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Keywords = gradient fracture mechanics

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14 pages, 2941 KiB  
Article
Experimental and Numerical Investigation of the Mechanical Properties of ABS Parts Fabricated via Fused Deposition Modeling
by Yanqin Li, Peihua Zhu and Dehai Zhang
Polymers 2025, 17(14), 1957; https://doi.org/10.3390/polym17141957 - 17 Jul 2025
Viewed by 328
Abstract
This study investigates the mechanical properties of ABS parts fabricated via used deposition modeling (FDM) through integrated experimental and numerical approaches. ABS resin was used as the experimental material, and tensile tests were conducted using a universal testing machine. Finite element analysis (FEA) [...] Read more.
This study investigates the mechanical properties of ABS parts fabricated via used deposition modeling (FDM) through integrated experimental and numerical approaches. ABS resin was used as the experimental material, and tensile tests were conducted using a universal testing machine. Finite element analysis (FEA) was performed via ANSYS 2021 to simulate stress deformation behavior, with key parameters including a gauge length of 10 mm (pre-stretching) and printing temperature gradients. The results show that the specimen exhibited a maximum tensile force of 7.3 kN, upper yield force of 3.7 kN, and lower yield force of 3.2 kN, demonstrating high strength and toughness. The non-proportional elongation reached 0.06 (6%), and the quantified enhancement multiple of AM relative to traditional manufacturing was 1.1, falling within the reasonable range for glass fiber-reinforced or specially formulated ABS. FEA results validated the experimental data, showing that the material underwent 15 mm of plastic deformation before fracture, consistent with ABS’s ductile characteristics. Full article
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20 pages, 4487 KiB  
Article
Coupled Productivity Prediction Model for Multi-Stage Fractured Horizontal Wells in Low-Permeability Reservoirs Considering Threshold Pressure Gradient and Stress Sensitivity
by Long Xiao, Ping Yue, Hongnan Yang, Wei Guo, Simin Qu, Hui Yao and Lingqiang Meng
Energies 2025, 18(14), 3654; https://doi.org/10.3390/en18143654 - 10 Jul 2025
Viewed by 251
Abstract
Multi-stage fractured horizontal wells (MSFHWs) represent a crucial development approach for low-permeability reservoirs, where accurate productivity prediction is essential for production operations. However, existing models suffer from limitations such as inadequate characterization of complex flow mechanisms within the reservoir or computational complexity. This [...] Read more.
Multi-stage fractured horizontal wells (MSFHWs) represent a crucial development approach for low-permeability reservoirs, where accurate productivity prediction is essential for production operations. However, existing models suffer from limitations such as inadequate characterization of complex flow mechanisms within the reservoir or computational complexity. This study subdivides the flow process into three segments: matrix, fracture, and wellbore. By employing discretization concepts, potential distribution theory, and the principle of potential superposition, a productivity prediction model tailored for MSFHWs in low-permeability reservoirs is established. Moreover, this model provides a clearer characterization of fluid seepage processes during horizontal well production, which aligns more closely with the actual production process. Validated against actual production data from an offshore oilfield and benchmarked against classical models, the proposed model demonstrates satisfactory accuracy and reliability. Sensitivity analysis reveals that a lower Threshold Pressure Gradient (TPG) corresponds to higher productivity; a production pressure differential of 10 MPa yields an average increase of 22.41 m3/d in overall daily oil production compared to 5 MPa, concurrently reducing the overall production decline rate by 26.59% on average. Larger stress-sensitive coefficients lead to reduced production, with the fracture stress-sensitive coefficient exerting a more significant influence; for an equivalent increment, the matrix stress-sensitive coefficient causes a production decrease of 1.92 m3/d (a 4.32% decline), while the fracture stress-sensitive coefficient results in a decrease of 4.87 m3/d (a 20.93% decline). Increased fracture half-length and number enhance production, with an initial productivity increase of 21.61% (gradually diminishing to 7.1%) for longer fracture half-lengths and 24.63% (gradually diminishing to 5.22%) for more fractures; optimal critical values exist for both parameters. Full article
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22 pages, 6042 KiB  
Article
Critical Threshold for Fluid Flow Transition from Linear to Nonlinear in Self-Affine Rough-Surfaced Rock Fractures: Effects of Shear and Confinement
by Hai Pu, Yanlong Chen, Kangsheng Xue, Shaojie Zhang, Xuefeng Han and Junce Xu
Processes 2025, 13(7), 1991; https://doi.org/10.3390/pr13071991 - 24 Jun 2025
Viewed by 334
Abstract
Understanding nonlinear fluid flow in fractured rocks is critical for various geoengineering and geosciences. This study investigates the evolution of seepage behavior under varying fracture surface roughness, confining pressures, and shear displacements. A total of four sandstone fracture specimens were prepared using controlled [...] Read more.
