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Search Results (392)

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Keywords = laser bending

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15 pages, 1938 KB  
Article
Low-Loss and Stable Light Transmission in Nano-Core Plus Node-Free Anti-Resonant Hollow-Core Fiber
by Yuyi Yin, Tingwu Ge, Tong Zhang and Zhiyong Wang
Nanomaterials 2025, 15(18), 1458; https://doi.org/10.3390/nano15181458 - 22 Sep 2025
Viewed by 442
Abstract
Anti-resonant hollow-core fibers (AR-HCFs) are emerging as highly promising candidates for high-power laser transmission and low-loss optical communication. Despite their advantages, issues such as scattering loss and core-mode instability remain significant obstacles for their practical implementation. In this study, we propose a novel [...] Read more.
Anti-resonant hollow-core fibers (AR-HCFs) are emerging as highly promising candidates for high-power laser transmission and low-loss optical communication. Despite their advantages, issues such as scattering loss and core-mode instability remain significant obstacles for their practical implementation. In this study, we propose a novel hybrid fiber structure, the nano-core plus node-free anti-resonant hollow-core fiber (NPNANF), which integrates a solid, high-index nano-core within a six-tube node-free anti-resonant cladding. This hybrid design effectively enhances optical confinement while minimizing scattering losses, without relying solely on anti-resonant guidance. Numerical simulations employing the beam propagation method (BPM) and finite element analysis (FEA) demonstrate that an optimal nano-core diameter of 600 nm leads to a remarkable reduction in transmission loss to 0.025 dB/km at 1550 nm, representing a 99.8% decrease compared to conventional NANF designs. A comprehensive loss model is developed, incorporating contributions from confinement, scattering, and absorption losses in both the hollow cladding and the solid core. Parametric studies further illustrate the tunability of the fiber’s design for various high-performance applications. The proposed NPNANF achieves an ultra-low transmission loss of 0.025 dB/km, representing a >99.8% reduction compared to conventional NANF, while confining more than 92% of optical power within the nano-core. Its resistance to bending loss, strong modal stability, and balance between hollow-core and solid-core guidance highlight the advantages of NPNANF for long-haul optical communication and high-power photonics. Full article
(This article belongs to the Section Theory and Simulation of Nanostructures)
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22 pages, 7835 KB  
Article
Anodizing 3D-Printed AlSi10Mg Alloy and Its Fatigue Properties
by Hirotaka Kurita, Shinya Tako, Chika Tanaka, Kenji Hara, Kazunori Matsushima, Koji Satsukawa, Keita Watanabe and Hideki Kyogoku
Metals 2025, 15(9), 1022; https://doi.org/10.3390/met15091022 - 15 Sep 2025
Viewed by 507
Abstract
Two ways of anodizing 3D-printed AlSi10Mg alloy were characterized, and then their fatigue properties were evaluated. Test specimens were fabricated via a laser-powder bed fusion (L-PBF) process followed by machining. Normal and hard anodizing were both conducted in a sulfuric acid bath. The [...] Read more.
Two ways of anodizing 3D-printed AlSi10Mg alloy were characterized, and then their fatigue properties were evaluated. Test specimens were fabricated via a laser-powder bed fusion (L-PBF) process followed by machining. Normal and hard anodizing were both conducted in a sulfuric acid bath. The anodized layer was observed using FE-SEM/EDS. Fine Si particles dispersed in the matrix showing web-like patterns were incorporated in the anodized layer. By etching the Si particles away with Keller’s reagent, a characteristic maze-like 3D structure of anodized Al was observed. Then, rotating bending fatigue tests were carried out to evaluate the fatigue strength at 107 cycles. The fatigue strength of the as-machined, normal-anodized and hard-anodized specimens was 106, 100 and 95 MPa, respectively. The fatigue limits were proportional to the surface roughness with higher linearity. By reducing the surface roughness, the fatigue strength of the hard-anodized specimen was improved. This result demonstrates the possibility of improving the fatigue properties of anodized components by reducing their surface roughness. Lastly, a CASS (copper-accelerated acetic acid salt spray) test was conducted, and superior corrosion resistance of the normal- and hard-anodized layers was verified. Full article
(This article belongs to the Section Additive Manufacturing)
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18 pages, 3264 KB  
Article
Road Performance Evaluation of Preventive Maintenance Techniques for Asphalt Pavements
by Fansheng Kong, Yalong Li, Ruilin Wang, Xing Hu, Miao Yu and Dongzhao Jin
Lubricants 2025, 13(9), 410; https://doi.org/10.3390/lubricants13090410 - 13 Sep 2025
Viewed by 502
Abstract
Preventive maintenance treatments are widely applied to asphalt pavements to mitigate deterioration and extend service life. This study evaluated four common technologies: a high-elasticity ultra-thin overlay, an Stone Mastic Asphalt (SMA)-10 thin overlay, micro-surfacing (MS-III), and a chip seal. Laboratory testing focused on [...] Read more.
