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15 pages, 4548 KB  
Article
Influence Mechanism of Process Parameters on Nanosecond Laser Polishing Quality of Ti6Al4V Titanium Alloy
by Xulin Wang and Jianwei Ma
J. Manuf. Mater. Process. 2026, 10(2), 73; https://doi.org/10.3390/jmmp10020073 - 20 Feb 2026
Viewed by 432
Abstract
This study presents a novel numerical framework that elucidates the critical, yet previously underexplored, role of Marangoni vortex dynamics in determining the final surface quality during the laser polishing of Ti6Al4V (TC4). TC4 titanium alloy is widely used in aerospace, biomedicine, and other [...] Read more.
This study presents a novel numerical framework that elucidates the critical, yet previously underexplored, role of Marangoni vortex dynamics in determining the final surface quality during the laser polishing of Ti6Al4V (TC4). TC4 titanium alloy is widely used in aerospace, biomedicine, and other high-precision applications due to its excellent specific strength, corrosion resistance, and biocompatibility. However, its surface quality directly affects the fatigue life and service performance of parts, and traditional polishing methods suffer from low efficiency and high pollution. As a non-contact, controllable surface treatment technology, nanosecond laser polishing has demonstrated unique advantages in balancing processing efficiency and surface quality. This study systematically discussed the influence of key process parameters (spot overlap rate, laser power, and scanning times) on the nanosecond laser polishing of TC4 titanium alloy. It revealed the internal physical mechanism by analyzing the temperature and velocity fields and vortex dynamics during molten-pool evolution. It is found that the polishing effect is determined by the process parameters, which adjust the thermal–fluid coupling physical field (temperature distribution, melt flow, and vortex structure) in the molten pool. There is an optimal combination of parameters (spot overlap rate of 79%, laser power of 0.8 W, scanning speed of 5 m/min, scanning 3 times) that can place the molten pool in an optimal dynamic balance state and achieve effective flatness. The experimental results show that, under this parameter, the surface roughness of the specimen with an initial roughness of 1.223 μm is reduced by about 32%. The research further clarified the mechanism by which the initial roughness of the base metal influences the molten pool: the greater the initial roughness, the more pronounced the “peak shaving and valley filling” effect. Under the same parameters, the improvement rate of the specimen with the initial roughness of 1.623 μm could reach about 40%. This study not only establishes the optimized process window but also reveals the essential relationship between “process parameters–bath behavior–surface quality” from the level of the physical field of the molten pool. The findings provide a practical guideline for parameter optimization, directly applicable to the high-precision laser finishing of critical titanium components in the aerospace and biomedical industries. Full article
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17 pages, 8263 KB  
Article
Study on Material Removal Mechanisms for TBCs in Drag-Finishing
by Huanyu Gu, Jinquan Dong, Qing He and Shixing Wang
Coatings 2026, 16(2), 230; https://doi.org/10.3390/coatings16020230 - 12 Feb 2026
Viewed by 967
Abstract
Reducing the surface roughness of thermal barrier coatings (TBCs) improves engine aerodynamic efficiency and mitigates CMAS adhesion, but turbine blades’ complex geometries demand low-cost, damage-mzitigated finishing. This work employed drag finishing with spherical ceramic media, establishing a discrete element method (DEM) model to [...] Read more.
