Search Results (114)

The evolution of neutron scattering from reactor-based steady-state sources to high-power pulsed spallation sources has necessitated a paradigm shift in neutron optics. While pulsed sources offer high peak brilliance and energy-resolved measurements via the time-of-flight (TOF) technique, the intrinsic divergence and broad wavelength bandwidth of the incident beam pose significant challenges for focusing, particularly in the realm of very small-angle neutron scattering (VSANS, Q < 0.001 Å⁻¹). This review presents a comprehensive analysis of diverse focusing techniques, including converging multi-slit apertures, electrical and superconducting magnetic sextupole lenses, grazing-incidence focusing mirrors, compound refractive lenses with oscillation apertures, and a special multi-beam VSANS configuration. Special attention is given to the transition from permanent magnet systems to nested rotating sextupole permanent magnets (Nest-Rot-SPM) and modulated superconducting sextupoles (SSM), detailing the physical and engineering challenges involved. Furthermore, grazing-incidence reflective optics, notably toroidal Wolter mirrors, are discussed as an achromatic alternative. The integration of these technologies into world-leading pulsed neutron sources is reviewed to project the future landscape of extended Q-range coverage for SANS instruments. Full article

Pore-throat structures in a carbonate reservoir were classified into ten petrophysical facies representing coarse, medium, or fine throat types based on Mercury Injection Capillary Pressure (MICP) data from 77 core samples, directly reflecting distinct flow capacities. Using Nuclear Magnetic Resonance (NMR) data from 20 samples, an artificial neural network (ANN) model was developed with four conventional logs, namely Gamma Ray (GR), Deep Laterolog Resistivity (RD), Density (DEN), and Compensated Neutron Log (CNL), as inputs to predict the T₂ spectrum continuously. A cumulative pore-throat size distribution matching method was then used to transform predicted T₂ spectra into capillary pressure curves. The resulting pore-throat parameters show excellent agreement with core measurements, with relative errors for key parameters—such as median pore-throat radius (R₅₀) and sorting coefficient (Sp)—below 15%. This approach extends discrete core data to continuous wellbore profiles, enabling pore-throat prediction and facies classification in intervals lacking MICP data. It effectively identifies dominant flow channels and tight interlayers, with facies validated by thin-section petrography, providing a robust basis for evaluating highly heterogeneous carbonate reservoirs. Full article

Accurate estimation of the barometric coefficient ($\beta$) is important for correcting pressure effects in soil moisture data from cosmic-ray neutron sensing (CRNS) due to the barometric effect. To evaluate estimation strategies for $\beta$, we compared analytical and empirical approaches using 71 CRNS and 46 neutron monitor (NM) stations across the United States, Europe, and globally. Our results show spatio-temporal variation in the barometric effect, with $\beta$ ranging from 0.66 to 0.82 %hPa for NM and from 0.63 to 0.80 %hPa for CRNS. These coefficients exhibit higher variability than previously published semi-analytical models. In addition, we found that the analytically determined $\beta$ values were systematically lower compared with empirical estimates, with stronger agreement between the two empirical methods ($r\approx 0.67$) than between empirical and analytical approaches. Furthermore, NM stations produced higher $\beta$ values than CRNS, indicating that differences in detector energy sensitivity affected the values of $\beta$. Principal Component Analysis (PCA) further showed that the analytical and empirical $\beta$ estimates clustered together, reflecting shared sensitivity to elevation. In contrast, soil moisture and atmospheric humidity projected nearly orthogonally to the $\beta$ vectors, indicating negligible influence, while cut-off rigidity contributed to a separate, inverse gradient. Analytical $\beta$ estimates were fully orthogonal to AH, while empirical methods showed only slight deviations beyond orthogonality. The barometric coefficient ($\beta$), therefore, varies with location, altitude, atmospheric conditions, and sensor type, highlighting the necessity of station-specific values for precise correction. Overall, our study emphasizes the need for atmospheric correction in CRNS measurements and introduces a method for deriving site- and sensor-specific $\beta$ values for accurate soil moisture estimation. Full article