Preventive maintenance treatments are widely applied to asphalt pavements to mitigate deterioration and extend service life. This study evaluated four common technologies: a high-elasticity ultra-thin overlay, an Stone Mastic Asphalt (SMA)-10 thin overlay, micro-surfacing (MS-III), and a chip seal. Laboratory testing focused on skid resistance, surface texture, and low-temperature cracking resistance. Skid resistance was measured with a tire–pavement dynamic friction analyzer under controlled load and speed, while surface macrotexture was assessed using a laser scanner. Low-temperature cracking resistance was determined through three-point bending beam tests at −10 °C. The results showed that chip seal achieved the highest initial friction and texture depth, immediately enhancing skid resistance but exhibiting rapid texture loss and gradual friction decay. Micro-surfacing also demonstrated good initial skid resistance but experienced a sharp reduction of over 30% due to fine aggregate polishing. By contrast, the high-elastic ultra-thin overlay and SMA thin overlay provided more stable skid resistance, lower long-term friction loss, and excellent crack resistance. The polymer-modified ultra-thin overlay achieved the highest low-temperature bending strain ≈40% higher than untreated pavement, indicating superior crack resistance, followed by the SMA thin overlay. Micro-surfacing with a chip seal layer only slightly improved low-temperature performance. Overall, the high-elastic ultra-thin overlay proved to be the most balanced preventive maintenance option under heavy-load traffic and cold climate conditions, combining durable skid resistance with enhanced crack resistance. Full article
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17 pages, 2298 KB  
Article
Influence of the Process-Related Surface Structure of L-PBF Manufactured Components on Residual Stress Measurement Using the Incremental Hole Drilling Method
by Sebastian Gersch, Ulf Noster, Carsten Schulz and Jörg Bagdahn
Appl. Sci. 2025, 15(18), 9861; https://doi.org/10.3390/app15189861 - 9 Sep 2025
Viewed by 460
Abstract
Laser Powder Bed Fusion (L-PBF) parts combine geometric freedom with process-induced rough surfaces that challenge residual-stress metrology. We evaluated the accuracy of the incremental hole-drilling (IHD) method with electronic speckle pattern interferometry (ESPI) by applying defined stresses via four-point bending to stress-relieved AlSi10Mg [...] Read more.
