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28 pages, 906 KB  
Review
Lignin-Based Adhesives for Various Packaging Applications
by Urška Klenovšek and Urška Vrabič-Brodnjak
Polymers 2026, 18(15), 1905; https://doi.org/10.3390/polym18151905 - 3 Aug 2026
Viewed by 278
Abstract
Growing demand for more sustainable packaging has increased interest in bio-based adhesives as alternatives to conventional fossil-derived systems. Among renewable raw materials, lignin is particularly attractive because of its aromatic structure, phenolic functionality, and availability as a side stream of pulp, paper, and [...] Read more.
Growing demand for more sustainable packaging has increased interest in bio-based adhesives as alternatives to conventional fossil-derived systems. Among renewable raw materials, lignin is particularly attractive because of its aromatic structure, phenolic functionality, and availability as a side stream of pulp, paper, and biorefinery processes. This review critically examines the potential of lignin-based adhesives for packaging applications. Selected polysaccharide-, protein-, vegetable-oil-, and tannin-based systems are briefly discussed as comparative references, while the main focus is placed on the properties of kraft lignin, lignosulfonates, organosolv lignin, and soda lignin. Their structural differences, adhesive behaviour, and suitability for chemical modification through hydroxymethylation, phenolation, demethylation, depolymerization, oxidation, and epoxidation are evaluated. Because most lignin-adhesive research concerns wood bonding, the transferability of these findings to paper, paperboard, labels, coatings, films, and hot-melt packaging adhesives is critically assessed. Direct evidence for packaging applications remains limited, although existing studies demonstrate promising opportunities for paper bonding, pressure-sensitive systems, and paperboard hot-melt adhesives. Key challenges include lignin heterogeneity, processing complexity, moisture resistance, colour, food-contact safety, scalability, and compatibility with recycling. Full article
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25 pages, 21894 KB  
Article
Dynamic Impact Characteristics of Airdrop Cushioning Materials and a Cσm Curve-Based Cushioning Pad Design Method
by Zhongda Wu, Zhaojun Xi, Yichao Li, Xuesong Xiang and Renfu Li
Materials 2026, 19(12), 2526; https://doi.org/10.3390/ma19122526 - 11 Jun 2026
Viewed by 380
Abstract
To mitigate impact damage to airdropped supplies during landing, this study proposes a cushioning pad design method based on the Cσm (cushioning coefficient–maximum stress) curve, aiming to balance energy absorption efficiency with lightweight requirements. A medium-sized airdrop impact simulation model is [...] Read more.
To mitigate impact damage to airdropped supplies during landing, this study proposes a cushioning pad design method based on the Cσm (cushioning coefficient–maximum stress) curve, aiming to balance energy absorption efficiency with lightweight requirements. A medium-sized airdrop impact simulation model is established and validated via drop impact tests, and systematic dynamic impact analyses are performed on three representative cushioning materials: honeycomb paperboard, polyurethane foam, and aluminum foam. Their cushioning characteristic curves are compared, revealing that all three materials exhibit a concave Cσm profile (first decreasing, then increasing) with distinct optimal stress ranges for airdrop cushioning applications: aluminum foam for high stress (≥500 kPa), polyurethane foam for medium stress (350–450 kPa), and honeycomb paperboard for low stress (≤200 kPa). The energy absorption potential decreases with the optimal stress threshold, while cushion thickness positively correlates with the airdrop load range. In the low-stress stage, the maximum stress shows a strong functional dependence on energy density, rendering thickness effects negligible for energy absorption. Under the material fragility constraint, the Cσm curve-based graphical method can accurately determine the cushion pad’s optimal thickness and bearing area. In design Case 3, optimizing the bearing area reduced the required cushion thickness from 100.5 cm to 25.0 cm, substantially decreasing the cushion volume. The findings provide reliable material-level insights and theoretical support for impact protection design in airdrop cargo, with clear guidance on selecting cushioning materials based on their intrinsic mechanical response. Full article
(This article belongs to the Section Materials Simulation and Design)
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19 pages, 2947 KB  
Article
Hydrophobic and Optical-Barrier Films from Chemically Recycled EPS Reinforced with Cellulose Nanocrystals and Sunflower Oil
by Nathalia Vieira Villar de Nunes, Sarah Kalli Silva da Silva, Eduarda Vieira Silva, André Lamounier Caixeta, Chiara das Dores do Nascimento, Everton Granemann Souza, Amanda Dantas de Oliveira and André Luiz Missio
Polysaccharides 2026, 7(2), 41; https://doi.org/10.3390/polysaccharides7020041 - 3 Apr 2026
Cited by 1 | Viewed by 1109
Abstract
Expanded polystyrene (EPS) waste is a major environmental concern, yet practical routes to upgrade it into higher value-added materials remain limited. Here, post-consumer EPS was dissolved in ethyl acetate and solvent-cast into films containing cellulose nanocrystals (CNCs) and a sunflower oil. Three formulations [...] Read more.