Understanding nonlinear fluid flow in fractured rocks is critical for various geoengineering and geosciences. This study investigates the evolution of seepage behavior under varying fracture surface roughness, confining pressures, and shear displacements. A total of four sandstone fracture specimens were prepared using controlled splitting techniques, with surface morphology quantified by Joint Roughness Coefficient (JRC) values ranging from 2.8 to 17.7. Triaxial seepage tests were conducted under four confining pressures (3–9 MPa) and four shear displacements (0–1.5 mm). Experimental results reveal that permeability remains stable under low hydraulic gradients but transitions to nonlinear regimes as the flow rate increases, accompanied by significant energy loss and deviation from the cubic law. The onset of nonlinearity occurs earlier with higher roughness, stress, and displacement. A critical hydraulic gradient Jc was introduced to define the threshold at which inertial effects dominate. Forchheimer’s equation was employed to model nonlinear flow, and empirical regression models were developed to predict coefficients A, B, and Jc using hydraulic aperture and JRC as input variables. These models demonstrated high accuracy (R2 > 0.92). This work provides theoretical insights and predictive approaches for assessing nonlinear fluid transport in rock fracture. Future research will address mechanical–hydraulic coupling and incorporate additional factors such as scale effects and flow anisotropy. Full article
(This article belongs to the Special Issue Recent Developments in Enhanced Oil Recovery (EOR) Processes)
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21 pages, 4887 KiB  
Article
The Formation Mechanisms of Ultra-Deep Effective Clastic Reservoir and Oil and Gas Exploration Prospects
by Yukai Qi, Zongquan Hu, Jingyi Wang, Fushun Zhang, Xinnan Wang, Hanwen Hu, Qichao Wang and Hanzhou Wang
Appl. Sci. 2025, 15(13), 6984; https://doi.org/10.3390/app15136984 - 20 Jun 2025
Viewed by 413
Abstract
This study systematically analyzes reservoir formation mechanisms under deep burial conditions, integrating macroscopic observations from representative ultra-deep clastic reservoirs in four major sedimentary basins in central and western China. Developing effective clastic reservoirs in ultra-deep strata (6000–8000 m) remains a critical yet debated [...] Read more.
This study systematically analyzes reservoir formation mechanisms under deep burial conditions, integrating macroscopic observations from representative ultra-deep clastic reservoirs in four major sedimentary basins in central and western China. Developing effective clastic reservoirs in ultra-deep strata (6000–8000 m) remains a critical yet debated topic in petroleum geology. Recent advances in exploration techniques and geological understanding have challenged conventional views, confirming the presence of viable clastic reservoirs at such depths. Findings reveal that reservoir quality in ultra-deep strata is preserved and enhanced through the interplay of sedimentary, diagenetic, and tectonic processes. Key controlling factors include (1) high-energy depositional environments promoting primary porosity development, (2) proximity to hydrocarbon source rocks enabling multi-phase hydrocarbon charging, (3) overpressure and low geothermal gradients reducing cementation and compaction, and (4) late-stage tectonic fracturing that significantly improves permeability. Additionally, dissolution porosity and fracture networks formed during diagenetic and tectonic evolution collectively enhance reservoir potential. The identification of favorable reservoir zones under the sedimentation–diagenesis-tectonics model provides critical insights for future hydrocarbon exploration in ultra-deep clastic sequences. Full article
(This article belongs to the Special Issue Advances in Reservoir Geology and Exploration and Exploitation)
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35 pages, 8248 KiB  
Article
Pre-Failure Deformation Response and Dilatancy Damage Characteristics of Beishan Granite Under Different Stress Paths
by Yang Han, Dengke Zhang, Zheng Zhou, Shikun Pu, Jianli Duan, Lei Gao and Erbing Li
Processes 2025, 13(6), 1892; https://doi.org/10.3390/pr13061892 - 15 Jun 2025
Viewed by 344
Abstract
Different from general underground engineering, the micro-damage prior to failure of the surrounding rock has a significant influence on the geological disposal of high-level radioactive waste. However, the quantitative research on pre-failure dilatancy damage characteristics and stress path influence of hard brittle rocks [...] Read more.