Laser Powder Bed Fusion (L-PBF) parts combine geometric freedom with process-induced rough surfaces that challenge residual-stress metrology. We evaluated the accuracy of the incremental hole-drilling (IHD) method with electronic speckle pattern interferometry (ESPI) by applying defined stresses via four-point bending to stress-relieved AlSi10Mg coupons, rather than measuring unknown process stresses. Flat specimens (2 mm, thin per ASTM E837) were analyzed on up-skin, side-skin, and CNC-milled surfaces; thin-specimen calibration coefficients were used. After a preliminary inter-specimen check (three specimens per surface; spread < 8 MPa), one representative specimen per surface was tested with three drill sites to assess intra-specimen uniformity. Measured IHD–ESPI stresses agreed best at 70 MPa: deviations were ~4.1% (up-skin), 6.0% (side-skin), and 6.24% (CNC-milled). At 10 MPa the relative errors increased (23.6%, 18.4%, and 1.40%), consistent with reduced ESPI signal-to-noise and fixture compliance in the low-stress regime. At 140 MPa, deviations rose again (21.1%, 14.3%, and 13.1%), reflecting operation near the ~60% Rp0.2 elastic limit of hole-drilling and potential local plasticity. Surface-dependent artifacts also mattered as follows: the side-skin required no coating and performed comparably to CNC-milled, whereas the up-skin’s roughness plus matting spray introduced fringe distortions and chip/coating debris near the hole. This controlled study indicates that IHD–ESPI can provide reliable results on L-PBF AlSi10Mg in the mid-stress range when surface preparation, coating, and rig compliance are carefully managed. Limitations include excluding down-skin surfaces and testing only one specimen per condition; thus, results should be generalized cautiously. Full article
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25 pages, 5456 KB  
Article
Optimized Hot Pressing of High-Speed Steel–Bronze Composites for Diamond-Reinforced Tool Applications
by Filip Průša, Andrzej Romański, Marzanna Książek, Hana Thürlová, Dorota Tyrała, Petr Kratochvíl, Janusz Konstanty, Ilona Voňavková, František Růžička, Jan Riedl, Robert Dąbrowski, Krzysztof Sołek, Jan Pokorný and Lucyna Jaworska
Materials 2025, 18(17), 3999; https://doi.org/10.3390/ma18173999 - 26 Aug 2025
Viewed by 601
Abstract
This study investigates the optimization of hot-pressing parameters for ASP60 high-speed steel composites incorporating CuSn20 bronze alloy for use in diamond-reinforced tool applications. ASP60 and CuSn20 powders were characterized using XRD, XRF, DSC, SEM, and laser diffraction. The effects of CuSn20 addition at [...] Read more.
This study investigates the optimization of hot-pressing parameters for ASP60 high-speed steel composites incorporating CuSn20 bronze alloy for use in diamond-reinforced tool applications. ASP60 and CuSn20 powders were characterized using XRD, XRF, DSC, SEM, and laser diffraction. The effects of CuSn20 addition at varying concentrations and compaction temperatures (950–1050 °C) on porosity, mechanical properties, and tribological performance were evaluated. Results showed that adding CuSn20 significantly reduced residual porosity due to its partial melting during compaction, which facilitated particle rearrangement and densification. Optimal conditions were identified at 1050 °C with 9.8 wt.% CuSn20, yielding minimal porosity (~3.7%) and the highest bending strength (374.51 ± 36.73 MPa). The optimized matrix was further reinforced with TiC-coated diamond particles at concentration c = 20, producing a composite material with excellent wear resistance, despite minor defects in the TiC coating observed on fracture surfaces. Tribological testing demonstrated that CuSn20 consistently lowered friction coefficients across all tested temperatures due to its self-lubricating properties and partial melting at elevated temperatures. Furthermore, ASP60 exhibited no measurable wear, making it a promising candidate for highly demanding applications. Overall, the study demonstrates that CuSn20 alloy enhances densification, mechanical performance, and tribological behavior of ASP60-based composites, indicating their strong potential for aggressive wire sawing and stone-cutting tool applications. Full article
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30 pages, 9001 KB  
Article
Laser-Induced Graphene on Biocompatible PDMS/PEG Composites for Limb Motion Sensing
by Anđela Gavran, Marija V. Pergal, Teodora Vićentić, Milena Rašljić Rafajilović, Igor A. Pašti, Marko V. Bošković and Marko Spasenović
Sensors 2025, 25(17), 5238; https://doi.org/10.3390/s25175238 - 22 Aug 2025
Viewed by 1238
Abstract
The advancement of laser-induced graphene (LIG) has significantly enhanced the development of wearable and flexible electronic devices. Due to its exceptional physical, chemical, and electronic properties, LIG has emerged as a highly effective active material for wearable sensors. However, despite the wide range [...] Read more.