Reducing the surface roughness of thermal barrier coatings (TBCs) improves engine aerodynamic efficiency and mitigates CMAS adhesion, but turbine blades’ complex geometries demand low-cost, damage-mzitigated finishing. This work employed drag finishing with spherical ceramic media, establishing a discrete element method (DEM) model to quantify abrasive trajectories, contact forces, and energy distributions, combined with surface characterization to study abrasive effects on columnar YSZ and modified GZO topcoats. Results show roughness reduction is constrained by fracture toughness and columnar unit local fracture, leading to different decay rates and late-stage improvement between YSZ and GZO. Introducing smaller abrasives enhances packing density via void filling, strengthens microscale cutting, and reduces strong normal impacts, promoting surface uniformization and suppressing localized damage. These findings guide mechanistic understanding of drag finishing on multi-material TBCs, as well as abrasive grading design and process parameter optimization. Full article
(This article belongs to the Section Ceramic Coatings and Engineering Technology)
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16 pages, 13859 KB  
Article
Micromanufacturing Process of Complex 3D FeCo Core Microwindings for Magnetic Flux Modulation in Micromotors
by Efren Diez-Jimenez, Diego Lopez-Pascual, Gabriel Villalba-Alumbreros, Ignacio Valiente-Blanco, Miguel Fernandez-Munoz, Jesús del Olmo-Anguix, Oscar Manzano-Narro, Alexander Kanitz, Jan Hoppius and Jan Philipp
Micromachines 2026, 17(1), 115; https://doi.org/10.3390/mi17010115 - 15 Jan 2026
Cited by 1 | Viewed by 1118
Abstract
This work presents the design, fabrication, and characterization of a three-dimensional FeCo-based flux-modulator microwinding intended for integration into high-torque axial-flux Vernier micromotors. The proposed micromotor architecture modulates the stator magnetic flux using 12 magnetically isolated FeCo teeth interacting with an 11-pole permanent-magnet rotor. [...] Read more.
This work presents the design, fabrication, and characterization of a three-dimensional FeCo-based flux-modulator microwinding intended for integration into high-torque axial-flux Vernier micromotors. The proposed micromotor architecture modulates the stator magnetic flux using 12 magnetically isolated FeCo teeth interacting with an 11-pole permanent-magnet rotor. The design requires the manufacturing of complex three-dimensional micrometric parts, including three teeth and a cylindrical core. Such a complex design cannot be manufactured using conventional micromanufacturing lithography or 2D planar methods. The flux-modulator envelope dimensions are 250 μm outer diameter and 355 μm height. It is manufactured using a femtosecond laser-machining process that preserves factory-finished surfaces and minimizes heat-affected zones. In addition, this micrometric part has been wound using 20 μm diameter enamelled copper wire. A dedicated magnetic clamping fixture is developed to enable multilayer microwinding of the integrated core, producing a 17-turn inductor with a 60.6% fill factor—the highest reported for a manually wound ferromagnetic-core microcoil of this scale. Geometric and magnetic characterization validates the simulation model and demonstrates the field distribution inside the isolated core. The results establish a viable micromanufacturing workflow for complex 3D FeCo microwindings, supporting the development of next-generation high-performance MEMS micromotors. Full article
(This article belongs to the Section E:Engineering and Technology)
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11 pages, 1564 KB  
Article
Surface Treatment and Analysis of 3D-Printed Plastic Molds for Prototype and Small-Series Injection Molding
by Karel Raz, Zdenek Chval, Frantisek Hula and Angelos Markopoulos
Polymers 2025, 17(22), 2977; https://doi.org/10.3390/polym17222977 - 8 Nov 2025
Cited by 2 | Viewed by 1192
Abstract
Additive manufacturing (AM) has emerged as a promising technology for producing low-cost, customized tooling, particularly for prototyping and small-series injection molding. However, the inherent surface roughness and anisotropic properties of 3D-printed parts pose significant challenges for their direct use as functional mold inserts. [...] Read more.