Different from general underground engineering, the micro-damage prior to failure of the surrounding rock has a significant influence on the geological disposal of high-level radioactive waste. However, the quantitative research on pre-failure dilatancy damage characteristics and stress path influence of hard brittle rocks under high stress levels is insufficient currently, and especially, the stress path under simultaneous unloading of axial and confining pressures is rarely discussed. Therefore, three representative mechanical experimental studies were conducted on the Beishan granite in the pre-selected area for high-level radioactive waste (HLW) geological disposal in China, including increasing axial pressure with constant confining pressure (path I), increasing axial pressure with unloading confining pressure (path II), and simultaneous unloading of axial and confining pressures (path III). Using the deviatoric stress ratio as a reference, the evolution laws and characteristics of stress–strain relationships, deformation modulus, generalized Poisson’s ratio, dilatancy index, and dilation angle during the path bifurcation stage were quantitatively analyzed and compared. The results indicate that macro-deformation and the plastic dilatancy process exhibit strong path dependency. The critical value and growth gradient of the dilatancy parameter for path I are both the smallest, and the suppressive effect of the initial confining pressure is the most significant. The dilation gradient of path II is the largest, but the degree of dilatancy before the critical point is the smallest due to its susceptibility to fracture. The critical values of the dilatancy parameters for path III are the highest and are minimally affected by the initial confining pressure, indicating the most significant dilatancy properties. Establish the relationship between the deformation parameters and the crack-induced volumetric strain and define the damage variable accordingly. The critical damage state and the damage accumulation process under various stress paths were examined in detail. The results show that the damage evolution is obviously differentiated with the bifurcation of the stress paths, and three different types of damage curve clusters are formed, indicating that the damage accumulation path is highly dependent on the stress path. The research findings quantitatively reveal the differences in deformation response and damage characteristics of Beishan granite under varying stress paths, providing a foundation for studying the nonlinear mechanical behavior and damage failure mechanisms of hard brittle rock under complex loading conditions. Full article
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23 pages, 11820 KiB  
Article
High-Speed Nanoindentation and Local Residual Stress Analysis for Cut Edge Damage in Complex Phase Steels for Automotive Applications
by Laia Ortiz-Membrado, Sergi Parareda, Daniel Casellas, Emilio Jiménez-Piqué and Antonio Mateo
Metals 2025, 15(6), 651; https://doi.org/10.3390/met15060651 - 11 Jun 2025
Viewed by 1140
Abstract
Advanced high-strength steels (AHSSs) are used as lightweight solutions for vehicles, mainly focusing on the Body-in-White. However, the implementation of such steels for chassis parts requires a profound knowledge of the key design parameters for these components, particularly those concerning fatigue performance. Manufacturing [...] Read more.
