Structure–property–function relationships are analysed qualitatively with respect to bond and seal strength, seal initiation temperature, hot-tack behaviour, and end-of-life compatibility. Part I establishes the classification and functional groundwork for the two-part review; Part II will extend the analysis to quantitative performance data, advanced materials, and emerging technologies. Full article

Silicone pressure-sensitive adhesives are a prominent group of adhesive materials used in many contemporary industrial sectors. This is due to their high resistance to difficult operating conditions, especially high temperatures. They are used, among other areas, in the automotive industry or in power engineering, as fastening or insulation systems operating at high temperatures. Previous studies have demonstrated the beneficial effect of mineral fillers on further increases in thermal resistance and dimensional stability of silicone pressure-sensitive adhesives. This paper presents the results of research on the effect of adding rose quartz as a filler to silicone pressure-sensitive adhesives based on polydimethylsiloxanes, on the adhesion parameters of the obtained adhesives and their thermal resistance and dimensional stability at elevated temperatures. The self-adhesive tapes obtained showed increased resistance and thermal stability while maintaining the required performance parameters. Among the tested compositions, optimal PSA parameters were achieved for Q2-7358 resin filled with 0.5 pph of rose quartz particles: adhesion exceeded industrial requirements by more than 15%, and tack met those requirements. Furthermore, low (and consistent) shrinkage (0.4% after one week) and cohesion—evaluated as hold time > 72 h—were recorded. As the most important parameter for studied compositions, thermal resistance (SAFT) substantially increased (>225 h) in comparison to neat resin (150 h). Full article

To address the demand for underwater acoustic detection with hydrostatic pressure resistance, this paper proposes a fiber-optic Fabry–Perot (F-P) underwater acoustic sensor based on micro-electromechanical system (MEMS) technology. According to the F-P interference principle, the diaphragm deforms under acoustic pressure, inducing variations in the F-P cavity length which modulate the interference spectrum and enable the measurement of underwater acoustic signals. A sensing diaphragm with a composite structure consisting of a central boss and a micro-hole array is designed, which improves the optical signal quality while reducing the influence of the pressure difference between the inner and outer surfaces of the diaphragm on sensor operation. MEMS fabrication, computer numerical control (CNC) machining, and laser fusion splicing technologies are employed to achieve batch fabrication of the sensing units and adhesive-free integration of the sensor. Experimental results show that the proposed sensor exhibits a flat frequency response within ±1.5 dB over the range of 1 kHz to 10 kHz, with an average signal-to-noise ratio (SNR) of 86.35 dB. The sensitivity reaches −181.79 dB re 1 rad/μPa at 10 kHz, with a maximum nonlinearity of 0.48% F.S., a repeatability error of 0.15% F.S. and a dynamic range of 100.83 dB. The proposed sensor features miniaturization, high consistency, hydrostatic pressure self-balancing capability, and immunity to electromagnetic interference, providing a solid foundation for hydrostatic-pressure-resistant underwater acoustic measurements in deep-sea environments. Full article

MEMS hydrophones, as critical sensors for maritime security and underwater information acquisition, have sensitive membrane structures that exhibit insufficient ability to withstand hydrostatic pressure, necessitating an overload-protection design. Based on buckling stability theory, a collaborative optimization method for overload-protection column design was proposed, integrating theoretical analysis, finite-element simulation, and process feasibility. An optimized design scheme for hydrophone overload-protection columns was established by comprehensively considering geometric buckling-resistant design, micro-gap anti-adhesion requirements, minimal impact on sensitivity, and micro/nano-fabrication constraints. The results indicate that intermediate slenderness columns with radii between 5.5 μm and 7.5 μm sufficiently meet both fabrication and operational requirements, effectively providing overload protection. Furthermore, at water depths not exceeding 382 m, the MEMS hydrophone can maintain the integrity of its membrane structure without column buckling. Full article