Additive manufacturing (AM) has emerged as a promising technology for producing low-cost, customized tooling, particularly for prototyping and small-series injection molding. However, the inherent surface roughness and anisotropic properties of 3D-printed parts pose significant challenges for their direct use as functional mold inserts. This study investigates the effectiveness of various post-processing techniques on 3D-printed plastic inserts made from polyamide 12 (PA12) and glass bead-filled PA12 (PA12GB). The primary objective was to evaluate the impact of these surface treatments on the functional properties and service life of the mold inserts. A comprehensive analysis was conducted, including a detailed characterization of roughness using a confocal microscope, cross-sectional analysis to determine layer thickness, and tribological tests employing the ball-on-disc method to assess wear resistance. The study employed a modular injection mold and tested a range of surface finishing processes, including PostProcess Suspended Rotational Force (SRF) technology, metal decomposition coatings from HVM Plasma, and various methods from DyeMansion (Powershot S and Powerfuse). Results show a significant reduction in surface roughness across all methods. Notably, the vapor-based Powefuse treatment from DyeMansion achieved a surface roughness (Ra) of 1.2797 μm, which is below the typical Ra value of 1.6 μm for conventional metal molds, thereby making it suitable for high-quality molding applications. The tribological analysis provided critical insights into the durability and wear resistance of the treated surfaces, supporting their potential for extended use. This research validates the potential of specific post-processing methods to transform AM parts into functional tooling, enabling cost-effective and rapid prototyping in the plastics industry. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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24 pages, 5146 KB  
Review
From Manual to Automated: Exploring the Evolution of Switchover Methods in Injection Molding Processes—A Review
by Christian Bielenberg, Markus Stommel and Peter Karlinger
Polymers 2025, 17(8), 1096; https://doi.org/10.3390/polym17081096 - 18 Apr 2025
Cited by 5 | Viewed by 2639
Abstract
Thermoplastic injection molding is a widely used process for producing complex three-dimensional plastic parts with tight dimensional tolerances. A key determinant of part quality is the switchover point—the transition from velocity-controlled filling to pressure-controlled packing. This transition affects critical product attributes, such as [...] Read more.
Thermoplastic injection molding is a widely used process for producing complex three-dimensional plastic parts with tight dimensional tolerances. A key determinant of part quality is the switchover point—the transition from velocity-controlled filling to pressure-controlled packing. This transition affects critical product attributes, such as d imensional accuracy, weight consistency, and surface finish. Precise control of the switchover point enhances process stability, robustness, and adaptability. This review consolidates recent advancements in switchover methods and adaptive control techniques. Improvements in traditional methods include the use of pressure gradient detection to mitigate viscosity variations and adaptive control to refine stroke- and time-dependent switchovers. In addition, deformation-based strategies detect the mold-opening force associated with cavity pressure through clamping force, mold separation, or tie-bar elongation. The integration of machine learning and feature extraction techniques enables the real-time adjustment of the switchover point by mapping relationships between process parameters and quality criteria. In addition, ultrasonic sensors provide non-invasive melt front detection, reducing the risk of mold damage. Real-time simulations, updated through nozzle pressure feedback, complement these methods to achieve precise switchover timing. This review also identifies persistent challenges, such as sensitivity to material properties, machine wear, and environmental conditions, and it explores future directions for improving the accuracy and adaptability of switchover control in modern injection molding processes. Full article
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17 pages, 1250 KB  
Article
Quality Risk Management in the Final Operational Stage of Sterile Pharmaceutical Manufacturing: A Case Study Highlighting the Management of Sustainable Related Risks in Product Sterilization, Inspection, Labeling, Packaging, and Storage Processes
by Bassam Elmadhoun, Rawidh Alsaidalani and Frank Burczynski
Sustainability 2025, 17(4), 1670; https://doi.org/10.3390/su17041670 - 17 Feb 2025
Cited by 4 | Viewed by 9257
Abstract
Quality risk management, commonly known as QRM, is designed to systematically assess, control, communicate, and review potential risks at every stage of the pharmaceutical manufacturing process. The preservation of consistent product quality across the entirety of the product’s life cycle is of paramount [...] Read more.