The advancement of laser-induced graphene (LIG) has significantly enhanced the development of wearable and flexible electronic devices. Due to its exceptional physical, chemical, and electronic properties, LIG has emerged as a highly effective active material for wearable sensors. However, despite the wide range of materials suitable as precursors for LIG, the scarcity of stretchable and biocompatible polymers amenable to laser graphenization has remained a persistent challenge. In this study, laser-induced graphene (LIG) was fabricated directly on biocompatible and flexible cross-linked PDMS/PEG (with Mn (PEG) = 400 g/mol) composites for the first time, enabling their application in wearable sensors. The addition of PEG compensates for the low carbon content in PDMS, enabling efficient laser graphenization. Laser parameters were systematically optimized to achieve high-quality graphene, and a comprehensive characterization with varying PEG content (10–40 wt.%) was conducted using multiple analytical techniques. Tensile tests revealed that incorporating PEG significantly enhanced elongation at break, reaching 237% for PDMS/40 wt.% PEG while reducing Young’s modulus to 0.25 MPa, highlighting the excellent flexibility of the substrate material. Surface analysis using X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), and Raman spectroscopy demonstrated the formation of high-quality few-layer graphene with the fewest defects in PDMS/40 wt.% PEG composites. Nevertheless, the adhesion of electrical contacts to LIG that was directly induced on PDMS/PEG proved to be challenging. To overcome this challenge, we produced devices by means of laser induction on polyimide and transfer to PDMS/PEG. We demonstrate the practical utility of such devices by applying them to monitor limb motion in real time. The sensor showed a stable and repeatable piezoresistive response under multiple bending cycles. These results provide valuable insights into the fabrication of biocompatible LIG-based flexible sensors, paving the way for their broader implementation in medical and sports technologies. Full article
(This article belongs to the Special Issue Materials and Devices for Flexible Electronics in Sensor Applications)
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12 pages, 951 KB  
Article
Fundus Blood Flow in Patients with Sellar Lesions with Optic Nerve Bending and Chiasmal Compression
by Yoichiro Shinohara, Rei Yamaguchi, Masahiko Tosaka, Soichi Oya and Hideo Akiyama
J. Clin. Med. 2025, 14(16), 5790; https://doi.org/10.3390/jcm14165790 - 15 Aug 2025
Viewed by 506
Abstract
Background/objectives: Optic nerve bending and chiasmal compression impair vision in patients with sellar lesions; however, their effect on optic nerve head (ONH) blood flow remains unclear. This study used laser speckle flowgraphy to examine the relationship between clinical features and ONH blood [...] Read more.
Background/objectives: Optic nerve bending and chiasmal compression impair vision in patients with sellar lesions; however, their effect on optic nerve head (ONH) blood flow remains unclear. This study used laser speckle flowgraphy to examine the relationship between clinical features and ONH blood flow in patients with optic nerve bending and chiasmal compression. Methods: This retrospective study included 32 eyes (16 eyes with and 16 without optic nerve bending on the contralateral side) from 16 patients with sellar lesions. The best-corrected visual acuity (BCVA), simple visual field impairment score (SVFIS), optic nerve head mean blur rate (ONH-MBR), and six-segmented macular ganglion cell layer + inner plexiform layer (GCL + IPL) thickness were examined. Results: Preoperative BCVA and SVFIS in eyes with optic nerve bending were significantly worse than those in eyes without bending, and significantly correlated with the optic nerve-canal bending angle (ONCBA). After tumor resection, BCVA and SVFIS significantly improved in both groups. Preoperative ONH-MBR was significantly lower in bending eyes but increased significantly post-treatment in both groups. Preoperative ONH-MBR correlated with ONCBA, while postoperative ONH-MBR correlated with nasal GCL + IPL thickness. Conclusions: Optic nerve bending and chiasmal compression showed reduced blood flow to the ONH. These changes in blood flow may be associated with GCL + IPL thickness and optic nerve bending angle. Full article
(This article belongs to the Special Issue New Advances in Optic Nerve Diseases)
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19 pages, 4202 KB  
Article
Effect of Plate Thickness on Residual Stress Distribution of GH3039 Superalloy Subjected to Laser Shock Peening
by Yandong Ma, Maozhong Ge and Yongkang Zhang
Materials 2025, 18(15), 3682; https://doi.org/10.3390/ma18153682 - 5 Aug 2025
Viewed by 410
Abstract
To accurately assess the effect of different plate thicknesses on the residual stress field of laser shock peened GH3039 superalloy, residual stress measurements were performed on GH3039 alloy plates with thicknesses of 2 mm and 5 mm after laser shock peening (LSP) treatment. [...] Read more.