Expanded polystyrene (EPS) waste is a major environmental concern, yet practical routes to upgrade it into higher value-added materials remain limited. Here, post-consumer EPS was dissolved in ethyl acetate and solvent-cast into films containing cellulose nanocrystals (CNCs) and a sunflower oil. Three formulations were produced: F-EPS (100% EPS), F-EPS + CEL (80% EPS/20% CNC), and F-EPS + CEL + OIL (80% EPS/15% CNC/5% oil). CNC markedly enhanced optical shielding, reducing transmittance at 400 nm from ≈58% (F-EPS) to ≈18% (CNC containing films). All films remained hydrophobic, showed negligible water uptake, and exhibited low mass loss after 30 days of accelerated weathering (ΔM=13%). Tensile testing showed that F-EPS had the highest UTS and elongation at break (10.0 ± 0.6 MPa and 10.5 ± 0.4%), whereas adding cellulose increased the elastic modulus (249.5 ± 29.0 MPa to 358.4 ± 64.8 MPa) but reduced UTS and elongation (8.2 ± 0.2 MPa and 5.4 ± 2.5%). Oil addition led to a further reduction in UTS and elongation (6.2 ± 0.4 MPa and 3.6 ± 0.0%), while the modulus returned to a value statistically similar to neat F-EPS. FTIR and XRD confirmed preservation of the EPS chemical fingerprint and a predominantly amorphous structure (2θ20–30°). Overall, EPS + CNC + OIL films combine hydrophobicity, UV-screening, and elastic modulus similar to neat F-EPS, supporting their use as moisture-resistant, UV screening protective topcoats for non-food-contact paperboard packaging. Full article
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20 pages, 5832 KB  
Article
Impact of Sample Size and Deformation Measurement Techniques on Uniaxial Tensile Testing of Fiber-Based Materials
by Yuchen Leng, Cedric W. Sanjon, Peter Groche, Marek Hauptmann and Jens-Peter Majschak
Materials 2026, 19(6), 1197; https://doi.org/10.3390/ma19061197 - 18 Mar 2026
Viewed by 723
Abstract
The uniaxial tensile test is a common and fundamental test in materials science and engineering, in which a specimen is subjected to controlled tension until failure. From this, the stress–strain curve and many property parameters of the material can be calculated, such as [...] Read more.
The uniaxial tensile test is a common and fundamental test in materials science and engineering, in which a specimen is subjected to controlled tension until failure. From this, the stress–strain curve and many property parameters of the material can be calculated, such as tensile strength, ultimate strength, maximum elongation, Young’s modulus, Poisson’s ratio, and yield strength. As fibrous materials, such as paper and paperboard, become more popular, accurately measuring their mechanical properties becomes essential for developing and applying these materials, especially in packaging. However, since they are anisotropic and inherently inhomogeneous due to the arrangement of the fibers, accurately determining their mechanical properties is not straightforward. This study investigated how several key factors influence the results of tensile tests on fiber-based materials: sample size and deformation measurement techniques using three fiber materials. This study also compared three different strain recording methods: digital image correlation (DIC), video extensometer, and conventional extensometer (Traverse). The DIC technique emphasized the effect of the inherent inhomogeneity of the paperboard on the overall mechanical properties obtained from tensile tests. The results indicated that sample size has a negligible effect on the stress–strain curve, and any apparent influence likely stems from slip at the grips during tensile testing. However, sample size does affect paperboard fracture to some extent. The study also provided recommendations for optimal specimen geometry and deformation recording methods to improve the accuracy and repeatability of tensile testing of fiber-based materials. Full article
(This article belongs to the Section Materials Simulation and Design)
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25 pages, 7930 KB  
Article
Multilayer Barrier Coatings with Starch/Bentonite for Paperboard—The Effects of the Number of Layers and the Drying Strategy on the Barrier Properties
by Lars Järnström, Hanna Christophliemk, Erik Bohlin, Johan Larsson and Per Emilsson
Coatings 2026, 16(3), 299; https://doi.org/10.3390/coatings16030299 - 28 Feb 2026
Cited by 1 | Viewed by 1743
Abstract
This study investigates the impact of multilayer structures and drying strategies on the barrier properties of high-speed starch/bentonite-coated paperboard. The study examines the impact of drying at a high machine speed of 400 m min−1, addressing a key knowledge gap. The [...] Read more.