Quality risk management, commonly known as QRM, is designed to systematically assess, control, communicate, and review potential risks at every stage of the pharmaceutical manufacturing process. The preservation of consistent product quality across the entirety of the product’s life cycle is of paramount importance. The aim of this article is to formulate a best practice guide that will assist pharmaceutical manufacturers in comprehending and implementing the International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH) Q9: quality risk management principles. A widely recognized methodology for defining and monitoring risk mitigation strategies within the pharmaceutical sector is the Failure Mode and Effects Analysis (FMEA). ICH Q9 does not, however, offer detailed instructions for applying FMEA to real-world pharmaceutical situations. We previously provided real-world case studies that identify and mitigate risks in the early stages of the manufacturing process of sterile products, such as (1) supply chain and procurement; (2) logistics and warehousing; (3) raw material dispensing; (4) glass bottle washing and handling; (5) product filling; and (6) final product receiving and handling. The final steps of the sterile manufacturing process are the subject of the case study we present in this paper. We identify and control the risks related to (I) product sterilization; (II) product inspection, labeling, and packaging; (III) the finished product’s transfer to storage; and (IV) storing finished products in a warehouse. In order to maximize decision-making and reduce the risk of regulatory noncompliance, this case study describes a proactive strategy for the identification, management, and communication of risks associated with crucial tasks. While each organization’s products and methods are distinct, with varying tolerances for risk, certain stages and associated risks are common. Consequently, the examples provided here offer relevant insights into any pharmaceutical production environment. Managing sustainability-related risks and ensuring the transparency of pharmaceutical company operations are key tasks of success today. These risks, if not managed, will cause serious problems and a negative reputation, as well as environmental and public impact. Full article
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24 pages, 13675 KB  
Article
Low-Waste Technology for High-Precision Connecting Rod Forging Manufacturing
by Łukasz Dudkiewicz and Marek Hawryluk
Materials 2025, 18(2), 443; https://doi.org/10.3390/ma18020443 - 18 Jan 2025
Cited by 4 | Viewed by 2486
Abstract
This study refers to the application of an advanced tool in the form of numerical modelling in order to develop a low-waste hot die forging technology to produce a connecting rod forging. The technology aims at ensuring a limited amount of the charge [...] Read more.
This study refers to the application of an advanced tool in the form of numerical modelling in order to develop a low-waste hot die forging technology to produce a connecting rod forging. The technology aims at ensuring a limited amount of the charge material is necessary to produce one forging, as well as minimizing forging forces, and thus the electric energy consumption. The study includes a verification of the current production technology, which constituted the basis for the construction and development of a numerical model. A new construction of the forging tools was developed, with an additional pre-roughing pass (0X). The new process consists of die forging in the pre-roughing pass (0X), the roughing pass (1X) and the finishing impression (2X). Numerical modelling was subsequently conducted with the use of the Forge 3.0 NxT software. A detailed analysis was conducted on the accuracy of the tool impression filling (including the pre-roughing pass) by the deformed material, the distribution of temperatures for the forgings and the plastic deformations, as well as the courses of forging forces and energy. The results were verified under industrial conditions and compared with the forgings obtained in the previous technology (a roughing pass and a finishing impression). As a result of introducing the pre-roughing pass 0X, the forces were distributed between three impressions, including the especially developed pre-roughing pass. It was confirmed that the abovementioned changes in terms of forging tool construction had a positive effect on relieving the roughing pass and the finishing impression as well as limiting the charge material, and they also lowered the process energy consumption by 10%. This study also validated the relevance of using FE modelling to verify processes under virtual conditions before being implemented under industrial conditions. Therefore, the proposed approach based on multi-variant numerical simulations can be successfully used to improve other manufacturing processes in terms of reducing energy and material consumption and increasing tool service life. Full article
(This article belongs to the Special Issue Non-conventional Machining: Materials and Processes)
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20 pages, 5159 KB  
Article
Analysis of Electrical Conductivity in Commercial Adhesives Incorporating Graphene Nanoplatelets for Industrial Applications
by Pablo Rodríguez Fernández and Cristina Alía García
Polymers 2025, 17(1), 47; https://doi.org/10.3390/polym17010047 - 28 Dec 2024
Viewed by 1493
Abstract
Polymers are often insulators, but this not a universal intrinsic characteristic of all polymers. For this work, the adhesives used, epoxy and polyurethane, do demonstrate this insulating characteristic. However, there has been significant interest in the development of conductive polymers, specifically adhesives, because [...] Read more.