To accurately assess the effect of different plate thicknesses on the residual stress field of laser shock peened GH3039 superalloy, residual stress measurements were performed on GH3039 alloy plates with thicknesses of 2 mm and 5 mm after laser shock peening (LSP) treatment. Both quasi-static and high strain rate mechanical tests of GH3039 were conducted, and the Johnson-Cook (J-C) constitutive equation for GH3039 alloy at specific strain rates was fitted based on the experimental results. To obtain the parameter C in the J-C constitutive equation of GH3039 alloy under ultra-high strain rates, a modified method was proposed based on LSP experiment and finite element simulation results. Using the modified GH3039 alloy J-C constitutive equation, numerical simulations and comparative analyses of the residual stress field of GH3039 alloy plates of different thicknesses under LSP were carried out using ABAQUS software. The simulated residual stress fields of laser-shocked GH3039 alloy plates of different thicknesses were in good agreement with the experimental measurements, indicating that the modified GH3039 alloy J-C constitutive equation can accurately predict the mechanical behavior of GH3039 alloy under ultra-high strain rates. Based on the modified GH3039 alloy J-C constitutive equation, the effect of different plate thicknesses on the residual stress distribution of laser-shocked GH3039 alloy was studied, along with the underlying mechanisms. The unique distribution characteristics of residual stresses in laser-shocked GH3039 plates with varying thicknesses are primarily attributed to differences in plate bending stiffness and the detrimental coupling effects of reflected tensile waves. Full article
(This article belongs to the Section Metals and Alloys)
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17 pages, 4711 KB  
Article
Empirical Investigation of the Structural Response of Super-Span Soil–Steel Arches During Backfilling
by Bartłomiej Kunecki
Materials 2025, 18(15), 3650; https://doi.org/10.3390/ma18153650 - 3 Aug 2025
Viewed by 537
Abstract
This paper presents field investigations of a corrugated steel soil–steel arch structure with a span of 25.7 m and a rise of 9.0 m—currently the largest single-span structure of its kind in Europe. The structure, serving as a wildlife crossing along the DK16 [...] Read more.
This paper presents field investigations of a corrugated steel soil–steel arch structure with a span of 25.7 m and a rise of 9.0 m—currently the largest single-span structure of its kind in Europe. The structure, serving as a wildlife crossing along the DK16 expressway in northeastern Poland, was constructed using deep corrugated steel plates (500 mm× 237 mm) made from S315MC steel, without additional reinforcements such as stiffening ribs or geosynthetics. The study focused on monitoring the structural behavior during the critical backfilling phase. Displacements and strains were recorded using 34 electro-resistant strain gauges and a geodetic laser system at successive backfill levels, with particular attention to the loading stage at the crown. The measured results were compared with predictions based on the Swedish Design Method (SDM). The SDM equations did not accurately predict internal forces during backfilling. At the crown level, bending moments and axial forces were overestimated by approximately 69% and 152%, respectively. At the final backfill level, the SDM underestimated bending moments by 55% and overestimated axial forces by 90%. These findings highlight limitations of current design standards and emphasize the need for revised analytical models and long-term monitoring of large-span soil–steel structures. Full article
(This article belongs to the Section Construction and Building Materials)
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14 pages, 3905 KB  
Article
Stability of Ultrafast Laser-Induced Stress in Fused Silica and Ultra-Low Expansion Glass
by Carolyn C. Hokin and Brandon D. Chalifoux
Photonics 2025, 12(8), 778; https://doi.org/10.3390/photonics12080778 - 1 Aug 2025
Viewed by 1221
Abstract
Stress fields imparted with an ultrafast laser can correct low spatial frequency surface figure error of mirrors through ultrafast laser stress figuring (ULSF): the formation of nanograting structures within the bulk substrate generates localized stress, creating bending moments that equilibrize via wafer deformation. [...] Read more.