This study investigates the impact of multilayer structures and drying strategies on the barrier properties of high-speed starch/bentonite-coated paperboard. The study examines the impact of drying at a high machine speed of 400 m min−1, addressing a key knowledge gap. The hypotheses were that thin multilayer coatings reduce oxygen permeability more effectively than thick single or double coatings and that gentle infrared (IR) drying would be required to achieve this effect. The experiments comprised up to six consecutive coating applications, each providing a dry coat weight between 0.5 and 1.5 g m−2. The IR dryer power ranged from 207 kW to 829 kW, and different IR frame positions were tested. The results indicated that thin multilayer coatings resulted in fewer pinholes, lower oxygen transmission rates, and improved grease resistance compared with one or two thick layers. However, the effectiveness of the multilayer-coated paperboard was influenced by the employed drying strategy. Specifically, gentle IR drying reduced pinholes, lowered oxygen transmission rates and enhanced grease resistance. Full article
(This article belongs to the Special Issue Advanced Materials and Films for Food Packaging)
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18 pages, 2374 KB  
Article
Parametric Sensitivity of Shear Correction Factors for Multiwall Corrugated Structures
by Julia Graczyk, Jędrzej Tworzydło and Tomasz Garbowski
Materials 2026, 19(5), 863; https://doi.org/10.3390/ma19050863 - 26 Feb 2026
Cited by 2 | Viewed by 478
Abstract
Transverse shear deformation plays a non-negligible role in lightweight periodic-core structures and motivates the use of shear-corrected reduced-order plate and beam models. However, the shear correction factor ks is often treated as a constant despite its strong dependence on cross-sectional heterogeneity and [...] Read more.
Transverse shear deformation plays a non-negligible role in lightweight periodic-core structures and motivates the use of shear-corrected reduced-order plate and beam models. However, the shear correction factor ks is often treated as a constant despite its strong dependence on cross-sectional heterogeneity and geometry. This work quantifies the global sensitivity of ks in corrugated paperboard by combining an energy-consistent pixel-based identification of the effective shear stiffness GA)eff with a space-filling exploration of the parameter domain. Representative three-ply (single-wall) and five-ply (double-wall) configurations are generated directly in the pixel domain using sinusoidal fluting descriptions and non-overlapping liner bands. The effective shear stiffness is obtained from a heterogeneous shear-energy equivalence, where a normalized two-dimensional shear-stress shape function is computed from pixel-based sectional descriptors and integrated with spatially varying shear moduli. Latin Hypercube Sampling is employed to explore wide ranges of flute period, height, and thickness, liner thicknesses, and liner–flute shear-modulus contrasts. Global sensitivity is reported using unit-free normalized indices, including log-elasticities (based on the slope of lnks versus lnx) and partial rank correlation coefficients. The results demonstrate that flute geometry is the primary driver of ks variability, while material contrast significantly modulates shear-energy localization, particularly in double-wall boards with two distinct flutings. The proposed framework enables high-throughput shear correction assessment and supports robust parameterized reduced-order models for corrugated structures. Full article
(This article belongs to the Section Materials Simulation and Design)
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26 pages, 5898 KB  
Article
Research on Disturbance Factors of Transformer Insulation Using Submersible Internal Inspection Robot
by Wenbin Zhao, Shiyuan Wang and Lei Su
Energies 2026, 19(3), 581; https://doi.org/10.3390/en19030581 - 23 Jan 2026
Viewed by 424
Abstract
Large oil-immersed power transformers are core equipment in power grids, and the use of robots for internal inspection can significantly enhance efficiency. However, existing research has primarily focused on the development of robotic bodies, neglecting the potential impact of their operation on the [...] Read more.