Polymers are often insulators, but this not a universal intrinsic characteristic of all polymers. For this work, the adhesives used, epoxy and polyurethane, do demonstrate this insulating characteristic. However, there has been significant interest in the development of conductive polymers, specifically adhesives, because of the potential properties and ease of processing of these polymers. The electrical-conductivity values for two composites reinforced with graphene nanoplatelets (GNPs) were measured. Both matrices are intended for industrial usage. One composite used an epoxy matrix, while the other employed a polyurethane resin as the matrix. To achieve dispersion and exfoliation of the filler, the catalyst for each resin, mixed with the GNP in proportion, was subjected to an ultrasonic bath for 30 min. The molds were filled by gravity, with the polyurethane specimens leveled to improve surface finish. The two-point uniaxial method was used to measure the conductivity of the specimens at room temperature, both before and after annealing at 120 °C for 120 min. Conductivity values were obtained for all samples, showing an increase after annealing; however, this increase was less pronounced compared to similar studies. The time and power in the ultrasonic bath, as well as the annealing conditions, must be optimized and the electrical conductivity should be studied periodically. Full article
(This article belongs to the Special Issue Polymer Functionalization Modification)
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24 pages, 4541 KB  
Article
Development of a Low-Cost Automated Injection Molding Device for Sustainable Plastic Recycling and Circular Economy Applications
by Ananta Sinchai, Kunthorn Boonyang and Thanakorn Simmala
Inventions 2024, 9(6), 124; https://doi.org/10.3390/inventions9060124 - 17 Dec 2024
Cited by 2 | Viewed by 4396
Abstract
In response to the critical demand for innovative solutions to tackle plastic pollution, this research presents a low-cost, fully automated plastic injection molding system designed to convert waste into sustainable products. Constructed entirely from repurposed materials, the apparatus focuses on processing high-density polyethylene [...] Read more.
In response to the critical demand for innovative solutions to tackle plastic pollution, this research presents a low-cost, fully automated plastic injection molding system designed to convert waste into sustainable products. Constructed entirely from repurposed materials, the apparatus focuses on processing high-density polyethylene (HDPE) efficiently without hydraulic components, thereby enhancing eco-friendliness and accessibility. Performance evaluations identified an optimal molding temperature of 200 °C, yielding consistent products with a minimal weight deviation of 4.17%. The key operational parameters included a motor speed of 525 RPM, a gear ratio of 1:30, and an inverter frequency of 105 Hz. Further tests showed that processing temperatures of 210 °C and 220 °C, with injection times of 15 to 35 s, yielded optimal surface finish and complete filling. The surface finish, assessed through image intensity variation, had a low coefficient of variation (≤5%), while computer vision evaluation confirmed the full filling of all specimens in this range. A laser-based overflow detection system has minimized material waste, proving effective in small-scale, community recycling. This study underscores the potential of low-cost automated systems to advance the practices of circular economies and enhance localized plastic waste management. Future research will focus on automation, temperature precision, material adaptability, and emissions management. Full article
(This article belongs to the Section Inventions and Innovation in Advanced Manufacturing)
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22 pages, 3075 KB  
Article
Co-Optimization of Mechanical Properties and Radiopacity Through Radiopaque Filler Incorporation for Medical Tubing Applications
by Alan Nugent, Joseph Molloy, Maurice Kelly and Declan Mary Colbert
Polymers 2024, 16(22), 3220; https://doi.org/10.3390/polym16223220 - 20 Nov 2024
Cited by 1 | Viewed by 3232
Abstract
Medical tubing, particularly cardiovascular tubing, is a critical area of research where continuous improvements are necessary to advance medical devices and improve patient care. While polymers are fundamental for these applications, on their own they present several limitations such as insufficient X-ray contrasting [...] Read more.