Wavelength-shifting (WLS) materials are used in radiation detectors to convert ultraviolet photons into visible light, enabling improved photon detection in systems such as scintillators and optical diagnostics for nuclear fusion devices. However, the long-term performance of these materials under radiation is still a critical issue in high-dose environments. In this work, we investigated the radiation tolerance of three WLS compounds (TPB, NOL1, and SB2001), each deposited on reflective substrates (ESR and E-PTFE), resulting in six distinct WLS/substrate systems. The samples underwent gamma irradiation at absorbed doses of 100 kGy, 500 kGy, and 1000 kGy, as well as fast neutron (14.1 MeV) irradiation up to a fluence of 1.9 × 10¹³ n/cm². Qualitative photoluminescence and reflectance measurements were performed before and after irradiation to assess changes in optical performance. Gamma exposure caused spectral broadening in several samples, particularly those with TPB and SB2001, with variations of the two metrics used to compare the performance of the materials exceeding 10% at the highest doses. Neutron-induced effects were generally weaker and did not exhibit a clear fluence dependence. Reflectance degradation was also observed, with variations depending on both the WLS material and the deposition method. These findings contribute to the understanding of WLS material stability under radiation and support their qualification for use in optical components exposed to harsh nuclear environments. Full article

Polarized neutron reflectometry (PNR) analyzes surface and interfacial structures of materials. For the SHARAKU reflectometer at the Materials and Life Science Experimental Facility in the Japan Proton Accelerator Research Complex, precise measurements under weak magnetic fields, which are critical for modern spintronics, have long been challenging. To address this issue, we developed a precise weak-field sample environment equipped with a newly designed coil system. The magnetic field at the sample position can be applied within the surface/interface plane, either in the scattering plane (horizontal configuration) or perpendicular to it (vertical configuration). The horizontal configuration achieved high polarization efficiency across a stable field range, whereas the vertical configuration enabled the experiments to cross zero into negative fields. We demonstrated the instrument’s capability by resolving the remanent magnetic structure of an Fe film. Its applicability to soft matter was proven through analysis of a cellulose thin film with roughness using magnetic contrast variation PNR. In this case, precise weak-field control is essential to tune the magnetic contrast from the reference layer beneath the soft film. These results establish the system as a versatile platform for future PNR and polarized off-specular scattering experiments across a wide range of materials. Full article

The increasing demand for sustainable and multifunctional materials in radiation shielding and optical applications has driven research toward utilizing natural and waste-derived reinforcements in polymer matrices. However, achieving effective attenuation performance across different radiation types using eco-friendly fillers remains a significant challenge. In this study, polyvinyl chloride (PVC)/Polystyrene (PSt) blend composites (1:1 weight ratio) were reinforced with powdered snail shell (SSP) as a biogenic additive, aiming to enhance their shielding and optical performance. Composites containing 5%, 10%, 20%, and 30% SSP (w/v) were fabricated and characterized. Key parameters including linear attenuation coefficient (LAC), mass attenuation coefficient (MAC), mean free path (MFP), half-value layer (HVL), and effective atomic number (Zeff) were measured using a variable-energy X-ray source (13.37–59.54 keV) and ULEGe detector. Fast neutron shielding performance and theoretical values for build-up factor (EBF) and macroscopic neutron cross-sections were also calculated. The results showed a marked improvement in X-ray attenuation with increasing SSP content (SSP30 > SSP20 > SSP10 > SSP5), while neutron shielding declined due to the high oxygen content of SSP. Among the tested samples, the SSP30 composite exhibited the highest X-ray attenuation efficiency, whereas the SSP5 composition showed the greatest enhancement in optical reflectance and neutron absorption, indicating optimal performance in these respective tests. Additionally, 5% SSP incorporation improved optical reflectance by 12%, indicating enhanced photon backscattering at the material surface. This behavior contributes to improved gamma shielding efficiency by reducing photon penetration and enhancing surface-level attenuation. These findings highlight the potential of snail shell-based fillers as low-cost, sustainable reinforcements in multifunctional polymer composites. Full article