Large oil-immersed power transformers are core equipment in power grids, and the use of robots for internal inspection can significantly enhance efficiency. However, existing research has primarily focused on the development of robotic bodies, neglecting the potential impact of their operation on the transformer’s oil–paper insulation system. This paper addresses this issue, evaluates the risk of underwater inspection robots colliding with internal structures, and finds that the maximum elongation rate of insulation paperboard at a speed of 0.1 m/s is far below the damage limit. Simultaneously, it analyzes the process by which propellers induce bubbles in oil, pointing out the need to optimize propeller design to ensure insulation safety. The study also extends the classical cavitation theory in water to the oil medium, reveals the conditions for gas generation by the propeller and the variation in the patterns of gas components (such as C2H2, H2, etc.) through experiments, and discusses the gas source issue of cavitation in oil. Full article
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24 pages, 6387 KB  
Article
Properties of Plastic-Based Composite Panels Manufactured from Municipal Waste Under Accelerated Weathering as Potential Paving Slabs
by Chatree Homkhiew, Pruttipong Pantamanatsopa, Sriwan Khamtree, Chainarong Srivabut, Worapong Boonchouytan, Surasit Rawangwong and Salim Hiziroglu
Polymers 2025, 17(22), 2998; https://doi.org/10.3390/polym17222998 - 11 Nov 2025
Cited by 1 | Viewed by 1471
Abstract
This research examined the mechanical, physical, thermal, and durability properties of plastic-based composites made from MSW, namely ultra-high-temperature (UHT) cartons, plastic bags, aluminum foil, and foil bags under both unweathered and accelerated weathering conditions to evaluate their potential as paving slab materials. Composite [...] Read more.
This research examined the mechanical, physical, thermal, and durability properties of plastic-based composites made from MSW, namely ultra-high-temperature (UHT) cartons, plastic bags, aluminum foil, and foil bags under both unweathered and accelerated weathering conditions to evaluate their potential as paving slab materials. Composite samples with varying mixing ratios were fabricated and tested based on an experimental design. Statistical analyses using one-way ANOVA confirmed the significant effects of composition on material performance (p < 0.05). The results demonstrated that the mixing ratio markedly influenced mechanical properties. The composite containing 50 wt% UHT carton and 50 wt% foil bags (U50F50) achieved the highest modulus of rupture (121.20 MPa) and modulus of elasticity (2.98 GPa), as well as compressive strength (28.56 MPa), compressive modulus (2.12 GPa), screw withdrawal resistance (54.25 MPa), and hardness (66.25). Under accelerated weathering, all of the composites showed moderate reductions in strength (10 to 30%) due to plastic degradation and surface cracking. In contrast, the composites containing high paperboard fractions (U80P15A5) exhibited greater WA (3.55%) and TS (3.04%), attributed to the hydrophilic nature of cellulose. The inclusion of foil bags effectively reduced WA and TS by limiting moisture penetration. Density measurements demonstrated a gradual increase (0.99 to 1.05 g/cm3) with higher foil content, while accelerated weathering induced an average 10% density reduction. Abrasion resistance improved in foil-rich composites, with U50F50 showing the lowest weight loss (8.56 to 14.02%), confirming its superior structural integrity under mechanical wear. Thermal analysis indicated low conductivity values (0.136 to 0.189 W/m·K), demonstrating favorable insulation performance compared to conventional paving materials. However, higher foil bag fractions enhanced heat conduction, balancing mechanical strength with thermal functionality. Overall, MSW-derived composites containing 30 to 50 wt% foil bags exhibited optimal mechanical durability, abrasion resistance, and thermal stability, making them promising candidates for sustainable paving slab production with low environmental impact and enhanced service life. Full article
(This article belongs to the Section Polymer Applications)
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22 pages, 333 KB  
Review
Bio-Based Coatings on Cellulosic Materials Resistant to Humidity and Fats
by Bastián Rozas, Julio E. Bruna, Abel Guarda, María José Galotto, Cristopher Reyes, Ximena Valenzuela, Francisco Rodríguez-Mercado and Alejandra Torres
Polymers 2025, 17(20), 2755; https://doi.org/10.3390/polym17202755 - 15 Oct 2025
Cited by 5 | Viewed by 2498
Abstract
Cellulose stands out as a promising alternative to conventional polymers in food packaging due to its abundance, renewability, biodegradability and structural robustness. Despite these advantages, its natural low resistance to water and fats limits its direct application, necessitating the use of protective coatings [...] Read more.
