Search Results (849)

To study the mechanical properties and modification mechanism of thermosetting polyurethane (PU)-modified asphalt, the effects of polyurethane dosage on the workability of polyurethane-modified asphalt were analyzed by means of rotational viscosity tests. The mechanical properties of polyurethane-modified asphalt with different polyurethane dosages were explored using tensile tests and dynamic mechanical analysis (DMA). In addition, the thermodynamic behavior and micromorphology of polyurethane-modified asphalt were also thoroughly investigated using the test results of differential scanning calorimetry (DSC) and scanning electron microscopy (SEM). The results showed that PU obtained the optimum workability when the polyurethane dose was 50%: at 120 min, its rotational viscosity was 1005 cp, which was lower than 2800 cp (40% PU) and 760 cp (60% PU). Additionally, the results of fracture elongation and fracture strength indicated that the PU-modified asphalt had good flexibility and strength. Compared with base asphalt, the tensile strength of 50% PU-modified asphalt increased by 509%, which was significantly higher than 157% (40% PU) and more balanced than 897% (60% PU) in terms of strength and flexibility. Added PU can significantly improve the elasticity of asphalt at high temperatures, while increasing the proportion of asphalt adhesive components, enhancing the deformation ability and temperature stability of asphalt. As the dose of PU increases, the interface between asphalt and PU blended more fully, and the surface became smoother. When the dose of PU was 50% or more, the interface between asphalt and PU was well integrated with a smooth and flat surface, forming a more uniform and stable cross-linked network structure. Full article

Aluminum matrix composites provide an ideal solution for lightweight brake disks, but conventional casting processes are prone to crack initiation due to inhomogeneous reinforcement dispersion, gas porosity, and inadequate toughness. To break the conventional trade-off between high wear resistance and low toughness of brake disks, this study fabricated a bimetallic structure of SiC_p/Al–Fe–V–Si aluminum matrix composite and cast ZL101 alloy using friction stir lap welding (FSLW). Then, the microstructural evolution, mechanical properties, and tribological behavior of the FSLW joints were studied by XRD, SEM, TEM, tensile testing, and tribological tests. The results showed that the FSLW process homogenized the distribution of SiC particle reinforcements in the SiC_p/Al–Fe–V–Si composites. The Al₁₂(Fe,V)₃Si heat-resistant phase was not decomposed or coarsened, and the mechanical properties were maintained. The FSLW process refined the grains of the ZL101 aluminum alloy through recrystallization and fragmented eutectic silicon, improving elongation to 22%. A metallurgical bond formed at the joint interface. Tensile fracture occurred within the ZL101 matrix, demonstrating that the interfacial bond strength exceeded the alloy’s load-bearing capacity. In addition, the composites exhibited significantly enhanced wear resistance after FSLW, with their wear rate reduced by approximately 40% compared to the as-received materials, which was attributed to the homogenized SiC particle distribution and the activation of an oxidative wear mechanism. Full article

Shoulder-assisted heating friction plug welding (SAH-FPW) experiments were conducted to repair keyhole-like volumetric defects in 6082-T6 aluminum alloy, employing a novel concave backing hole technique on a flat backing plate. This approach yielded well-formed plug welded joints without significant macroscopic defects. Notably, the joints exhibited no thinning on the top surface while forming a reinforcing boss structure within the concave backing hole on the backside, resulting in a slight increase in the overall load-bearing thickness. The introduction of the concave backing hole led to distinct microstructural zones compared to joints welded without it. The resulting joint microstructure comprised five regions: the nugget zone, a recrystallized zone, a shoulder-affected zone, the thermo-mechanically affected zone, and the heat-affected zone. Significantly, this process eliminated the poorly consolidated ‘filling zone’ often associated with conventional plug repairs. The microhardness across the joints was generally slightly higher than that of the base metal (BM), with the concave backing hole technique having minimal influence on overall hardness values or their distribution. However, under identical welding parameters, joints produced using the concave backing hole consistently demonstrated higher tensile strength than those without. The joints displayed pronounced ductile fracture characteristics. A maximum ultimate tensile strength of 278.10 MPa, equivalent to 89.71% of the BM strength, was achieved with an elongation at fracture of 9.02%. Analysis of the grain structure revealed that adjacent grain misorientation angle distributions deviated from a random distribution, indicating dynamic recrystallization. The nugget zone (NZ) possessed a higher fraction of high-angle grain boundaries (HAGBs) compared to the RZ and TMAZ. These findings indicate that during the SAH-FPW process, the use of a concave backing hole ultimately enhances structural integrity and mechanical performance. Full article