Advanced high-strength steels (AHSSs) are used as lightweight solutions for vehicles, mainly focusing on the Body-in-White. However, the implementation of such steels for chassis parts requires a profound knowledge of the key design parameters for these components, particularly those concerning fatigue performance. Manufacturing of chassis parts include mechanical cutting operations. Therefore, the deformation and damage induced at the cut edge may affect the fatigue resistance of the parts in service. To characterize and study this critical area, damage and micromechanical properties have been evaluated at the cut edge for three different AHSS grades, CP800, CP980, and DP600, analyzing the impact of cutting parameters and post-processing treatments, such as sandblasting. Large high-speed nanoindentation maps of 400 × 200 µm2 have been carried out along the cut edge in the three different target zones: burnish, fracture, and burr. In the hardness maps, the deformation lines and the gradient of hardness with increasing distance from the cut edge are perfectly observed. Residual stresses at the target zones of the cut edges were measured using the FIB-DIC method for CP980 to complement the micromechanical study in these critical areas. The results found show that reduced cutting clearance leads to larger hardened zones and favorable compressive stress distributions, correlating with improved fatigue resistance. Hardened zones extending up to 100 µm from the cut edge and compressive residual stresses exceeding −300 MPa were observed at low clearance. These findings are consistent with numerical simulations and previous fatigue tests, highlighting the potential of combining high-speed nanoindentation and local stress analysis for optimizing shear cutting processes in AHSS components. Full article
(This article belongs to the Special Issue Microstructure and Mechanical Behavior of High-Strength Steel)
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18 pages, 1390 KiB  
Article
Durability and Mechanical Analysis of Basalt Fiber Reinforced Metakaolin–Red Mud-Based Geopolymer Composites
by Ouiame Chakkor
Buildings 2025, 15(12), 2010; https://doi.org/10.3390/buildings15122010 - 11 Jun 2025
Viewed by 497
Abstract
Cement is widely used as the primary binder in concrete; however, growing environmental concerns and the rapid expansion of the construction industry have highlighted the need for more sustainable alternatives. Geopolymers have emerged as promising eco-friendly binders due to their lower carbon footprint [...] Read more.
Cement is widely used as the primary binder in concrete; however, growing environmental concerns and the rapid expansion of the construction industry have highlighted the need for more sustainable alternatives. Geopolymers have emerged as promising eco-friendly binders due to their lower carbon footprint and potential to utilize industrial byproducts. Geopolymer mortar, like other cementitious substances, exhibits brittleness and tensile weakness. Basalt fibers serve as fracture-bridging reinforcements, enhancing flexural and tensile strength by redistributing loads and postponing crack growth. Basalt fibers enhance the energy absorption capacity of the mortar, rendering it less susceptible to abrupt collapse. Basalt fibers have thermal stability up to about 800–1000 °C, rendering them appropriate for geopolymer mortars designed for fire-resistant or high-temperature applications. They assist in preserving structural integrity during heat exposure. Fibers mitigate early-age microcracks resulting from shrinkage, drying, or heat gradients. This results in a more compact and resilient microstructure. Using basalt fibers improves surface abrasion and impact resistance, which is advantageous for industrial flooring or infrastructure applications. Basalt fibers originate from natural volcanic rock, are non-toxic, and possess a minimal ecological imprint, consistent with the sustainability objectives of geopolymer applications. This study investigates the mechanical and thermal performance of a geopolymer mortar composed of metakaolin and red mud as binders, with basalt powder and limestone powder replacing traditional sand. The primary objective was to evaluate the effect of basalt fiber incorporation at varying contents (0.4%, 0.8%, and 1.2% by weight) on the durability and strength of the mortar. Eight different mortar mixes were activated using sodium hydroxide (NaOH) and sodium silicate (Na2SiO3) solutions. Mechanical properties, including compressive strength, flexural strength, and ultrasonic pulse velocity (UPV), were tested 7 and 28 days before and after exposure to elevated temperatures (200, 400, 600, and 800 °C). The results indicated that basalt fiber significantly enhanced the performance of the geopolymer mortar, particularly at a content of 1.2%. Specimens with 1.2% fiber showed up to 20% improvement in compressive strength and 40% in flexural strength after thermal exposure, attributed to the fiber’s role in microcrack bridging and structural densification. Subsequent research should concentrate on refining fiber type, dose, and dispersion techniques to improve mechanical performance and durability. Examinations of microstructural behavior, long-term durability under environmental settings, and performance following high-temperature exposure are crucial. Furthermore, investigations into hybrid fiber systems, extensive structural applications, and life-cycle evaluations will inform the practical and sustainable implementation in the buildings. Full article
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25 pages, 5915 KiB  
Article
Experimental Study on the Effect of Fractures on the Irreducible and Movable Water in Water-Bearing Tight Sandstone Gas Reservoirs
by Aiguo Hu, Li Su, Gang Cao, Zhuo Luo, Changhui Yan and Qing Chen
Processes 2025, 13(6), 1685; https://doi.org/10.3390/pr13061685 - 27 May 2025
Viewed by 437
Abstract
Hydraulic fracturing significantly impacts water production. This makes it crucial to determine whether its effects on formation water production are beneficial or detrimental in complex reservoir stimulations. This paper gives the influence that acts on pore structure variations and irreducible water transformation by [...] Read more.