Cellulose stands out as a promising alternative to conventional polymers in food packaging due to its abundance, renewability, biodegradability and structural robustness. Despite these advantages, its natural low resistance to water and fats limits its direct application, necessitating the use of protective coatings to enhance its functionality. In this context, the use of biopolymeric coatings such as poly(lactic acid) (PLA), starch, lignin, chitin and chitosan has emerged as a sustainable solution, providing effective barriers against moisture and oils. These coatings not only improve the functional performance of cellulosic substrates but also reduce reliance on fossil-based plastics, fostering compostable systems and supporting a circular economy. This review analyzes recent developments in biopolymer-coated cellulosic packaging materials, focusing on their resistance to water and fats. The aim is to assess their potential for sustainable food packaging applications. The findings highlight how these innovations contribute to global sustainability goals, such as reducing plastic waste, lowering carbon emissions, and decreasing dependence on non-renewable resources. Full article
(This article belongs to the Special Issue Polymer-Based Coatings: Principles, Development and Applications)
17 pages, 4830 KB  
Article
Experimental and Numerical Studies of Two- and Three-Layer Corrugated Boards in Bending Test
by Gabriela Kmita-Fudalej and Leszek Czechowski
Materials 2025, 18(18), 4351; https://doi.org/10.3390/ma18184351 - 17 Sep 2025
Viewed by 1035
Abstract
This paper deals with the analysis of four-point bending two- and three-layer corrugated boards along the direction perpendicular to the machine direction. The taken segments of paperboard were examined to determine the bending stiffness for three different configurations. The investigations were carried out [...] Read more.
This paper deals with the analysis of four-point bending two- and three-layer corrugated boards along the direction perpendicular to the machine direction. The taken segments of paperboard were examined to determine the bending stiffness for three different configurations. The investigations were carried out experimentally and numerically. The tests of bending were analysed only in the elastic range of the material. Each configuration of paperboard was modelled as an orthotropic material. The numerical analysis was based on the finite element method by applying Ansys® software. Several material properties and the thicknesses of papers were assumed to determine the general stiffness in bending. In the analysis, two different discrete models based on geometries of the paperboard were elaborated to adjust the results to the experimental ones. The results of analyses for some configurations showed good agreement with the experiment. This paper indicates some differences in stiffness between two- and three-layer paperboards. Full article
(This article belongs to the Section Materials Simulation and Design)
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14 pages, 1329 KB  
Article
Biopolymer Paperboard Impregnation Based on Chitosan and Nanocellulose with Addition of Caffeine and Gallic Acid
by Joanna Młodziejewska, Magdalena Woźniak, Anna Sip, Renata Dobrucka and Izabela Ratajczak
Coatings 2025, 15(9), 1034; https://doi.org/10.3390/coatings15091034 - 3 Sep 2025
Cited by 2 | Viewed by 1489
Abstract
In this study, the preparation and detailed characterization of a chitosan (CHT) impregnation system modified with cellulose nanofibrils (CNFs) and enriched with bioactive compounds—caffeine (CAF) and gallic acid (GA)—applied to the surface of unbleached paperboard were described. Their mechanical properties (tensile strength, elongation [...] Read more.