In the framework of hydrogen production and storage for clean energy generation, the resistance to hydrogen embrittlement of a newly developed austenitic stainless steel is presented. Gas-atomized metal powders prepared from secondary-sourced metals were employed to manufacture test specimens with Laser Powder Bed Fusion (LPBF) technology. After machining and exposure to a controlled, pressurized hydrogen atmosphere at high temperature, the effect of hydrogen charging on the mechanical performance under static and dynamic conditions was investigated. The stabilizing effect of the optimized chemical composition is reflected in the absence of degradation effects on Yield Stress (YS), Ultimate Tensile Stress (UTS), and fatigue life observed for specimens exposed to hydrogen. Moreover, despite a moderate reduction in the elongation at fracture observed by increasing the hydrogen charging time, ductility loss calculated as Relative Reduction of Area (RRA) remains substantially unaffected by the duration of exposure to hydrogen and demonstrates that the austenitic steel is capable of resisting hydrogen embrittlement (HE). Full article

This study investigates the mechanical behavior of X52 steel pipes and their weld regions under pure hydrogen transport conditions, with a focus on assessing potential hydrogen embrittlement risks. Through experimental analysis, the research evaluates how different pipeline regions—including the base metal, weld metal, and heat-affected zones—respond to varying hydrogen pressures. Key mechanical properties such as elongation, fracture toughness, and crack growth resistance are analyzed to determine their implications for structural integrity and safety. Based on the findings, this study proposes criteria for the safety evaluation of X52 pipelines operating in hydrogen service environments. The results are intended to inform decisions regarding the repurposing of existing pipelines or the design of new infrastructure dedicated to pure hydrogen transport, offering insights into material performance and critical safety considerations for hydrogen pipeline applications. Full article

In the industrial practice of metal forming, the consistent and reasonable characterization of the material behavior under the coupling effect of strain, strain rate, and temperature on the material flow stress is very important for the design and optimization of process parameters. The purpose of this work was to establish an appropriate constitutive model to characterize the rheological behavior of a hot-formed steel plate (22MnB5 steel) produced through the TSCR (Thin Slab Casting and Rolling) process under practical deformation temperatures (150–250 °C) and strain rates (0.001–3000 s⁻¹). Subsequently, the material flow behavior was modeled and predicted using the Johnson–Cook flow stress constitutive model. In this study, uniaxial tensile tests were conducted on 22MnB5 steel at room temperature under varying strain rates, along with elevated-temperature tensile tests at different strain rates, to obtain the engineering stress–strain curves and analyze the mechanical properties under various conditions. The results show that during room-temperature tensile testing within the strain rate range of 10⁻³ to 300 s⁻¹, the 22MnB5 steel exhibited overall yield strength and tensile strength of approximately 1500 MPa, and uniform elongation and fracture elongation of about 7% and 12%, respectively. When the strain rate reached 1000–3000 s⁻¹, the yield strength and tensile strength were approximately 2000 MPa, while the uniform elongation and fracture elongation were about 6% and 10%, respectively. Based on the experimental results, a modified Johnson–Cook constitutive model was developed and calibrated. Compared with the original model, the modified Johnson–Cook model exhibited a higher coefficient of determination (R²), indicating improved fitting accuracy. In addition, to predict the material’s damage behavior, three distinct specimen geometries were designed for quasi-static strain rate uniaxial tensile testing at ambient temperature. The Johnson–Cook failure criterion was implemented, with its constitutive parameters calibrated through integrated finite element analysis to establish the damage model. The determined damage parameters from this investigation can be effectively implemented in metal forming simulations, providing valuable predictive capabilities regarding workpiece material performance. Full article

This study investigates the mechanical properties of ABS parts fabricated via used deposition modeling (FDM) through integrated experimental and numerical approaches. ABS resin was used as the experimental material, and tensile tests were conducted using a universal testing machine. Finite element analysis (FEA) was performed via ANSYS 2021 to simulate stress deformation behavior, with key parameters including a gauge length of 10 mm (pre-stretching) and printing temperature gradients. The results show that the specimen exhibited a maximum tensile force of 7.3 kN, upper yield force of 3.7 kN, and lower yield force of 3.2 kN, demonstrating high strength and toughness. The non-proportional elongation reached 0.06 (6%), and the quantified enhancement multiple of AM relative to traditional manufacturing was 1.1, falling within the reasonable range for glass fiber-reinforced or specially formulated ABS. FEA results validated the experimental data, showing that the material underwent 15 mm of plastic deformation before fracture, consistent with ABS’s ductile characteristics. Full article