Stress fields imparted with an ultrafast laser can correct low spatial frequency surface figure error of mirrors through ultrafast laser stress figuring (ULSF): the formation of nanograting structures within the bulk substrate generates localized stress, creating bending moments that equilibrize via wafer deformation. For ULSF to be used as an optical figuring process, the ultrafast laser generated stress must be effectively permanent or risk unwanted figure drift. Two isochronal annealing experiments were performed to measure ultrafast laser-generated stress stability in fused silica and Corning ultra-low expansion (ULE) wafers. The first experiment tracked changes to induced astigmatism up to 1000 °C on 25.4 mm-diameter wafers. Only small changes were measured after each thermal cycle up to 500 °C for both materials, but significant changes were observed at higher temperatures. The second experiment tracked stress changes in fused silica and ULE up to 500 °C but with 4 to 16× higher signal-to-noise ratio. Change in trefoil on 100 mm-diameter wafers was measured, and the induced stress in fused silica and ULE was found to be stable after thermal cycling up to 300 °C and 200 °C, respectively, with larger changes at higher temperatures. Full article
(This article belongs to the Special Issue Advances in Ultrafast Laser Science and Applications)
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17 pages, 4992 KB  
Article
Effect of Heat Treatments and Related Microstructural Modifications on High-Cycle Fatigue Behavior of Powder Bed Fusion–Laser Beam-Fabricated Ti-6Al-2Sn-4Zr-6Mo Alloy
by Gianluca Pirro, Alessandro Morri, Alessandra Martucci, Mariangela Lombardi and Lorella Ceschini
Metals 2025, 15(8), 849; https://doi.org/10.3390/met15080849 - 29 Jul 2025
Viewed by 423
Abstract
The study investigates the influence of microstructures on fatigue behavior and failure mechanisms of the α-β titanium alloy Ti6246, fabricated via Powder Bed Fusion-Laser Beam (PBF-LB). In particular, the investigation assesses the effect of two post-processing heat treatments, namely α-β annealing at 875 [...] Read more.
The study investigates the influence of microstructures on fatigue behavior and failure mechanisms of the α-β titanium alloy Ti6246, fabricated via Powder Bed Fusion-Laser Beam (PBF-LB). In particular, the investigation assesses the effect of two post-processing heat treatments, namely α-β annealing at 875 °C (AN875) and solution treatment at 825 °C followed by aging at 500 °C (STA825), on the alloy’s rotating and bending fatigue behavior. The results indicate that the STA825 condition provides superior fatigue resistance (+25%) compared to AN875, due to the presence of a finer bilamellar microstructure, characterized by thinner primary α lamellae (αp) and a more homogeneous distribution of secondary α lamellae (αs) within the β matrix. Additionally, an investigation conducted using the Kitagawa–Takahashi (KT) approach and the El-Haddad model, based on the relationship between the fatigue limit and defect sensitivity, revealed improved crack propagation resistance from pre-existing defects (ΔKth) for the STA825 condition compared to AN875. Notably, the presence of fine αs after aging for STA825 is effective in delaying crack nucleation and propagation at early stages, while refined αp contributes to hindering macrocrack growth. The fatigue behavior of the STA825-treated Ti6246 alloy was even superior to that of the PBF-LB-processed Ti64, representing a viable alternative for the production of high-performance components in the automotive and aerospace sectors. Full article
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16 pages, 10306 KB  
Article
Fabrication and Characterization of Flexible pH Sensors Based on Pulsed Laser-Ablated Graphene/MoS2 Interdigitated Electrodes
by Zhaochi Chen, Chengche Liu and Minh-Quang Tran
Nanomaterials 2025, 15(14), 1115; https://doi.org/10.3390/nano15141115 - 18 Jul 2025
Viewed by 944
Abstract
Point-of-care (POC) diagnostic technologies have become essential for the real-time monitoring and management of chronic wounds, where maintaining a moist environment and controlling pH levels are critical for effective healing. In this study, a flexible pH sensor based on a graphene/molybdenum disulfide (graphene/MoS [...] Read more.