Medical tubing, particularly cardiovascular tubing, is a critical area of research where continuous improvements are necessary to advance medical devices and improve patient care. While polymers are fundamental for these applications, on their own they present several limitations such as insufficient X-ray contrasting capabilities. As such, polymer composites utilizing radiopaque fillers are a necessity for this application. For medical tubing in vivo, radiopacity is a crucial parameter that virgin polymers alone fall short in achieving due to limited X-ray absorption. To address this shortcoming, inorganic radiopaque fillers such as barium sulphate (BaSO4) and bismuth oxychloride (BiOCl) are incorporated into polymer matrices to increase the X-ray contrast of the manufactured tubing. It is also known, however, that the incorporation of these fillers can affect the mechanical, physical, and thermal properties of the finished product. This research evaluated the impact of incorporating the two aforementioned fillers into Pebax® 6333 SA01 MED at three different loading levels (10, 20, and 30 wt.%) on the physical, thermal, and mechanical properties of the composite. Composites were prepared by twin screw extrusion and injection molding followed by characterization of the mechanical (tensile, impact, and flexural), thermal (DSC), rheological (MFI), and physical (density and ash content) properties. The performed analysis shows that BiOCl enhanced the aesthetic properties, increased stiffness, and maintained flexibility while having minimal impact on the tensile and impact properties. When comparing BiOCl to BaSO4-filled composites, it was clear that depending on the application of the polymer composite, BiOCl may provide more desirable properties. The study highlights the importance of optimizing filler concentration and processing conditions to achieve desired composite properties for specific medical applications. Full article
(This article belongs to the Section Polymer Applications)
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14 pages, 3203 KB  
Article
One-Pot Synthesis of Alkyl Functionalized Reduced Graphene Oxide Nanocomposites as the Lubrication Additive Enabling Enhanced Tribological Performance
by Guangfa Zhang, Chao Zhu, Yehai Yan, Jian Cui and Jingxian Jiang
Molecules 2024, 29(9), 2004; https://doi.org/10.3390/molecules29092004 - 26 Apr 2024
Cited by 7 | Viewed by 1887
Abstract
Recently, aiming for the enhanced dispersibility of graphene-based nanomaterials in lubricating oil matrices to serve as highly efficient lubricant additives, numerous modification approaches have been extensively studied. However, these previous modification routes usually involve a tedious multistep modification process or multitudinous toxic reagents, [...] Read more.
Recently, aiming for the enhanced dispersibility of graphene-based nanomaterials in lubricating oil matrices to serve as highly efficient lubricant additives, numerous modification approaches have been extensively studied. However, these previous modification routes usually involve a tedious multistep modification process or multitudinous toxic reagents, restricting their extensive practical application. In this work, novel graphene oxide (GO) nanoadditives (RGO-g-BO) featuring excellent durable dispersion capability and remarkable tribological performance were successfully prepared via an environmentally friendly one-step approach consisting of surface grafting of long-chain bromooctadecane (BO) and in situ chemical reduction. Benefiting from the greatly improved lipophilicity (resulting from the introduction of hydrophobic long-chain alkane groups and chemical reduction), along with the miniaturization effect, RGO-g-BO exhibits superior long-term dispersion stability in the finished oil. Moreover, the tribological properties results demonstrated that the finished oil filled with RGO-g-BO nanolubricants achieved an outstanding friction-reducing and antiwear performance. Particularly, under the optimum content of RGO-g-BO (as low as 0.005 wt%), the friction coefficient as well as the wear volume of the composite finished oil were greatly reduced by 13% and 53%, respectively, as compared with nascent finished oil. Therefore, in view of the advantages of low-cost, one-step facile synthesis, desirable dispersion capability, and remarkable tribological performance, RGO-g-BO holds great prospects as a highly efficient lubrication additive in the tribology field. Full article
(This article belongs to the Special Issue Advanced Carbon Nanomaterials and Their Applications)
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17 pages, 6099 KB  
Article
Influence of Lubrication Status on Milling Performance of Bionic Micro-Textured Tools
by Hu Shi, Chunlu Ma, Baizhong Wang and Qinghua Li
Lubricants 2024, 12(4), 118; https://doi.org/10.3390/lubricants12040118 - 2 Apr 2024
Cited by 7 | Viewed by 2628
Abstract
Titanium alloy material has physical properties such as low thermal conductivity, high hardness, and surface resilience, which are prone to problems such as large milling force, low machining efficiency, and poor surface quality in processed products during dry milling. This document details our [...] Read more.