Continuous plantar-pressure monitoring is important for objective gait analysis and early detection of abnormal loading; however, many existing solutions remain laboratory-bound (force plates and instrumented walkways) or rely on costly in-shoe multilayer sensor arrays. Here, we developed and optimized a fully screen-printed pressure-sensing insole based on carbon–polymer nanocomposite layers, with an emphasis on manufacturability and process control to bridge the gap between proof-of-concept force-sensitive resistor (FSR)-based insoles and scalable printed-electronics manufacturing workflows. Composite pastes containing carbon fillers (graphene nanoplatelets, carbon black, and graphite) were formulated to improve sensor repeatability and sensitivity. Sensors were characterized under compression loads from 100 N to 1300 N, showing a sensitivity of 10.5 ± 2.8 Ω per 100 N and a sheet-to-sheet coefficient of variation of 22.1% in resistance response. The effects of paste composition, screen mesh density, electrode layout, and lamination on sensitivity and repeatability were systematically evaluated. In addition, correlation analysis of resistance values from integrated quality-control meanders proved useful for monitoring screen-printing process stability. The final insole integrates printed carbon sensing pads and contacts, a dielectric spacer, and an adhesive layer in a thin, flexible format suitable for integration with wearable electronics. In practical static-load tests, repeated manual placement of weights yielded coefficients of variation as low as 4% at 500 g and a detection limit of ~0.1 N, comparable to a very light finger touch. These results demonstrate that low-cost screen-printed electronics can provide robust pressure sensing for wearable plantar-pressure monitoring. Full article

Polytetrafluoroethylene (PTFE) is attractive for high-frequency communications but adheres very poorly to other materials due to its very low surface energy. Conventionally, surface treatments of PTFE are used to increase the polarity of the PTFE surface and enable bonding to materials with increased surface free energy. However, surface treatments are difficult to scale, can damage surfaces, and often lack reproducibility. Therefore, developing a material that can make PTFE adhere well to other materials without surface treatment is highly desirable. In this study, we aimed to develop a new material with strong adhesion to PTFE. We synthesized three polymer gels from dodecyl acrylate (DA) and 2-(dimethylamino) ethyl acrylate (DMAE): the homopolymer gels PDEAE and PDA, and the copolymer gel P(DEAE-co-DA). The copolymer gel P(DEAE-co-DA) exhibited high pressure-sensitive adhesion to PTFE, recording the highest adhesive strength (F = 430.0 N/m) and the highest peel energy (G = 713.4 J/m²) compared to the homopolymer gels PDEAE and PDA. Mechanical testing showed PDEAE had the greatest strength and toughness, PDA balanced stiffness and extensibility, and P(DEAE-co-DA) was the most flexible and extensible. The P(DEAE-co-DA) with the smoothest surface (Sz ≈ 0.176 µm) showed the highest F and G, implying that surface roughness did not contribute significantly to the interfacial adhesion between the gels and the PTFE. Based on the surface free energy ${\sigma }_s$ and work of adhesion $W_a$ values, the adhesive strength to PTFE was predicted to be PDEAE > P(DEAE-co-DA) > PDA, but the measured G in peel tests contradicted this, indicating that the gels’ viscoelastic deformation and energy dissipation dominate the measured F and G. The frequency-dependent viscoelastic data and relaxation times τ and activation energies $E_a$ suggested optimal adhesion requires a balance of adhesion (mobility for energy dissipation (short τ, low $E_a$)) and sufficient cohesion (high G′). P(DEAE-co-DA) achieved this balance, explaining its high measured F and G. With precise control of polymer chain mobility, the adhesion of P(DEAE-co-DA) gels can likely be improved further. Future work will employ block copolymerization and monomer-ratio control to tune molecular motion and enhance adhesion to PTFE. Full article