Point-of-care (POC) diagnostic technologies have become essential for the real-time monitoring and management of chronic wounds, where maintaining a moist environment and controlling pH levels are critical for effective healing. In this study, a flexible pH sensor based on a graphene/molybdenum disulfide (graphene/MoS2) composite interdigitated electrode (IDE) structure was fabricated using pulsed laser ablation. The pH sensor, with an active area of 30 mm × 30 mm, exhibited good adhesion to the polyethylene terephthalate (PET) substrate and maintained structural integrity under repeated bending cycles. Precise ablation was achieved under optimized conditions of 4.35 J/cm2 laser fluence, a repetition rate of 300 kHz, and a scanning speed of 500 mm/s, enabling the formation of defect-free IDE arrays without substrate damage. The influence of laser processing parameters on the surface morphology, electrical conductivity, and wettability of the composite thin films was systematically characterized. The fabricated pH sensor exhibited high sensitivity (~4.7% change in current per pH unit) across the pH 2–10 range, rapid response within ~5.2 s, and excellent mechanical stability under 100 bending cycles with negligible performance degradation. Moreover, the sensor retained > 95% of its stable sensitivity after 7 days of ambient storage. Furthermore, the pH response behavior was evaluated for electrode structures with different pitches, demonstrating that structural design parameters critically impact sensing performance. These results offer valuable insights into the scalable fabrication of flexible, wearable pH sensors, with promising applications in wound monitoring and personalized healthcare systems. Full article
(This article belongs to the Special Issue Laser-Based Nano Fabrication and Nano Lithography: Second Edition)
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15 pages, 4749 KB  
Article
Selective Laser Melting of a Ti-6Al-4V Lattice-Structure Gear: Design, Topology Optimization, and Experimental Validation
by Riad Ramadani, Snehashis Pal, Aleš Belšak and Jožef Predan
Appl. Sci. 2025, 15(14), 7949; https://doi.org/10.3390/app15147949 - 17 Jul 2025
Viewed by 707
Abstract
The manufacture of lightweight components is one of the most important requirements in the automotive and aerospace industries. Gears, on the other hand, are among the heaviest parts in terms of their total weight. Accordingly, a spur gear was considered, the body of [...] Read more.
The manufacture of lightweight components is one of the most important requirements in the automotive and aerospace industries. Gears, on the other hand, are among the heaviest parts in terms of their total weight. Accordingly, a spur gear was considered, the body of which was configured as a lattice structure to make it lightweight. In addition, the structure was optimized by topology optimization using ProTOP software. Subsequently, the gear was manufactured by a selective laser melting process by using a strong and lightweight material, namely Ti-6Al-4V. This study defeated the problems of manufacturing orientation, surface roughness, support structure, and bending due to the high thermal gradient in the selective laser melting process. To experimentally investigate the benefits of such a lightweight gear body structure, a new test rig with a closed loop was developed. This rig enabled measurements of strains in the gear ring, hub, and tooth root. The experimental results confirmed that a specifically designed and selectively laser-melted, lightweight cellular lattice structure in the gear body can significantly influence strain. This is especially significant with respect to strain levels and their time-dependent variations in the hub section of the gear body. Full article
(This article belongs to the Section Additive Manufacturing Technologies)
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29 pages, 7799 KB  
Article
Substrate Flexibility and Metal Deposition Method Effects on Piezoelectric-Enhanced SERS in Metal–ZnO Nanorod Nanocomposites
by Nguyen Thi Quynh Nhu, Le Tran Thanh Thi, Le Vu Tuan Hung and Vincent K. S. Hsiao
Materials 2025, 18(14), 3299; https://doi.org/10.3390/ma18143299 - 13 Jul 2025
Viewed by 665
Abstract
This study investigates the effects of substrate flexibility and metal deposition methods on piezoelectric-enhanced Surface-Enhanced Raman Scattering (SERS) in metal-deposited ZnO nanorod (NR) nanocomposites (NCPs). ZnO NRs were grown on both rigid (ITO–glass) and flexible (ITO-PET) substrates, followed by gold (Au) deposition by [...] Read more.