Hydraulic fracturing significantly impacts water production. This makes it crucial to determine whether its effects on formation water production are beneficial or detrimental in complex reservoir stimulations. This paper gives the influence that acts on pore structure variations and irreducible water transformation by hydraulic fracturing; by using NMR and Micro-CT, pore-throat reconfiguration in core samples induced fracturing. Two main pore variation types were identified from CT images. To analyze the gas–water flow mechanisms in pre-fracturing and post-fracturing reservoir conditions, we tested quantifying changes in irreducible water transforms into movable water saturation by using a triaxial in situ flow system, thereby elucidating the impact of the hydraulic fracture on irreducible water saturation. The experiments demonstrate that pore structures are significantly modified in terms of connectivity and diameter through hydraulic fracturing. During damage zone formation, 12.4–19.2% of small pores coalesce into larger pores through integration of isolated spaces. This variation enhances fluid mobility, transforms 1.38–11.61% of irreducible water, and decreases starting pressure gradients by 1 MPa/100 m to 0.1 MPa/100 m. Modified pore structure leads to the iso-permeability point shifting toward higher water saturation. The gas-phase relative permeability at irreducible water saturation is two times as high as that of the matrix sample. Fractured zones show a 20–23% conversion efficiency of irreducible to movable water. In addition, based on the results of experimental data, hydraulic fracturing increased water production by 3607 to 9163 m3. However, this effect is only maintained during the first 3 to 6 months post-fracture. These results quantify the transformation of irreducible water into movable water in hydraulic fracturing. This study provides key performance indicators for gas reservoir applications. Full article
(This article belongs to the Special Issue Advances in Unconventional Reservoir Development and CO2 Storage)
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14 pages, 4779 KiB  
Article
Effect of Sintering Temperature and Time on Microstructure and Mechanical Properties of CoCrFeNiMn High-Entropy Alloys
by Ning Li, Chengbo Wu, Zhennan Wu, Mengyuan Jiang, Junfeng Hou and Fuyuan Dong
Metals 2025, 15(6), 591; https://doi.org/10.3390/met15060591 - 26 May 2025
Viewed by 458
Abstract
In this study, Cantor alloys were prepared via powder metallurgy using spark plasma sintering (SPS) technology. The sintering parameters were systematically controlled, as follows: three temperature gradients (850 °C, 950 °C, and 1050 °C with a fixed holding time of 5 min) and [...] Read more.
In this study, Cantor alloys were prepared via powder metallurgy using spark plasma sintering (SPS) technology. The sintering parameters were systematically controlled, as follows: three temperature gradients (850 °C, 950 °C, and 1050 °C with a fixed holding time of 5 min) and three holding time gradients at 1050 °C (3, 5, and 10 min). The effects of the sintering parameters on the microstructure and mechanical properties were thoroughly analyzed. As the sintering temperature increased, the elemental particle bonding became more uniform, the internal porosity decreased, and densification improved, leading to gradual enhancements in the tensile strength and ductility. Conversely, a prolonged holding time reduced the grain boundary energy and induced grain growth, resulting in improved ductility but decreased strength. The critical shear stress (τ0) and normal fracture stress (σ0) were introduced to analyze the influence of the sintering temperature and holding time on the tensile strength and fracture modes. Wear morphology observations revealed scratches and stepped features in all of the samples, indicating that the dominant wear mechanism was adhesive wear. Full article
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29 pages, 67369 KiB  
Article
Fractal–Fractional Synergy in Geo-Energy Systems: A Multiscale Framework for Stress Field Characterization and Fracture Network Evolution Modeling
by Qiqiang Ren, Tianhao Gao, Rongtao Jiang, Jin Wang, Mengping Li, Jianwei Feng and He Du
Fractal Fract. 2025, 9(5), 322; https://doi.org/10.3390/fractalfract9050322 - 19 May 2025
Viewed by 681
Abstract
This research introduces an innovative fractal–fractional synergy framework for multiscale analysis of stress field dynamics in geo-energy systems. By integrating fractional calculus with multiscale fractal dimension analysis, we develop a coupled approach examining stress redistribution patterns across different geological scales. The methodology combines [...] Read more.