Titanium alloy material has physical properties such as low thermal conductivity, high hardness, and surface resilience, which are prone to problems such as large milling force, low machining efficiency, and poor surface quality in processed products during dry milling. This document details our process of isolating micro-textures from biological structures, applying them to cutting tool surfaces to create micro-texture milling cutters, and employing this micro-texture technique to reduce friction and prevent wear on these cutters. According to the milling dosage and the installation position between the tool and the workpiece, the effective working area of the cutting edge of the ball-end milling cutter is calculated. At the same time, a self-lubricating cutter was constructed by using a laser to process micro-textures and filling solid lubricant inside the micro-textures. An analysis was conducted to compare the milling efficiency of bionic microtextured cutters in both dry and micro-lubricated environments. It was found that the self-lubricating tool promoted a 3% to 5% decrease in milling force, a reduction in the coefficient of friction, a high surface finish of the machined workpiece, and an alleviation of chip sticking at the edge area. Full article
(This article belongs to the Special Issue Friction and Wear of Alloys)
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22 pages, 11621 KB  
Article
A Finite Element Method Study on a Simulation of the Thermal Behaviour of Four Methods for the Restoration of Class II Cavities
by Adela Nicoleta Staicu, Mihaela Jana Țuculină, Cristian Niky Cumpătă, Ana Maria Rîcă, Maria Cristina Beznă, Dragoș Laurențiu Popa, Alexandru Dan Popescu and Oana Andreea Diaconu
J. Funct. Biomater. 2024, 15(4), 86; https://doi.org/10.3390/jfb15040086 - 30 Mar 2024
Cited by 9 | Viewed by 3174
Abstract
The possibility of dental pulp damage during dental procedures is well known. According to studies, during finishing and polishing without cooling, temperatures of up to 140 °C or more can be generated. There are many studies that have analysed the influence of the [...] Read more.
The possibility of dental pulp damage during dental procedures is well known. According to studies, during finishing and polishing without cooling, temperatures of up to 140 °C or more can be generated. There are many studies that have analysed the influence of the finishing and polishing of fillings on the mechanical parameters, but the analysis of thermal parameters has led to uncertain results due to the difficulty of performing this in vivo. Background: We set out to conduct a study, using the finite element method, to determine the extent to which the type of class II cavity and the volume of the composite filling influence the duration of heat transfer to the pulp during finishing and polishing without cooling. Materials and Methods: A virtual model of an upper primary molar was used, with a caries process located on the distal aspect, in which four types of cavities were digitally prepared: direct access, horizontal slot, vertical slot and occlusal–proximal. All four cavity types were filled using a Filtek Supreme XT nanocomposite. Results: The study showed that the filling volume almost inversely proportionally influences the time at which the dental pulp reaches the critical temperature of irreversible damage. The lowest duration occurred in occlusal–distal restorations and the highest in direct access restorations. Conclusions: based on the results of the study, a working protocol can be issued so that finishing and polishing restorations without cooling are safe for pulpal health. Full article
(This article belongs to the Special Issue Biomaterials in Conservative Dentistry and Prosthodontics)
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22 pages, 5117 KB  
Article
Studying Flotation of Gold Microdispersions with Carrier Minerals and Pulp Aeration with a Steam–Air Mixture
by Sergei Ivanovich Evdokimov, Nikolay S. Golikov, Alexey F. Pryalukhin, Viktor V. Kondratiev, Anatolii Mishedchenko, Alexandra Vl. Kuzina, Natalia Nikolaevna Bryukhanova and Antonina I. Karlina
Minerals 2024, 14(1), 108; https://doi.org/10.3390/min14010108 - 19 Jan 2024
Cited by 19 | Viewed by 2644
Abstract
This work is aimed at obtaining new knowledge in the field of interactions of polydisperse hydrophobic surfaces in order to increase the extraction of mineral microdispersions via flotation. The effect of high velocity and the probability of aggregating fine particles with large ones [...] Read more.