In this study, the preparation and detailed characterization of a chitosan (CHT) impregnation system modified with cellulose nanofibrils (CNFs) and enriched with bioactive compounds—caffeine (CAF) and gallic acid (GA)—applied to the surface of unbleached paperboard were described. Their mechanical properties (tensile strength, elongation at break, and bursting strength), structural features, and surface barrier parameters (water absorption) were evaluated. The antibacterial activity of the formulations comprising 1% chitosan (1% CHT), 1% chitosan with 1% caffeine (1% CHT/1% CAF), and 1% chitosan with 1% gallic acid (1% CHT/1% GA)—applied to enhance the functionality of the coated paperboard—was additionally assessed. The incorporation of cellulose nanofibrils into the coating matrix markedly improved the mechanical performance of the paperboard, particularly in terms of puncture resistance and elongation at break, while all modified coatings retained high burst strength. Impregnations containing gallic acid or caffeine showed similar mechanical characteristics but improved flexibility without compromising structural integrity. Chitosan solutions containing gallic acid and solutions containing caffeine exhibited activity against the tested Gram-positive (S. aureus, L. monocytogenes) and Gram-negative (E. coli, P. aeruginosa) bacterial strains. Antibacterial analysis showed moderate activity against Gram-positive strains and strong inhibition of Gram-negative bacteria, with the 1% CHT/1% GA impregnation giving the largest zone of growth inhibition around the sample—19 mm in the agar diffusion test—indicating the strongest suppression of E. coli. It was found that incorporation of nanocellulose into the chitosan matrix significantly reduces water uptake by treated paperboard surface, which is critical in the context of food packaging. The best result—Cobb60 value of 32.85 g/m2—was achieved for the 1% CHT/1% CNF formulation, corresponding to an 87% reduction in water absorption compared to the uncoated control. The results obtained in this study indicate a promising potential for the use of these impregnation systems in sustainable packaging applications. Full article
(This article belongs to the Special Issue Advanced Coatings and Films for Food Packing and Storage, 2nd Edition)
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11 pages, 1665 KB  
Article
Substitution of Fossil Layers with Biobased Ones in Sustainable Cellulosic Packaging for Dairy Products
by Maria-Beatrice Coltelli, Simone Giangrandi, Vincenzo Tricoli, Luca Panariello and Andrea Lazzeri
Appl. Sci. 2025, 15(17), 9615; https://doi.org/10.3390/app15179615 - 31 Aug 2025
Viewed by 1582
Abstract
Home-compostable, biobased films were developed by blending poly(lactic acid) (PLA) with poly(butylene succinate-co-adipate) (PBSA). Among the formulations, the PLA/PBSA 60/40 blend demonstrated strong potential for industrial film production due to its enhanced flexibility and tear resistance. Thanks to their thermoplastic nature, [...] Read more.
Home-compostable, biobased films were developed by blending poly(lactic acid) (PLA) with poly(butylene succinate-co-adipate) (PBSA). Among the formulations, the PLA/PBSA 60/40 blend demonstrated strong potential for industrial film production due to its enhanced flexibility and tear resistance. Thanks to their thermoplastic nature, these films can be applied to various substrates—such as paper or paperboard—and are easily recyclable within industrial processing environments. In this study, nanostructured clay and talc were incorporated into PLA/PBSA 60/40-based films to produce composites, which were evaluated for their effectiveness in limiting the diffusion of moisture from high-humidity soft cheeses. The materials’ melt fluidity and tensile properties were also characterized, and the composite morphology was examined using electron microscopy. The results revealed that the filler type significantly affected both the morphological structure and barrier performance, highlighting the critical role of material composition in the development of effective and environmentally sustainable packaging solutions. The biobased PLA/PBSA (60/40) films, particularly those filled with talc, exhibited high processability, flexibility, and effectiveness as a moisture barrier for dairy packaging. Although not yet feasible as a direct LDPE substitute without increasing their thickness, their low mass loss points to their strong potential for sustainable applications—especially when paired with paperboard in rigid packaging. Full article
(This article belongs to the Special Issue Innovation in Dairy Products)
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12 pages, 2320 KB  
Article
Hydrophobic Coating of Paperboard Using Oak Wood-Derived Lignin Nanoparticles and Chitosan Composites
by Le Van Hai, Eun Sol Heo, Cheol Yoon and Tae Hyun Kim
Molecules 2025, 30(16), 3387; https://doi.org/10.3390/molecules30163387 - 14 Aug 2025
Cited by 1 | Viewed by 2348
Abstract
This study explores the potential application of lignin nanoparticles and chitosan–lignin nanoparticles (CLNs) as hydrophobic barrier coatings for paperboard. The lignin nanoparticles were initially prepared using a mixed solvent of ethanol and acetone. Their characteristics were examined via scanning electron microscopy (SEM) and [...] Read more.