Denture stomatitis is a common issue among denture users, primarily caused by pathogenic microorganisms such as Candida albicans that adhere to and multiply on the denture surface. While previous approaches have focused on incorporating antimicrobial agents into denture base resins, this study introduces a novel surface coating strategy for polymethyl-methacrylate (PMMA) using hinokitiol—a natural antibacterial and antifungal compound derived from Hiba. This method enables the formation of a uniform silica–resin layer containing hinokitiol, achieved through a simple immersion process. Using X-ray and neutron reflectivity techniques, we discovered that a uniform silica–resin layer could form on PMMA with significant amounts of hinokitiol present. Time-dependent neutron reflectivity analysis revealed the presence of the following two types of hinokitiol molecules within the silica–resin layer: one type desorbs rapidly with weak capture near the surface, and the other desorbs slowly with strong capture near the PMMA interface, facilitated by hydrogen bonding in the silica–resin nanopores. These findings demonstrate a new mechanism for controlled release of antimicrobial agents from denture surfaces and highlight the potential of this coating technique as a practical and effective strategy for preventing denture-related infections. Full article

The High Temperature Gas-cooled Reactor (HTGR) is characterized by a high output temperature and inherent safety due to its fuel design. However, the double heterogeneity of the reactor component structure poses a challenge in thermal analyses, where fuel temperature is a key safety parameter. In this paper, a methodology for coupled thermal and neutron calculations with power discretization is developed to accurately reflect the spatial phenomena occurring in the moderator. The method is based on the point generation of power in the thermal model, and these points are determined based on the location of the fuel in the neutron model. The multi-physics interface capabilities of the Serpent code were used to investigate several configurations of the thermal model mesh and its alignment with the fuel. The impact of the radial discretization of power density was further analyzed in detail. The study revealed that the highest accuracy was achieved when the thermal model mesh was aligned with the TRi-structural ISO-tropic (TRISO) fuel particle size, and the TRISO particle arrangement was centered relative to the mesh cells. Moreover, it was found that due to the power–temperature feedback phenomena, the power is shifted outwards within a range of 1% of the relative power density. Full article

Neutron–antineutron oscillation (nnbar-osc) is a baryon number-violating process and a sensitive probe for physics beyond the standard model. Ultra-cold neutrons (UCNs) are attractive for nnbar-osc searches because of their long storage time, but earlier analyses indicated that phase shifts on wall reflection differ for neutrons and antineutrons, leading to severe decoherence and a loss of sensitivity. Herein, we revisit this problem by numerically solving the time-dependent Schrödinger equation for the two-component n/nbar wave function, explicitly including wall interactions. We show that decoherence can be strongly suppressed by selecting a wall material whose neutron and antineutron optical potentials are nearly equal. Using coherent scattering length data and estimates for antineutrons, we identify a Ni–Al alloy composition that matches the potentials within a few percent while providing a high absolute value, enabling long UCN storage. With such a bottle and an improved UCN source, the sensitivity could reach an oscillation period ${\tau }_{nnbar}$ of the order 10¹⁰ s, covering most of the range predicted with certain grand unified models. This approach revives the feasibility of high-sensitivity nnbar-osc searches using stored UCNs and offers a clear path to probe baryon number violation far beyond existing limits. Full article

The preservation of archaeological bone is of great importance for both archaeological and conservation science studies. Traditional methods of preservation assessment, such as attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), are minimally invasive and destructive. Neutron and X-ray tomography offer a totally non-invasive novel analysis method for the state of preservation of archaeological bones. Seven archaeological animal bones were selected for analysis based on animal maturity, species, visual factors, and ATR-FTIR analysis results. Archaeological bone is a hierarchical composite material constructed from both organic and mineral components; therefore, neutron tomography and synchrotron X-ray tomography have been combined in this novel approach to assess the state of preservation of animal archaeological bone. The neutron data demonstrated that the organic distribution along the diaphysis of archaeological bones varied significantly both within bones and between different animal bones. There is minimal consistency between the samples, emphasizing the inhomogeneity in archaeological bone collections. X-ray tomography revealed unseen physical details, including cracks and substantial damage. The collection of this information via non-invasive methods is highly valuable for cultural heritage, providing a deeper understanding of the observed inhomogeneity in ATR-FTIR analysis data and revealing obscured physical details. Full article