This study investigates the effects of substrate flexibility and metal deposition methods on piezoelectric-enhanced Surface-Enhanced Raman Scattering (SERS) in metal-deposited ZnO nanorod (NR) nanocomposites (NCPs). ZnO NRs were grown on both rigid (ITO–glass) and flexible (ITO-PET) substrates, followed by gold (Au) deposition by pulsed-laser-induced photolysis (PLIP) or silver (Ag) deposition by thermal evaporation. Structural analysis revealed that ZnO NRs on flexible substrates exhibited smaller diameters (60–80 nm vs. 80–100 nm on glass), a higher density, and diverse orientations that enhanced piezoelectric responsiveness. Optical characterization showed distinct localized surface plasmon resonance (LSPR) peaks at 420 nm for Ag and 525 nm for Au systems. SERS measurements demonstrated that Ag-ZnO NCPs achieved superior detection limits (10−9 M R6G) with enhancement factors of 108–109, while Au-ZnO NCPs reached 10−8 M detection limits. Mechanical bending of flexible substrates induced dramatic signal enhancement (50–100-fold for Au-ZnO/PET and 2–3-fold for Ag-ZnO/PET), directly confirming piezoelectric enhancement mechanisms. This work establishes quantitative structure–property relationships in piezoelectric-enhanced SERS and provides design principles for high-performance flexible sensors. Full article
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24 pages, 5782 KB  
Article
Gamma Irradiation-Induced Synthesis of Nano Au-PNiPAAm/PVA Bi-Layered Photo-Thermo-Responsive Hydrogel Actuators with a Switchable Bending Motion
by Nikolina Radojković, Jelena Spasojević, Ivana Vukoje, Zorica Kačarević-Popović, Una Stamenović, Vesna Vodnik, Goran Roglić and Aleksandra Radosavljević
Polymers 2025, 17(13), 1774; https://doi.org/10.3390/polym17131774 - 26 Jun 2025
Viewed by 658
Abstract
In this study, we present bi-layered hydrogel systems that incorporate different sizes and shapes of gold nanoparticles (nanospheres and nanorods) for potential use in areas such as photoactuators, soft robotics, artificial muscles, drug delivery and tissue engineering. The synthesized nano Au-PNiPAAm/PVA bi-layered hydrogel [...] Read more.
In this study, we present bi-layered hydrogel systems that incorporate different sizes and shapes of gold nanoparticles (nanospheres and nanorods) for potential use in areas such as photoactuators, soft robotics, artificial muscles, drug delivery and tissue engineering. The synthesized nano Au-PNiPAAm/PVA bi-layered hydrogel nanocomposites provide the unique ability to exhibit controlled motion upon light exposure, indicating that the above systems possess the capability of photo–thermal energy conversion. The chosen synthesis approach is a combination of chemical production of gold nanoparticles (AuNPs) followed by gamma radiation formation of crosslinked polymer networks around them, as the final step, which also allows for sterilization in a single technological step. According to the TEM analysis, the gold nanospheres (AuNSs) with mean diameters of around 17 and 30 nm, as well as nanorods (AuNRs) with an aspect ratio of around 4.5, were synthesized and used as nanofillers in the formation of nanocomposites. Their stability within the polymer matrix was confirmed by UV–Vis spectral studies, by the presence of local surface plasmon resonance (LSPR) bands, typical for nanoparticles of various shapes and sizes. Morphological studies (FE-SEM) of hydrogels revealed the formation of a porous structure with PNiPAAm hydrogel as an active layer and PVA hydrogel as a passive layer, as well as a stable interfacial layer with a thickness of around 80 μm. The synthesized bi-layered photoactuators showed a photo–thermal response upon exposure to irradiation of green lasers and lamps that simulate sunlight, resulting in bending motion. This bending response reveals the huge potential of the obtained materials as soft actuators, which are more flexible than rigid systems, making them effective for specific applications where controlled movement and flexibility are essential. Full article
(This article belongs to the Special Issue Polymer Hydrogels: Synthesis, Properties and Applications)
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