This study explores the potential application of lignin nanoparticles and chitosan–lignin nanoparticles (CLNs) as hydrophobic barrier coatings for paperboard. The lignin nanoparticles were initially prepared using a mixed solvent of ethanol and acetone. Their characteristics were examined via scanning electron microscopy (SEM) and dynamic light scattering, which revealed particle sizes in the range of 180–400 nm. The results indicated that the coatings with pure lignin nanoparticles failed to impart hydrophobicity to the paperboard, whereas the CLN coatings significantly enhanced hydrophobicity and reduced water absorption. The water contact angle increased from 109° to over 128° after the first CLN coating, remained at 127° with the second and third coating layers, and was maintained at 119° with four layers. Multilayer coatings were applied to improve barrier performance; however, no further enhancement in hydrophobicity was observed. The CLN-coated paper exhibited a significantly improved surface smoothness, as confirmed by SEM. The results indicate that a single-layer CLN coating is effective for imparting water-barrier properties to paperboard. In contrast, the coating with pure lignin nanoparticles resulted in cracked surfaces and inconsistent coating thicknesses. Full article
(This article belongs to the Special Issue Advances in Polymer Materials Based on Lignocellulosic Biomass)
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15 pages, 7056 KB  
Article
Effects of Packaging Constraints on Vibration Damage of ‘Huangguan’ Pear During Simulated Transport
by Lijun Wang, Zechen Xie, Yumeng Wu, Jinguo Gao and Haiyan Song
Horticulturae 2025, 11(7), 749; https://doi.org/10.3390/horticulturae11070749 - 1 Jul 2025
Cited by 4 | Viewed by 2276
Abstract
Fruit is typically transported in stacked packaging units, where external packaging constraints play a critical role in influencing mechanical damage during transit. This study primarily investigated the effects of external packaging constraints on vibration-induced damage and response vibration in ‘Huangguan’ pears (Pyrus [...] Read more.
Fruit is typically transported in stacked packaging units, where external packaging constraints play a critical role in influencing mechanical damage during transit. This study primarily investigated the effects of external packaging constraints on vibration-induced damage and response vibration in ‘Huangguan’ pears (Pyrus bretschneideri Rehd. ‘Huangguan’). Three external packaging constraint types—free constraint, elastic constraint, and fixed constraint—were applied to a two-layer stacked packaging system to limit vertical movement. The pears inside the containers were divided by a corrugated paperboard. Vibration excitation was simulated using the ASTM D4169 spectrum at three vibration levels. Damage indicators, including damage area, flesh firmness, respiratory rate, weight loss, titratable acidity, ascorbic acid, and tissue microstructure, were analyzed after vibration experiments. The results demonstrated that external packaging constraint type significantly affects the mechanical damage of ‘Huangguan’ pears, with damage severity being closely related to constraint strength. Comprehensive analysis revealed that the most severe damage occurred under free constraint, while the least damage was observed under fixed constraint. Stacking position also influenced damage, as pears on the top layer exhibited more severe damage compared to those on the bottom layer. The response vibration results aligned with the observed damage patterns. SEM analysis further revealed that vibration disrupted the tissue microstructure and damaged stone cells, which decreased in number and even disappeared at higher vibration levels. This study provides valuable insights for improving postharvest transport packaging designs and minimizing fruit loss during logistics. Full article
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17 pages, 7015 KB  
Article
Studying the Behavior of a Paperboard Box: Experiment and Finite Element Model
by Boussad Abbès, Fazilay Abbès, Lien Tien Dao, Pham Tuong Minh Duong and Viet Dung Luong
Vibration 2025, 8(2), 23; https://doi.org/10.3390/vibration8020023 - 6 May 2025
Cited by 1 | Viewed by 2559
Abstract
In the transportation and distribution of goods, cardboard boxes are often subjected to mechanical impacts such as shocks and random vibrations, which can cause damage to the goods. In this study, static and dynamic tests on cardboard boxes were designed and conducted to [...] Read more.
In the transportation and distribution of goods, cardboard boxes are often subjected to mechanical impacts such as shocks and random vibrations, which can cause damage to the goods. In this study, static and dynamic tests on cardboard boxes were designed and conducted to determine the compression strength, natural frequencies, and modal characteristics of the boxes. A finite element model of cardboard boxes considering the in-plane orthotropic elastic–plastic behavior of the cardboard was implemented in the Abaqus software through a VUMAT subroutine to perform numerical simulations under compression and random vibrations. The parameters of the model were determined through an inverse identification process. As a first result, the predicted force–displacement curves show good agreement with the measured curves. Furthermore, the power spectral density (PSD) response of the mass/box system under random vibrations obtained through numerical simulations is consistent with the responses obtained from experimental measurements. Full article
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