This work systematically investigates the Zn-content-dependent phase evolution (1–12 at.%) and its correlation with mechanical properties in as-cast Mg–2Y–xZn alloys. A sequential phase transformation is observed with the Zn content increasing: the microstructure evolves from X-phase dominance (1–2 at.% Zn) through W-phase formation (3–6 at.% Zn) to I-phase emergence (12 at.% Zn). Optimal mechanical performance is attained in the 2 at.% Zn-containing alloy, with measured tensile properties reaching 239 MPa UTS and 130 MPa YS, while maintaining an elongation of 12.62% prior to its gradual decline at higher Zn concentrations. Crystallographic analysis shows that the most significant strengthening effect of the X-phase originates from its coherent orientation relationship with the α-Mg matrix and the development of deformation-induced kink bands. Meanwhile, fine W-phase particles embedded within the X-phase further enhance alloy performance by suppressing X-phase deformation, revealing pronounced synergistic strengthening between the two phases. Notably, although both the I-phase and W-phase act as crack initiation sites during deformation, their coexistence triggers a competitive fracture mechanism: the I-phase preferentially fractures to preserve the structural integrity of the W-phase, effectively mitigating crack propagation. These dynamic interactions of second phases during plastic deformation—synergistic strengthening and competitive fracture—provide a novel strategy and insights for designing high-performance Mg–RE–Zn alloys. Full article

A novel approach to estimating the absorbed energy (toughness) in a uniaxial tensile test with only knowledge of the microstructure is presented. The flow behavior of each Dual-Phase (DP) steel grade is predicted using idealized Representative Volume Elements (RVEs) up to uniform elongation. To estimate the flow behavior beyond uniform elongation, the stress-modified fracture strain in a non-local damage model was implemented in Abaqus. Damage parameters were calibrated using Finite Element (FE) simulations of purely ferritic tensile specimens. The damage parameters remained unchanged, except for the coefficient of triaxiality. This coefficient was adjusted based on the average triaxiality of ferrite elements at the instability point of the uniaxially loaded RVEs for each DP steel grade. The proposed approach comprises two steps: micron-sized RVEs to predict the flow behavior up to the point of uniform elongation and the average triaxiality and full-scale tensile-test simulations to predict the rest of the curves. The results show that the damage parameters calibrated for high-strain ferrite effectively estimate the absorbed energy during failure in tension tests. This approach is also geometry-independent; varying the geometry of the tensile specimen, including miniature or notched specimens, still yields predicted absorbed energies that are in good agreement with the experimental results. Full article

This study investigates the deformation and fracture mechanisms of a Ti₆₁Al₁₆Cr₁₀Nb₈V₅ multi-principal element alloy (Ti61V5 alloy) under quasi-static and dynamic compression. The alloy comprises an equiaxed BCC matrix (~35 μm) with uniformly dispersed nano-sized B2 precipitates and a ~3.5% HCP phase along grain boundaries, exhibiting a density of 4.82 g/cm³, an ultimate tensile strength of 1260 MPa, 12.8% elongation, and a specific strength of 262 MPa·cm³/g. The Ti61V5 alloy exhibits a pronounced strain-rate-strengthening effect, with a strain rate sensitivity coefficient (m) of ~0.0088 at 0.001–10/s. Deformation activates abundant {011} and {112} slip bands in the BCC matrix, whose interactions generate jogs, dislocation dipoles, and loops, evolving into high-density forest dislocations and promoting screw-dominated mixed dislocations. The B2 phase strengthens the alloy via dislocation shearing, forming dislocation arrays, while the HCP phase enhances strength through a dislocation bypass mechanism. At higher strain rates (960–5020/s), m increases to ~0.0985. Besides {011} and {112}, the BCC matrix activates high-index slip planes {123}. Intensified slip band interactions generate dense jogs and forest dislocations, while planar dislocations combined with edge dislocation climb enable obstacle bypassing, increasing the fraction of edge-dominated mixed dislocations. The Ti61V5 alloy shows low sensitivity to adiabatic shear localization. Under forced shear, plastic-flow shear bands form first, followed by recrystallized shear bands formed through a rotational dynamic recrystallization mechanism. Microcracks initiate throughout the shear bands; during inward propagation, they may terminate upon encountering matrix microvoids or deflect and continue when linking with internal microcracks. Full article

Temperature and Cr content on the tensile and fracture mechanics properties of welded joints made of two Cr-Mo steels (A387 Gr. B and SA387 Gr. 91) are presented and analyzed. Tensile strength, yield stress and elongation, as well as the stress–strain curves are obtained by standard tensile tests using specimens extracted from welded joints. Fracture toughness testing was carried out to determine the critical stress intensity factor, K_Ic, and the critical crack length, a_c, for all three zones of the welded joint, parent metal (PM), heat-affected zone (HAZ) and weld metal (WM). Based on these results, the tensile and fracture mechanics properties of welded joints made of A387 Gr. B and SA387 Gr. 91 steels are compared and analyzed. Full article