This research introduces an innovative fractal–fractional synergy framework for multiscale analysis of stress field dynamics in geo-energy systems. By integrating fractional calculus with multiscale fractal dimension analysis, we develop a coupled approach examining stress redistribution patterns across different geological scales. The methodology combines fractal characterization of rock mechanical parameters with fractional-order stress gradient modeling, validated through integrated analysis of core testing, well logging, and seismic inversion data. Our fractal–fractional operators enable simultaneous characterization of stress memory effects and scale-invariant fracture propagation patterns. Key insights reveal the following: (1) Non-monotonic variations in rock mechanical properties (fractal dimension D = 2.31–2.67) correlate with oil–water ratio changes, exhibiting fractional-order transitional behavior. (2) Critical stress thresholds (12.19–25 MPa) for fracture activation follow fractional power-law relationships with fracture orientation deviations. (3) Fracture network evolution demonstrates dual-scale dynamics—microscale tip propagation governed by fractional stress singularities (order α = 0.63–0.78) and macroscale expansion obeying fractal growth patterns (Hurst exponent H = 0.71 ± 0.05). (4) Multiscale modeling reveals anisotropic development with fractal dimension increasing by 18–22% during multi-well fracturing operations. The fractal–fractional formalism successfully resolves the stress-shadow paradox while quantifying water channeling risks through fractional connectivity metrics. This work establishes a novel paradigm for coupled geomechanical–fluid dynamics analysis in complex reservoir systems. Full article
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16 pages, 5110 KiB  
Article
Effects of Nitrogen Partial Pressure on the Microstructure and Mechanical Properties of High-Entropy Ti(C,N)-Based Gradient Cermets
by Yunhao Zhang, Houan Zhang, Dongxu Qiao, Xin Tao, Peng Xia and Siyong Gu
Crystals 2025, 15(5), 479; https://doi.org/10.3390/cryst15050479 - 19 May 2025
Viewed by 336
Abstract
Titanium carbonitride (Ti(C,N))-based ceramics are widely utilized in mechanical machining, aerospace, and electronics, particularly in cutting tools and wear-resistant components. Two single-phase solid solution powders, non-high-entropy (Ti0.83,W0.07,Mo0.04,Nb0.03,Ta0.04)(C0.7,N0.3) and high-entropy [...] Read more.
Titanium carbonitride (Ti(C,N))-based ceramics are widely utilized in mechanical machining, aerospace, and electronics, particularly in cutting tools and wear-resistant components. Two single-phase solid solution powders, non-high-entropy (Ti0.83,W0.07,Mo0.04,Nb0.03,Ta0.04)(C0.7,N0.3) and high-entropy (Ti0.6,W0.1,Mo0.1,Nb0.1,Ta0.1)(C0.78,N0.22), were synthesized via the carbothermal reduction–nitridation (CRN) method. Gradient-structured non-high-entropy (C-TiCN) and high-entropy (HE-TiCN) cermets were fabricated at 1450 °C by tailoring the nitrogen partial pressure in the range of 1–8 kPa. The effect of nitrogen partial pressure on the microstructure and mechanical properties of both materials was thoroughly analyzed. Both materials exhibited a three-layer gradient structure comprising a hard-phase-enriched surface layer, a binder-rich subsurface layer, and a chemically uniform core. Optimal performance was achieved at 4 kPa nitrogen partial pressure, at which both HE-TiCN and C-TiCN exhibited a desirable combination of surface hardness and fracture toughness. Compared with C-TiCN, HE-TiCN showed improvements in surface hardness and fracture toughness at subsurface and core regions (40 µm from the surface) by 4.9%, 11.2%, and 12.0%, respectively. The enhanced surface hardness of HE-TiCN is attributed to the significant lattice distortion and the synergistic effects associated with its high-entropy configuration. The improved toughness of the binder-rich layer is primarily ascribed to mechanisms such as crack deflection, crack branching, and the formation of tear ridges. These findings offer a promising strategy for developing gradient Ti(C,N)-based cermets with enhanced mechanical performance. Full article
(This article belongs to the Special Issue Structure and Properties of Ceramic Materials)
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18 pages, 11277 KiB  
Article
Mechanical Characteristics and Mechanisms of Destruction of Trapezoidal Sandstone Samples Under Uneven Loading
by Bao Pan, Weijian Yu, Ke Li, Zilu Liu, Tao Huang and Jie Yang
Processes 2025, 13(4), 1169; https://doi.org/10.3390/pr13041169 - 12 Apr 2025
Viewed by 417
Abstract
Predicting rock failure under excavation-induced non-uniform stress remains challenging due to the inability of conventional homogeneous specimens to replicate field-scale stress gradients. A novel trapezoidal sandstone specimen with adjustable top-surface inclinations (S75/S85) is proposed, uniquely simulating asymmetric stress gradients to mimic excavation unloading. [...] Read more.