The adhesion performance of pressure-sensitive adhesive (PSA) thin films on additively manufactured polymers is strongly governed by surface anisotropy induced during printing. In this study, PSA thin films based on 2-ethylhexyl acrylate (EHA) and acrylic acid (AA) were deposited by initiated chemical vapor deposition (iCVD) onto fused deposition modeling (FDM) printed PLA substrates with different raster orientations (0°, 30°, 60°, and 90°). The deposited films exhibited high optical transparency on glass, and thicknesses consistent with the targeted deposition. Adhesion performance was evaluated using tensile and three-point bending tests, revealing a strong dependence on raster orientation. The 0° raster orientation yielded the highest shear adhesion strengths, reaching 12.03 N/cm² under tensile loading and 4.59 N/cm² under bending, along with the largest failure displacements. In contrast, specimens printed at 90° exhibited an approximately 47% reduction in tensile shear adhesion strength and limited deformation prior to failure. SEM analysis showed that raster alignment parallel to the loading direction promoted extensive adhesive deformation and PSA fibrillation, whereas higher raster angles resulted in predominantly interfacial debonding. These results demonstrate that raster orientation is a critical design parameter for tuning PSA adhesion on FDM-printed PLA substrates without modifying adhesive chemistry. Full article

In this study, a high-performance MoS₂-based strain-gauge pressure was sensor fabricated entirely below 80 °C, enabling direct integration onto flexible polyethylene terephthalate (PET) substrates. The sensor comprised a three-layer MoS₂ channel (~2 nm) patterned via dry transfer and O₂/Ar plasma etching, interfaced with Cr/Au electrodes. This wafer-scale and cost-effective fabrication route preserves the crystallinity of the film and prevents substrate degradation. The sensor achieved a gauge factor of ~104 under compression, representing a fifty-fold improvement over conventional metal foil gauges (~2), with a linear response across both compressive and tensile regimes. Mechanical robustness was confirmed through repeated bending and tape adhesion tests, with no degradation in electrical performance. When configured as a Wheatstone bridge, this device exhibits normalized sensitivity suitable for real-time monitoring, with response and recovery times below 200 ms. These results establish O₂/Ar-plasma-patterned MoS₂ architectures as a scalable, cost-effective platform for next-generation flexible sensors, outperforming metal-foil technology in applications including seat-occupancy detection, wearable physiological monitoring, and tactile interfaces for soft robotics. Full article

This study proposes a cylindrical high-temperature-resistant fiber-optic composite sensor based on the EFPI-FBG hybrid structure for simultaneous temperature and pressure measurement, addressing the demand for high-performance monitoring in harsh environments. The sensor’s core consists of a cylindrical pressure chamber, a metal substrate, and an EFPI-FBG sensing structure fixed via resistance welding and high-temperature ceramic adhesive. The cylindrical pressure chamber converts pressure into axial deformation to modulate the EFPI cavity length, while the FBG with one end floating is exclusively used for temperature compensation, avoiding pressure interference. The EFPI cavity length exhibits a linear relationship with pressure, achieving a sensitivity of 0.171 μm/MPa and a linear correlation coefficient of 0.9986. Stable operation up to 600 °C and 20 MPa is demonstrated, with a decoupling matrix enabling accurate dual-parameter sensing. Full article

This article presents a comparison of empirical and simulation studies and the parameters declared by the membrane manufacturer. The analysis concludes that these values differ at each stage. Therefore, a numerical and simulation analysis of an optimal flat membrane was undertaken, which will successfully perform measurement functions across the full pressure range without causing inelastic deformations based on a membrane made of 316 L stainless steel with the following mechanical parameters: Young’s modulus $\mathrm{E}=2\times {10}^{11} \mathrm{P}\mathrm{a}$, Poisson’s ratio $\mathsf{\nu }=0.28$, density $\mathsf{\rho }=7980 \mathrm{k}\mathrm{g}/{\mathrm{m}}^3$, and yield strength 2.8 × 10⁸ Pa. A diaphragm with an outer diameter of 25.4 mm, an inner diameter of $2.22\times {10}^{-4} \mathrm{m}$, and a thickness of t = $5.08\times {10}^{-5} \mathrm{m}$ was designed for a pressure sensor in vacuum extinguishing chambers of medium-voltage devices, with a pressure difference $\Delta \mathrm{p}$ from 7 × 10⁻⁴ Pa to 1.013 × 10⁵ Pa. Finite element method (FEM) simulations in the COMSOL Multiphysics environment showed maximum von Mises reduced stresses 1.96 × 10⁸ Pa below the yield strength, confirming operation in the linear-elastic range. The central deflection, described analytically by the equation $\mathrm{y}={\displaystyle \frac{3(1-{\mathsf{\nu }}^2)\mathrm{P}{\mathrm{r}}^4}{16\mathrm{E}{\mathrm{t}}^3}}$, increased fivefold with an increase in diameter to $3.81\times {10}^{-2} \mathrm{m}$ (active area A = 1.14 × 10⁻³ m² compared to 5.07 × 10⁻⁴ m²), achieving a metrological sensitivity of 9.1 × 10⁻¹⁰ m/Pa. Experimental studies integrated with Bragg FBG and epoxy adhesive (E = 5 × 10⁹ Pa, tensile strength $4.2\times {10}^7 \mathrm{P}\mathrm{a}$) revealed a significant deviation from the manufacturer’s catalog data (e.g., deflection of $2.0\times {10}^{-5} \mathrm{m}$ at $6.89\times {10}^2 \mathrm{P}\mathrm{a}$), resulting from uneven bonding and a lack of coaxiality. Corrugated membranes with t = $2.0\times {10}^{-5} \mathrm{m}$ exceeded plasticity, while the optimized configuration of a smooth membrane with rounded adhesive edges ($\mathrm{R}=1\times {10}^{-4} \mathrm{m}$) enabled precise pressure monitoring below ${10}^{-1} \mathrm{P}\mathrm{a}$, despite technological restrictions on assembly and miniaturization. Full article