Maintaining well integrity is essential in the oil and gas industry to prevent environmental hazards, operational risks, and economic losses. Cement bond log (CBL) tools are essential in evaluating cement bonding and ensuring wellbore stability. This study presents a patent landscape review of CBL technologies, based on 3473 patent documents from the Lens.org database. After eliminating duplicates and irrelevant entries, 167 granted patents were selected for in-depth analysis. These were categorized by technology type (wave, electrical, radiation, neutron, and other tools) and by material focus (formation, casing, cement, and borehole fluid). The findings reveal a dominant focus on formation evaluation (59.9%) and a growing reliance on wave-based (22.2%) and other advanced tools (25.1%), indicating a shift toward high-precision diagnostics. Geographically, 75% of granted patents were filed through the U.S. Patent and Trademark Office, and 97.6% were held by companies, underscoring the dominance of corporate innovation and the minimal presence of academia and individuals. The review also identifies notable patents that reflect significant technical innovations and discusses their role in advancing diagnostic capabilities. These insights emphasize the need for broader collaboration and targeted research to advance well integrity technologies in line with industry goals for operational performance and safety. Full article

The elliptical cylindrical mirror has been utilized in neutron small-angle scattering and reflectometry to enhance the neutron intensity at the sample position. However, the performance of the elliptical cylindrical mirror can be impacted by surface slope errors, reflectivity, and misalignments. In this work, the performance of the elliptical cylindrical mirror under different error conditions has been analyzed comprehensively, and a 250-mm-long elliptical cylindrical mirror was designed and developed. The simulations show that a source size below 1 mm is required to achieve a peak gain above 6, with a theoretical peak gain of 16× with a 0.1 mm source. The rotational misalignment of 0.03° around the Y-axis can decrease gain from 16× to 6×. The designed mirror was fabricated with a surface figure error of 110 nm (RMS), and a roughness below 0.5 nm (RMS), and was coated with an m = 4 supermirror. The mirror was aligned and tested in the dedicated neutron beamline of the Chinese mianyang research reactor, and the results show a peak gain of 12.77 with a 0.1 mm slit source. Full article

The need to model the effect of the assembly environment on the neutronic data has been felt since Smith’s topical article on assembly homogenization techniques. Indeed, simply homogenizing the cross sections using the spatial distribution and energy spectrum of the neutron flux calculated in a single assembly with reflective boundary conditions, neglecting the effect of the proximity of other types of assemblies, can induce inaccuracies affecting the results of core calculations. Many approaches have been proposed to take into account the real environment of the assembly. The purpose of this article is to review these methods to allow the reader to compare them. Full article

We performed extensive molecular dynamics simulations using a bead–spring model to investigate the interfacial behavior of blends of linear and cyclic polymer chains confined between two planar, attractive substrates. The model system was studied over a range of chain lengths spanning an order of magnitude in the number of beads for varying blend compositions and for two different levels of substrate affinity. For short chains, we observed the preferential adsorption of linear chains at the substrate interface when they are the majority component (10% cyclic chains) as well as at equimolar composition. In contrast, for longer chains, cyclic chains are preferentially enriched at the interface. These results extend recent findings from neutron reflectivity experiments—where the enrichment of cyclic polystyrene chains at low-energy surfaces was demonstrated—to systems under solid confinement, providing deeper insight into the structural behavior of topologically distinct polymers near interfaces. This work highlights the potential for tuning interfacial composition and properties in polymer blends through topological design, with implications for advanced coatings, membranes, and nanostructured materials. Full article

Previous studies of elliptical neutron guides have shown that they transport neutrons with fewer reflections than traditional guides with a constant cross section, thus reducing neutron losses. True elliptical guides, however, are tedious to produce. Therefore, we use the neutron simulation package McStas to investigate the effect of approximating the elliptical shape by linearly tapering guide pieces. The study concerns both simple model guides and a more complex guide system corresponding to that of the BIFROST instrument, currently under construction at the European Spallation Source (ESS). Our results show that it is possible to split a simple elliptical guide into linearly tapering pieces with lengths of up to 3 m, without sacrificing transport properties. We also find that the piecewise tapering guides in some cases will have a slightly higher neutron transfer than the perfectly shaped guides for shorter wavelengths. For a ballistic guide systems with elliptical expanding and focusing sections, and for the BIFROST guide, linearly tapered pieces of 0.5 m can be used with no cost in transport properties or penalties in form of inhomogeneous phase space, but with significantly lower production costs. Full article