Predicting rock failure under excavation-induced non-uniform stress remains challenging due to the inability of conventional homogeneous specimens to replicate field-scale stress gradients. A novel trapezoidal sandstone specimen with adjustable top-surface inclinations (S75/S85) is proposed, uniquely simulating asymmetric stress gradients to mimic excavation unloading. Geometric asymmetry combined with multi-scale characterization (CT, SEM, PFC) decouples stress gradient effects from material heterogeneity. The key findings include the following points. (1) Inclination angles > 15° reduce peak strength by 24.2%, transitioning failure from brittle (transgranular cracks > 60) to mixed brittle-ductile modes (2) Stress gradients govern fracture pathways: transgranular cracks dominate high-stress zones, while intergranular cracks propagate along weak cementation interfaces. (3) PFC simulations reveal a 147% stress disparity between specimen sides and validate shear localization angles θ = 52° ± 3°), aligning with field data. This experimental–numerical framework resolves limitations of traditional methods, providing mechanistic insights into non-uniform load-driven failure. The methodology enables targeted support strategies for deep asymmetric roadways, including shear band mitigation and plastic zone reinforcement. By bridging lab-scale tests and engineering stress states, the study advances safety and sustainability in deep roadway excavation. Full article
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18 pages, 11188 KiB  
Article
Evaluation of the Impact of Multi-Scale Flow Mechanisms and Natural Fractures on the Pressure Transient Response in Fractured Tight Gas Reservoirs
by Xiaoben Hou, Feng Li, Fangfang Bai, Yuanyuan Bai, Yuhui Zhou and Zhuyi Zhu
Processes 2025, 13(4), 1163; https://doi.org/10.3390/pr13041163 - 11 Apr 2025
Viewed by 376
Abstract
The coupling mechanism between the multi-scale flow mechanisms and the pressure dynamic response of complex fracture networks in fractured tight sandstone gas reservoirs remains unclear. In this study, a mathematical model was developed by incorporating the non-Darcy flow (non-DF) behavior in both matrix [...] Read more.
The coupling mechanism between the multi-scale flow mechanisms and the pressure dynamic response of complex fracture networks in fractured tight sandstone gas reservoirs remains unclear. In this study, a mathematical model was developed by incorporating the non-Darcy flow (non-DF) behavior in both matrix and fracture systems within the framework of the embedded discrete fracture model (EDFM). The governing equations were solved numerically through finite volume discretization. By employing numerical well-testing techniques, the dynamic impacts of low-velocity non-DF (matrix domain) and high-velocity non-DF (fracture domain) on the pressure transient response were systematically evaluated. Furthermore, the characteristic patterns of transient pressure responses under different natural fracture development modes were revealed. This study demonstrates that the pressure and pressure derivative (PD) log–log curves of fractured tight sandstone gas wells exhibit a wide opening shape, indicative of complex fracture morphologies. The presence of a threshold pressure gradient in the matrix system results in an upward convex shape in the PD profile, whereas the high-velocity non-DF in the fracture network causes a downward concave characteristic in the derivative curve. The spatial distribution of the natural fracture network significantly influences the response characteristics during the mid-term radial flow stage. As the fracture density decreases, the system gradually transitions toward a dual-porosity medium. This research contributes to the theoretical foundation required for the accurate interpretation of dynamic well tests and the optimization of effective development schemes in gas reservoirs with extremely low permeability. Full article
(This article belongs to the Section Energy Systems)
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14 pages, 8698 KiB  
Article
Interfacial Characteristics and Mechanical Performance of IN718/CuSn10 Fabricated by Laser Powder Bed Fusion
by Xiao Yang, Guangsai Zou, Zheng Wang, Xinze He, Mina Zhang and Jingyu Xu
Crystals 2025, 15(4), 344; https://doi.org/10.3390/cryst15040344 - 6 Apr 2025
Viewed by 539
Abstract
To address the critical applications of heterogeneous structures involving nickel-based superalloys (IN718) and copper alloys (CuSn10) under extreme operating conditions, and to address the limitations of traditional joining techniques in terms of interfacial brittleness and geometric constraints, this study employs Laser Powder Bed [...] Read more.