Combined oral contraceptives (COCs) remain one of the most popular reversible contraceptive methods worldwide. Still, regardless of the drug composition and duration of therapy, almost all COCs are associated with the risk of venous thrombosis. This review highlights the main pathogenetic mechanisms of thrombosis development during oral contraceptive use. Increase the production of certain clotting factors; a decrease in antithrombin and protein S levels; acquired resistance to activated protein C; a reduction in tissue factor pathway inhibitor (TFPI); indirect endothelial activation; inhibition of endogenous fibrinolysis; regulation of tissue factor by estradiol-sensitive microRNA; homocysteine imbalance caused by decreased intestinal reabsorption of folates and vitamin B-12; reduced bioavailability of nitric oxide (NO) due to high homocysteine levels; higher blood pressure, water retention, insulin resistance, increased levels of pro-inflammatory C-reactive protein (CRP) and uric acid, and antifibrinolytic (plasminogen activator inhibitor 1 type, PAI-1) biomarkers as consequences of NO deficiency; increased platelet adhesiveness and ADP-induced aggregation, which promote fibrinogen binding; and increased expression of pro-inflammatory cytokines are the main thrombotic effects of COCs use. Clinicians should carefully evaluate each patient’s individual risk factors when prescribing COCs and conduct regular monitoring to reduce the risk of complications. Full article

Underground gas storage (UGS) is critical to national reserves and seasonal peak-shaving, and its safe operation is integral to energy security. In UGS surface process pipelines, heterogeneous bimetal composite pipes—carbon-steel substrates lined with stainless steel—are widely used but susceptible under coupled thermal–pressure–flow loading to geometry-induced instabilities (local buckling, adhesion, and collapse), which can restrict flow, concentrate stress, and precipitate rupture and unplanned shutdowns. Conventional ultrasonic testing and magnetic flux leakage have limited sensitivity to such instabilities, while standard eddy-current testing is impeded by the ferromagnetic substrate’s high permeability and electromagnetic shielding. This study introduces magnetically saturated pulsed eddy-current testing (MS-PECT). A quasi-static bias field drives the substrate toward magnetic saturation, reducing differential permeability and increasing effective penetration; combined with pulsed excitation and differential reception, the approach improves defect responsiveness and the signal-to-noise ratio. A prototype was developed and evaluated through mechanistic modeling, numerical simulation, laboratory pipe trials, and in-service demonstrations. Field deployment on composite pipelines at the Hutubi UGS (Xinjiang, China) enabled rapid identification and spatial localization of liner collapse under non-shutdown or minimally invasive conditions. MS-PECT provides a practical tool for composite-pipeline integrity management, reducing the risk of unplanned outages, enhancing peak-shaving reliability, and supporting resilient UGS operations. Full article