This study investigated how long-term aging (750 °C and 950 °C) affects the microstructure and room-temperature tensile properties of the Ni-Co-Cr superalloy GH3617. Characterization (SEM, EDS, EBSD) showed that initial aging (750 °C, 500 h) formed discontinuous M₂₃C₆ carbides, pinning grain boundaries and improving strength. Prolonged aging (750 °C, 5000 h) caused M₂₃C₆ to coarsen into brittle chain-like structures (width up to 1.244 μm) and precipitated M₆C carbides, degrading grain boundaries. Aging at 950 °C accelerated this coarsening via LSW kinetics (rate constant: 6.83 × 10⁻² μm³/s), with Mo segregation promoting M₆C formation. Tensile properties resulted from competing γ′ precipitation strengthening (post-aging strength increased up to 23.3%) and grain boundary degradation (elongation dropped from 70.1% to 43.3%). Fracture shifted from purely intergranular (cracks along M₂₃C₆/γ interfaces at 750 °C) to mixed mode (cracks initiated by M₆C fragmentation at 950 °C). These insights support superalloy microstructure optimization and lifetime prediction. Full article

Gelatin hydrogels for food packaging applications have aroused interest in recent years. However, these hydrogels exhibit several limitations, such as poor mechanical strength and low swelling and water uptake. To overcome these challenges, nanocellulose can be used as a nanofiller. Thus, cellulose nanofibrils (CNFs) were obtained from soybean straw and used as a nanofiller for hydrogels produced with type A and B gelatin. The effects of the biopolymer type and the influence of CNF concentrations (0–3.0%, w/w) on the properties of hydrogels were studied. The CNFs exhibited a fiber morphology with micrometer length and nanometer diameter (16.8 ± 1.2 nm). The addition of CNFs (0–3%, w/w) caused a decrease in the stress (~50%) and elongation (~14%) at the fracture of the hydrogels for both type of gelatin. However, the elastic modulus increased (~20%). The addition of CNFs increased the hardness of the hydrogels up to 25%. The swelling capacity decreased by ~30% when the CNF concentration increased from 0 to 3%, while the thermal properties and chemical structure were not altered. These findings provide valuable insights for ongoing research into the incorporation of nanocellulose in biopolymer-based hydrogels produced by physical and sustainable methods for food packaging applications. Full article

This study examines the mechanical and microstructural properties of graphene-reinforced AA2219 composites developed for hydrogen storage tank inner liner applications. A novel processing route combining high-energy ball milling, ultrasonic-assisted stir casting, and squeeze casting was used to achieve homogeneous dispersion of 0.5 wt.% graphene nanoplatelets and minimise agglomeration. The composites were subjected to T6 and T8 ageing treatments to optimize their properties. Microstructural analysis revealed refined grains, uniform Al₂Cu precipitate distribution, and stable graphene retention. Mechanical testing showed that the as-cast composite exhibited a UTS of 308.6 MPa with 13.68% elongation. After T6 treatment, the UTS increased to 353.6 MPa with an elongation of 11.24%. T8 treatment further improved the UTS to 371.5 MPa, with an elongation of 8.54%. Hardness improved by 46%, from 89.6 HV (as-cast) to 131.3 HV (T8). Fractography analysis indicated a shift from brittle to ductile fracture modes after heat treatment. The purpose of this work is to develop lightweight, high-strength composites for hydrogen storage applications. The novelty of this study lies in the integrated processing approach, which ensures uniform graphene dispersion and superior mechanical performance. The results demonstrate the suitability of these composites for advanced aerospace propulsion systems. Full article

Traditional narrow gap welding of thick titanium alloy plates easily produces dynamic molten pool flow instability, poor sidewall fusion, and excessive residual stress after welding, which leads to defects such as pores, cracks, and large welding deformations. In view of the above problems, this study takes 16-mm-thick TC4 titanium alloy as the research object, uses low-power pulsed laser-GTA flexible heat source welding technology, and uses the flexible regulation of space between the laser, arc, and wire to promote good fusion of the molten pool and side wall metal. By implementing instant ultrasonic impact treatment on the weld surface, the residual stress of the welded specimen is controlled within a certain range to reduce deformation after welding. The results show that the new welding process makes the joint stable, the side wall is well fused, and there are no defects such as pores and cracks. The weld zone is composed of a large number of α′ martensites interlaced with each other to form a basketweave structure. The tensile fracture of the joint occurs at the base metal. The joint tensile strength is 870 MPa, and the elongation after fracture can reach 17.1%, which is 92.4% of that of the base metal. The impact toughness at the weld is 35 J/cm², reaching 81.8% of that of the base metal. After applying ultrasound, the average residual stress decreased by 96% and the peak residual stress decreased by 94.8% within 10 mm from the weld toe. The average residual stress decreased by 95% and the peak residual stress decreased by 95.5% within 10 mm from the weld root. The residual stress on the surface of the whole welded test plate could be controlled within 200 MPa. Finally, a high-performance thick Ti-alloy plate welded joint with good forming and low residual stress was obtained. Full article