To address the critical applications of heterogeneous structures involving nickel-based superalloys (IN718) and copper alloys (CuSn10) under extreme operating conditions, and to address the limitations of traditional joining techniques in terms of interfacial brittleness and geometric constraints, this study employs Laser Powder Bed Fusion (LPBF) technology, specifically multi-material LPBF (MM-LPBF). By precisely melting IN718 and CuSn10 powders layer by layer, the study directly fabricates multi-material IN718/CuSn10 joint specimens, thereby simplifying the complexity of traditional joining processes. The research systematically investigates the interfacial microstructure and mechanical property evolution laws and underlying mechanisms. It reveals that sufficient element diffusion and hardness gradients are present at the IN718/CuSn10 interface, indicating good metallurgical bonding. However, due to significant differences in thermophysical properties, cracks inevitably appear at the interface. Mechanical property tests indicate that the strength of the IN718/CuSn10 joint specimens falls between that of IN718 and CuSn10, but with lower elongation, and fractures primarily occur at the interface. This research provides theoretical support for establishing a process database for LPBF formed of nickel–copper heterogeneous materials, advancing the manufacturing technology of aerospace multi-material components. Full article
(This article belongs to the Special Issue Advances of High Entropy Alloys (2nd Edition))
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32 pages, 9579 KiB  
Article
DFT Study of Au3In and Au3In2 Intermetallic Compounds: Structural Stability, Fracture Toughness, Anisotropic Elasticity, and Thermophysical Properties for Advanced Applications
by Ching-Feng Yu and Yang-Lun Liu
Materials 2025, 18(7), 1561; https://doi.org/10.3390/ma18071561 - 29 Mar 2025
Cited by 2 | Viewed by 580
Abstract
This study systematically explores the structural stability, mechanical properties, elastic anisotropy, fracture toughness, and thermophysical characteristics of Au3In and Au3In2 intermetallic compounds (IMCs) through density functional theory (DFT) simulations. Employing the generalized gradient approximation (GGA) and the Voigt–Reuss–Hill [...] Read more.
This study systematically explores the structural stability, mechanical properties, elastic anisotropy, fracture toughness, and thermophysical characteristics of Au3In and Au3In2 intermetallic compounds (IMCs) through density functional theory (DFT) simulations. Employing the generalized gradient approximation (GGA) and the Voigt–Reuss–Hill approximation enables precise predictions of polycrystalline elastic behavior, providing critical insights into the intrinsic stability and mechanical anisotropy of these IMCs. Structural optimization identifies the equilibrium lattice parameters and cohesive energies, indicating stronger atomic bonding and superior structural stability in Au3In relative to Au3In2. Elastic constant calculations confirm mechanical stability and reveal pronounced anisotropic elastic behavior; Au3In exhibits significant stiffness along the [010] crystallographic direction, while Au3In2 demonstrates notable stiffness predominantly along the [001] direction. Both Au3In and Au3In2 exhibit ductile characteristics, confirmed by positive Cauchy pressures and elevated bulk-to-shear modulus (K/G) ratios. Fracture toughness analysis further establishes that Au3In offers greater resistance to crack propagation compared to Au3In2, suggesting its suitability in mechanically demanding applications. Thermophysical property evaluations demonstrate that Au3In possesses higher thermal conductivity, elevated Debye temperature, and superior volumetric heat capacity relative to Au3In2, reflecting its enhanced capability for effective thermal management in electronic packaging. Anisotropy assessments, utilizing both universal and Zener anisotropy indices, reveal significantly higher mechanical anisotropy in Au3In2, influencing its practical applicability. Full article
(This article belongs to the Special Issue Physical Metallurgy of Metals and Alloys (3rd Edition))
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