This work is aimed at obtaining new knowledge in the field of interactions of polydisperse hydrophobic surfaces in order to increase the extraction of mineral microdispersions via flotation. The effect of high velocity and the probability of aggregating fine particles with large ones are used to increase the extraction of finely dispersed gold in this work. Large particles act as carrier minerals, which are intentionally introduced into a pulp. The novelty of this work lies in the fact that a rougher concentrate is used as the carrier mineral. For this purpose, it is isolated from three parallel pulp streams by mixing the rougher concentrate, isolated from the first stream of raw materials, with an initial feed of the second stream; accordingly, the rougher concentrate of the second stream is mixed with the initial feed of the third stream, and the finished rougher concentrate is obtained. In this mode of extracting the rougher concentrate, the content of the extracted metal increases from stream to stream, which contributes to the growth in its content in the end product. Moreover, in order to supplement forces involved in the separation of minerals with surface forces of structural origin in the third flotation stream, the pulp is aerated for a short time (about 15%–25% of the total) with air bubbles filled with a heat carrier, i.e., hot water vapor. Within this accepted flotation method, the influence that the surface currents occurring in the wetting film have on its thinning and breakthrough kinetics is proposed to be in the form of a correction to a length of a liquid slip in the hydrophobic gap. The value of the correction is expressed as a fraction of the limiting thickness of the wetting film, determined by the condition of its thickness invariability when the streams are equal in an interphase gap: outflowing (due to an action of the downforce) and inflowing (Marangoni flows and a thermo-osmotic stream). Gold flotation experiments are performed on samples of gold-bearing ore obtained from two deposits with conditions that simulate a continuous process. Technological advantages of this developed scheme and a flotation mode of gold microdispersions are shown in comparison with the basic technology. The purpose of this work is to conduct comparative tests on the basic and developed technologies using samples of gold-bearing ore obtained from the Natalka and Olimpiada deposits. Through the use of the developed technology, an increase in gold extraction of 7.99% and in concentrate quality (from 5.09 to 100.3 g/t) is achieved when the yield of the concentrate decreases from 1.86 to 1.30%, which reduces the costs associated with its expensive metallurgical processing. Full article
(This article belongs to the Special Issue Design, Modeling, Optimization and Control of Flotation Process)
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15 pages, 5825 KB  
Article
Increasing the Efficiency of Synthetic Iron Production by the Use of New Kit Lining
by Viktor Alekseevich Kukartsev, Alina Igorevna Trunova, Vladislav Viktorovich Kukartsev, Vadim Sergeevich Tynchenko, Sergei Olegovich Kurashkin, Yadviga Aleksandrovna Tynchenko, Ismael Flores Vivián and Kirill Aleksandrovich Bashmur
Metals 2023, 13(7), 1184; https://doi.org/10.3390/met13071184 - 26 Jun 2023
Cited by 20 | Viewed by 1720
Abstract
The production of synthetic iron castings in Russia comprises 50% of all alloys produced; therefore, increasing their smelting efficiency is an urgent task in the industry. This process depends primarily on the efficiency of industrial frequency induction crucible furnaces using acid lining. In [...] Read more.
The production of synthetic iron castings in Russia comprises 50% of all alloys produced; therefore, increasing their smelting efficiency is an urgent task in the industry. This process depends primarily on the efficiency of industrial frequency induction crucible furnaces using acid lining. In the present study, the properties of quartzite, which forms the basis of such a lining, were investigated. An analysis of the proposed variants for changing the composition of the acid lining for use at temperatures of 1550–1600 °C was conducted. Following the preliminary temperature treatment of raw quartzite, which was then subjected to a sintering regime, we determined the conditions under which it was possible to obtain a phase state, allowing for the operation of the lining at temperatures above 1450 °C. We determined the use of an electrocorundum of two fractions as an additive to the traditional composition of the acid lining. The industrial testing of a new liner composition for the smelting of synthetic cast iron in an induction crucible melting furnace with a single steel scrap-metal filling was assessed, which required the use of an increased amount of carburizing agent. The positive results obtained can be explained by the study of the spent lining, which withstood 345 smelting methods of genophasic rent analysis. The results of the test are based on the results obtained in a study conducted on the finished coating of the product. Full article
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